#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2012913.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012913_Fobs loop_ _publ_author_name 'Kuratieva, Natalia V.' 'Naumova, Marina I.' 'Naumov, Dmitry Yu.' _publ_section_title ; Hexaaquacobalt(II) bis(hypophosphite) and hexaaquacobalt(II)/nickel(II) bis(hypophosphite) ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first i129 _journal_page_last i131 _journal_volume 58 _journal_year 2002 _space_group_IT_number 142 _symmetry_space_group_name_Hall '-I 4bd 2c' _symmetry_space_group_name_H-M 'I 41/a c d :2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 10.3406 _cell_length_b 10.3406 _cell_length_c 20.4023 _exptl_crystal_F_000 1224.00 _reflns_d_resolution_high 0.7304 _[local]_cod_data_source_file av1112Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' [Co(H2O)6](H2PO2)2 in I4(1)/acd, CAD4, T=293K, PSI' _shelx_refln_list_code 4 _shelx_f_calc_maximum 424.03 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-y+1/4, x+3/4, z+1/4' 'y+1/4, -x+1/4, z+3/4' '-x+1/2, y, -z' 'x, -y, -z+1/2' 'y+1/4, x+3/4, -z+3/4' '-y+1/4, -x+1/4, -z+1/4' 'x+1/2, y+1/2, z+1/2' '-x+1, -y+1/2, z+1' '-y+3/4, x+5/4, z+3/4' 'y+3/4, -x+3/4, z+5/4' '-x+1, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z+1' 'y+3/4, x+5/4, -z+5/4' '-y+3/4, -x+3/4, -z+3/4' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'y-1/4, -x-3/4, -z-1/4' '-y-1/4, x-1/4, -z-3/4' 'x-1/2, -y, z' '-x, y, z-1/2' '-y-1/4, -x-3/4, z-3/4' 'y-1/4, x-1/4, z-1/4' '-x+1/2, -y+1/2, -z+1/2' 'x, y+1/2, -z' 'y+1/4, -x-1/4, -z+1/4' '-y+1/4, x+1/4, -z-1/4' 'x, -y+1/2, z+1/2' '-x+1/2, y+1/2, z' '-y+1/4, -x-1/4, z-1/4' 'y+1/4, x+1/4, z+1/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 2 0 298.02 232.99 23.66 o 2 2 0 111221.77 108162.08 289.00 o 0 4 0 179501.23 170889.64 1356.21 o 2 4 0 9386.07 10041.20 124.69 o 4 4 0 143260.03 159497.61 511.09 o 0 6 0 47289.93 62518.76 3461.69 o 2 6 0 35820.70 32457.98 501.42 o 4 6 0 168.98 191.09 20.95 o 6 6 0 62663.44 54893.50 383.69 o 0 8 0 25607.46 22982.53 566.99 o 2 8 0 20.56 106.42 78.25 o 4 8 0 24150.22 23376.32 759.85 o 6 8 0 51.36 50.93 21.52 o 8 8 0 7350.37 7040.55 174.17 o 0 10 0 342.73 340.94 30.56 o 2 10 0 21499.51 21092.52 1367.50 o 4 10 0 2016.18 1949.87 63.93 o 6 10 0 7871.61 7939.95 129.02 