#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2012780.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012780_Fobs loop_ _publ_author_name 'Harrison, William T. A.' 'Howie, R. Alan' 'Skakle, Janet M. S.' 'Wardell, James L.' _publ_section_title ; 6,6-Diphenyl-6,7-dihydro-5H-1,3,4,8-tetrathia-6-stannazulene-2-thione and 6,6'-spirobi[6,7-dihydro-5H-1,3,4,8-tetrathia-6-stannazulene]-2,2'-dithione ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m351 _journal_page_last m354 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 114.625 _cell_angle_gamma 90.000 _cell_length_a 11.3973 _cell_length_b 14.2749 _cell_length_c 12.5609 _exptl_crystal_F_000 1112.00 _reflns_d_resolution_high 0.6939 _[local]_cod_data_source_file tr1026Vsup3.hkl _[local]_cod_data_source_block V #BEGIN Tags that were not found in dictionaries: _shelx_title ' C10H8S10Sn1 (P21/n, Z=4)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 263.81 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y+1/2, z+1/2' '-x, -y, -z' '-x-1/2, y-1/2, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5306.17 5794.37 111.29 o 4 0 0 3293.89 3468.70 41.86 o 6 0 0 1258.41 1192.78 35.95 o 8 0 0 2138.49 2062.93 128.61 o 10 0 0 6135.49 4769.07 116.01 o 12 0 0 85.96 89.06 34.29 o 14 0 0 291.18 239.79 45.50 o 1 1 0 4212.14 4319.94 139.38 o 2 1 0 96.73 80.74 6.37 o 3 1 0 834.16 937.95 18.49 o 4 1 0 1874.88 2197.99 18.28 o 5 1 0 309.09 290.52 10.10 o 6 1 0 10008.95 10089.97 49.75 o 7 1 0 1827.08 1794.98 54.41 o 8 1 0 485.63 458.39 16.71 o 9 1 0 373.68 331.48 20.34 o 10 1 0 4771.46 4152.34 110.62 o 11 1 0 267.78 244.95 27.95 o 12 1 0 50.40 68.56 26.31 o 13 1 0 0.07 26.83 34.50 o 14 1 0 699.41 658.63 62.54 o 0 2 0 39270.75 38432.11 221.97 o 1 2 0 4643.00 5090.24 182.59 o 2 2 0 2676.60 2606.95 153.52 o 3 2 0 31873.38 33320.86 967.10 o 4 2 0 28065.09 28961.50 699.90 o 5 2 0 100.05 96.94 10.23 o 6 2 0 19538.92 18789.18 547.45 o 7 2 0 830.16 832.86 19.68 o 8 2 0 4561.42 4285.77 165.90 o 9 2 0 330.49 288.80 20.77 o 10 2 0 2834.47 2482.01 61.51 o 11 2 0 55.08 59.84 30.84 o 12 2 0 92.98 78.54 30.19 o 13 2 0 3.01 4.47 22.38 o 14 2 0 92.39 110.92 27.25 o 1 3 0 15310.54 16377.27 434.37 o 2 3 0 237.86 317.26 25.53 o 3 3 0 1.13 -4.77 11.36 o 4 3 0 2724.10 2476.72 137.56 o 5 3 0 18.23 11.02 9.17 o 6 3 0 13476.57 13283.42 424.92 o 7 3 0 316.22 284.74 15.14 o 8 3 0 71.88 66.49 13.98 o 9 3 0 1195.53 1203.03 25.18 o 10 3 0 3091.14 2678.27 