#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/28/2012851.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012851_Fobs loop_ _publ_author_name 'Linden, Anthony' 'Majchrzak, Agnieszka' 'Cavegn, Jovita' 'Mloston, Grzegorz' 'Heimgartner, Heinz' _publ_section_title ; Four bis(1-chloro-2,2,4,4-tetramethyl-3-oxocyclobutan-1-yl)oligosulfanes ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o480 _journal_page_last o484 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 114.667 _cell_angle_gamma 90.000 _cell_length_a 13.0673 _cell_length_b 25.7808 _cell_length_c 13.1619 _exptl_crystal_F_000 1744.00 _reflns_d_resolution_high 0.7099 _[local]_cod_data_source_file bm1503Vsup3.hkl _[local]_cod_data_source_block V #BEGIN Tags that were not found in dictionaries: _shelx_title ' AM/6B.3.2.3 (HG0155)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 242.35 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 3719.15 3431.79 58.29 o 4 0 0 602.55 491.37 10.87 o 5 0 0 0.79 7.27 3.93 o 6 0 0 170.35 227.31 11.20 o 7 0 0 985.64 925.17 24.66 o 8 0 0 2979.36 2987.71 106.97 o 9 0 0 761.28 698.35 18.66 o 10 0 0 136.52 173.56 10.41 o 11 0 0 3858.04 3974.47 80.25 o 12 0 0 2372.40 2459.14 65.18 o 13 0 0 48.73 29.45 14.65 o 14 0 0 1664.63 1628.31 60.20 o 15 0 0 82.04 46.69 23.10 o 16 0 0 90.52 83.35 30.13 o 3 1 0 4720.11 4812.06 46.71 o 4 1 0 8183.29 8015.09 81.85 o 5 1 0 12556.25 12085.01 122.46 o 6 1 0 1146.93 1145.05 16.94 o 7 1 0 4001.41 3844.64 50.65 o 8 1 0 673.13 619.91 13.15 o 9 1 0 1394.70 1431.86 21.90 o 10 1 0 2056.36 2100.57 29.05 o 11 1 0 139.18 152.79 11.00 o 12 1 0 316.75 301.56 13.96 o 13 1 0 30.91 16.90 9.45 o 14 1 0 180.23 173.97 16.69 o 15 1 0 126.68 107.40 15.98 o 16 1 0 44.45 19.71 16.13 o 2 2 0 5471.01 5742.67 55.37 o 3 2 0 2211.86 2428.03 22.57 o 4 2 0 14592.02 14938.27 143.78 o 5 2 0 760.09 726.68 9.38 o 6 2 0 328.02 293.09 8.52 o 7 2 0 488.46 542.51 11.23 o 8 2 0 4970.90 5029.24 65.54 o 9 2 0 1607.68 1684.31 24.61 o 10 2 0 5.74 -3.82 5.09 o 11 2 0 3212.72 3354.36 51.09 o 12 2 0 276.00 302.45 13.86 o 13 2 0 39.52 11.02 10.99 o 14 2 0 289.50 298.77 18.37 o 15 2 0 201.55 193.60 20.48 o 16 2 0 133.80 118.06 20.77 o 1 3 0 845.05 639.71 55.92 o 2 3 0 82.43 75.03 1.45 o 3 3 0 233.84 195.72 3.08 o 4 3 0 24985.15 23921.51 250.07 o 5 3 0 1751.96 1584.39 17.95 o 6 3 0 19227.44 18995.44 209.31 o 7 3 0 448.31 479.26 9.95 o 8 3 0 448.43 363.90 11.06 o 9 3 0 6499.58 6425.89 83.96 o 10 3 0 1834.33 1734.99 26.79 o 11 3 0 953.34 1025.95 24.33 o 12 3 0 486.90 539.45 23.22 o 13 3 0 13.44 15.08 9.73 o 14 3 0 5.50 16.59 12.25 o 15 3 0 948.19 923.39 32.29 o 16 3 0 0.46 -11.80 21.45 o 0 4 0 3097.27 2723.63 87.18 o 1 4 0 28022.34 23532.14 3407.49 o 2 4 0 271.23 