#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/29/2012925.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012925_Fobs loop_ _publ_author_name 'Geller, Jordan' 'Wharf, Ivor' 'B\'elanger-Gari\'epy, Francine' 'Lebuis, Anne-Marie' 'Butler, Ian S.' 'Gilson, Denis F. R.' _publ_section_title ; Chlorotris(2,4,6-trimethylphenyl)tin(IV) and its ethanol hemisolvate ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m466 _journal_page_last m468 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.270 _cell_angle_gamma 90.000 _cell_length_a 8.2337 _cell_length_b 30.7435 _cell_length_c 30.3142 _exptl_crystal_F_000 3144.00 _reflns_d_resolution_high 0.8063 _[local]_cod_data_source_file fg1654Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' butl71 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 716.41 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 895.64 934.55 62.77 o 4 0 0 63828.07 69336.16 1052.39 o 1 1 0 1999.95 2254.43 40.66 o 2 1 0 13865.72 15342.42 254.01 o 3 1 0 43.08 44.67 33.73 o 4 1 0 128.81 93.92 41.96 o 5 1 0 2024.66 2245.73 109.25 o 6 1 0 22075.96 21553.45 758.29 o 0 2 0 669.73 1078.59 29.96 o 1 2 0 26492.50 29095.17 387.29 o 2 2 0 730.27 910.62 43.83 o 3 2 0 2664.77 2323.21 74.24 o 4 2 0 64.67 80.83 40.54 o 5 2 0 855.59 735.69 84.68 o 6 2 0 1459.80 1301.67 275.59 o 1 3 0 13957.10 14810.77 162.57 o 2 3 0 70157.70 78011.22 1039.76 o 3 3 0 134.74 112.06 35.46 o 4 3 0 3376.29 3318.35 93.00 o 5 3 0 11104.44 10674.65 227.34 o 6 3 0 5730.99 4677.91 415.63 o 0 4 0 385021.81 360354.31 4079.79 o 1 4 0 22590.67 25847.84 281.93 o 2 4 0 52885.36 58409.71 555.53 o 3 4 0 3505.75 3596.79 81.00 o 4 4 0 51957.61 53424.02 353.65 o 5 4 0 5802.63 5618.28 178.03 o 6 4 0 10405.55 9448.05 445.52 o 7 4 0 1763.19 2477.26 501.44 o 1 5 0 158.80 290.16 31.51 o 2 5 0 57211.10 65430.70 773.28 o 3 5 0 493.69 531.15 42.96 o 4 5 0 20369.81 21571.65 249.73 o 5 5 0 15135.95 14912.82 324.55 o 6 5 0 13423.92 12339.10 378.30 o 7 5 0 4.37 -188.98 347.71 o 8 5 0 832.77 1511.67 444.85 o 0 6 0 49053.80 49679.27 941.12 o 1 6 0 962.70 1082.08 49.67 o 2 6 0 78661.43 88842.80 695.47 o 3 6 0 103.63 93.03 38.80 o 4 6 0 154.74 136.54 52.83 o 5 6 0 1471.96 1262.04 132.94 o 6 6 0 6831.40 6885.61 303.60 o 7 6 0 3717.45 3864.20 1313.21 o 8 6 0 495.57 455.60 388.98 o 1 7 0 51.30 120.82 49.94 o 2 7 0 4758.61 5599.08 109.09 o 3 7 0 2549.53 2700.55 95.87 o 4 7 0 2184.41 2192.62 109.22 o 5 7 0 5687.45 5489.79 221.82 o 6 7 0 33.37 190.83 127.95 o 7 7 0 691.70 761.13 253.95 o 8 7 0 7117.90 6865.47 896.46 o 0 8 0 994.61 1008.97 65.92 o 1 8 0 95021.75 104621.34 922.21 o 2 8 0 59293.47 66562.64 805.72 o 3 8 0 4385.99 4428.21 117.53 o 4 8 0 18732.34 18563.07 291.49 o 5 8 0 4214.50 4094.33 