83.02 o 11 3 0 204.75 177.77 25.53 o 12 3 0 790.91 672.84 39.79 o 13 3 0 382.43 380.17 34.76 o 0 4 0 7340.47 7464.53 583.41 o 1 4 0 2.74 33.18 9.03 o 2 4 0 5608.00 5612.76 154.13 o 3 4 0 1028.72 948.33 52.11 o 4 4 0 33034.63 32082.70 1249.49 o 5 4 0 122.51 109.94 14.27 o 6 4 0 6652.74 6302.23 252.21 o 7 4 0 2929.03 2836.97 89.54 o 8 4 0 6736.91 6186.53 168.51 o 9 4 0 186.20 167.16 15.48 o 10 4 0 470.49 457.38 40.00 o 11 4 0 6.89 4.58 20.13 o 12 4 0 238.53 222.68 31.70 o 13 4 0 90.90 55.92 24.38 o 1 5 0 6449.08 6650.09 123.88 o 2 5 0 1306.76 1428.34 48.38 o 3 5 0 382.28 411.89 15.09 o 4 5 0 5.45 -9.57 12.45 o 5 5 0 1961.55 1842.14 148.07 o 6 5 0 5831.49 5208.69 348.08 o 7 5 0 107.41 112.41 13.04 o 8 5 0 8728.51 7998.64 168.29 o 9 5 0 234.55 233.99 16.04 o 10 5 0 874.14 850.59 39.54 o 11 5 0 9.38 21.97 21.88 o 12 5 0 1108.75 1117.01 71.59 o 13 5 0 2.55 -0.82 22.19 o 14 5 0 105.38 111.70 42.27 o 0 6 0 29539.92 28374.21 200.98 o 1 6 0 1620.53 2107.98 57.08 o 2 6 0 32992.42 33245.54 278.77 o 3 6 0 511.62 575.86 27.42 o 4 6 0 5113.71 5128.22 200.74 o 5 6 0 2642.67 2555.83 117.70 o 6 6 0 834.71 841.00 44.47 o 7 6 0 15.34 21.66 11.89 o 8 6 0 1769.76 1679.18 65.05 o 9 6 0 547.40 455.32 19.33 o 10 6 0 849.09 799.57 39.14 o 11 6 0 1.33 2.19 21.34 o 12 6 0 207.38 193.45 30.03 o 13 6 0 3.95 25.33 25.42 o 1 7 0 4940.78 4674.93 228.24 o 2 7 0 12831.62 13057.17 133.11 o 3 7 0 26.31 101.10 11.69 o 4 7 0 8913.88 8852.47 312.79 o 5 7 0 199.20 170.86 19.25 o 6 7 0 432.39 424.44 35.26 o 7 7 0 1736.78 1497.44 70.08 o 8 7 0 84.74 74.02 12.92 o 9 7 0 2096.55 2050.92 37.51 o 10 7 0 582.37 581.13 35.84 o 11 7 0 1155.82 1161.52 48.49 o 12 7 0 954.88 953.74 51.86 o 13 7 0 4.50 91.49 26.67 o 0 8 0 767.49 725.27 51.54 o 1 8 0 5017.40 4565.23 280.89 o 2 8 0 9369.47 9560.56 147.47 o 3 8 0 271.33 285.24 10.64 o 4 8 0 5419.54 5448.63 98.32 o 5 8 0 251.73 250.21 23.78 o 6 8 0 9313.10 8977.37 426.47 o 7 8 0 446.10 456.31 31.25 o 8 8 0 2055.36 1950.68 32.57 o 9 8 0 522.38 522.99 20.30 o 10 8 0 500.84 460.59 46.36 o 11 8 0 316.55 250.97 30.42 o 12 8 0 162.01 162.29 29.65 o 13 8 0 167.96 173.03 30.42 o 1 9 0 5385.76 4986.12 229.76 o 2 9 0 8.72 -6.76 13.88 o 3 9 0 4663.65 4546.90 63.87 o 4 9 0 2088.35 1954.55 49.90 o 5 9 0 22.55 15.12 8.72 o 6 9 0 252.42 219.62 16.57 o 7 9 0 617.55 601.10 21.08 o 8 9 0 533.37 570.78 30.04 o 9 9 0 1.14 -2.10 12.29 o 10 9 0 641.51 638.40 37.57 o 11 9 0 592.80 579.77 38.33 o 12 9 0 