#------------------------------------------------------------------------------
#$Date: 2016-04-02 21:39:39 +0300 (Sat, 02 Apr 2016) $
#$Revision: 180796 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/27/2012794.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2012794_Fobs
loop_
_publ_author_name
'Ayed, Brahim'
'Krifa, Mohamed'
'Haddad, Amor'
_publ_section_title
;
 Na~1.72~Mn~3.28~(AsO~4~)~3~
;
_journal_issue                   7
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              i98
_journal_page_last               i100
_journal_volume                  58
_journal_year                    2002
_space_group_IT_number           15
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_cell_angle_alpha                90.000
_cell_angle_beta                 113.845
_cell_angle_gamma                90.000
_cell_length_a                   12.1975
_cell_length_b                   12.9531
_cell_length_c                   6.7544
_exptl_crystal_F_000             1184.41
_reflns_d_resolution_high        0.7838
_cod_data_source_file            br1372Isup2.hkl
_cod_data_source_block           I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     '  hd36 in C 2/c'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            538.81
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 20547.68 16988.65 547.45 o
4 0 0 229111.50 224083.59 1970.14 o
6 0 0 531.46 420.08 508.55 o
8 0 0 78765.32 80074.02 2270.42 o
10 0 0 3056.07 2814.96 409.33 o
12 0 0 6804.22 6877.41 664.99 o
14 0 0 5159.32 7078.39 935.87 o
1 1 0 395.96 -56.78 440.99 o
3 1 0 34545.11 32648.39 805.90 o
5 1 0 32116.19 30197.79 1670.17 o
7 1 0 26060.97 23909.41 1011.43 o
9 1 0 3785.01 3737.38 834.59 o
11 1 0 14953.93 15491.25 1790.01 o
13 1 0 9557.84 9653.25 698.24 o
0 2 0 31545.62 35011.18 878.00 o
2 2 0 11176.45 14054.80 678.63 o
4 2 0 24842.64 24496.94 789.08 o
6 2 0 4110.97 4218.01 893.25 o
8 2 0 900.40 1296.99 663.79 o
10 2 0 5434.35 5759.90 440.61 o
12 2 0 85.35 32.43 858.58 o
14 2 0 2797.48 2852.82 1139.28 o
1 3 0 1848.34 2522.27 383.24 o
3 3 0 29746.75 27111.59 960.36 o
5 3 0 17389.86 16027.42 772.79 o
7 3 0 54988.94 54580.12 1409.62 o
9 3 0 4614.79 4575.11 409.11 o
11 3 0 24464.11 24969.73 1362.70 o
13 3 0 1416.49 1854.05 1012.90 o
0 4 0 17627.49 18142.39 968.20 o
2 4 0 251571.31 277069.03 4348.58 o
4 4 0 70.58 -160.11 940.88 o
6 4 0 119545.45 123049.93 1912.19 o
8 4 0 221.63 -176.41 730.83 o