208.55 o 6 8 0 3463.01 3787.10 281.49 o 7 8 0 950.08 1062.58 244.75 o 8 8 0 880.16 1646.42 443.62 o 9 8 0 110.04 294.50 485.28 o 1 9 0 3895.02 4551.21 102.72 o 2 9 0 2849.09 3246.13 98.67 o 3 9 0 11261.24 12988.43 268.14 o 4 9 0 286.16 322.41 73.69 o 5 9 0 17732.72 17900.81 388.78 o 6 9 0 320.05 337.41 137.69 o 7 9 0 2288.32 2215.23 278.19 o 8 9 0 734.26 993.58 293.69 o 9 9 0 1387.83 1497.27 524.17 o 0 10 0 8673.36 8355.38 158.05 o 1 10 0 13001.21 13450.51 168.05 o 2 10 0 106762.89 122037.64 1097.36 o 3 10 0 13182.71 15073.05 219.27 o 4 10 0 8157.40 8228.05 223.89 o 5 10 0 2094.41 2172.45 180.00 o 6 10 0 14058.44 12761.13 400.41 o 7 10 0 118.50 109.88 182.84 o 8 10 0 2012.71 2307.16 322.86 o 9 10 0 14.49 49.18 289.48 o 1 11 0 91.77 130.41 41.85 o 2 11 0 2526.83 2924.05 103.52 o 3 11 0 3930.67 4305.17 128.82 o 4 11 0 9721.42 9995.80 252.43 o 5 11 0 294.40 303.75 116.53 o 6 11 0 619.58 606.44 192.34 o 7 11 0 379.82 465.68 188.68 o 8 11 0 8375.38 8186.51 408.14 o 9 11 0 0.42 119.13 300.47 o 0 12 0 9996.81 11234.84 193.60 o 1 12 0 14430.59 16009.70 197.04 o 2 12 0 119736.91 137943.86 2289.98 o 3 12 0 6.41 -27.93 50.92 o 4 12 0 250.60 334.48 99.94 o 5 12 0 905.68 899.45 145.24 o 6 12 0 17328.51 16383.69 448.39 o 7 12 0 571.44 790.23 195.81 o 8 12 0 860.30 1119.10 231.12 o 9 12 0 61.66 -37.64 269.41 o 1 13 0 269.93 300.58 51.14 o 2 13 0 2136.41 2150.74 102.06 o 3 13 0 11607.03 12560.10 297.08 o 4 13 0 1675.69 1519.43 145.51 o 5 13 0 3881.67 3559.26 228.15 o 6 13 0 2713.62 2940.12 248.19 o 7 13 0 2979.26 2780.21 260.90 o 8 13 0 361.83 330.38 190.21 o 9 13 0 987.82 941.10 334.22 o 0 14 0 76816.36 76718.20 2255.39 o 1 14 0 11705.28 11737.92 184.25 o 2 14 0 16528.34 14193.24 545.86 o 3 14 0 17680.01 19004.01 337.28 o 4 14 0 17939.20 18026.38 398.13 o 5 14 0 29.74 182.96 113.67 o 6 14 0 3971.83 3857.74 271.97 o 7 14 0 80.44 188.63 166.78 o 8 14 0 1003.41 1001.96 199.67 o 9 14 0 246.38 189.04 207.71 o 1 15 0 18014.76 19130.24 238.18 o 2 15 0 212.67 173.53 58.96 o 3 15 0 13063.38 13494.24 294.69 o 4 15 0 1134.33 895.44 134.59 o 5 15 0 16.72 100.57 120.91 o 6 15 0 1707.93 1436.14 200.91 o 7 15 0 5369.53 5186.22 327.01 o 8 15 0 1647.03 1340.42 207.28 o 9 15 0 274.84 545.18 206.04 o 0 16 0 84.36 232.18 88.68 o 1 16 0 5528.19 5533.19 144.45 o 2 16 0 28045.11 23997.70 1635.83 o 3 16 0 10187.28 10096.58 265.10 o 4 16 0 33.86 8.52 97.31 o 5 16 0 455.86 513.52 179.19 o 6 16 0 622.11 695.26 173.09 o 7 16 0 1924.62 1717.75 219.21 o 8 16 0 418.97 329.53 152.00 o 9 16 0 714.74 712.52 251.99 o 1 17 0 21.75 54.31 56.23 o 2 17 0 3636.05 4055.20 159.04 o 3 17 0 629.31 604.80 115.38 o 4 17 0 4519.77 3957.84 236.95 o 5 17 0 1088.29 1360.41 204.33 o 6 17 0 6875.21 6578.05 321.63 o 7 17 