269.62 3.38 o 3 4 0 3722.83 3734.61 31.77 o 4 4 0 881.35 921.40 9.46 o 5 4 0 8361.42 8847.38 77.11 o 6 4 0 258.24 210.12 5.28 o 7 4 0 2108.57 2009.65 25.60 o 8 4 0 3657.46 3652.51 44.83 o 9 4 0 901.27 919.56 16.30 o 10 4 0 9.61 14.13 4.13 o 11 4 0 13.71 9.51 7.97 o 12 4 0 260.81 250.12 17.08 o 13 4 0 698.86 670.98 22.35 o 14 4 0 60.81 52.22 13.24 o 15 4 0 40.38 22.98 18.27 o 16 4 0 65.88 34.38 26.13 o 1 5 0 3255.42 3223.68 34.96 o 2 5 0 178.62 256.44 3.82 o 3 5 0 70.13 46.60 2.05 o 4 5 0 2265.42 2500.80 23.21 o 5 5 0 2532.51 2112.18 21.37 o 6 5 0 505.39 343.44 8.16 o 7 5 0 3551.97 3392.59 41.35 o 8 5 0 621.73 635.54 14.89 o 9 5 0 7605.82 7772.90 102.84 o 10 5 0 1141.73 1129.40 19.23 o 11 5 0 422.96 384.46 13.50 o 12 5 0 679.81 700.54 21.93 o 13 5 0 157.15 157.23 13.91 o 14 5 0 135.17 119.43 13.45 o 15 5 0 273.10 239.83 23.88 o 16 5 0 10.74 -12.65 24.50 o 0 6 0 112.41 102.82 3.87 o 1 6 0 656.22 656.32 7.97 o 2 6 0 588.46 539.34 10.63 o 3 6 0 2660.37 2443.84 21.82 o 4 6 0 12.21 17.81 4.78 o 5 6 0 120.23 132.29 3.97 o 6 6 0 4905.96 5319.13 55.56 o 7 6 0 2928.60 2785.11 32.76 o 8 6 0 64.75 76.71 5.35 o 9 6 0 4201.87 4401.10 59.50 o 10 6 0 55.85 66.81 7.56 o 11 6 0 99.18 103.55 9.02 o 12 6 0 308.92 279.71 15.33 o 13 6 0 523.03 511.40 20.77 o 14 6 0 460.29 428.44 20.61 o 15 6 0 624.04 686.36 38.06 o 16 6 0 49.99 70.63 26.08 o 1 7 0 5491.64 5295.36 50.91 o 2 7 0 36543.48 35709.58 634.67 o 3 7 0 4437.61 4488.84 38.15 o 4 7 0 8465.99 8172.70 80.03 o 5 7 0 1117.89 949.85 10.85 o 6 7 0 111.06 100.23 4.02 o 7 7 0 937.30 850.29 12.92 o 8 7 0 4590.42 4460.48 56.92 o 9 7 0 528.25 464.54 11.55 o 10 7 0 1166.92 1139.06 20.76 o 11 7 0 860.26 769.66 21.02 o 12 7 0 5.28 11.06 10.70 o 13 7 0 211.30 224.82 16.33 o 14 7 0 411.62 414.75 23.70 o 15 7 0 769.97 760.99 39.33 o 16 7 0 142.67 135.01 29.69 o 0 8 0 3049.26 3050.34 50.06 o 1 8 0 27167.84 26545.33 349.60 o 2 8 0 38102.98 39704.02 630.97 o 3 8 0 6101.84 5762.94 62.10 o 4 8 0 4421.35 4201.04 40.76 o 5 8 0 2959.31 3243.46 37.55 o 6 8 0 53.38 37.47 3.61 o 7 8 0 6287.01 6385.45 68.35 o 8 8 0 318.86 300.75 9.73 o 9 8 0 9.67 7.05 5.38 o 10 8 0 2145.25 2061.94 35.55 o 11 8 0 1952.31 1993.93 36.72 o 12 8 0 178.73 195.47 12.96 o 13 8 0 804.05 815.02 27.99 o 14 8 0 292.12 322.20 29.50 o 15 8 0 272.48 240.23 26.34 o 16 8 0 1.73 18.63 27.02 o 1 9 0 32.44 4.80 3.17 o 2 9 0 10774.98 11145.67 234.61 o 3 9 0 32118.46 32918.65 415.59 o 4 9 0 802.80 748.84 8.69 o 5 9 0 5900.29 6129.10 67.14 o 6 9 0 7.90 11.79 3.90 o 7 9 0 6450.72 6543.13 73.61 o 8 9 0 2046.29 2023.58 28.36 o 9 9 0 930.84 844.97 14.92 o 10 9 0 155.38 189.34 10.33 o 11 9 0 505.77 447.24 15.68 o 12 9 0 976.21 972.55 25.72 o 13 9 0 161.19 134.43 15.18 o 14 9 0 73.24 38.42 