10 4 0 11726.05 11826.05 873.69 o
12 4 0 3874.28 4133.67 561.72 o
1 5 0 1300.13 1046.77 586.99 o
3 5 0 32946.65 34486.45 1275.17 o
5 5 0 30075.01 29246.42 1882.84 o
7 5 0 296.16 588.67 675.86 o
9 5 0 23832.12 23529.26 2353.70 o
11 5 0 31.36 -597.63 852.87 o
13 5 0 14751.44 15745.78 2290.60 o
0 6 0 6972.16 5811.14 552.73 o
2 6 0 6022.60 5953.35 425.32 o
4 6 0 415.26 1082.42 738.51 o
6 6 0 3656.04 3731.71 366.61 o
8 6 0 7103.34 7584.40 528.09 o
10 6 0 503.85 1322.83 854.05 o
12 6 0 1428.30 1859.69 984.45 o
1 7 0 15104.77 15535.97 808.27 o
3 7 0 44.48 -496.80 617.90 o
5 7 0 33324.33 31606.46 1181.38 o
7 7 0 2435.04 2423.86 820.58 o
9 7 0 15658.99 16874.72 1126.67 o
11 7 0 441.96 252.43 2276.42 o
0 8 0 32551.03 34967.28 1606.41 o
2 8 0 1191.19 1511.06 685.28 o
4 8 0 11395.43 11816.01 929.44 o
6 8 0 1182.09 576.04 868.59 o
8 8 0 10390.97 10379.88 715.82 o
10 8 0 163.15 -821.84 1323.49 o
12 8 0 2628.46 3446.78 707.32 o
1 9 0 18770.30 19073.52 1799.18 o
3 9 0 8817.81 8932.29 638.07 o
5 9 0 8136.33 8287.51 592.97 o
7 9 0 12184.76 11414.35 768.79 o
9 9 0 4223.30 4342.66 846.40 o
11 9 0 10725.43 10452.66 804.17 o
0 10 0 21740.00 24682.15 1624.50 o
2 10 0 701.96 758.03 1095.90 o
4 10 0 9306.51 9450.25 636.53 o
6 10 0 10.78 -457.28 755.64 o
8 10 0 8891.71 8825.43 658.78 o
10 10 0 949.02 -974.04 974.04 o
1 11 0 5696.52 6253.40 482.15 o
3 11 0 786.87 1371.37 760.18 o
5 11 0 6349.55 6107.77 485.64 o
7 11 0 1672.76 116.41 1529.47 o
9 11 0 2077.15 810.05 990.30 o
0 12 0 92.46 401.95 1021.26 o
2 12 0 2996.57 2108.52 557.65 o
4 12 0 2308.85 1587.42 1047.14 o
6 12 0 377.31 184.33 899.57 o
8 12 0 1376.83 2337.76 994.17 o
1 13 0 2336.84 2802.41 464.20 o
3 13 0 5108.61 5567.37 517.32 o
5 13 0 2784.58 2518.41 761.20 o
7 13 0 625.10 1909.75 1049.66 o
0 14 0 125.94 -294.77 1265.42 o
2 14 0 24294.69 23621.63 1359.64 o
4 14 0 13.07 942.83 1598.85 o
6 14 0 13277.56 13013.80 1776.46 o
1 15 0 23.20 1413.07 926.26 o
3 15 0 1046.53 2553.30 864.33 o
5 15 0 1238.73 587.77 1058.95 o
0 16 0 4721.35 4562.78 846.39 o
2 16 0 58.82 710.77 1161.19 o
-13 1 1 147.59 1628.67 1107.62 o
-11 1 1 1786.30 1048.52 1254.05 o
-9 1 1 51.31 -1051.03 1051.03 o
-7 1 1 2826.57 1994.10 408.36 o
-5 1 1 2434.35 3401.75 351.80 o
-3 1 1 9030.74 9713.34 804.19 o
-1 1 1 458.62 387.30 503.49 o
1 1 1 1689.75 2746.81 331.05 o
3 1 1 1785.51 1281.68 301.04 o
5 1 1 595.63 1399.72 604.56 o
7 1 1 2811.70 3316.89 426.16 o
9 1 1 4916.74 5071.25 560.49 o
11 1 1 2313.11 2213.37 1349.47 o