0 20.03 100.80 147.06 o 8 17 0 548.28 465.28 154.87 o 9 17 0 0.55 177.91 212.77 o 0 18 0 79741.85 80927.66 1780.31 o 1 18 0 8240.01 8029.45 188.88 o 2 18 0 3722.63 3547.48 158.18 o 3 18 0 5904.69 6126.34 247.25 o 4 18 0 21060.89 21049.38 510.53 o 5 18 0 1194.73 1247.60 218.24 o 6 18 0 4574.71 4443.43 276.63 o 7 18 0 66.55 67.16 146.00 o 8 18 0 1118.63 943.91 167.50 o 1 19 0 3901.33 4001.28 179.30 o 2 19 0 75.25 52.97 84.55 o 3 19 0 13314.89 12898.73 361.98 o 4 19 0 595.61 757.75 127.39 o 5 19 0 294.20 327.72 165.56 o 6 19 0 2618.34 2679.54 225.66 o 7 19 0 3231.37 3127.92 244.66 o 8 19 0 3.62 3.42 122.80 o 0 20 0 101.68 173.26 103.96 o 1 20 0 3143.74 3138.09 174.12 o 2 20 0 78.33 70.26 91.08 o 3 20 0 9742.53 9470.76 340.57 o 4 20 0 498.32 540.57 161.20 o 5 20 0 27.49 -83.06 149.92 o 6 20 0 7.54 74.26 137.21 o 7 20 0 555.71 766.72 152.14 o 8 20 0 24.17 -42.59 120.01 o 1 21 0 1112.11 955.90 124.86 o 2 21 0 2647.39 2375.29 192.07 o 3 21 0 2.68 -29.62 105.02 o 4 21 0 453.30 453.59 157.82 o 5 21 0 5666.09 5887.34 315.09 o 6 21 0 3816.09 3485.85 243.48 o 7 21 0 493.15 382.93 143.81 o 8 21 0 26.80 84.37 125.88 o 0 22 0 50962.10 47521.35 747.35 o 1 22 0 6339.78 5946.17 240.60 o 2 22 0 804.75 919.88 207.72 o 3 22 0 1.25 64.97 159.85 o 4 22 0 12126.82 11313.09 353.88 o 5 22 0 525.86 574.85 154.69 o 6 22 0 3034.14 2945.90 227.59 o 7 22 0 92.06 284.35 126.60 o 8 22 0 346.74 511.71 125.40 o 1 23 0 279.93 312.61 132.49 o 2 23 0 1189.15 1164.16 165.99 o 3 23 0 1047.45 1056.62 186.07 o 4 23 0 1313.06 1446.45 190.37 o 5 23 0 573.38 624.82 156.70 o 6 23 0 1767.11 1658.27 178.62 o 7 23 0 337.27 429.91 137.64 o 8 23 0 669.29 878.82 132.43 o 0 24 0 6009.10 5800.79 387.03 o 1 24 0 1310.47 1505.08 151.32 o 2 24 0 7923.66 7800.22 324.59 o 3 24 0 1640.80 1560.96 211.90 o 4 24 0 165.41 35.51 141.56 o 5 24 0 2.47 -44.10 129.26 o 6 24 0 892.89 955.23 157.52 o 7 24 0 92.70 147.93 117.50 o 1 25 0 5754.45 5988.86 415.28 o 2 25 0 16.82 274.77 181.72 o 3 25 0 148.74 392.02 170.13 o 4 25 0 689.49 702.90 165.35 o 5 25 0 6108.61 6562.44 300.51 o 6 25 0 36.65 -18.75 126.15 o 7 25 0 105.31 124.94 116.34 o 0 26 0 2085.44 2496.77 447.34 o 1 26 0 11320.32 10258.57 515.17 o 2 26 0 2632.12 3055.11 275.71 o 3 26 0 62.62 134.78 167.61 o 4 26 0 6026.61 6206.42 284.92 o 5 26 0 1767.50 1841.31 192.53 o 6 26 0 1400.15 1368.18 159.35 o 7 26 0 277.56 246.42 110.77 o 1 27 0 2410.00 2303.54 294.53 o 2 27 0 150.55 228.57 175.52 o 3 27 0 377.07 198.13 167.60 o 4 27 0 660.54 795.03 166.14 o 5 27 0 2043.39 1942.13 185.98 o 6 27 0 482.11 478.89 127.22 o 7 27 0 66.07 138.83 106.86 o 0 28 0 44.23 -16.13 268.09 o 1 28 0 102.80 191.14 181.49 o 2 28 0 4968.07 5149.04 322.73 o 3 28 0 48.19 -26.59 157.23 o 4 28 0 6.25 -44.77 139.89 o 5 28 0 197.29 113.05 126.95 o 6 28 0 768.60 776.39 137.54 o 1 29 0 2420.80 2396.21 290.60 o 2 29 0 1.83 -120.75 167.62 o 3 29 0 1488.34 1623.95 202.67 o 4 29 0 782.20 886.71 156.76 o 5 29 0 1677.75 1783.43 184.25 o 6 29 0 150.04 310.74 116.25 o 0 30 0 12.28 -10.40 273.20 o 1 30 0 2494.47 2307.00 260.91 o 2 30 0 3204.44 3051.77 273.49 o 3 30 0 466.58 471.50 159.94 o 4 30 0 71.91 -0.33 144.72 o 5 30 0 627.63 748.68 162.60 o 6 30 0 680.79 774.50 183.83 o 1 31 0 1183.18 917.40 217.03 o 2 31 0 155.53 129.32 167.63 o 3 31 0 396.34 437.48 149.74 o 4 31 0 26.97 104.22 135.49 o 5 31 0 1026.71 1130.31 195.16 o 0 32 0 154.55 396.88 261.07 o 1 32 0 786.73 668.20 196.00 o 2 32 0 2829.93 2731.01 306.36 o 3 32 0 429.09 363.71 151.78 o 4 32 0 214.01 306.78 141.78 o 5 32 0 116.84 325.53 152.59 o 1 33 0 1279.30 985.38 202.59 o 2 33 0 19.21 70.06 182.97 o 3 33 0 1319.37 1504.37 200.96 o 4 33 0 568.13 742.22 161.58 o 0 34 0 672.18 464.18 254.71 o 1 34 0 14.75 -51.35 155.42 o 2 34 0 1252.80 1215.28 201.95 o 3 34 0 43.36 89.26 157.67 o 4 34 0 275.87 315.56 192.57 o 1 35 0 11.35 159.55 142.88 o 2 35 0 454.45 259.91 168.48 o 3 35 0 210.19 227.08 165.57 o 0 36 0 2113.50 2207.32 312.32 o 1 36 0 548.78 463.47 175.76 o 2 36 0 110.60 472.87 173.66 o 3 36 0 277.16 -48.16 218.56 o 1 37 0 775.17 814.66 169.89 o 2 37 0 7.57 69.67 173.61 o 0 38 0 263.96 631.60 374.14 o -5 0 1 38575.81 37800.36 465.26 o -3 0 1 27810.11 30924.24 542.28 o -1 0 1 27696.07 31992.46 415.76 o 1 0 1 159441.62 169580.44 3616.34 o 3 0 1 1167.37 1252.90 84.12 o 5 0 1 19562.92 17568.81 359.75 o -6 1 1 12707.78 12383.78 850.16 o -5 1 1 1499.64 1449.32 92.23 o -4 1 1 1955.41 2167.82 86.69 o -3 1 1 55780.41 59867.56 837.50 o -2 1 1 7289.08 7988.37 164.75 o -1 1 1 6907.03 7749.94 152.08 o 0 1 1 7447.99 7664.41 104.18 o 1 1 1 110107.87 121667.20 1365.29 o 2 1 1 1269.49 1255.10 48.22 o 3 1 1 305.23 215.29 38.55 o 4 1 1 3159.93 3304.51 94.29 o 5 1 1 13872.13 13031.65 234.48 o 6 1 1 356.82 247.63 212.21 o -6 2 1 318.99 -55.57 313.02 o -5 2 1 665.58 710.14 79.93 o -4 2 1 6074.60 5691.28 120.43 o -3 2 1 17.15 19.98 32.93 o -2 2 1 266.31 244.00 31.47 o -1 2 1 35912.24 40767.47 630.58 o 0 2 1 742.43 851.57 20.41 o 1 2 1 14350.00 14957.74 251.04 o 2 2 1 3458.08 4434.35 102.34 o 3 2 1 200.30 102.69 31.76 o 4 2 1 1633.99 1435.83 70.68 o 5 2 1 4919.84 4724.87 156.41 o 6 2 1 1512.43 1668.45 296.16 o -6 3 1 11243.48 10812.14 564.49 o -5 3 1 5925.35 5929.82 178.86 o -4 3 1 4638.18 4712.54 111.46 o -3 3 1 18492.15 19528.63 250.61 o -2 3 1 61551.86 68788.01 1052.38 o -1 3 1 42636.54 47815.95 451.93 o 0 3 1 9863.65 10788.06 163.96 o 1 3 1 173695.55 184923.81 2180.62 o 2 3 1 9169.34 10015.41 145.61 o 3 3 1 38926.14 41217.68 