18.85 o 15 9 0 65.35 41.37 20.28 o 16 9 0 13.87 15.89 38.08 o 0 10 0 4906.59 5013.37 115.94 o 1 10 0 2702.63 2787.03 34.72 o 2 10 0 58735.60 58754.70 1628.08 o 3 10 0 5179.86 5532.10 55.74 o 4 10 0 9232.63 9430.14 103.28 o 5 10 0 329.43 251.34 5.45 o 6 10 0 1531.87 1397.17 19.74 o 7 10 0 726.72 640.76 13.08 o 8 10 0 204.73 229.91 8.10 o 9 10 0 0.09 17.93 5.52 o 10 10 0 544.28 578.06 15.39 o 11 10 0 2256.91 2299.70 44.05 o 12 10 0 250.87 261.85 15.50 o 13 10 0 235.92 237.68 19.88 o 14 10 0 680.63 593.72 36.27 o 15 10 0 274.14 303.12 29.60 o 16 10 0 351.29 260.71 38.71 o 1 11 0 3.83 5.45 2.55 o 2 11 0 901.95 842.06 13.28 o 3 11 0 624.04 575.42 9.60 o 4 11 0 4649.21 4888.24 53.49 o 5 11 0 55.36 28.15 4.56 o 6 11 0 764.31 835.22 12.78 o 7 11 0 768.88 685.11 13.08 o 8 11 0 823.26 855.08 17.96 o 9 11 0 1369.15 1300.70 26.52 o 10 11 0 7.07 1.02 5.89 o 11 11 0 1271.36 1309.90 34.95 o 12 11 0 258.88 269.69 15.54 o 13 11 0 1276.45 1321.64 64.69 o 14 11 0 1.08 2.27 19.72 o 15 11 0 86.49 33.75 22.76 o 0 12 0 4562.02 4875.33 94.72 o 1 12 0 852.46 967.39 15.46 o 2 12 0 145.97 99.26 3.93 o 3 12 0 816.50 797.15 12.47 o 4 12 0 536.40 609.86 11.00 o 5 12 0 1908.99 1989.68 28.13 o 6 12 0 151.98 136.78 4.80 o 7 12 0 375.62 392.92 10.67 o 8 12 0 3136.55 3061.12 47.98 o 9 12 0 1000.01 948.98 21.32 o 10 12 0 1113.03 1063.44 28.51 o 11 12 0 90.44 91.64 15.38 o 12 12 0 58.99 45.35 12.39 o 13 12 0 19.26 25.13 22.16 o 14 12 0 52.97 37.70 22.15 o 15 12 0 135.31 139.20 30.32 o 1 13 0 455.46 463.54 11.54 o 2 13 0 1556.25 1620.36 22.94 o 3 13 0 3930.91 3768.74 49.16 o 4 13 0 1624.03 1529.42 22.63 o 5 13 0 4788.41 4810.68 58.58 o 6 13 0 241.64 225.52 9.30 o 7 13 0 7652.25 7933.92 104.68 o 8 13 0 3.71 16.76 5.44 o 9 13 0 756.89 712.43 22.87 o 10 13 0 784.06 806.45 26.73 o 11 13 0 1514.26 1498.83 35.56 o 12 13 0 188.38 154.63 16.94 o 13 13 0 1183.76 1185.04 42.44 o 14 13 0 193.32 146.86 25.05 o 15 13 0 338.61 289.19 39.13 o 0 14 0 6325.26 6444.37 300.92 o 1 14 0 1043.97 1111.56 17.83 o 2 14 0 430.94 448.36 10.40 o 3 14 0 6774.69 6635.44 88.40 o 4 14 0 31.75 53.61 4.94 o 5 14 0 52.46 41.96 5.26 o 6 14 0 238.47 241.28 8.18 o 7 14 0 240.05 232.02 12.27 o 8 14 0 259.01 274.24 11.16 o 9 14 0 723.65 690.25 22.07 o 10 14 0 21.20 11.24 10.69 o 11 14 0 1028.20 1038.92 39.70 o 12 14 0 265.64 269.10 20.86 o 13 14 0 246.16 229.06 23.92 o 14 14 0 0.34 -20.59 20.85 o 15 14 0 137.55 113.89 29.68 o 1 15 0 346.43 349.62 11.07 o 2 15 0 42.68 21.65 6.19 o 3 15 0 1059.55 1004.65 20.60 o 4 15 0 396.47 411.85 10.37 o 5 15 0 4679.74 4664.24 66.85 o 6 15 0 67.04 49.25 7.69 o 7 15 0 821.87 777.09 21.29 o 8 15 0 300.39 332.52 15.77 o 9 15 0 3035.87 3112.11 61.39 o 10 15 0 52.28 58.36 12.17 o 11 15 0 1063.94 