13 1 1 4912.45 5910.06 765.95 o
-14 2 1 8975.42 9727.42 888.92 o
-12 2 1 3893.70 2854.96 1355.96 o
-10 2 1 7273.54 8073.12 772.70 o
-8 2 1 5402.99 5234.97 522.01 o
-6 2 1 7517.88 7862.80 782.70 o
-4 2 1 9504.81 12511.31 874.62 o
-2 2 1 6706.05 9054.54 704.11 o
0 2 1 419.14 1399.96 604.66 o
2 2 1 13016.13 15738.48 895.39 o
4 2 1 1949.36 1105.65 736.11 o
6 2 1 11399.97 12069.76 1088.28 o
8 2 1 3698.22 3576.72 521.61 o
10 2 1 3032.85 2869.36 586.98 o
12 2 1 314.60 217.36 1170.18 o
-13 3 1 2240.18 1730.70 673.22 o
-11 3 1 151.91 -416.85 1158.24 o
-9 3 1 594.55 1751.00 955.91 o
-7 3 1 99.83 1220.77 774.14 o
-5 3 1 5738.74 5675.93 582.22 o
-3 3 1 4149.07 3499.21 432.92 o
-1 3 1 23281.69 27337.88 1037.80 o
1 3 1 16282.02 17547.73 912.78 o
3 3 1 6754.27 6995.12 636.46 o
5 3 1 19078.90 19620.38 1221.02 o
7 3 1 14667.95 15623.14 1337.07 o
9 3 1 8961.69 8768.19 784.90 o
11 3 1 4517.41 4750.81 634.83 o
13 3 1 4138.85 5426.33 756.89 o
-14 4 1 14.90 -1473.80 1473.80 o
-12 4 1 3965.83 2407.92 1338.06 o
-10 4 1 2800.78 2428.38 560.17 o
-8 4 1 23981.96 26615.18 1554.13 o
-6 4 1 14361.65 12717.38 1095.96 o
-4 4 1 11309.64 9049.72 874.43 o
-2 4 1 5139.58 3599.48 349.49 o
0 4 1 44243.84 43481.42 1320.22 o
2 4 1 594.27 285.92 631.41 o
4 4 1 3644.75 3873.62 405.55 o
6 4 1 10468.73 9600.26 941.20 o
8 4 1 26.17 -580.59 967.65 o
10 4 1 6435.41 6652.76 781.27 o
12 4 1 748.61 565.79 1134.56 o
-13 5 1 1061.52 2016.13 649.21 o
-11 5 1 3464.74 2225.96 1346.90 o
-9 5 1 892.09 0.00 1170.40 o
-7 5 1 512.62 -53.60 911.23 o
-5 5 1 1151.70 -512.35 798.31 o
-3 5 1 247.80 899.28 631.28 o
-1 5 1 2267.37 1860.22 327.92 o
1 5 1 278.04 -35.73 655.12 o
3 5 1 7702.32 7244.41 687.10 o
5 5 1 6202.62 5857.48 581.87 o
7 5 1 1789.01 1957.16 1081.36 o
9 5 1 432.02 592.56 1083.88 o
11 5 1 242.78 842.64 1161.23 o
-12 6 1 7964.85 6606.53 784.43 o
-10 6 1 4757.93 5675.71 855.53 o
-8 6 1 9376.21 9004.42 901.64 o
-6 6 1 4756.96 5839.31 486.11 o
-4 6 1 10297.23 11774.38 974.72 o
-2 6 1 3707.51 4974.80 605.45 o
0 6 1 5683.70 6442.41 626.93 o
2 6 1 64.99 -44.66 696.72 o
4 6 1 9248.87 11453.58 1042.59 o
6 6 1 1750.83 577.92 1021.78 o
8 6 1 2750.97 2720.30 1200.74 o
10 6 1 289.28 -887.31 1122.54 o
12 6 1 1.51 -241.17 1402.34 o
-13 7 1 2567.72 3416.84 1653.31 o
-11 7 1 6058.17 6806.77 727.49 o
-9 7 1 301.71 470.46 1054.07 o
-7 7 1 1021.93 1408.73 1048.35 o
-5 7 1 8848.37 7773.85 782.46 o
-3 7 1 954.83 1346.27 857.80 o
-1 7 1 39895.80 41803.09 1616.08 o
