#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/28/2012854.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012854_Fobs loop_ _publ_author_name 'Ftini, Mohamed Mongi' 'Krifa, Mohamed' 'Amor, Haddad' _publ_section_title ; KMo~5~O~13~ and KNb~1.76~Sb~3.24~O~13~ ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first i106 _journal_page_last i108 _journal_volume 58 _journal_year 2002 _space_group_IT_number 63 _symmetry_space_group_name_Hall '-C 2c 2' _symmetry_space_group_name_H-M 'C m c m' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.6027 _cell_length_b 8.9552 _cell_length_c 16.8441 _exptl_crystal_F_000 1331.09 _reflns_d_resolution_high 0.7115 _[local]_cod_data_source_file br1369Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' hd35 in C m c m' _shelx_refln_list_code 4 _shelx_f_calc_maximum 784.52 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' 'x, -y, -z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z+1/2' 'x+1/2, -y+1/2, -z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, y, -z-1/2' '-x, y, z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, y+1/2, -z-1/2' '-x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 615468.75 418481.91 1458.59 o 4 0 0 427881.34 368254.78 1650.84 o 6 0 0 211267.63 195886.13 1304.40 o 8 0 0 95190.61 94060.96 1024.78 o 1 1 0 1.99 39.59 34.20 o 3 1 0 2803.06 1514.25 49.43 o 5 1 0 656.22 140.32 117.68 o 7 1 0 0.19 179.21 106.87 o 9 1 0 66.35 -167.35 167.35 o 0 2 0 15720.97 14328.15 174.60 o 2 2 0 878.14 1193.19 47.01 o 4 2 0 5601.76 5266.17 154.98 o 6 2 0 1784.78 1674.19 82.01 o 8 2 0 1246.59 1009.90 92.98 o 1 3 0 13228.06 14999.86 492.19 o 3 3 0 14007.40 13453.42 242.43 o 5 3 0 8681.59 9150.75 239.91 o 7 3 0 6013.98 5539.49 162.00 o 9 3 0 4926.16 5182.39 154.25 o 0 4 0 55639.83 50452.17 422.08 o 2 4 0 2631.50 2788.48 78.95 o 4 4 0 10946.51 9605.56 270.60 o 6 4 0 6499.05 7187.06 208.29 o 8 4 0 1505.83 1673.07 100.69 o 1 5 0 184231.77 196151.64 5333.90 o 3 5 0 184765.72 161370.67 1044.66 o 5 5 0 78914.16 78633.33 818.23 o 7 5 0 67505.27 69114.30 861.70 o 0 6 0 16861.83 17570.69 313.47 o 2 6 0 12052.94 11184.30 277.92 o 4 6 0 11595.77 10552.50 264.32 o 6 6 0 6505.22 5870.60 162.53 o 8 6 0 4773.34 5122.31 159.80 o 1 7 0 3688.77 4247.45 84.17 o 3 7 0 4397.75 4316.88 122.75 o 5 7 0 2498.72 2452.03 109.85 o 7 7 0 3360.32 3638.09 134.30 o 0 8 0 130321.25 140430.34 1069.65 o 2 8 0 89645.93 87878.92 852.54 o 4 8 0 80358.78 