1641.39 1633.21 60.10 o 13 9 0 119.68 176.18 45.72 o 0 10 0 10303.08 10957.83 625.03 o 1 10 0 0.11 -5.28 13.10 o 2 10 0 3790.08 3431.84 202.29 o 3 10 0 3646.19 3302.93 84.72 o 4 10 0 4596.32 4450.30 117.96 o 5 10 0 1022.16 1023.19 31.70 o 6 10 0 3582.99 3544.90 125.70 o 7 10 0 298.01 288.85 18.50 o 8 10 0 414.78 436.41 20.67 o 9 10 0 101.06 121.43 17.26 o 10 10 0 20.63 10.41 19.98 o 11 10 0 0.62 -30.84 30.84 o 12 10 0 214.66 247.77 44.64 o 1 11 0 238.06 250.25 44.85 o 2 11 0 7.41 11.15 27.01 o 3 11 0 8923.67 9101.92 98.80 o 4 11 0 648.32 566.99 25.80 o 5 11 0 1454.49 1379.19 81.99 o 6 11 0 1627.01 1544.15 109.39 o 7 11 0 5504.25 5599.81 417.51 o 8 11 0 308.73 341.80 23.61 o 9 11 0 323.65 324.39 27.11 o 10 11 0 912.50 1021.63 42.74 o 11 11 0 111.01 84.10 39.03 o 0 12 0 1574.75 1477.77 68.57 o 1 12 0 2389.30 2475.32 128.95 o 2 12 0 3339.72 3444.03 103.72 o 3 12 0 27.95 17.27 26.13 o 4 12 0 2010.98 1923.62 50.38 o 5 12 0 267.50 264.45 28.28 o 6 12 0 2964.53 3050.24 61.91 o 7 12 0 1123.10 1191.83 43.75 o 8 12 0 174.87 205.27 27.27 o 9 12 0 64.87 121.74 22.32 o 10 12 0 22.06 50.46 27.17 o 1 13 0 1593.10 1642.44 63.07 o 2 13 0 235.19 310.59 31.32 o 3 13 0 1717.82 1645.40 49.66 o 4 13 0 36.91 21.77 25.53 o 5 13 0 146.59 162.86 28.06 o 6 13 0 1205.06 1329.80 47.09 o 7 13 0 1912.46 2063.19 122.48 o 8 13 0 19.99 29.49 39.68 o 9 13 0 240.17 275.83 57.04 o 10 13 0 193.50 241.73 37.31 o 0 14 0 2274.14 2087.17 82.16 o 1 14 0 36.91 48.63 28.26 o 2 14 0 109.64 103.12 30.11 o 3 14 0 1214.97 1267.87 51.00 o 4 14 0 1911.18 2019.25 75.26 o 5 14 0 165.86 102.83 41.94 o 6 14 0 130.26 93.16 27.86 o 7 14 0 16.75 23.45 26.91 o 8 14 0 849.33 989.65 80.33 o 9 14 0 281.04 358.13 30.97 o 10 14 0 36.24 78.28 31.91 o 1 15 0 2532.73 2627.93 135.42 o 2 15 0 155.61 142.61 29.05 o 3 15 0 1165.38 1119.25 46.85 o 4 15 0 135.22 142.46 29.73 o 5 15 0 408.16 392.38 34.73 o 6 15 0 332.80 296.20 33.68 o 7 15 0 597.99 621.80 40.62 o 8 15 0 86.35 76.42 50.57 o 9 15 0 15.55 82.37 36.01 o 10 15 0 413.27 624.27 53.48 o 0 16 0 1296.08 1318.42 70.51 o 1 16 0 149.86 141.89 28.74 o 2 16 0 676.79 603.73 39.38 o 3 16 0 1801.27 1838.48 56.99 o 4 16 0 308.27 303.16 34.46 o 5 16 0 1025.14 1098.93 49.06 o 6 16 0 76.64 104.83 31.96 o 7 16 0 2.98 13.73 67.60 o 8 16 0 153.08 240.01 43.56 o 1 17 0 689.17 710.50 43.79 o 2 17 0 104.92 84.42 30.34 o 3 17 0 402.83 385.76 40.76 o 4 17 0 236.88 305.90 36.04 o 5 17 0 1233.03 1352.13 55.17 o 6 