#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/27/2012778.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012778_Fobs loop_ _publ_author_name 'Wang, Xin Qiang' 'Yu, Wen Tao' 'Xu, Dong' 'Lu, Meng Kai' 'Yuan, Duo Rong' _publ_section_title ; catena-Poly[[bis(thiocyanato-\kN)cadmium(II)]-di-\m-thiourea-\k^4^S:S] ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m336 _journal_page_last m337 _journal_volume 58 _journal_year 2002 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 84.607 _cell_angle_beta 80.825 _cell_angle_gamma 75.318 _cell_length_a 4.0368 _cell_length_b 7.7237 _cell_length_c 10.1355 _exptl_crystal_F_000 186.00 _reflns_d_resolution_high 0.7109 _[local]_cod_data_source_file ta1373BTCTsup2.hkl _[local]_cod_data_source_block BTCT #BEGIN Tags that were not found in dictionaries: _shelx_title ' 0034 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 117.15 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1624.47 1642.78 28.93 o 2 0 0 550.55 593.95 17.40 o 3 0 0 1682.94 1591.01 38.14 o 4 0 0 131.38 135.47 6.15 o 5 0 0 134.89 135.70 6.37 o -5 1 0 27.66 23.07 2.83 o -4 1 0 15.45 13.88 1.88 o -3 1 0 1085.68 1114.87 32.42 o -2 1 0 262.89 248.87 8.10 o -1 1 0 1772.40 1879.16 29.87 o 0 1 0 1400.86 1381.75 16.63 o 1 1 0 1032.81 1059.99 11.54 o 2 1 0 3260.80 3323.50 40.36 o 3 1 0 46.45 51.70 2.26 o 4 1 0 366.98 345.04 13.53 o 5 1 0 222.51 210.31 9.77 o -5 2 0 66.15 71.92 4.11 o -4 2 0 544.97 545.51 19.78 o -3 2 0 45.35 48.71 2.54 o -2 2 0 1362.13 1408.71 30.90 o -1 2 0 5410.81 5116.39 33.27 o 0 2 0 169.02 192.23 5.30 o 1 2 0 3892.53 3734.40 23.81 o 2 2 0 3599.81 3554.92 42.98 o 3 2 0 180.06 179.70 7.55 o 4 2 0 296.39 315.93 12.42 o 5 2 0 50.82 52.28 3.45 o -4 3 0 419.78 434.80 16.69 o -3 3 0 30.70 30.55 2.45 o -2 3 0 475.66 503.01 21.00 o -1 3 0 179.89 186.99 12.79 o 0 3 0 1042.12 1028.75 14.03 o 1 3 0 1228.74 1179.82 15.49 o 2 3 0 37.68 35.78 1.82 o 3 3 0 1104.01 1077.25 30.75 o 4 3 0 266.48 280.15 11.09 o 5 3 0 14.84 12.88 2.08 o -4 4 0 2.65 -0.47 1.36 o -3 4 0 712.73 758.22 32.66 o -2 4 0 741.05 742.18 28.10 o -1 4 0 4.61 6.95 0.88 o 0 4 0 2679.21 2584.93 71.10 o 1 4 0 372.30 344.40 9.92 o 2 4 0 5.48 3.86 1.18 o 3 4 0 404.03 431.28 20.61 o 4 4 0 69.60 77.48 3.53 o 5 4 0 123.26 130.06 6.31 o -4 5 0 1.48 2.57 1.73 o -3 5 0 270.51 282.61 12.05 o -2 5 0 144.49 147.71 6.52 o -1 5 0 694.09 703.23 18.52 o 0 5 0 161.30 156.46 4.44 o 1 5 0 70.58 76.45 2.25 o 2 5 0 1507.12 1545.50 35.23 o 3 5 0 11.48 17.74 1.87 o 4 5 0 14.18 18.96 2.48 o 5 5 0 128.19 127.65 5.52 o -3 6 0 11.90 11.56 2.13 o -2 6 0 7.08 7.14 1.57 o -1 6 0 894.04 945.80 80.06 o 0 6 0 70.91 77.16 2.25 o 1 6 0 311.33 326.17 8.31 o 2 6 0 326.01 319.73 11.92 o 3 6 0 32.96 34.91 2.49 o 4 6 0 121.14 124.84 6.31 o 5 6 0 3.23 3.86 2.22 o -3 7 0 5.77 4.30 2.24 o -2 7 0 173.44 178.79 7.61 o -1 7 0 37.06 33.66 2.72 o 0 7 0 281.08 280.42 7.90 o 1 7 0 632.56 612.80 33.97 o 2 7 0 1.88 2.48 1.09 o 3 7 0 299.18 302.29 12.21 o 4 7 0 173.48 184.12 7.93 o 5 7 0 4.93 1.94 1.95 o -2 8 0 175.13 176.83 8.72 o -1 8 0 0.89 0.54 0.80 o 0 8 0 122.78 113.20 3.62 o 1 8 0 62.19 58.40 3.35 o 2 8 0 116.47 122.17 5.01 o 3 8 0 161.72 154.91 7.14 o 4 8 0 8.04 6.66 2.23 o -1 9 0 140.44 149.69 4.60 o 0 9 0 112.85 118.02 6.58 o 1 9 0 11.14 3.39 4.43 o 2 9 0 243.97 249.17 10.14 o 3 9 0 23.55 24.53 2.99 o 4 9 0 20.11 16.43 3.09 o 0 10 0 23.36 22.51 2.07 o 1 10 0 55.16 52.78 2.70 o 2 10 0 15.87 13.32 2.49 o 3 10 0 5.04 4.39 2.45 o -3 -10 1 0.25 0.42 1.33 o -2 -10 1 70.18 79.07 4.27 o -1 -10 1 151.95 137.37 4.93 o 0 -10 1 7.22 3.07 1.58 o -4 -9 1 17.15 14.84 2.45 o -3 -9 1 13.30 13.03 2.27 o -2 -9 1 170.71 174.31 7.30 o -1 -9 1 50.32 53.90 2.54 o 0 -9 1 178.19 183.49 6.11 o 1 -9 1 100.38 99.13 6.22 o -4 -8 1 7.83 6.76 2.17 o -3 -8 1 257.81 239.04 10.48 o -2 -8 1 61.63 63.48 3.28 o -1 -8 1 3.56 3.16 1.22 o 0 -8 1 362.43 380.44 9.98 o 1 -8 1 95.94 97.82 3.09 o 2 -8 1 92.38 84.86 4.50 o -4 -7 1 91.06 100.05 5.06 o -3 -7 1 173.36 182.63 7.10 o -2 -7 1 102.86 97.75 4.52 o -1 -7 1 571.05 577.53 18.38 o 0 -7 1 98.02 106.37 3.50 o 1 -7 1 192.80 207.55 6.34 o 2 -7 1 428.07 445.17 17.62 o 3 -7 1 14.34 11.18 2.73 o -5 -6 1 31.02 26.95 3.15 o -4 -6 1 305.87 319.40 13.56 o -3 -6 1 26.33 21.50 2.38 o -2 -6 1 266.17 275.93 10.76 o -1 -6 1 843.67 821.00 19.69 o 0 -6 1 31.19 31.30 1.42 o 1 -6 1 114.13 123.30 4.04 o 2 -6 1 70.64 71.86 3.47 o 3 -6 1 151.87 151.40 7.14 o -5 -5 1 44.11 44.94 3.76 o -4 -5 1 144.38 154.59 6.89 o -3 -5 1 458.22 459.76 15.55 o -2 -5 1 809.23 830.46 26.34 o -1 -5 1 101.60 99.77 3.03 