77868.41 863.15 o 6 8 0 58062.69 60238.82 872.37 o 1 9 0 7697.12 8406.72 170.52 o 3 9 0 12350.90 11880.83 327.11 o 5 9 0 2377.20 2489.80 130.29 o 0 10 0 9932.86 10232.67 282.23 o 2 10 0 7008.53 6349.19 191.44 o 4 10 0 6638.21 6553.59 190.35 o 1 11 0 2944.70 2836.23 127.67 o 3 11 0 3094.50 2711.17 153.92 o 0 12 0 128.87 769.31 264.45 o 2 12 0 301.20 813.75 261.11 o 1 1 1 12134.42 12157.27 279.60 o 3 1 1 21005.93 17952.11 251.60 o 5 1 1 2537.48 2969.45 82.19 o 7 1 1 5357.28 5578.66 152.43 o 9 1 1 1858.29 2036.68 103.29 o 0 2 1 20049.53 22550.60 210.44 o 2 2 1 8711.51 8421.50 172.40 o 4 2 1 9804.22 10370.24 236.77 o 6 2 1 6570.33 6694.82 209.33 o 8 2 1 4204.70 3912.51 118.64 o 1 3 1 74323.27 74072.31 840.98 o 3 3 1 73724.24 64710.24 544.20 o 5 3 1 27143.41 27735.91 432.38 o 7 3 1 24316.12 23535.13 482.87 o 9 3 1 11749.59 12107.96 338.83 o 0 4 1 14645.30 13188.35 221.38 o 2 4 1 3225.80 2700.11 78.65 o 4 4 1 4090.54 3499.55 91.49 o 6 4 1 1805.01 1836.62 88.40 o 8 4 1 679.71 148.37 196.04 o 1 5 1 51342.94 49406.20 757.49 o 3 5 1 46531.73 40646.19 486.94 o 5 5 1 19004.90 17796.44 393.22 o 7 5 1 15214.65 17653.57 444.62 o 0 6 1 4975.82 4206.54 132.70 o 2 6 1 345.22 434.70 143.17 o 4 6 1 1178.36 1161.80 79.79 o 6 6 1 395.93 616.16 85.21 o 8 6 1 45.99 492.66 164.36 o 1 7 1 1035.29 785.96 62.29 o 3 7 1 120.03 -172.48 172.48 o 5 7 1 317.44 73.78 186.16 o 7 7 1 1.27 -152.66 193.73 o 0 8 1 25687.52 26234.92 462.48 o 2 8 1 13977.76 14699.83 344.99 o 4 8 1 15374.76 15069.35 397.59 o 6 8 1 10344.46 10372.25 282.41 o 1 9 1 964.86 937.23 66.84 o 3 9 1 1193.06 868.12 108.35 o 5 9 1 741.13 638.57 212.68 o 0 10 1 21828.76 23537.15 482.86 o 2 10 1 14131.15 13107.82 346.40 o 4 10 1 15317.93 14761.33 380.80 o 1 11 1 8254.93 8954.92 180.32 o 3 11 1 7152.83 7214.18 216.66 o 0 12 1 1801.20 1710.59 153.65 o 2 12 1 635.66 554.30 251.84 o 0 0 2 77582.31 90305.12 341.47 o 2 0 2 29279.42 27206.53 261.06 o 4 0 2 25247.59 24533.41 341.96 o 6 0 2 18275.98 18834.02 379.86 o 8 0 2 9089.83 7678.37 239.36 o 1 1 2 706.55 383.85 28.93 o 3 1 2 888.34 715.96 43.13 o 5 1 2 243.46 268.58 111.19 o 7 1 2 67.21 226.43 114.12 o 9 1 2 43.27 323.77 163.08 o 0 2 2 55991.73 56104.75 350.62 o 2 2 2 14327.21 14541.75 209.07 o 4 2 2 16763.27 17711.51 304.33 o 6 2 2 12452.63 13185.77 328.89 o 8 2 2 5247.25 5064.45 148.41 o 1 3 2 64055.21 62783.99 1322.02 o 3 3 2 60815.68 51862.37 482.68 o 5 3 2 21026.87 21256.80 395.18 o 7 3 2 16016.23 