1076.68 51.66 o 12 15 0 567.00 651.86 31.80 o 13 15 0 612.99 607.12 48.19 o 14 15 0 297.22 326.39 31.97 o 15 15 0 330.03 310.60 41.25 o 0 16 0 4770.31 4311.52 97.85 o 1 16 0 765.97 762.55 17.19 o 2 16 0 343.93 318.63 11.97 o 3 16 0 648.07 575.82 18.29 o 4 16 0 6.95 8.19 5.87 o 5 16 0 3232.60 3336.32 43.74 o 6 16 0 523.89 460.31 17.36 o 7 16 0 99.30 127.65 10.52 o 8 16 0 4371.38 4389.32 76.54 o 9 16 0 535.87 511.79 21.11 o 10 16 0 1186.09 1163.71 32.05 o 11 16 0 0.42 28.44 15.45 o 12 16 0 61.08 47.23 18.06 o 13 16 0 131.35 118.37 22.72 o 14 16 0 238.04 222.97 29.42 o 15 16 0 41.49 26.47 39.15 o 1 17 0 2940.94 2961.60 52.91 o 2 17 0 3134.94 3156.35 46.64 o 3 17 0 2219.54 2159.65 36.63 o 4 17 0 1011.24 1033.90 25.52 o 5 17 0 253.19 320.56 19.53 o 6 17 0 16.35 4.84 6.73 o 7 17 0 283.07 304.41 14.37 o 8 17 0 151.60 159.25 11.16 o 9 17 0 872.75 858.60 33.41 o 10 17 0 1.80 11.98 12.61 o 11 17 0 742.50 756.12 31.48 o 12 17 0 2268.25 2533.19 69.66 o 13 17 0 79.74 134.63 28.56 o 14 17 0 99.70 106.04 25.70 o 0 18 0 28653.81 29069.21 1041.80 o 1 18 0 9495.31 9337.23 174.79 o 2 18 0 3876.58 4000.86 63.26 o 3 18 0 127.11 111.92 11.06 o 4 18 0 157.90 209.44 12.16 o 5 18 0 238.62 275.94 12.59 o 6 18 0 210.19 224.86 14.92 o 7 18 0 33.31 38.39 10.75 o 8 18 0 1240.37 1199.75 31.40 o 9 18 0 2908.80 3059.28 60.44 o 10 18 0 556.84 532.91 33.77 o 11 18 0 23.56 18.10 16.49 o 12 18 0 619.70 613.41 34.05 o 13 18 0 0.04 16.27 23.38 o 14 18 0 688.01 636.80 42.65 o 1 19 0 1275.30 1266.03 30.26 o 2 19 0 691.90 751.37 16.90 o 3 19 0 446.01 374.46 19.82 o 4 19 0 63.21 78.86 10.63 o 5 19 0 230.83 218.19 11.09 o 6 19 0 348.06 324.90 17.01 o 7 19 0 1499.18 1468.96 33.70 o 8 19 0 19.84 -7.31 8.95 o 9 19 0 1.31 -3.09 10.75 o 10 19 0 2418.77 2486.85 62.41 o 11 19 0 7.98 -14.40 17.93 o 12 19 0 1220.71 1344.98 77.51 o 13 19 0 260.28 262.01 29.76 o 14 19 0 1235.78 1176.39 73.67 o 0 20 0 609.11 520.55 28.45 o 1 20 0 5470.47 5423.35 97.25 o 2 20 0 0.68 -0.45 4.23 o 3 20 0 5163.79 4801.25 71.52 o 4 20 0 545.31 553.20 20.51 o 5 20 0 238.46 238.92 12.80 o 6 20 0 2854.90 2851.69 62.92 o 7 20 0 3636.37 3580.70 77.20 o 8 20 0 292.00 276.58 15.41 o 9 20 0 2007.70 2093.71 53.35 o 10 20 0 497.28 527.44 30.62 o 11 20 0 975.97 963.12 43.22 o 12 20 0 58.42 40.56 24.42 o 13 20 0 15.36 10.65 25.01 o 1 21 0 1079.57 992.50 27.35 o 2 21 0 1435.83 1403.20 29.19 o 3 21 0 18.74 8.69 7.12 o 4 21 0 2597.42 2800.11 51.24 o 5 21 0 1983.07 1955.55 44.44 o 6 21 0 352.79 335.58 18.09 o 7 21 0 9.21 4.79 9.39 o 8 21 0 2986.35 2956.71 72.62 o 9 21 0 69.43 54.10 18.98 o 10 21 0 227.02 248.49 32.11 o 11 21 0 148.49 136.69 23.50 o 12 21 0 76.23 108.74 29.52 o 13 21 0 18.37 31.03 25.53 o 0 22 0 5120.81 5051.23 117.91 o 1 22 0 3202.92 