o 0 -5 1 1461.07 1455.08 22.73 o 1 -5 1 804.48 804.45 18.90 o 2 -5 1 3.50 5.63 1.27 o 3 -5 1 318.99 307.33 12.65 o 4 -5 1 56.46 49.62 3.79 o -5 -4 1 110.63 112.45 5.00 o -4 -4 1 0.98 1.33 1.50 o -3 -4 1 393.23 387.35 13.95 o -2 -4 1 440.04 397.99 17.58 o -1 -4 1 123.17 133.03 5.06 o 0 -4 1 778.00 765.29 14.70 o 1 -4 1 398.96 415.19 31.64 o 2 -4 1 516.37 516.06 22.78 o 3 -4 1 19.45 21.72 2.27 o 4 -4 1 14.17 12.55 2.11 o -5 -3 1 66.60 66.51 4.01 o -4 -3 1 167.77 187.23 8.16 o -3 -3 1 96.14 89.61 4.20 o -2 -3 1 235.69 242.40 8.67 o -1 -3 1 4195.03 4025.54 36.64 o 0 -3 1 262.26 263.26 8.95 o 1 -3 1 138.98 145.53 4.17 o 2 -3 1 1835.44 1801.01 37.75 o 3 -3 1 145.53 150.71 6.72 o 4 -3 1 87.35 85.02 3.98 o -5 -2 1 2.03 0.36 1.88 o -4 -2 1 507.54 550.21 26.09 o -3 -2 1 148.39 156.97 6.19 o -2 -2 1 85.61 85.75 3.80 o -1 -2 1 149.47 149.50 3.74 o 0 -2 1 620.04 591.60 13.50 o 1 -2 1 1769.71 1810.40 19.02 o 2 -2 1 93.79 101.52 4.66 o 3 -2 1 615.36 555.54 24.68 o 4 -2 1 511.62 519.96 18.96 o 5 -2 1 0.18 -0.26 0.26 o -5 -1 1 166.35 161.85 7.32 o -4 -1 1 124.31 125.26 5.15 o -3 -1 1 669.41 700.76 25.86 o -2 -1 1 2184.26 2054.73 33.35 o -1 -1 1 245.90 281.34 6.76 o 0 -1 1 2749.67 2490.56 14.44 o 1 -1 1 3304.30 3156.84 29.03 o 2 -1 1 9.78 13.21 1.28 o 3 -1 1 420.93 423.66 20.80 o 4 -1 1 226.00 234.29 9.94 o 5 -1 1 145.19 142.43 5.99 o -5 0 1 280.45 281.33 12.16 o -4 0 1 20.14 18.47 2.38 o -3 0 1 370.18 390.02 13.40 o -2 0 1 1304.52 1302.27 27.34 o -1 0 1 3851.37 3685.11 22.94 o 0 0 1 2408.85 1813.11 13.25 o 1 0 1 1.70 1.96 0.47 o 2 0 1 3297.06 3272.96 40.45 o 3 0 1 752.37 807.89 26.00 o 4 0 1 8.70 6.68 2.17 o 5 0 1 386.35 397.61 15.79 o -5 1 1 8.16 7.71 2.48 o -4 1 1 396.03 369.79 14.08 o -3 1 1 724.97 680.86 26.47 o -2 1 1 115.67 140.20 5.47 o -1 1 1 7086.87 6430.68 33.48 o 0 1 1 1751.31 1734.77 11.75 o 1 1 1 186.26 174.86 5.11 o 2 1 1 2060.21 2044.79 31.50 o 3 1 1 307.46 313.66 11.33 o 4 1 1 228.97 225.12 9.07 o 5 1 1 45.58 40.71 3.25 o -5 2 1 1.80 -0.52 1.36 o -4 2 1 352.44 368.01 15.03 o -3 2 1 422.44 415.73 15.25 o -2 2 1 1036.90 1047.07 27.87 o -1 2 1 1117.90 1170.44 31.59 o 0 2 1 2901.81 2872.43 19.72 o 1 2 1 13723.30 10771.44 91.24 o 2 2 1 474.13 494.31 16.03 o 3 2 1 210.57 212.22 8.76 o 4 2 1 1007.58 1006.50 36.16 o 5 2 1 