16241.69 393.35 o 0 4 2 4441.19 2405.45 79.10 o 2 4 2 29.92 -96.66 96.66 o 4 4 2 53.21 0.00 119.66 o 6 4 2 9.19 -139.66 139.66 o 8 4 2 235.59 327.54 117.98 o 1 5 2 46868.80 47307.28 1283.99 o 3 5 2 44369.65 40137.29 483.67 o 5 5 2 20304.03 20231.55 400.17 o 7 5 2 14994.21 15996.76 416.62 o 0 6 2 7196.90 7667.81 198.31 o 2 6 2 1589.46 2080.22 79.90 o 4 6 2 2746.25 2708.16 94.99 o 6 6 2 2679.59 2889.24 114.14 o 8 6 2 987.52 900.87 107.86 o 1 7 2 1075.46 1655.78 66.65 o 3 7 2 3230.10 2778.75 102.79 o 5 7 2 886.28 738.49 97.21 o 7 7 2 1776.55 1574.56 115.23 o 0 8 2 22923.09 24108.12 430.50 o 2 8 2 14909.67 14242.08 351.60 o 4 8 2 14047.80 12015.75 319.33 o 6 8 2 11316.61 11953.54 328.16 o 1 9 2 1081.73 842.29 67.70 o 3 9 2 356.03 266.37 180.63 o 5 9 2 819.51 742.00 111.68 o 0 10 2 18749.76 19218.73 457.92 o 2 10 2 13431.32 12524.67 335.18 o 4 10 2 12318.12 12397.41 346.37 o 1 11 2 5940.09 5888.50 260.55 o 3 11 2 6890.91 6489.55 184.35 o 0 12 2 691.12 -64.22 276.16 o 2 12 2 162.29 556.17 221.03 o 1 1 3 432.23 645.45 30.45 o 3 1 3 534.31 174.34 74.64 o 5 1 3 1120.54 1340.15 66.58 o 7 1 3 4.79 -68.59 127.31 o 9 1 3 253.54 747.31 78.80 o 0 2 3 131754.86 142811.88 628.48 o 2 2 3 85101.63 75489.05 511.73 o 4 2 3 55461.47 50390.59 523.96 o 6 2 3 30427.70 30700.31 498.05 o 8 2 3 17070.07 18037.54 467.26 o 1 3 3 64394.77 71466.23 589.96 o 3 3 3 66191.89 61780.23 539.05 o 5 3 3 30632.10 31671.08 474.28 o 7 3 3 27620.09 26639.74 516.89 o 0 4 3 17.18 -100.06 100.06 o 2 4 3 1140.70 819.00 55.10 o 4 4 3 44.37 -62.69 153.29 o 6 4 3 53.03 182.17 145.20 o 8 4 3 73.00 -149.89 149.89 o 1 5 3 28913.91 31139.09 386.46 o 3 5 3 28667.70 27952.67 412.46 o 5 5 3 13480.94 13469.64 346.36 o 7 5 3 12043.50 11662.74 331.74 o 0 6 3 15424.82 15498.40 309.48 o 2 6 3 22319.30 20697.95 358.41 o 4 6 3 11059.34 10442.84 264.42 o 6 6 3 7371.14 7265.82 218.25 o 8 6 3 4831.79 5513.59 162.38 o 1 7 3 8803.46 8800.14 168.00 o 3 7 3 5819.29 5686.37 153.16 o 5 7 3 6384.07 7188.77 206.81 o 7 7 3 3426.39 3179.72 133.02 o 0 8 3 23909.76 26535.89 454.59 o 2 8 3 14576.54 14614.53 360.06 o 4 8 3 15509.83 14932.31 386.68 o 6 8 3 10809.71 10970.45 351.69 o 1 9 3 1553.80 1746.40 71.38 o 3 9 3 1355.44 1437.35 106.24 o 5 9 3 545.43 400.01 222.85 o 0 10 3 42306.30 45569.79 686.53 o 2 10 3 31550.74 31874.46 594.71 o 4 10 3 28543.14 28629.38 604.89 o 1 11 3 16766.35 15170.57 286.57 o 3 11 3 15221.85 14636.81 378.37 o 0 12 3 345.62 779.86 247.49 o 2 