17 0 526.14 523.89 41.63 o 7 17 0 141.94 202.47 89.92 o 8 17 0 83.20 133.48 39.89 o 0 18 0 824.98 856.09 65.99 o 1 18 0 251.87 229.62 35.53 o 2 18 0 94.25 41.43 31.02 o 3 18 0 300.63 296.70 37.58 o 4 18 0 230.58 193.82 34.78 o 5 18 0 0.15 -11.82 78.82 o 6 18 0 5.86 40.18 40.00 o 1 19 0 228.95 140.86 47.44 o 2 19 0 77.56 65.47 31.47 o 3 19 0 325.65 344.21 39.37 o 4 19 0 0.47 -47.44 47.44 o -13 0 1 3843.97 3558.69 115.80 o -11 0 1 6153.07 5424.18 130.46 o -9 0 1 215.07 240.89 20.66 o -7 0 1 2928.22 3271.43 73.35 o -5 0 1 1401.85 1478.26 52.95 o -3 0 1 28345.97 29834.54 919.55 o -1 0 1 198.79 452.64 8.08 o 1 0 1 4888.14 4476.23 111.49 o 3 0 1 45.29 72.81 11.93 o 5 0 1 7926.00 8318.09 88.94 o 7 0 1 4841.31 4939.92 51.86 o 9 0 1 447.85 392.03 42.27 o 11 0 1 1121.26 888.22 60.16 o 13 0 1 1852.77 1493.73 84.96 o -14 1 1 3.68 4.37 23.07 o -13 1 1 118.09 161.87 42.59 o -12 1 1 260.23 267.95 37.95 o -11 1 1 152.82 146.43 24.30 o -10 1 1 28.09 4.91 21.05 o -9 1 1 499.52 503.73 15.76 o -8 1 1 54.86 44.06 12.09 o -7 1 1 15595.54 15421.95 120.38 o -6 1 1 82.58 63.57 9.13 o -5 1 1 5005.35 5129.91 70.24 o -4 1 1 6859.76 6929.69 98.49 o -3 1 1 46363.94 46399.92 308.76 o -2 1 1 10439.50 11851.51 226.40 o -1 1 1 8186.12 8981.06 120.70 o 0 1 1 232.80 283.99 7.59 o 1 1 1 34924.71 34727.63 656.87 o 2 1 1 10930.52 12926.59 261.73 o 3 1 1 24994.71 26522.55 224.63 o 4 1 1 1690.39 1765.82 25.75 o 5 1 1 13686.62 14499.11 128.23 o 6 1 1 0.89 19.96 17.24 o 7 1 1 10565.28 9985.78 171.52 o 8 1 1 1282.57 1245.84 31.79 o 9 1 1 714.76 582.24 29.68 o 10 1 1 64.20 68.72 25.98 o 11 1 1 1249.26 920.56 61.89 o 12 1 1 7.27 28.39 22.26 o 13 1 1 414.78 413.19 37.81 o -14 2 1 11.96 46.82 24.99 o -13 2 1 1331.45 1152.16 49.21 o -12 2 1 318.29 287.27 28.96 o -11 2 1 909.63 885.98 40.92 o -10 2 1 189.65 167.27 25.15 o -9 2 1 3862.92 3664.56 106.29 o -8 2 1 9.87 8.55 9.80 o -7 2 1 2489.48 2594.78 32.20 o -6 2 1 14646.42 15651.37 231.87 o -5 2 1 23674.55 24707.23 154.37 o -4 2 1 3380.85 3589.75 52.60 o -3 2 1 12745.95 13024.83 253.47 o -2 2 1 18686.73 20812.49 201.31 o -1 2 1 25574.29 27090.79 562.16 o 0 2 1 87.00 118.59 3.31 o 1 2 1 3939.10 4508.10 80.55 o 2 2 1 35344.69 38415.45 695.92 o 3 2 1 4889.13 5193.81 71.34 o 4 2 1 5222.13 5281.77 109.66 o 5 2 1 19.54 35.68 9.77 o 6 2 1 12.71 7.39 11.86 o 7 2 1 1073.39 1112.03 30.65 o 8 2 1 2609.78 2317.09 88.65 o 9 2 1 1.50 6.59 15.71 o 10 2 1 435.76 367.88 30.64 o 11 2 1 1791.58 