24.04 23.09 2.52 o -4 3 1 41.99 47.05 3.25 o -3 3 1 16.26 18.51 2.13 o -2 3 1 1869.95 1847.39 39.65 o -1 3 1 171.21 160.03 4.33 o 0 3 1 978.98 1071.85 14.72 o 1 3 1 2434.80 2465.45 22.09 o 2 3 1 324.10 321.92 13.92 o 3 3 1 828.38 757.12 26.06 o 4 3 1 107.69 102.16 5.45 o 5 3 1 90.85 93.90 4.42 o -4 4 1 54.69 57.06 3.70 o -3 4 1 375.62 385.84 14.05 o -2 4 1 295.05 300.22 11.63 o -1 4 1 1021.98 1080.65 20.31 o 0 4 1 2589.09 2512.71 51.15 o 1 4 1 0.77 0.39 0.89 o 2 4 1 1792.40 1704.80 34.24 o 3 4 1 1458.24 1442.46 37.04 o 4 4 1 6.23 2.93 1.71 o 5 4 1 147.36 143.12 6.79 o -4 5 1 108.74 102.82 5.13 o -3 5 1 540.57 546.56 18.47 o -2 5 1 6.85 7.40 1.62 o -1 5 1 397.58 437.70 14.63 o 0 5 1 418.49 406.87 12.53 o 1 5 1 98.06 94.80 2.99 o 2 5 1 530.97 500.11 21.32 o 3 5 1 8.47 8.83 1.60 o 4 5 1 240.16 249.73 9.72 o 5 5 1 107.80 103.33 4.94 o -3 6 1 40.83 40.07 3.12 o -2 6 1 391.07 373.02 15.41 o -1 6 1 555.66 580.58 28.39 o 0 6 1 10.76 12.97 1.50 o 1 6 1 1220.91 1225.19 23.31 o 2 6 1 115.18 112.99 5.19 o 3 6 1 1.58 2.58 1.56 o 4 6 1 295.98 307.07 13.12 o 5 6 1 21.64 24.47 2.74 o -3 7 1 5.29 7.67 2.24 o -2 7 1 353.24 300.44 13.25 o -1 7 1 83.08 87.45 2.63 o 0 7 1 87.19 94.20 3.38 o 1 7 1 201.65 193.86 6.03 o 2 7 1 12.90 16.21 1.73 o 3 7 1 299.82 315.99 12.26 o 4 7 1 7.42 9.39 2.57 o 5 7 1 0.94 1.95 1.76 o -2 8 1 33.97 29.85 3.19 o -1 8 1 3.90 2.83 1.12 o 0 8 1 527.66 553.36 15.58 o 1 8 1 20.27 26.07 1.52 o 2 8 1 94.05 93.52 4.27 o 3 8 1 189.51 204.57 8.57 o 4 8 1 0.31 2.32 1.62 o -1 9 1 57.80 55.62 2.73 o 0 9 1 78.75 68.62 4.08 o 1 9 1 33.35 32.83 2.26 o 2 9 1 183.03 174.15 7.03 o 3 9 1 2.50 0.48 1.44 o 4 9 1 55.52 57.21 3.98 o 0 10 1 5.44 1.96 1.28 o 1 10 1 54.74 48.87 2.47 o 2 10 1 44.99 49.65 3.59 o 3 10 1 9.44 9.37 2.04 o -2 -10 2 83.66 76.90 4.55 o -1 -10 2 47.66 43.33 2.57 o 0 -10 2 1.61 1.90 1.20 o -3 -9 2 28.50 30.22 3.02 o -2 -9 2 255.83 270.86 10.96 o -1 -9 2 0.16 0.07 0.84 o 0 -9 2 52.49 51.40 3.29 o 1 -9 2 99.05 102.94 3.64 o -4 -8 2 13.67 20.64 2.70 o -3 -8 2 150.92 150.12 7.17 o -2 -8 2 31.02 27.62 2.74 o -1 -8 2 193.94 193.47 6.10 o 0 -8 2 534.09 529.81 14.27 o 1 -8 2 3.62 2.25 1.19 o 2 -8 2 145.06 156.06 7.30 o -4 -7 2 69.97 70.53 4.27 o -3 -7 2 177.45 177.80 7.13 o -2 -7 2 0.45 0.13 1.21 o -1 -7 2 557.89 591.94 