12 3 1011.32 1349.87 131.74 o 0 0 4 55511.82 59455.91 342.25 o 2 0 4 15415.11 16528.74 217.41 o 4 0 4 23173.04 21932.54 334.93 o 6 0 4 10668.77 10364.03 297.56 o 8 0 4 7198.36 7101.54 209.03 o 1 1 4 45545.95 43513.05 640.60 o 3 1 4 40707.39 33263.34 365.29 o 5 1 4 14030.25 15481.00 317.85 o 7 1 4 9733.78 9771.22 264.50 o 9 1 4 5634.46 6413.05 186.57 o 0 2 4 131247.69 151352.47 680.35 o 2 2 4 15859.00 21571.22 265.06 o 4 2 4 44996.97 47030.07 504.78 o 6 2 4 32446.69 33382.50 531.23 o 8 2 4 15059.93 12259.12 337.72 o 1 3 4 1210.75 2753.46 52.34 o 3 3 4 11393.61 11985.70 242.40 o 5 3 4 1417.65 1688.95 79.84 o 7 3 4 5148.79 5378.39 162.62 o 0 4 4 5593.09 3625.03 112.21 o 2 4 4 663.64 491.30 52.47 o 4 4 4 1467.46 1194.63 77.73 o 6 4 4 102.32 -69.33 144.36 o 8 4 4 31.47 182.16 160.53 o 1 5 4 7803.20 7512.76 150.92 o 3 5 4 5763.89 5076.57 152.58 o 5 5 4 2941.36 3065.60 103.99 o 7 5 4 2484.82 2796.02 109.39 o 0 6 4 86742.43 93023.16 739.48 o 2 6 4 38721.05 42145.28 511.65 o 4 6 4 43717.45 42295.80 580.41 o 6 6 4 31558.98 32484.58 595.01 o 8 6 4 16002.70 15315.59 403.19 o 1 7 4 32460.89 36586.54 358.05 o 3 7 4 44490.65 44251.28 592.07 o 5 7 4 17622.89 18193.54 450.69 o 7 7 4 20898.96 22110.07 539.85 o 0 8 4 1291.79 1694.20 91.33 o 2 8 4 1641.27 1714.28 90.95 o 4 8 4 1621.76 1732.96 102.02 o 6 8 4 1025.47 900.23 115.55 o 1 9 4 86.25 -34.10 158.00 o 3 9 4 4.90 74.49 158.82 o 5 9 4 145.57 249.32 198.45 o 0 10 4 10178.38 10169.27 312.08 o 2 10 4 6076.65 5942.35 164.09 o 4 10 4 6186.37 5956.15 194.50 o 1 11 4 17949.00 16364.86 307.16 o 3 11 4 23015.47 21412.51 551.44 o 0 12 4 3692.00 4187.67 162.58 o 2 12 4 2005.06 1609.64 135.32 o 1 1 5 123692.63 134740.13 640.09 o 3 1 5 120247.52 106151.00 706.73 o 5 1 5 42598.13 44405.12 540.75 o 7 1 5 37818.02 37373.25 597.96 o 9 1 5 18093.00 19711.90 508.81 o 0 2 5 6229.60 7321.28 152.93 o 2 2 5 11427.44 11789.61 207.58 o 4 2 5 4977.27 5328.01 162.33 o 6 2 5 3460.60 3465.00 97.65 o 8 2 5 2612.17 2613.43 110.25 o 1 3 5 485.87 98.49 61.19 o 3 3 5 1505.27 1835.87 63.68 o 5 3 5 11.73 166.67 106.45 o 7 3 5 1263.32 1392.76 84.04 o 0 4 5 28436.03 28600.64 344.42 o 2 4 5 11359.84 11469.76 241.90 o 4 4 5 12395.44 12096.67 298.45 o 6 4 5 7222.95 7252.31 220.08 o 8 4 5 3757.86 3764.47 130.94 o 1 5 5 8729.83 9300.20 178.71 o 3 5 5 11938.26 11586.59 287.53 o 5 5 5 3476.58 3158.64 107.07 o 7 5 5 4694.35 4799.31 150.44 o 0 6 5 36698.41 41818.72 492.19 o 2 6 5 19107.66 21144.37 