1468.40 52.97 o 12 2 1 305.74 295.05 31.17 o 13 2 1 661.91 561.99 40.47 o -14 3 1 12.24 31.16 25.48 o -13 3 1 208.91 207.25 29.73 o -12 3 1 807.18 747.44 40.47 o -11 3 1 59.57 56.67 22.29 o -10 3 1 67.44 57.45 21.58 o -9 3 1 21.17 18.38 12.25 o -8 3 1 824.46 816.13 23.16 o -7 3 1 4119.39 4166.23 125.31 o -6 3 1 7324.67 7676.45 53.91 o -5 3 1 9770.00 9513.18 109.16 o -4 3 1 1.68 14.99 11.64 o -3 3 1 34044.33 36880.54 366.41 o -2 3 1 4505.62 5226.90 35.96 o -1 3 1 12294.05 13732.44 365.31 o 0 3 1 32.30 26.42 13.82 o 1 3 1 35843.07 37219.58 894.14 o 2 3 1 21574.81 24258.37 369.12 o 3 3 1 20517.99 22595.53 901.46 o 4 3 1 7085.60 6999.22 124.37 o 5 3 1 13620.11 13322.38 91.84 o 6 3 1 673.80 704.09 17.67 o 7 3 1 13211.26 12442.76 302.45 o 8 3 1 397.24 378.76 24.22 o 9 3 1 326.01 308.87 20.42 o 10 3 1 264.53 205.38 25.97 o 11 3 1 1059.40 945.78 44.28 o 12 3 1 289.98 240.88 30.26 o 13 3 1 27.48 32.02 25.46 o -14 4 1 8.18 24.67 23.24 o -13 4 1 1225.58 1023.42 67.93 o -12 4 1 73.62 32.18 22.57 o -11 4 1 1853.44 1738.20 169.49 o -10 4 1 96.84 94.19 15.87 o -9 4 1 5476.96 5248.28 196.08 o -8 4 1 960.05 958.83 22.14 o -7 4 1 4220.02 4183.94 39.01 o -6 4 1 3026.86 2888.68 29.92 o -5 4 1 6226.09 6330.34 126.20 o -4 4 1 11388.82 12406.68 122.93 o -3 4 1 1432.01 1268.35 23.81 o -2 4 1 4690.97 4899.14 126.09 o -1 4 1 102.85 305.31 39.84 o 0 4 1 1253.18 1489.03 51.32 o 1 4 1 15436.20 17021.48 248.41 o 2 4 1 12058.03 13893.46 485.25 o 3 4 1 513.50 552.61 24.36 o 4 4 1 127.12 152.05 14.26 o 5 4 1 1601.70 1615.54 32.27 o 6 4 1 2330.67 2519.91 113.28 o 7 4 1 885.60 937.93 36.70 o 8 4 1 1076.51 988.44 64.65 o 9 4 1 184.80 162.13 18.47 o 10 4 1 182.12 163.37 24.30 o 11 4 1 1066.86 896.05 45.39 o 12 4 1 231.57 247.09 31.10 o 13 4 1 294.08 268.86 32.94 o -14 5 1 49.72 66.64 25.08 o -13 5 1 60.36 107.47 26.11 o -12 5 1 824.66 758.74 41.24 o -11 5 1 18.24 31.15 20.39 o -10 5 1 13.68 21.81 13.82 o -9 5 1 3054.33 3030.03 108.35 o -8 5 1 22.01 33.31 13.21 o -7 5 1 3905.39 3694.58 37.29 o -6 5 1 1.76 -7.81 10.56 o -5 5 1 10120.91 10717.40 111.99 o -4 5 1 3557.95 4216.70 61.91 o -3 5 1 9071.26 9655.19 132.34 o -2 5 1 966.39 908.06 27.24 o -1 5 1 3385.40 3662.02 221.44 o 0 5 1 3788.55 4474.14 193.53 o 1 5 1 52099.43 51453.18 150.88 o 2 5 1 127.36 96.79 24.81 o 3 5 1 184.83 151.84 13.38 o 4 5 1 235.98 236.45 15.26 o 5 5 1 18075.76 17719.21 463.68 o 6 5 1 2065.58 1929.73 94.19 o 7 5 1 1502.59 1382.45 59.58 o 8 5 