19.98 o 0 -7 2 342.83 345.59 9.30 o 1 -7 2 129.30 118.06 3.96 o 2 -7 2 229.79 232.48 10.63 o 3 -7 2 43.52 44.70 3.44 o -5 -6 2 25.06 26.82 3.29 o -4 -6 2 159.08 150.96 6.01 o -3 -6 2 73.70 71.74 3.48 o -2 -6 2 681.33 682.26 27.14 o -1 -6 2 321.66 301.35 8.04 o 0 -6 2 1.91 2.22 1.60 o 1 -6 2 1192.71 1152.79 25.29 o 2 -6 2 231.43 236.59 9.90 o 3 -6 2 30.07 31.73 2.97 o -5 -5 2 215.40 224.16 10.00 o -4 -5 2 188.13 196.42 8.96 o -3 -5 2 50.61 57.25 2.93 o -2 -5 2 1031.91 1006.39 31.24 o -1 -5 2 365.53 379.00 12.41 o 0 -5 2 534.49 538.47 14.72 o 1 -5 2 570.37 567.00 16.24 o 2 -5 2 283.72 267.77 10.16 o 3 -5 2 495.10 500.43 18.29 o 4 -5 2 24.57 24.30 2.86 o -5 -4 2 121.22 109.32 6.56 o -4 -4 2 116.85 122.80 6.40 o -3 -4 2 802.76 814.45 29.69 o -2 -4 2 172.25 181.80 6.88 o -1 -4 2 505.48 542.50 13.18 o 0 -4 2 2864.85 2823.09 29.49 o 1 -4 2 1.15 1.48 0.83 o 2 -4 2 87.33 94.36 4.45 o 3 -4 2 459.61 450.16 16.73 o 4 -4 2 56.95 57.04 3.56 o -5 -3 2 1.66 -0.07 1.63 o -4 -3 2 69.94 68.58 4.12 o -3 -3 2 1198.96 1159.64 33.45 o -2 -3 2 693.95 735.76 22.77 o -1 -3 2 1321.68 1386.51 18.59 o 0 -3 2 1273.91 1257.65 17.08 o 1 -3 2 1552.17 1600.15 22.18 o 2 -3 2 922.44 908.99 27.07 o 3 -3 2 6.14 6.98 1.46 o 4 -3 2 311.76 295.54 12.24 o -5 -2 2 42.85 48.17 3.57 o -4 -2 2 279.04 293.43 12.17 o -3 -2 2 1.44 5.57 1.57 o -2 -2 2 899.68 852.61 23.41 o -1 -2 2 1661.01 1692.71 18.66 o 0 -2 2 84.32 96.89 4.55 o 1 -2 2 1694.40 1594.93 19.19 o 2 -2 2 888.81 887.78 24.60 o 3 -2 2 31.95 35.36 2.32 o 4 -2 2 72.85 72.43 3.54 o 5 -2 2 31.25 29.08 2.96 o -5 -1 2 184.71 189.51 8.91 o -4 -1 2 337.81 369.47 12.77 o -3 -1 2 23.25 25.89 1.94 o -2 -1 2 489.22 451.02 17.14 o -1 -1 2 1979.80 1959.02 24.25 o 0 -1 2 4513.92 4018.03 35.94 o 1 -1 2 799.24 780.30 14.93 o 2 -1 2 242.14 230.79 8.13 o 3 -1 2 1732.10 1757.58 40.43 o 4 -1 2 87.18 92.85 4.43 o 5 -1 2 16.64 18.18 2.49 o -5 0 2 68.80 70.75 4.10 o -4 0 2 1.98 11.41 1.97 o -3 0 2 962.68 947.27 30.35 o -2 0 2 167.97 157.33 6.30 o -1 0 2 184.17 212.93 6.52 o 0 0 2 1335.61 1362.31 20.17 o 1 0 2 339.37 337.56 7.26 o 2 0 2 290.31 288.95 12.75 o 3 0 2 489.19 452.83 20.16 o 4 0 2 250.16 252.53 10.55 o 5 0 2 165.44 167.49 7.86 o -5 1 2 47.95 47.08 3.75 o -4 1 2 109.93 110.35 5.71 o -3 1 2 754.07 815.40 29.52 o -2 1 2 