2808.69 57.99 o 2 22 0 3147.33 3236.16 53.45 o 3 22 0 144.20 165.82 14.01 o 4 22 0 1698.60 1664.57 35.28 o 5 22 0 2391.04 2413.79 56.73 o 6 22 0 2100.35 2058.10 50.89 o 7 22 0 20.15 33.32 11.01 o 8 22 0 9.90 1.89 14.11 o 9 22 0 167.69 132.43 16.48 o 10 22 0 25.15 3.52 19.49 o 11 22 0 161.83 158.40 27.15 o 12 22 0 121.85 86.33 30.28 o 13 22 0 583.79 436.48 47.04 o 1 23 0 88.27 94.11 10.00 o 2 23 0 2766.12 2968.41 51.12 o 3 23 0 2770.59 2665.68 55.03 o 4 23 0 172.78 139.37 13.79 o 5 23 0 4386.84 4485.39 82.16 o 6 23 0 3868.16 4022.74 90.39 o 7 23 0 663.10 705.55 25.38 o 8 23 0 2571.96 2877.59 67.62 o 9 23 0 1377.23 1575.41 57.39 o 10 23 0 47.23 69.32 25.05 o 11 23 0 64.29 50.16 21.15 o 12 23 0 379.51 333.85 37.06 o 0 24 0 1466.01 1525.15 54.63 o 1 24 0 1.08 6.64 7.68 o 2 24 0 2507.22 2578.79 46.10 o 3 24 0 247.17 181.95 12.20 o 4 24 0 1704.07 1773.10 40.08 o 5 24 0 105.03 91.06 13.89 o 6 24 0 441.77 400.79 21.49 o 7 24 0 1222.49 1391.40 39.55 o 8 24 0 757.33 762.82 58.82 o 9 24 0 448.61 489.27 35.62 o 10 24 0 1.65 22.44 24.00 o 11 24 0 104.97 70.01 28.19 o 12 24 0 74.25 49.48 27.77 o 1 25 0 346.64 369.46 15.47 o 2 25 0 712.32 717.66 23.87 o 3 25 0 1822.81 1957.49 41.86 o 4 25 0 2.56 14.90 9.98 o 5 25 0 2783.05 2853.68 68.92 o 6 25 0 93.19 56.37 13.40 o 7 25 0 1405.02 1459.35 40.22 o 8 25 0 277.55 298.27 23.84 o 9 25 0 273.65 279.19 25.87 o 10 25 0 9.70 -24.11 24.11 o 11 25 0 2.61 12.18 24.09 o 12 25 0 143.61 97.92 44.75 o 0 26 0 1951.97 1785.67 50.84 o 1 26 0 290.46 288.45 15.27 o 2 26 0 2295.51 2325.96 62.66 o 3 26 0 78.05 107.67 14.33 o 4 26 0 71.67 61.41 11.94 o 5 26 0 820.13 900.09 27.64 o 6 26 0 3671.58 3780.91 84.35 o 7 26 0 9.28 -5.93 15.25 o 8 26 0 940.19 964.54 38.70 o 9 26 0 17.31 23.20 20.46 o 10 26 0 164.24 166.24 34.56 o 11 26 0 467.25 477.54 39.10 o 1 27 0 10.15 12.00 10.27 o 2 27 0 8.44 -1.11 12.23 o 3 27 0 1744.80 1903.33 42.76 o 4 27 0 275.49 327.77 22.75 o 5 27 0 927.38 979.22 30.84 o 6 27 0 16.84 11.66 15.07 o 7 27 0 404.46 393.25 24.70 o 8 27 0 987.33 1014.81 69.80 o 9 27 0 75.00 27.08 28.77 o 10 27 0 88.04 65.13 28.45 o 11 27 0 143.81 127.58 41.63 o 0 28 0 5739.57 6191.41 163.15 o 1 28 0 79.15 114.29 16.32 o 2 28 0 2217.38 2226.08 81.01 o 3 28 0 3014.25 3287.18 73.31 o 4 28 0 404.31 393.99 22.92 o 5 28 0 9.00 3.21 12.79 o 6 28 0 34.03 27.21 17.37 o 7 28 0 506.17 543.18 31.33 o 8 28 0 11.48 -16.64 25.19 o 9 28 0 228.95 192.59 52.16 o 10 28 0 850.97 840.40 52.39 o 1 29 0 968.96 1011.41 32.94 o 2 29 0 1455.07 1582.92 50.33 o 3 29 0 422.34 441.60 26.53 o 4 29 0 102.30 135.57 16.93 o 5 29 0 1117.39 1189.03 44.91 o 6 29 0 71.00 88.25 27.82 o 7 29 0 477.78 454.99 36.61 o 8 29 0 37.66 35.80 29.07 o 9 29 0 8.34 2.19 35.09 o 10 29 0 111.80 