1 7 1 17312.95 17385.43 1184.21 o
3 7 1 57696.70 60878.20 1990.28 o
5 7 1 23637.17 23505.22 1637.60 o
7 7 1 35832.10 37690.16 1996.03 o
9 7 1 5489.34 5846.21 673.76 o
11 7 1 7736.88 7935.74 784.33 o
-12 8 1 1188.55 -446.72 1325.26 o
-10 8 1 11424.71 11669.78 1119.51 o
-8 8 1 17798.35 18247.53 1591.42 o
-6 8 1 35977.39 35378.79 1917.00 o
-4 8 1 16578.95 16071.63 1338.30 o
-2 8 1 39531.37 43873.01 1754.56 o
0 8 1 25521.30 29808.22 1466.52 o
2 8 1 30578.01 30396.97 1573.55 o
4 8 1 1581.16 2275.82 941.31 o
6 8 1 1024.85 -449.71 1098.96 o
8 8 1 4547.95 4631.93 661.70 o
10 8 1 555.56 655.10 1223.84 o
-11 9 1 10.84 431.72 1310.04 o
-9 9 1 2272.16 2835.99 610.69 o
-7 9 1 250.25 -1116.59 1116.59 o
-5 9 1 10563.19 9658.82 1030.39 o
-3 9 1 6187.33 5978.46 554.89 o
-1 9 1 59.71 232.24 934.91 o
1 9 1 6737.73 6475.03 689.28 o
3 9 1 1.15 922.98 1024.21 o
5 9 1 11499.30 11633.37 1137.95 o
7 9 1 500.48 -178.66 1051.14 o
9 9 1 2246.92 950.25 1328.57 o
11 9 1 3.49 503.18 1363.63 o
-10 10 1 4977.15 5004.44 724.29 o
-8 10 1 5793.17 4275.48 733.45 o
-6 10 1 3718.75 3546.54 602.02 o
-4 10 1 9035.21 9358.08 1023.87 o
-2 10 1 5142.86 5680.62 769.34 o
0 10 1 2122.23 2350.65 539.25 o
2 10 1 4812.02 4910.57 572.45 o
4 10 1 776.41 1623.00 1045.27 o
6 10 1 41.60 532.95 1107.59 o
8 10 1 1829.68 104.25 1292.71 o
10 10 1 375.77 0.00 1581.10 o
-11 11 1 823.26 488.37 1599.11 o
-9 11 1 9654.01 9285.20 1014.45 o
-7 11 1 2595.11 1462.79 1260.21 o
-5 11 1 2675.74 3065.82 598.86 o
-3 11 1 19001.33 18043.02 1690.88 o
-1 11 1 122.25 884.31 1036.16 o
1 11 1 42299.45 39119.59 2156.41 o
3 11 1 10600.60 12912.78 1286.80 o
5 11 1 43072.39 44056.00 2328.55 o
7 11 1 9405.08 10099.66 799.62 o
9 11 1 17622.19 16656.28 1461.23 o
-10 12 1 6313.41 3756.30 1735.05 o
-8 12 1 10958.36 9893.62 949.07 o
-6 12 1 21314.54 25257.27 1923.99 o
-4 12 1 12403.60 12830.07 1352.89 o
-2 12 1 17344.91 17019.47 1465.39 o
0 12 1 14554.89 16932.94 1631.73 o
2 12 1 8492.95 9619.47 1232.27 o
4 12 1 1397.22 1304.52 1259.85 o
6 12 1 521.52 940.96 1316.15 o
8 12 1 18.57 -357.29 1610.76 o
-9 13 1 2309.74 2153.65 765.54 o
-7 13 1 2256.45 3032.44 1319.62 o
-5 13 1 2486.15 1683.17 1349.51 o
-3 13 1 584.11 741.47 1328.09 o
-1 13 1 11900.50 10331.24 967.43 o
1 13 1 1552.19 554.00 1334.35 o
3 13 1 2463.06 2880.75 640.50 o
5 13 1 25.20 -1506.56 1506.56 o
7 13 1 5354.44 5389.03 810.74 o
-8 14 1 4.06 369.19 1560.14 o
-6 14 1 4279.24 2148.63 1731.42 o
-4 14 1 1194.99 0.00 1402.71 o