o 8 10 0 291.32 273.03 36.53 o 10 10 0 4826.69 4937.91 175.12 o 0 12 0 9897.00 9886.64 533.59 o 2 12 0 311.82 297.91 34.81 o 4 12 0 2682.51 2602.90 81.99 o 6 12 0 390.55 378.79 40.72 o 0 14 0 82.68 82.34 30.97 o 2 14 0 2785.89 2887.64 204.24 o 1 2 1 4279.11 4572.40 43.69 o 2 3 1 1.30 3.59 12.18 o 1 4 1 2351.47 2333.10 48.63 o 3 4 1 29.94 33.21 11.79 o 2 5 1 518.14 531.01 23.18 o 4 5 1 109.67 110.59 17.64 o 1 6 1 330.64 361.73 21.60 o 3 6 1 340.51 351.27 23.08 o 5 6 1 473.36 493.91 51.50 o 2 7 1 136.61 132.95 19.40 o 4 7 1 48.15 45.80 19.82 o 6 7 1 177.21 185.24 25.74 o 1 8 1 4.32 -0.13 16.79 o 3 8 1 262.35 260.83 25.94 o 5 8 1 1036.33 1064.72 44.81 o 7 8 1 280.91 274.14 31.47 o 2 9 1 83.13 75.97 22.09 o 4 9 1 180.35 166.58 26.74 o 6 9 1 86.25 94.78 26.50 o 8 9 1 91.69 92.53 28.51 o 1 10 1 121.08 101.87 24.61 o 3 10 1 370.67 391.27 34.49 o 5 10 1 499.99 491.11 39.53 o 7 10 1 274.77 271.01 35.84 o 9 10 1 51.59 14.12 31.74 o 2 11 1 119.54 107.38 27.66 o 4 11 1 117.36 115.55 29.42 o 6 11 1 15.72 2.11 25.24 o 8 11 1 0.08 -4.64 28.40 o 1 12 1 299.31 278.36 34.86 o 3 12 1 165.10 157.93 31.22 o 5 12 1 127.43 146.98 31.79 o 7 12 1 57.32 49.77 30.49 o 2 13 1 23.71 -1.62 35.83 o 4 13 1 52.37 60.70 30.16 o 1 14 1 267.52 248.43 38.53 o 1 1 2 77234.33 70706.02 183.99 o 0 2 2 23.51 26.40 8.53 o 1 3 2 40308.55 47407.08 4484.19 o 3 3 2 1339.23 1595.94 46.52 o 0 4 2 5.37 10.49 17.47 o 2 4 2 1.02 -3.67 10.25 o 1 5 2 50026.08 58933.73 206.44 o 3 5 2 31910.04 29308.24 825.55 o 5 5 2 30444.89 28446.32 249.70 o 0 6 2 3.04 -3.59 18.26 o 2 6 2 2.40 -3.98 13.05 o 4 6 2 0.21 1.88 15.86 o 1 7 2 4523.25 4620.75 148.80 o 3 7 2 4952.75 4663.33 75.40 o 5 7 2 5677.12 5588.41 118.04 o 7 7 2 946.01 909.51 61.89 o 0 8 2 0.08 -6.66 17.70 o 2 8 2 1.35 9.12 17.28 o 4 8 2 4.50 24.27 18.76 o 6 8 2 0.79 1.87 20.32 o 1 9 2 11023.51 10464.51 124.97 o 3 9 2 1896.01 1950.39 87.95 o 5 9 2 7338.66 7353.88 357.25 o 7 9 2 2743.80 2781.07 83.86 o 9 9 2 901.27 975.77 79.45 o 0 10 2 3.11 1.69 22.84 o 2 10 2 2.33 -21.98 29.94 o 4 10 2 0.65 -18.13 22.36 o 6 10 2 1.77 -15.31 26.53 o 8 10 2 0.09 -28.34 28.34 o 1 11 2 2879.89 2778.46 126.88 o 3 11 2 2471.39 2356.47 96.43 o 5 11 2 2280.27 2274.78 74.75 o 7 11 2 936.17 921.81 54.34 o 0 12 2 4.24 -27.38 27.38 o 2 12 2 0.01 11.35 22.80 o 4 12 2 0.27 -3.83 25.18 o 6 12 2 0.56 -15.43 32.94 o 1 13 2 488.33 514.04 43.75 o 3 13 2 731.33 744.21 50.69 o 5 13 2 492.57 485.22 46.93 o 0 14 2 0.01 7.20 28.87 o 1 2 3 11690.82 15040.16 1223.27 o 2 3 3 37.37 52.32 10.73 o 1 4 3 7344.88 7668.27 68.63 o 3 4 3 61.62 44.15 12.63 o 2 5 3 3395.10 3329.74 53.52 o 4 5 3 1258.70 1195.43 36.91 o 1 6 3 0.60 -0.89 12.98 o 3 6 3 188.81 206.45 20.02 o 5 6 3 295.11 291.02 26.11 o 2 7 3 797.06 802.69 44.72 o 4 7 3 427.45 458.41 30.21 o 6 7 3 338.87 357.35 30.62 o 1 8 3 154.50 138.54 20.76 o 3 8 3 456.75 472.59 30.63 o 5 8 3 1945.75 1949.03 76.17 o 7 8 3 618.61 609.62 39.17 o 2 9 3 144.97 126.57 23.02 o 4 9 3 165.13 171.76 26.30 o 6 9 3 47.42 63.64 24.75 o 8 9 3 24.69 13.79 25.53 o 1 10 3 17.57 34.37 21.44 o 3 10 3 311.00 319.17 31.56 o 5 10 3 506.54 507.83 40.12 o 7 10 3 568.80 575.23 43.33 o 9 10 3 10.42 0.84 30.31 o 2 11 3 482.27 455.77 37.75 o 4 11 3 229.45 229.74 32.18 o 6 11 3 50.61 59.04 27.31 o 8 11 3 80.59 93.67 32.29 o 1 12 3 405.90 418.31 38.30 o 3 12 3 163.97 175.97 31.05 o 5 12 3 86.22 99.78 30.56 o 7 12 3 19.22 15.17 28.08 o 2 13 3 85.10 92.78 30.89 o 4 13 3 85.46 74.08 32.46 o 1 14 3 324.60 305.77 41.63 o 0 0 4 334.73 287.08 16.57 o 0 2 4 106731.65 115593.48 8285.18 o 2 2 4 77075.24 81755.25 280.93 o 1 3 4 2.96 2.99 9.10 o 0 4 4 8759.93 9002.57 169.97 o 2 4 4 30437.56 36749.98 159.04 o 4 4 4 154.80 171.27 23.55 o 1 5 4 3.83 1.98 11.93 o 3 5 4 7.56 21.99 12.62 o 0 6 4 34791.90 31519.39 170.63 o 2 6 4 614.69 684.07 28.92 o 4 6 4 38302.83 34073.34 1397.09 o 6 6 4 649.30 575.72 47.31 o 1 7 4 0.08 -10.32 15.87 o 3 7 4 0.03 -2.93 16.47 o 5 7 4 0.04 -7.67 18.67 o 0 8 4 53.21 42.20 17.95 o 2 8 4 9324.53 9380.74 407.73 o 4 8 4 816.25 738.42 38.83 o 6 8 4 9462.58 9190.91 141.65 o 8 8 4 640.68 601.66 59.09 o 1 9 4 3.41 -23.31 23.31 o 3 9 4 0.18 -11.44 22.66 o 5 9 4 0.46 22.24 22.09 o 7 9 4 0.04 -10.40 29.24 o 0 10 4 21088.26 19455.35 245.31 o 2 10 4 12.41 40.25 23.65 o 4 10 4 9888.56 9265.80 275.11 o 6 10 4 332.69 347.65 36.76 o 8 10 4 3311.89 3560.18 226.82 o 1 11 4 0.06 -10.68 24.27 o 3 11 4 1.10 -6.85 30.54 o 5 11 4 0.20 2.47 23.79 o 7 11 4 0.00 10.11 27.86 o 0 12 4 341.94 361.68 36.18 o 2 12 4 3237.00 3150.82 87.46 o 4 12 4 26.05 57.92 25.75 o 6 12 4 1402.95 1556.35 69.79 o 1 13 4 0.16 24.19 26.21 o 3 13 4 