33.96 40.38 o 0 30 0 110.99 147.55 22.54 o 1 30 0 3266.19 3350.56 76.34 o 2 30 0 494.30 519.61 23.79 o 3 30 0 43.68 36.21 14.04 o 4 30 0 21.21 28.47 18.54 o 5 30 0 42.31 31.52 16.52 o 6 30 0 193.50 204.12 26.88 o 7 30 0 320.36 252.93 29.70 o 8 30 0 404.97 367.27 37.86 o 9 30 0 71.41 40.22 29.03 o 1 31 0 1734.64 1846.80 49.28 o 2 31 0 4.66 39.39 15.81 o 3 31 0 2814.44 2958.30 87.95 o 4 31 0 65.86 56.69 20.84 o 5 31 0 68.79 73.62 26.77 o 6 31 0 3160.77 3558.08 121.18 o 7 31 0 251.77 255.05 33.31 o 8 31 0 62.38 26.05 64.06 o 0 32 0 1698.79 1733.36 72.71 o 1 32 0 144.72 155.91 18.44 o 2 32 0 104.75 93.29 22.08 o 3 32 0 1625.04 1617.83 71.25 o 4 32 0 244.99 256.29 31.67 o 5 32 0 172.15 138.69 29.23 o 6 32 0 68.74 70.21 23.51 o 7 32 0 529.05 547.40 43.12 o 1 33 0 40.51 49.00 21.47 o 2 33 0 436.74 388.01 32.36 o 3 33 0 101.07 89.89 30.20 o 4 33 0 439.01 487.73 68.46 o 5 33 0 55.40 30.33 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17.65 o -5 24 2 71.04 56.52 12.34 o -4 24 2 4943.42 4937.89 90.39 o -3 24 2 276.49 291.11 18.16 o -2 24 2 785.08 755.53 20.37 o -1 24 2 274.64 256.87 12.27 o 0 24 2 497.63 508.87 17.52 o 1 24 2 395.53 355.51 15.70 o 2 24 2 226.74 268.25 14.43 o 3 24 2 145.69 158.01 14.31 o 4 24 2 178.83 180.14 14.61 o 5 24 2 528.01 575.59 32.96 o 6 24 2 30.35 31.07 16.32 o 7 24 2 201.42 223.97 25.70 o 8 24 2 464.44 469.14 34.86 o 9 24 2 872.47 851.41 50.29 o 10 24 2 952.25 952.81 55.23 o 11 24 2 135.71 143.77 30.62 o -12 25 2 106.67 74.55 29.85 o -11 25 2 6.59 7.29 26.93 o -10 25 2 181.90 208.19 24.20 o -9 25 2 29.66 15.57 18.19 o -8 25 2 133.21 134.96 17.18 o -7 25 2 331.83 338.61 19.71 o -6 25 2 2.96 -9.79 14.17 o -5 25 2 2398.81 2467.54 106.71 o -4 25 2 22.70 3.04 12.04 o -3 25 2 381.88 375.92 17.88 o -2 25 2 110.83 64.24 15.31 o -1 25 2 3644.13 3919.14 75.00 o 0 25 2 25.42 26.55 9.77 o 1 25 2 1991.43 2094.14 47.28 o 2 25 2 811.13 866.48 25.09 o 3 25 2 77.82 66.57 13.60 o 4 25 2 25.71 51.84 14.51 o 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38.58 15.88 o -6 27 2 48.83 58.14 17.02 o -5 27 2 1051.27 1203.65 40.94 o -4 27 2 0.76 2.05 13.24 o -3 27 2 1.07 6.34 11.78 o -2 27 2 1047.17 1044.61 33.23 o -1 27 2 4310.46 4488.67 110.71 o 0 27 2 17.33 2.24 11.20 o 1 27 2 342.72 333.82 18.44 o 2 27 2 53.22 65.31 13.03 o 3 27 2 153.30 124.71 19.12 o 4 27 2 835.87 918.71 38.64 o 5 27 2 1239.71 1255.13 55.87 o 6 27 2 1152.60 1316.46 65.59 o 7 27 2 790.31 781.70 41.47 o 8 27 2 0.06 16.57 27.58 o 9 27 2 207.14 155.69 34.70 o 10 27 2 198.62 232.78 41.38 o -11 28 2 80.07 13.84 37.98 o -10 28 2 61.82 61.35 32.78 o -9 28 2 9.21 2.35 20.08 o -8 28 2 24.22 13.38 20.13 o -7 28 2 31.63 56.42 17.56 o -6 28 2 0.14 0.35 14.35 o -5 28 2 217.97 227.19 20.53 