1 64.78 56.49 17.65 o 9 5 1 4614.19 4069.58 234.86 o 10 5 1 64.94 79.79 22.05 o 11 5 1 2483.39 2158.43 123.35 o 12 5 1 393.99 408.40 35.75 o 13 5 1 512.84 437.10 55.20 o -14 6 1 125.34 119.68 41.40 o -13 6 1 1389.98 1265.20 62.10 o -12 6 1 1.21 11.65 23.75 o -11 6 1 1900.90 1767.17 147.50 o -10 6 1 70.40 84.11 16.53 o -9 6 1 6696.92 6707.47 108.28 o -8 6 1 489.91 440.75 17.99 o -7 6 1 197.10 211.12 14.22 o -6 6 1 6091.60 6191.24 70.94 o -5 6 1 9034.78 9445.56 120.83 o -4 6 1 117.28 115.66 14.78 o -3 6 1 66.10 124.79 23.92 o -2 6 1 8952.94 8659.91 140.86 o -1 6 1 40.92 94.55 26.76 o 0 6 1 1827.11 1603.09 135.10 o 1 6 1 2365.35 2361.22 77.16 o 2 6 1 4117.56 4390.38 39.68 o 3 6 1 181.11 149.11 18.30 o 4 6 1 6771.87 6646.49 55.00 o 5 6 1 125.95 126.43 16.55 o 6 6 1 2323.42 2274.59 129.30 o 7 6 1 185.52 140.15 18.94 o 8 6 1 988.76 865.34 31.28 o 9 6 1 194.84 197.94 24.81 o 10 6 1 462.34 376.07 62.64 o 11 6 1 1116.21 1001.10 128.95 o 12 6 1 15.67 32.99 25.55 o 13 6 1 82.51 53.86 26.77 o -14 7 1 15.37 30.19 40.32 o -13 7 1 31.11 62.01 26.25 o -12 7 1 298.91 309.92 42.59 o -11 7 1 224.80 231.95 27.04 o -10 7 1 247.89 259.30 19.77 o -9 7 1 3385.64 3312.40 76.26 o -8 7 1 56.49 62.49 11.43 o -7 7 1 3236.63 3083.50 60.49 o -6 7 1 7665.62 7664.67 83.35 o -5 7 1 983.52 1159.47 22.55 o -4 7 1 4892.66 5154.47 59.54 o -3 7 1 1090.04 1020.56 29.58 o -2 7 1 5632.00 5417.00 148.60 o -1 7 1 8567.84 9006.88 449.09 o 0 7 1 1091.04 962.82 100.04 o 1 7 1 24114.76 24716.21 346.98 o 2 7 1 5241.53 5061.53 54.69 o 3 7 1 14287.22 14636.86 76.49 o 4 7 1 215.14 263.28 32.27 o 5 7 1 9334.19 9016.21 272.50 o 6 7 1 65.90 26.03 16.47 o 7 7 1 3891.65 3543.04 313.07 o 8 7 1 24.10 8.07 12.11 o 9 7 1 978.99 810.52 87.44 o 10 7 1 93.86 77.95 23.63 o 11 7 1 298.75 307.70 33.01 o 12 7 1 221.56 170.40 42.37 o 13 7 1 190.29 198.18 32.52 o -13 8 1 191.59 208.03 53.59 o -12 8 1 3.05 28.28 25.84 o -11 8 1 262.80 254.25 29.08 o -10 8 1 32.06 40.50 15.55 o -9 8 1 1894.94 1964.48 36.01 o -8 8 1 1046.50 1082.80 32.25 o -7 8 1 1909.39 1865.75 79.72 o -6 8 1 20.98 16.64 14.73 o -5 8 1 14286.47 14121.11 208.04 o -4 8 1 804.70 903.21 31.96 o -3 8 1 284.91 293.34 13.55 o -2 8 1 1208.95 1054.80 74.98 o -1 8 1 8356.56 8909.25 369.99 o 0 8 1 8323.65 8146.23 1058.46 o 1 8 1 14.33 39.34 11.36 o 2 8 1 2164.34 2340.55 79.20 o 3 8 1 2.44 -6.50 11.06 o 4 8 1 5865.90 5826.49 110.50 o 5 8 1 1519.53 1478.29 68.90 o 6 8 1 14.82 27.23 17.04 o 7 