0.02 -8.12 46.71 o 5 13 4 0.36 -45.33 46.51 o 0 14 4 2608.03 2620.98 89.78 o 1 2 5 2180.23 2403.25 34.32 o 2 3 5 184.97 189.64 14.61 o 1 4 5 397.47 430.17 27.35 o 3 4 5 458.89 473.11 22.37 o 2 5 5 1062.31 1010.77 31.54 o 4 5 5 1430.30 1334.44 77.56 o 1 6 5 581.95 561.14 26.75 o 3 6 5 644.80 596.96 38.83 o 5 6 5 0.02 -13.11 19.13 o 2 7 5 930.81 931.72 106.40 o 4 7 5 837.38 834.33 37.19 o 6 7 5 313.99 328.01 41.92 o 1 8 5 1550.38 1458.02 47.56 o 3 8 5 294.23 298.73 27.31 o 5 8 5 35.70 20.93 21.36 o 7 8 5 3.30 -14.20 25.45 o 2 9 5 13.87 8.40 19.09 o 4 9 5 69.20 76.96 24.04 o 6 9 5 1.88 13.81 21.93 o 8 9 5 219.53 226.39 34.07 o 1 10 5 783.39 842.10 65.48 o 3 10 5 474.22 526.41 37.71 o 5 10 5 4.65 3.20 22.70 o 7 10 5 127.12 150.62 30.33 o 9 10 5 8.88 -30.87 42.92 o 2 11 5 13.63 4.69 23.71 o 4 11 5 7.60 -22.03 25.05 o 6 11 5 173.79 200.34 34.86 o 8 11 5 109.81 115.66 33.73 o 1 12 5 182.54 171.07 31.31 o 3 12 5 136.09 156.14 30.33 o 5 12 5 352.02 374.50 40.51 o 7 12 5 67.33 63.93 31.96 o 2 13 5 35.20 48.34 27.91 o 4 13 5 0.14 5.97 27.71 o 1 1 6 42217.99 51437.25 216.61 o 0 2 6 54.42 53.81 10.37 o 1 3 6 1019.42 1289.77 29.64 o 3 3 6 16010.34 16303.81 156.73 o 0 4 6 3.28 -3.33 19.06 o 2 4 6 14.53 8.38 11.36 o 1 5 6 31498.71 28738.34 521.41 o 3 5 6 2588.03 2137.43 47.65 o 5 5 6 20482.44 19161.09 214.51 o 0 6 6 1.73 8.36 13.34 o 2 6 6 1.42 -8.70 12.99 o 4 6 6 0.99 0.00 15.95 o 1 7 6 4906.53 4705.90 76.10 o 3 7 6 439.43 426.25 28.20 o 5 7 6 4806.89 4602.51 129.61 o 7 7 6 1230.06 1286.24 72.67 o 0 8 6 0.02 -13.95 16.51 o 2 8 6 3.10 -11.68 18.76 o 4 8 6 3.65 8.15 18.70 o 6 8 6 0.10 -3.19 19.47 o 1 9 6 1862.07 1818.10 56.44 o 3 9 6 7650.61 7097.54 118.66 o 5 9 6 1954.36 2202.39 66.67 o 7 9 6 264.39 280.49 34.22 o 9 9 6 2291.88 2558.87 119.19 o 0 10 6 0.02 -28.49 35.43 o 2 10 6 0.02 3.48 21.77 o 4 10 6 0.42 -20.15 25.44 o 6 10 6 1.33 -0.48 24.75 o 8 10 6 0.18 4.59 25.24 o 1 11 6 2315.83 2409.80 72.28 o 3 11 6 628.63 632.52 42.96 o 5 11 6 1889.81 1938.91 69.95 o 7 11 6 618.03 660.80 65.18 o 0 12 6 2.75 -24.49 24.49 o 2 12 6 1.41 10.24 23.53 o 4 12 6 0.18 -28.34 28.34 o 6 12 6 0.41 10.30 27.45 o 1 13 6 717.13 733.25 50.55 o 3 13 6 16.84 38.54 29.09 o 1 2 7 1567.25 1585.87 36.84 o 2 3 7 1.81 -4.07 10.65 o 1 4 7 405.82 431.41 21.95 o 3 4 7 106.63 130.97 16.09 o 