o -4 28 2 111.63 114.35 16.12 o -3 28 2 18.59 7.69 10.90 o -2 28 2 288.81 300.93 21.38 o -1 28 2 1687.31 1739.04 59.92 o 0 28 2 1116.22 1169.64 47.42 o 1 28 2 545.17 571.88 39.94 o 2 28 2 2.67 -4.67 13.27 o 3 28 2 48.81 25.80 19.18 o 4 28 2 273.32 247.02 21.76 o 5 28 2 778.07 791.26 40.07 o 6 28 2 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839.77 820.10 27.09 o -8 20 3 3040.98 3092.25 53.63 o -7 20 3 11.71 26.01 9.40 o -6 20 3 190.23 167.58 8.82 o -5 20 3 746.47 773.11 20.60 o -4 20 3 31.72 21.53 5.90 o -3 20 3 2962.33 2796.56 44.80 o -2 20 3 7.83 11.61 4.96 o -1 20 3 3207.33 3135.67 58.07 o 0 20 3 266.13 247.37 11.62 o 1 20 3 15.97 10.21 4.14 o 2 20 3 805.26 757.89 19.18 o 3 20 3 1014.77 976.27 26.33 o 4 20 3 889.34 969.63 28.17 o 5 20 3 1102.34 1091.49 51.31 o 6 20 3 1830.47 1849.76 54.58 o 7 20 3 1.05 -9.39 15.18 o 8 20 3 74.95 52.16 21.95 o 9 20 3 87.58 68.04 24.26 o 10 20 3 561.12 570.02 39.96 o 11 20 3 414.26 455.23 50.02 o 12 20 3 682.07 641.59 51.65 o -14 21 3 125.59 110.66 30.54 o -13 21 3 177.47 131.67 32.25 o -12 21 3 94.19 80.79 21.94 o -11 21 3 77.24 44.33 15.69 o -10 21 3 136.03 108.82 15.14 o -9 21 3 666.42 669.98 24.35 o -8 21 3 1.02 5.53 10.26 o -7 21 3 72.05 57.47 12.01 o -6 21 3 165.56 193.54 12.24 o -5 21 3 44.35 44.50 7.57 o -4 21 3 13678.58 13810.16 216.16 o -3 21 3 2239.83 2183.88 37.03 o -2 21 3 70.70 46.84 7.38 o -1 21 3 669.65 627.45 20.41 o 0 21 3 704.81 670.11 21.12 o 1 21 3 54.47 60.13 6.91 o 2 21 3 1185.78 1232.44 33.32 o 3 21 3 5.83 6.40 7.93 o 4 21 3 1040.69 1013.82 28.63 o 5 21 3 604.73 641.60 25.58 o 6 21 3 113.06 117.17 18.80 o 7 21 3 4576.94 5164.22 123.61 o 8 21 3 46.03 95.17 22.32 o 9 21 3 16.37 27.11 22.49 o 10 21 3 70.27 52.42 34.06 o 11 21 3 448.81 422.00 46.33 o 12 21 3 642.79 590.42 54.22 o -14 22 3 352.96 379.48 57.07 o -13 22 3 8.44 13.63 23.18 o -12 22 3 616.27 702.72 49.66 o -11 22 3 378.20 377.43 23.79 o -10 22 3 597.36 664.37 29.49 o -9 22 3 670.19 679.11 26.25 o -8 22 3 0.27 3.57 11.04 o -7 22 3 156.56 167.14 15.32 o -6 22 3 1373.14 1382.04 35.44 o -5 22 3 1678.35 1708.35 35.00 o -4 22 3 183.67 182.16 16.68 o -3 22 3 1879.15 1720.37 39.64 o -2 22 3 2099.09 2205.60 48.37 o -1 22 3 560.93 499.24 19.05 o 0 22 3 523.37 489.69 15.95 o 1 22 3 2547.40 2568.51 48.98 o 2 22 3 114.58 90.96 10.99 o 3 22 3 208.41 189.59 12.73 o 4 22 3 976.77 888.84 25.56 o 5 22 3 1955.03 2233.28 69.17 o 6 22 3 275.32 317.19 20.87 o 7 22 3 112.09 109.28 20.69 o 8 22 3 752.96 731.38 41.91 o 9 22 3 0.29 -20.46 20.46 o 10 22 3 1354.78 1598.71 85.77 o 11 22 3 722.29 686.04 49.36 o -13 23 3 122.47 92.67 31.71 o -12 23 3 39.05 25.29 22.72 o -11 23 3 0.43 -1.44 19.04 o -10 23 3 361.11 348.60 21.31 o -9 23 3 12.51 -2.43 12.57 o -8 23 3 3443.28 3520.50 80.01 o -7 23 3 1333.01 1359.68 37.92 o -6 23 3 165.36 116.90 14.20 o -5 23 3 167.51 160.87 11.74 o -4 23 3 462.73 453.08 16.22 o -3 23 3 1191.95 1192.13 30.95 o -2 23 3 833.17 807.47 21.21 o -1 23 3 676.12 758.60 28.89 o 0 23 3 11.45 -1.53 6.30 o 1 23 3 2452.29 2459.12 51.05 o 2 23 3 11.77 -1.63 9.58 o 3 23 3 16.65 26.69 10.34 o 4 23 3 631.74 663.53 30.88 o 5 23 3 197.78 208.36 20.84 o 6 23 3 111.89 127.71 28.46 o 7 23 3 1026.86 989.72 42.69 o 8 23 3 106.45 106.22 24.69 o 9 23 3 311.73 329.10 38.59 o 10 23 3 21.80 -0.22 23.78 o 11 23 3 1.78 -20.57 32.09 o -13 24 3 2665.29 2588.27 143.61 o -12 24 3 4.31 -15.42 25.39 o -11 24 3 766.08 748.72 42.51 o -10 24 3 1965.34 1990.12 64.12 o -9 24 3 1709.84 1779.15 49.87 o -8 24 3 1040.50 1153.62 35.27 o -7 24 3 2141.40 2265.42 51.25 o -6 24 3 3102.73 3159.62 70.15 o -5 24 3 674.79 702.45 25.43 o -4 24 3 694.06 666.25 29.97 o -3 24 3 39.87 34.25 12.27 o -2 24 3 17.96 15.92 7.88 o -1 24 3 49.30 31.96 8.08 o 0 24 3 375.23 400.82 17.38 o 1 24 3 2424.69 2497.92 56.76 o 2 24 3 482.09 514.92 23.39 o 3 24 3 176.15 169.09 18.25 o 4 24 3 145.11 158.68 19.70 o 5 24 3 5799.80 6266.16 160.29 o 6 24 3 384.71 347.04 23.12 o 7 24 3 1751.00 1788.19 65.78 o 8 24 3 84.27 87.63 24.27 o 9 24 3 638.25 632.46 43.45 o 10 24 3 204.96 228.37 33.28 o 11 24 3 821.30 650.08 65.71 o -13 25 3 1310.29 1408.67 91.33 o -12 25 3 0.69 9.10 27.63 o -11 25 3 23.60 13.56 18.79 o -10 25 3 501.89 590.77 38.04 o -9 25 3 0.88 -2.12 15.12 o -8 25 3 520.82 563.20 26.24 o -7 25 3 1448.28 1470.63 42.51 o -6 25 3 1956.19 2017.20 52.83 o -5 25 3 1770.87 1930.49 50.19 o -4 25 3 723.85 748.85 31.05 o -3 25 3 193.44 202.73 14.52 o -2 25 3 1548.66 1564.98 36.95 o -1 25 3 274.88 249.46 14.02 o 0 25 3 179.50 179.02 13.87 o 1 25 3 142.93 129.56 13.76 o 2 25 3 22.94 44.78 11.47 o 3 25 3 11.00 16.33 13.73 o 4 25 3 2329.65 2490.92 74.23 o 5 25 3 244.27 256.08 51.78 o 6 25 3 368.42 451.37 30.23 o 7 25 3 689.51 706.91 39.23 o 8 25 3 0.18 -9.97 20.61 o 9 25 3 9.01 -24.56 35.41 o 10 25 3 11.38 19.76 28.15 o -12 26 3 292.58 289.03 43.26 o -11 26 3 32.50 3.03 21.19 o -10 26 3 4.00 15.35 15.97 o -9 26 3 32.67 12.71 17.44 o -8 26 3 448.66 458.54 27.11 o -7 26 3 157.69 132.13 19.95 o -6 26 3 2.59 1.64 12.50 o -5 26 3 951.28 829.17 30.57 o -4 26 3 997.17 994.73 43.11 o -3 26 3 313.33 312.83 17.72 o -2 26 3 1405.48 1425.06 39.47 o -1 26 3 133.57 128.62 17.54 o 0 26 3 440.14 435.42 20.61 o 1 26 3 45.88 45.87 12.06 o 2 26 3 14.82 4.70 13.14 o 3 26 3 662.97 654.12 31.42 o 4 26 3 194.97 251.77 22.75 o 5 26 3 2054.85 2137.50 64.44 o 6 26 3 108.59 103.46 22.43 o 7 26 3 226.79 210.46 45.72 o 8 26 3 144.93 159.43 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