8 1 3113.67 2798.13 260.74 o 8 8 1 504.47 442.83 30.57 o 9 8 1 38.94 39.15 13.67 o 10 8 1 233.59 162.14 26.45 o 11 8 1 428.00 373.17 34.84 o 12 8 1 44.63 15.24 25.20 o 13 8 1 1.33 20.05 38.82 o -13 9 1 545.40 613.49 59.73 o -12 9 1 1034.69 1068.06 71.38 o -11 9 1 1.52 -4.64 22.03 o -10 9 1 1325.92 1299.94 42.30 o -9 9 1 182.13 181.26 15.61 o -8 9 1 295.50 329.65 15.14 o -7 9 1 41.46 86.92 27.33 o -6 9 1 22.47 26.73 14.83 o -5 9 1 5.11 25.87 15.03 o -4 9 1 2202.26 2127.09 42.31 o -3 9 1 21678.23 20547.19 324.45 o -2 9 1 284.43 224.18 31.68 o -1 9 1 22545.52 22672.40 377.82 o 0 9 1 2169.92 1960.01 165.48 o 1 9 1 15666.44 15119.23 351.64 o 2 9 1 3079.24 3096.19 120.14 o 3 9 1 121.39 130.35 10.24 o 4 9 1 758.22 742.05 17.03 o 5 9 1 2612.57 2686.97 71.95 o 6 9 1 171.89 208.18 13.10 o 7 9 1 1719.31 1608.77 183.31 o 8 9 1 41.90 36.76 16.60 o 9 9 1 3881.61 3683.93 194.11 o 10 9 1 9.00 15.41 22.33 o 11 9 1 15.54 20.97 25.34 o 12 9 1 6.49 26.94 26.45 o -13 10 1 455.47 458.02 54.77 o -12 10 1 9.90 50.24 35.80 o -11 10 1 574.36 593.01 53.69 o -10 10 1 1286.57 1254.22 43.82 o -9 10 1 924.15 952.88 29.45 o -8 10 1 397.95 428.43 19.76 o -7 10 1 2891.63 3054.67 57.31 o -6 10 1 3054.90 3118.49 69.16 o -5 10 1 1865.10 1813.64 42.46 o -4 10 1 1470.90 1443.20 34.86 o -3 10 1 96.27 148.12 21.95 o -2 10 1 263.92 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182.88 o -5 6 2 6484.44 6777.09 164.03 o -4 6 2 1497.03 1616.50 44.55 o -3 6 2 1307.59 1430.28 29.41 o -2 6 2 13703.56 13891.75 300.47 o -1 6 2 29.48 6.92 11.89 o 0 6 2 2248.12 2435.90 55.46 o 1 6 2 184.89 240.08 9.52 o 2 6 2 25508.71 27910.07 429.49 o 3 6 2 3934.18 4003.27 123.27 o 4 6 2 21960.59 22692.69 237.53 o 5 6 2 112.47 132.05 17.86 o 6 6 2 5510.38 5351.21 59.34 o 7 6 2 63.02 113.39 18.85 o 8 6 2 3004.11 2865.91 156.18 o 9 6 2 149.20 148.35 18.40 o 10 6 2 46.32 20.69 16.46 o 11 6 2 177.74 152.81 28.71 o 12 6 2 476.64 370.99 52.83 o -14 7 2 58.74 65.92 24.31 o -13 7 2 1.48 24.31 23.08 o -12 7 2 2742.13 2726.13 181.03 o -11 7 2 3.40 15.56 15.30 o -10 7 2 675.94 607.76 25.13 o -9 7 2 576.44 596.56 33.80 o -8 7 2 7646.62 7677.36 199.29 o -7 7 2 89.22 114.03 12.60 o -6 7 2 4118.30 4397.32 40.92 o -5 7 2 5303.89 5345.50 132.55 o -4 7 2 11493.19 11635.80 301.59 o -3 7 2 2794.45 2904.29 59.26 o -2 7 2 888.53 898.33 33.49 o -1 7 2 496.86 410.86 18.28 o 0 7 2 504.25 512.62 17.04 o 1 7 2 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