-2 14 1 10154.81 11372.78 1011.64 o
0 14 1 4.50 -1289.20 1289.20 o
2 14 1 5653.03 7142.74 724.41 o
4 14 1 171.54 -774.14 1298.18 o
6 14 1 244.83 491.29 1461.96 o
-5 15 1 2703.81 2135.96 1537.18 o
-3 15 1 612.77 2120.16 1226.83 o
-1 15 1 9289.96 8105.65 918.86 o
1 15 1 1377.71 2004.36 1444.45 o
3 15 1 15674.19 16936.78 1747.45 o
5 15 1 2176.08 3181.22 786.37 o
-2 16 1 790.57 0.00 1557.41 o
0 16 1 9513.73 7365.41 874.06 o
2 16 1 98.58 3346.63 1339.84 o
-14 0 2 1986.25 2085.05 655.30 o
-12 0 2 46210.05 46464.34 2270.37 o
-10 0 2 162.10 619.32 1003.42 o
-8 0 2 138301.58 138630.61 2921.50 o
-6 0 2 11306.26 10765.33 900.85 o
-4 0 2 91998.98 85353.45 1743.77 o
-2 0 2 3771.98 3998.20 355.33 o
0 0 2 61438.29 56684.65 1375.36 o
2 0 2 20950.42 18606.85 1005.61 o
4 0 2 926.98 89.35 598.68 o
6 0 2 56731.05 55292.23 2006.88 o
8 0 2 680.34 2161.96 899.33 o
10 0 2 47760.84 49244.43 2468.24 o
12 0 2 3473.03 1552.31 1439.09 o
-15 1 2 46.44 604.41 1411.28 o
-13 1 2 288.45 1855.02 1199.96 o
-11 1 2 876.85 1783.86 947.02 o
-9 1 2 3189.30 3490.04 476.86 o
-7 1 2 13839.33 13103.97 1008.92 o
-5 1 2 2145.26 1138.63 315.96 o
-3 1 2 70006.64 67692.31 1449.41 o
-1 1 2 85051.00 91285.87 1618.08 o
1 1 2 63077.17 56109.45 1412.16 o
3 1 2 14948.22 13993.87 956.31 o
5 1 2 33409.94 34210.88 1551.62 o
7 1 2 9293.94 8932.43 943.40 o
9 1 2 5319.44 4731.29 572.41 o
11 1 2 405.84 -434.73 1253.58 o
-14 2 2 8044.04 7602.38 838.08 o
-12 2 2 4158.71 4559.99 664.63 o
-10 2 2 7506.68 7235.63 626.59 o
-8 2 2 27971.08 27372.22 1488.11 o
-6 2 2 21074.11 19898.90 1135.88 o
-4 2 2 19887.78 15949.32 906.31 o
-2 2 2 31068.02 30191.48 1057.86 o
0 2 2 27015.96 24086.46 1017.61 o
2 2 2 5667.54 4774.50 540.45 o
4 2 2 27524.01 28659.73 1294.10 o
6 2 2 12977.14 13369.47 1174.91 o
8 2 2 4231.97 4146.16 521.62 o
10 2 2 7883.59 8453.08 808.32 o
12 2 2 5272.87 6035.64 760.04 o
-15 3 2 3259.40 3223.63 1668.42 o
-13 3 2 21.53 580.59 1116.52 o
-11 3 2 11113.98 11000.19 1062.99 o
-9 3 2 7953.41 6846.75 620.80 o
-7 3 2 133.64 747.36 634.21 o
-5 3 2 72480.25 67594.40 1717.25 o
-3 3 2 59.07 -601.45 601.45 o
-1 3 2 119867.07 117016.80 1989.06 o
1 3 2 5386.91 9032.25 803.20 o
3 3 2 107687.23 103543.48 2233.36 o
5 3 2 4871.84 4768.72 468.22 o
7 3 2 38766.32 38201.25 1932.34 o
9 3 2 1233.27 1352.13 1072.17 o
11 3 2 1353.00 -1337.22 1367.01 o
-14 4 2 18196.48 18255.17 1694.61 o
-12 4 2 1825.55 2031.44 577.86 o
-10 4 2 46412.00 46229.45 2044.19 o