374.58 o 4 6 5 23552.10 23455.73 441.25 o 6 6 5 17532.59 17032.67 445.84 o 1 7 5 44091.71 46425.49 556.54 o 3 7 5 41614.11 41944.59 581.57 o 5 7 5 25370.73 24953.76 515.23 o 7 7 5 20047.22 21271.53 543.12 o 0 8 5 6382.61 6706.55 184.28 o 2 8 5 1658.55 1426.58 95.64 o 4 8 5 3246.55 2877.77 121.09 o 6 8 5 2127.92 2583.40 124.26 o 1 9 5 11258.41 11498.02 213.71 o 3 9 5 10192.69 10380.56 305.17 o 5 9 5 6253.56 6354.58 179.06 o 0 10 5 6702.49 8483.25 249.41 o 2 10 5 2565.07 2441.22 133.34 o 4 10 5 3402.53 3888.83 145.43 o 1 11 5 2410.30 2408.91 105.23 o 3 11 5 2152.84 2240.93 141.34 o 0 12 5 25196.38 26366.54 607.98 o 2 12 5 18705.99 17268.60 446.82 o 0 0 6 2920.12 2385.09 61.24 o 2 0 6 3158.52 2117.56 60.68 o 4 0 6 13.46 -14.01 86.01 o 6 0 6 64.57 106.21 98.79 o 8 0 6 114.07 371.74 115.83 o 1 1 6 45928.76 55751.13 288.75 o 3 1 6 56487.82 57050.34 503.09 o 5 1 6 26053.65 26834.91 429.00 o 7 1 6 23702.04 23348.04 473.95 o 0 2 6 260.76 238.44 85.24 o 2 2 6 1876.44 1746.76 53.10 o 4 2 6 694.20 800.64 58.85 o 6 2 6 144.82 241.21 115.41 o 8 2 6 298.08 468.49 147.38 o 1 3 6 2573.17 2482.93 52.71 o 3 3 6 309.14 283.40 54.11 o 5 3 6 1549.17 1522.03 79.42 o 7 3 6 474.98 408.85 138.48 o 0 4 6 248059.98 282982.09 1272.89 o 2 4 6 153096.39 160908.64 951.64 o 4 4 6 119419.77 118561.23 942.01 o 6 4 6 78287.86 80770.27 898.39 o 8 4 6 40876.62 39854.90 716.04 o 1 5 6 228.03 199.36 87.53 o 3 5 6 312.06 -15.50 144.86 o 5 5 6 533.68 580.17 73.73 o 7 5 6 5.52 -140.86 155.41 o 0 6 6 4875.70 5267.50 157.46 o 2 6 6 2156.70 2586.37 94.50 o 4 6 6 2853.26 2453.00 99.69 o 6 6 6 2970.98 2985.63 118.45 o 1 7 6 1919.37 2046.91 67.28 o 3 7 6 2875.13 3080.06 101.84 o 5 7 6 1592.82 1503.60 101.15 o 7 7 6 1659.23 1359.90 115.64 o 0 8 6 286.79 430.16 77.96 o 2 8 6 1594.68 1333.19 93.49 o 4 8 6 486.99 526.94 198.98 o 6 8 6 99.71 0.00 195.88 o 1 9 6 69779.57 70782.22 943.73 o 3 9 6 69791.37 74335.57 878.17 o 5 9 6 44367.64 45224.87 770.17 o 0 10 6 1762.29 1971.93 115.69 o 2 10 6 3108.56 3452.66 130.44 o 4 10 6 1866.12 2539.57 128.05 o 1 11 6 1.71 -122.88 148.74 o 3 11 6 28.03 162.25 204.81 o 0 12 6 21505.65 23040.80 579.29 o 1 1 7 1139.99 841.26 29.30 o 3 1 7 1.08 188.06 75.36 o 5 1 7 480.29 484.22 57.53 o 7 1 7 20.63 -132.85 132.85 o 0 2 7 2943.80 3413.99 94.17 o 2 2 7 1331.74 1636.00 55.56 o 4 2 7 1707.58 1760.80 70.51 o 6 2 7 1188.19 1274.62 76.36 o 8 2 7 830.95 766.36 83.12 o 1 3 7 10129.33 9166.26 187.47 o 3 3 7 10729.18 