2 5 7 322.32 367.17 22.37 o 4 5 7 189.89 195.10 21.87 o 1 6 7 213.96 227.31 20.85 o 3 6 7 218.16 223.95 22.79 o 5 6 7 280.34 263.02 26.18 o 2 7 7 72.80 78.02 18.59 o 4 7 7 87.59 79.26 20.61 o 6 7 7 54.11 51.20 21.51 o 1 8 7 30.05 -1.41 32.44 o 3 8 7 175.22 202.91 24.72 o 5 8 7 331.54 332.00 30.63 o 7 8 7 417.55 393.79 34.93 o 2 9 7 18.88 15.17 19.71 o 4 9 7 33.48 8.27 24.89 o 6 9 7 12.96 -0.84 23.24 o 8 9 7 18.31 10.77 26.75 o 1 10 7 204.28 216.04 28.58 o 3 10 7 191.76 208.30 29.85 o 5 10 7 330.46 327.86 34.64 o 7 10 7 41.23 49.90 28.20 o 9 10 7 34.82 -25.86 33.11 o 2 11 7 58.71 24.99 28.94 o 4 11 7 223.72 223.68 32.81 o 6 11 7 0.63 -28.88 35.43 o 8 11 7 27.40 -7.36 31.94 o 1 12 7 126.55 105.17 29.63 o 3 12 7 66.88 53.60 27.15 o 5 12 7 39.58 21.53 29.59 o 2 13 7 7.66 2.90 26.72 o 4 13 7 7.86 -1.92 28.00 o 0 0 8 179802.78 164540.52 434.90 o 0 2 8 10056.07 10234.41 80.83 o 2 2 8 30920.72 44279.62 249.73 o 1 3 8 19.18 27.48 11.64 o 0 4 8 143713.08 165422.53 6031.20 o 2 4 8 65.99 98.31 14.82 o 4 4 8 51301.95 45309.68 309.29 o 1 5 8 5.98 -15.03 15.03 o 3 5 8 0.00 -10.20 20.86 o 0 6 8 105.43 89.45 17.56 o 2 6 8 39699.04 35835.86 1612.34 o 4 6 8 2338.78 2310.02 56.83 o 6 6 8 14525.85 13524.88 205.70 o 1 7 8 13.96 -8.86 33.14 o 3 7 8 0.30 -7.85 16.97 o 5 7 8 5.20 -6.07 19.76 o 0 8 8 25292.86 24239.01 185.53 o 2 8 8 829.53 877.56 39.88 o 4 8 8 12120.77 11926.62 241.71 o 6 8 8 61.52 121.28 24.63 o 8 8 8 3924.61 4097.74 138.18 o 1 9 8 1.04 -3.95 19.77 o 3 9 8 0.08 -2.39 19.96 o 5 9 8 0.03 -11.58 23.35 o 7 9 8 2.53 -29.32 29.32 o 0 10 8 1845.25 1839.79 120.29 o 2 10 8 10194.36 9966.40 222.57 o 4 10 8 218.49 210.05 31.25 o 6 10 8 9144.12 9434.08 148.46 o 8 10 8 25.19 24.91 29.01 o 1 11 8 0.04 -22.85 26.72 o 3 11 8 7.53 12.97 22.82 o 5 11 8 0.03 -7.30 28.52 o 7 11 8 0.01 6.76 27.21 o 0 12 8 2617.19 2566.53 82.16 o 2 12 8 17.11 3.55 25.58 o 4 12 8 3524.16 3673.95 98.97 o 6 12 8 95.98 110.31 32.93 o 1 13 8 1.41 3.59 27.20 o 3 13 8 0.10 1.13 28.30 o 1 2 9 3069.16 3124.30 54.22 o 2 3 9 97.94 89.97 14.40 o 1 4 9 641.39 615.46 27.02 o 3 4 9 166.98 140.98 18.97 o 2 5 9 3584.70 3387.55 80.78 o 4 5 9 2514.42 2420.41 57.04 o 1 6 9 736.86 721.75 33.56 o 3 6 9 169.93 165.58 22.09 o 5 6 9 232.58 233.05 26.81 o 2 7 9 947.80 889.07 38.89 o 4 7 9 354.06 359.28 29.50 o 6 