-8 4 2 12984.39 11460.44 1067.41 o
-6 4 2 94106.06 86104.56 2132.63 o
-4 4 2 2511.69 2888.53 363.68 o
-2 4 2 12129.47 11267.59 812.11 o
0 4 2 38.17 -101.23 559.76 o
2 4 2 7290.91 7443.38 695.95 o
4 4 2 30802.93 29690.82 1423.88 o
6 4 2 2571.57 2663.82 429.07 o
8 4 2 35211.36 35474.78 1871.52 o
10 4 2 4455.98 4893.70 637.79 o
-13 5 2 168.89 101.23 1256.49 o
-11 5 2 5251.42 2733.80 1353.48 o
-9 5 2 7056.53 7625.56 832.37 o
-7 5 2 32365.66 31907.76 1453.77 o
-5 5 2 4328.65 4852.60 492.12 o
-3 5 2 61237.89 62812.32 1695.23 o
-1 5 2 15573.14 18709.78 1022.77 o
1 5 2 53938.50 57202.01 1712.16 o
3 5 2 2018.22 1957.60 372.45 o
5 5 2 39765.64 37304.76 1733.21 o
7 5 2 4234.74 4110.44 500.76 o
9 5 2 6354.71 6020.21 655.99 o
11 5 2 58.14 759.24 598.46 o
-14 6 2 353.89 -348.38 1521.54 o
-12 6 2 3159.03 1433.14 1331.84 o
-10 6 2 1631.88 2055.24 559.98 o
-8 6 2 2120.83 2225.49 479.66 o
-6 6 2 7022.58 6768.98 656.60 o
-4 6 2 206.72 223.32 702.72 o
-2 6 2 16990.54 17895.96 1091.51 o
0 6 2 5629.90 5288.14 584.92 o
2 6 2 3215.07 3380.36 381.56 o
4 6 2 2272.12 1042.84 920.68 o
6 6 2 3408.06 3394.42 506.63 o
8 6 2 2928.07 3795.85 545.24 o
10 6 2 760.94 1063.09 1030.34 o
-13 7 2 6016.90 6278.25 885.39 o
-11 7 2 2762.30 3241.47 610.75 o
-9 7 2 10205.89 10147.32 871.73 o
-7 7 2 15339.29 17013.25 1411.79 o
-5 7 2 12333.11 13848.90 1130.16 o
-3 7 2 81992.32 82828.25 2186.55 o
-1 7 2 5856.77 6895.96 638.57 o
1 7 2 84291.55 81525.91 2262.82 o
3 7 2 7618.40 8058.60 823.77 o
5 7 2 38188.46 32919.98 1874.86 o
7 7 2 7843.82 7043.30 712.98 o
9 7 2 6773.64 6273.80 682.84 o
11 7 2 2524.02 2186.49 1575.83 o
-12 8 2 5523.94 3135.91 1472.57 o
-10 8 2 2485.05 521.35 1221.44 o
-8 8 2 3304.54 3614.74 518.52 o
-6 8 2 5704.29 5108.92 608.42 o
-4 8 2 3154.68 3102.64 467.93 o
-2 8 2 2039.28 2767.91 426.06 o
0 8 2 289.55 440.69 848.63 o
2 8 2 4277.77 3610.45 527.70 o
4 8 2 5811.27 7020.30 781.36 o
6 8 2 1460.85 810.14 1063.31 o
8 8 2 1398.02 1748.27 580.77 o
10 8 2 2157.67 1861.68 1325.52 o
-11 9 2 1521.16 1995.50 634.39 o
-9 9 2 20113.66 21418.34 1690.37 o
-7 9 2 287.17 664.00 854.57 o
-5 9 2 11168.30 12214.03 1081.31 o
-3 9 2 67.55 672.90 920.03 o
-1 9 2 46741.25 49071.36 1996.69 o
1 9 2 212.83 830.74 899.22 o
3 9 2 16184.77 17969.10 1483.47 o
5 9 2 129.50 1372.61 902.17 o
7 9 2 10565.44 11072.94 1107.29 o
9 9 2 433.72 0.00 1289.32 o
-12 10 2 2108.57 1751.44 1292.73 o
-10 10 2 338.74 -396.02 1339.91 o
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