9821.30 235.55 o 5 3 7 3465.14 3298.38 109.67 o 7 3 7 3557.94 3452.92 113.84 o 0 4 7 1.53 544.99 51.95 o 2 4 7 340.00 229.54 114.20 o 4 4 7 3.66 -107.67 119.22 o 6 4 7 8.04 -150.30 150.30 o 8 4 7 6.12 254.43 137.53 o 1 5 7 4122.52 4130.80 88.11 o 3 5 7 4677.93 4433.55 125.04 o 5 5 7 1502.11 1676.70 88.35 o 7 5 7 1641.99 1747.35 109.25 o 0 6 7 1490.56 1066.72 84.14 o 2 6 7 124.55 165.23 137.99 o 4 6 7 242.68 171.90 69.43 o 6 6 7 12.55 113.57 148.60 o 1 7 7 2430.59 2465.30 118.43 o 3 7 7 1255.66 1263.74 87.04 o 5 7 7 1158.45 1192.32 97.67 o 7 7 7 327.33 196.25 196.37 o 0 8 7 1505.17 1564.48 91.78 o 2 8 7 451.27 343.92 80.53 o 4 8 7 962.74 1242.20 93.38 o 6 8 7 627.11 400.04 205.40 o 1 9 7 4.79 176.44 123.79 o 3 9 7 7.53 237.47 169.04 o 5 9 7 0.02 -212.04 212.04 o 0 10 7 1858.10 1709.63 122.10 o 2 10 7 807.79 359.56 225.07 o 4 10 7 1336.76 1224.17 116.87 o 1 11 7 1138.39 1264.55 86.28 o 3 11 7 1014.57 868.42 121.51 o 0 12 7 50.43 309.02 214.18 o 0 0 8 141146.47 132383.58 738.97 o 2 0 8 27058.09 26712.56 327.93 o 4 0 8 34235.45 31639.68 443.79 o 6 0 8 16514.65 16217.50 383.85 o 8 0 8 4505.71 4768.69 135.37 o 1 1 8 91659.05 96054.55 444.57 o 3 1 8 85627.55 82967.88 670.07 o 5 1 8 34512.14 33353.86 508.04 o 7 1 8 26208.83 26444.35 519.31 o 0 2 8 12510.08 11244.54 214.22 o 2 2 8 3406.29 3776.33 115.99 o 4 2 8 6079.55 5497.02 162.07 o 6 2 8 2263.16 2541.70 92.30 o 8 2 8 1592.55 1603.74 102.83 o 1 3 8 5543.05 4804.46 97.14 o 3 3 8 2403.11 2115.86 70.20 o 5 3 8 1908.31 1796.54 80.74 o 7 3 8 953.14 1070.06 83.99 o 0 4 8 204171.09 226926.94 1185.10 o 2 4 8 100355.35 108566.30 798.14 o 4 4 8 101177.02 105240.09 919.54 o 6 4 8 68692.33 72171.52 859.47 o 8 4 8 36453.56 33774.34 679.56 o 1 5 8 2850.75 3016.49 129.25 o 3 5 8 7888.70 7697.69 217.37 o 5 5 8 540.91 612.63 71.59 o 7 5 8 2288.93 2315.51 114.04 o 0 6 8 1432.03 1510.22 86.25 o 2 6 8 1799.74 1707.11 82.03 o 4 6 8 735.23 917.79 75.03 o 6 6 8 862.01 1249.33 87.39 o 1 7 8 1838.91 1752.30 63.11 o 3 7 8 1149.22 1254.60 83.18 o 5 7 8 1127.65 1430.83 106.19 o 7 7 8 252.13 445.58 92.85 o 0 8 8 8866.99 9045.01 265.25 o 2 8 8 2817.37 2975.03 107.78 o 4 8 8 3707.75 3826.72 121.15 o 6 8 8 2680.78 3268.90 134.59 o 1 9 8 75311.94 78401.38 1188.11 o 3 9 8 79321.36 81919.77 960.67 o 5 9 8 44084.68 45812.36 810.95 o 0 10 8 740.63 634.90 107.41 o 2 10 8 1393.15 1361.07 116.89 o 4 10 8 908.05 798.16 112.97 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