7 9 48.41 50.16 21.73 o 1 8 9 2753.17 2728.66 69.88 o 3 8 9 233.31 236.29 27.31 o 5 8 9 11.14 0.10 20.80 o 7 8 9 84.78 85.93 26.68 o 2 9 9 13.91 20.46 21.60 o 4 9 9 41.27 23.34 39.22 o 6 9 9 239.72 236.35 33.84 o 8 9 9 166.25 212.45 34.08 o 1 10 9 758.37 740.62 55.70 o 3 10 9 221.79 202.28 31.39 o 5 10 9 18.26 -9.74 28.47 o 7 10 9 40.83 57.84 29.56 o 2 11 9 167.02 185.10 30.19 o 4 11 9 169.82 184.59 33.65 o 6 11 9 63.14 64.35 31.26 o 1 12 9 154.81 175.25 32.74 o 3 12 9 243.40 222.55 36.13 o 5 12 9 236.86 266.51 39.15 o 2 13 9 16.34 -25.90 30.49 o 1 1 10 47640.11 58446.83 296.05 o 0 2 10 52.85 49.40 12.70 o 1 3 10 29971.37 28257.89 157.53 o 3 3 10 2733.71 2553.40 72.89 o 0 4 10 0.01 -2.34 14.54 o 2 4 10 6.84 18.98 14.71 o 1 5 10 30614.91 28761.32 177.84 o 3 5 10 19020.23 18052.93 146.85 o 5 5 10 20318.25 19073.93 230.86 o 0 6 10 1.29 -8.93 17.57 o 2 6 10 0.41 -8.47 17.78 o 4 6 10 0.03 -18.98 18.98 o 1 7 10 5515.30 5460.11 88.83 o 3 7 10 4944.25 4804.30 86.78 o 5 7 10 5053.71 4772.85 213.39 o 7 7 10 1190.96 1195.60 75.26 o 0 8 10 0.09 5.14 19.04 o 2 8 10 1.44 -8.72 18.61 o 4 8 10 0.10 -7.70 19.55 o 6 8 10 0.34 0.02 21.38 o 1 9 10 7205.88 7315.13 224.11 o 3 9 10 2080.23 2272.48 90.64 o 5 9 10 5280.50 5240.13 299.85 o 7 9 10 1906.55 2133.59 135.46 o 9 9 10 1152.74 1290.40 95.02 o 0 10 10 1.59 -20.81 23.54 o 2 10 10 0.77 -0.71 23.33 o 4 10 10 0.74 8.47 23.95 o 6 10 10 0.02 -0.96 27.88 o 8 10 10 0.01 -4.95 29.84 o 1 11 10 2427.43 2367.00 76.34 o 3 11 10 1668.38 1591.13 65.64 o 5 11 10 1898.97 2059.26 82.75 o 7 11 10 912.09 968.10 60.05 o 0 12 10 0.33 -27.94 27.94 o 2 12 10 1.00 8.38 25.65 o 4 12 10 0.00 2.28 26.28 o 1 13 10 491.24 489.36 45.96 o 1 2 11 1075.12 1063.43 32.88 o 2 3 11 0.00 -0.42 12.40 o 1 4 11 222.99 189.62 20.82 o 3 4 11 122.69 122.84 20.38 o 2 5 11 1229.75 1249.30 42.40 o 4 5 11 828.28 748.48 36.20 o 1 6 11 19.60 26.74 19.55 o 3 6 11 0.15 4.77 18.55 o 5 6 11 196.61 184.19 26.46 o 2 7 11 212.66 190.53 24.37 o 4 7 11 156.46 145.01 25.32 o 6 7 11 12.87 3.23 17.62 o 1 8 11 976.97 960.03 43.26 o 3 8 11 168.87 163.38 25.54 o 5 8 11 12.34 -11.86 21.97 o 7 8 11 11.75 12.00 25.93 o 2 9 11 24.90 29.80 22.96 o 4 9 11 0.25 -1.42 21.51 o 6 9 11 159.43 169.07 32.11 o 8 9 11 11.99 -8.10 30.34 o 1 10 11 214.45 201.39 31.60 o 3 10 11 28.62 8.00 