1019.53 1077.19 26.97 o -1 1 2 1427.86 1429.44 17.13 o 0 1 2 25.89 24.00 0.67 o 1 1 2 2437.01 2442.22 23.42 o 2 1 2 2660.46 2552.35 35.78 o 3 1 2 0.38 0.10 1.28 o 4 1 2 278.68 264.16 10.84 o 5 1 2 270.45 271.71 12.21 o -4 2 2 490.29 509.02 18.92 o -3 2 2 2.64 2.99 1.41 o -2 2 2 332.86 366.09 17.32 o -1 2 2 2857.86 2779.82 26.76 o 0 2 2 675.44 661.32 14.79 o 1 2 2 539.56 605.40 13.02 o 2 2 2 441.74 412.63 14.71 o 3 2 2 630.96 664.28 23.47 o 4 2 2 309.06 333.45 12.77 o 5 2 2 21.10 24.57 2.59 o -4 3 2 127.11 131.02 5.31 o -3 3 2 297.94 283.00 11.47 o -2 3 2 899.34 909.25 29.28 o -1 3 2 622.36 677.19 27.68 o 0 3 2 4386.48 4274.03 30.61 o 1 3 2 1213.87 1204.56 16.12 o 2 3 2 49.41 51.37 2.39 o 3 3 2 1244.94 1243.93 33.16 o 4 3 2 173.33 169.49 7.51 o 5 3 2 16.49 15.93 2.61 o -4 4 2 1.39 -1.24 1.24 o -3 4 2 499.36 478.17 17.81 o -2 4 2 586.84 578.76 25.22 o -1 4 2 151.80 167.15 4.71 o 0 4 2 1378.19 1432.35 20.52 o 1 4 2 1589.04 1596.99 21.20 o 2 4 2 1954.61 1920.20 35.73 o 3 4 2 242.45 231.43 9.18 o 4 4 2 58.03 60.56 3.28 o 5 4 2 277.23 275.39 13.16 o -4 5 2 123.17 132.13 6.66 o -3 5 2 108.00 107.63 5.42 o -2 5 2 46.82 49.60 2.81 o -1 5 2 1220.84 1221.82 24.56 o 0 5 2 216.98 235.99 10.44 o 1 5 2 408.24 433.25 12.57 o 2 5 2 1424.26 1387.54 33.50 o 3 5 2 64.65 55.59 2.71 o 4 5 2 175.31 160.03 7.59 o 5 5 2 112.30 115.95 6.49 o -3 6 2 26.58 27.15 2.78 o -2 6 2 133.69 125.15 5.77 o -1 6 2 567.20 543.55 25.52 o 0 6 2 263.90 259.92 7.41 o 1 6 2 586.23 559.29 16.12 o 2 6 2 77.03 70.84 3.76 o 3 6 2 414.68 424.97 15.80 o 4 6 2 404.16 392.10 14.91 o 5 6 2 1.43 -0.47 1.72 o -3 7 2 71.10 63.38 4.40 o -2 7 2 356.38 369.83 15.84 o -1 7 2 3.28 7.98 1.38 o 0 7 2 167.52 163.11 4.89 o 1 7 2 314.36 324.54 8.78 o 2 7 2 1.36 0.52 1.47 o 3 7 2 206.79 204.79 9.42 o 4 7 2 28.42 45.83 2.99 o 5 7 2 24.50 21.34 3.05 o -2 8 2 85.35 78.86 5.04 o -1 8 2 74.33 82.22 4.45 o 0 8 2 309.03 316.81 8.98 o 1 8 2 27.99 26.06 1.67 o 2 8 2 214.36 214.07 9.08 o 3 8 2 41.82 44.95 3.09 o 4 8 2 0.39 2.01 1.63 o -1 9 2 194.92 189.96 6.32 o 0 9 2 47.45 53.79 4.17 o 1 9 2 1.43 0.68 0.99 o 2 9 2 118.32 107.48 5.36 o 3 9 2 2.30 0.52 1.57 o 4 9 2 33.41 33.38 3.45 o 0 10 2 1.16 0.09 0.96 o 1 10 2 147.05 152.16 4.85 o 2 10 2 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