25.81 o 5 10 11 0.64 -1.60 26.93 o 7 10 11 5.13 16.63 27.37 o 2 11 11 63.83 70.74 28.27 o 4 11 11 93.88 106.11 31.81 o 6 11 11 9.66 14.59 28.07 o 1 12 11 130.48 120.86 32.60 o 3 12 11 128.27 109.27 32.53 o 5 12 11 31.84 37.81 29.62 o 0 0 12 41777.24 51208.85 300.10 o 0 2 12 32825.82 32378.52 1516.87 o 2 2 12 926.07 1164.88 51.71 o 1 3 12 2.82 0.00 13.58 o 0 4 12 58.18 57.82 15.93 o 2 4 12 37015.41 34643.51 256.26 o 4 4 12 1971.07 1867.78 73.07 o 1 5 12 1.81 -35.51 35.53 o 3 5 12 23.61 11.50 17.57 o 0 6 12 59463.34 55176.80 755.23 o 2 6 12 887.42 844.21 95.52 o 4 6 12 14012.39 13517.71 447.06 o 6 6 12 2249.04 2414.40 96.03 o 1 7 12 0.00 -19.56 19.56 o 3 7 12 2.82 7.38 18.84 o 5 7 12 0.50 -2.41 20.30 o 0 8 12 68.30 62.38 21.17 o 2 8 12 9520.83 9055.51 126.75 o 4 8 12 17.72 28.44 22.66 o 6 8 12 4940.00 5228.76 129.20 o 8 8 12 64.05 87.23 39.92 o 1 9 12 5.76 0.46 22.36 o 3 9 12 0.85 -14.60 19.89 o 5 9 12 0.10 -21.70 27.71 o 7 9 12 0.70 -3.07 25.11 o 0 10 12 7578.89 7373.62 236.19 o 2 10 12 246.72 285.84 33.52 o 4 10 12 8992.95 8747.08 143.00 o 6 10 12 6.10 13.07 27.84 o 1 11 12 0.05 -26.42 26.42 o 3 11 12 4.92 -12.68 27.11 o 5 11 12 0.17 -16.27 26.74 o 0 12 12 352.29 341.74 40.35 o 2 12 12 1366.49 1501.70 68.09 o 4 12 12 101.38 124.80 33.43 o 1 2 13 15.64 28.44 13.69 o 2 3 13 195.22 179.40 20.89 o 1 4 13 1.58 0.76 16.85 o 3 4 13 341.25 332.11 26.61 o 2 5 13 132.84 119.85 22.09 o 4 5 13 216.02 213.37 26.53 o 1 6 13 594.66 580.60 34.94 o 3 6 13 478.98 465.55 32.39 o 5 6 13 6.17 7.62 20.25 o 2 7 13 145.44 138.40 24.98 o 4 7 13 345.26 347.02 31.25 o 6 7 13 157.30 169.87 28.23 o 1 8 13 386.79 383.26 32.81 o 3 8 13 177.32 186.16 27.79 o 5 8 13 54.69 67.90 24.67 o 7 8 13 126.51 146.52 29.78 o 2 9 13 39.66 23.42 23.56 o 4 9 13 10.38 12.29 24.35 o 6 9 13 2.90 12.59 24.63 o 8 9 13 169.59 178.37 36.19 o 1 10 13 454.15 504.57 46.71 o 3 10 13 308.28 345.82 38.04 o 5 10 13 68.64 50.90 45.41 o 7 10 13 101.32 61.52 67.57 o 2 11 13 0.01 -8.65 25.83 o 4 11 13 24.22 16.85 29.34 o 6 11 13 96.89 131.28 35.19 o 1 12 13 79.01 82.25 29.84 o 3 12 13 90.18 110.01 32.62 o 1 1 14 4090.04 4792.18 102.65 o 0 2 14 29.65 44.08 15.80 o 1 3 14 4706.33 4620.29 75.84 o 3 3 14 559.88 547.37 44.12 o 0 4 14 2.13 -16.86 16.86 o 2 4 14 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