599.76 o 4 3 1 34.47 85.42 40.76 o 5 3 1 33112.87 33459.55 375.58 o 6 3 1 81.23 189.00 159.75 o 7 3 1 11649.43 10824.23 1205.78 o -7 4 1 805.69 275.98 598.26 o -6 4 1 4354.81 4000.57 414.86 o -5 4 1 32748.23 32744.89 634.49 o -4 4 1 1250.13 1530.45 82.58 o -3 4 1 7929.99 8492.00 138.73 o -2 4 1 2971.32 2933.61 65.43 o -1 4 1 183155.00 208836.55 2217.67 o 0 4 1 5251.30 5311.43 89.81 o 1 4 1 24590.13 26214.46 292.52 o 2 4 1 7260.10 7380.77 102.46 o 3 4 1 376.55 354.43 39.39 o 4 4 1 10316.71 10315.33 174.02 o 5 4 1 19919.18 19654.27 295.61 o 6 4 1 8251.36 7311.98 334.33 o 7 4 1 2226.05 2205.30 1233.56 o -8 5 1 1744.50 1479.90 663.09 o -7 5 1 734.01 976.39 442.51 o -6 5 1 2398.27 2463.95 221.37 o -5 5 1 2274.96 2683.86 173.74 o -4 5 1 11666.54 11328.23 211.21 o -3 5 1 49796.39 54275.48 645.51 o -2 5 1 7930.35 8674.21 109.35 o -1 5 1 12577.25 13905.68 248.19 o 0 5 1 3937.04 4455.31 74.80 o 1 5 1 26171.02 29145.57 265.17 o 2 5 1 18496.37 20494.19 295.08 o 3 5 1 3069.32 3168.09 76.26 o 4 5 1 13569.21 14147.66 208.57 o 5 5 1 804.95 764.30 96.78 o 6 5 1 3579.25 3163.79 234.00 o 7 5 1 3751.15 4004.59 534.36 o 8 5 1 43.32 8.90 371.57 o -8 6 1 3210.58 4317.47 594.69 o -7 6 1 6568.45 6858.23 686.82 o -6 6 1 5839.83 5955.28 298.06 o -5 6 1 1631.64 1419.53 135.38 o -4 6 1 2623.14 2780.52 109.01 o -3 6 1 2200.04 2296.08 80.49 o -2 6 1 125439.54 141353.41 965.52 o -1 6 1 46261.34 52932.40 605.14 o 0 6 1 341.05 320.40 29.70 o 1 6 1 8177.99 9649.31 136.67 o 2 6 1 3327.90 3363.89 108.49 o 3 6 1 21688.60 22865.57 208.74 o 4 6 1 1169.78 1165.09 92.19 o 5 6 1 10591.52 10469.27 240.63 o 6 6 1 91.28 29.96 126.59 o 7 6 1 2880.86 2720.87 488.83 o 8 6 1 303.47 110.23 370.62 o -8 7 1 431.36 399.00 356.83 o -7 7 1 52.68 48.74 233.10 o -6 7 1 1210.59 1464.08 193.28 o -5 7 1 38901.80 40175.78 546.65 o -4 7 1 529.22 475.27 63.50 o -3 7 1 9575.59 9958.28 158.67 o -2 7 1 7541.93 8616.39 130.86 o -1 7 1 20218.00 20218.32 271.24 o 0 7 1 356.74 397.33 33.94 o 1 7 1 706.46 795.30 41.84 o 2 7 1 1344.16 1596.68 68.43 o 3 7 1 92125.16 103164.36 1068.39 o 4 7 1 78.42 97.64 60.17 o 5 7 1 26509.79 25570.43 441.99 o 6 7 1 384.55 496.14 140.14 o 7 7 1 4333.97 4668.64 407.91 o 8 7 1 1655.16 1817.16 437.32 o -9 8 1 154.75 753.84 572.33 o -8 8 1 87.79 284.64 346.57 o -7 8 1 4573.78 4152.29 386.42 o -6 8 1 3959.86 3814.19 243.44 o -5 8 1 2296.95 2074.73 165.53 o -4 8 1 9676.82 10283.16 213.90 o -3 8 1 11725.96 14322.94 193.91 o -2 8 1 8138.02 9739.04 143.31 o -1 8 1 65071.27 71566.57 743.56 o 0 8 1 8084.92 8174.65 126.12 o 1 8 1 2319.45 2339.17 73.86 o 2 8 1 76991.94 88590.85 789.63 o 3 8 1 2574.93 2899.71 101.61 o 4 8 1 10267.58 11062.02 228.10 o 5 8 1 46.93 1.83 86.60 o 6 8 1 12681.26 11403.69 385.40 o 7 8 1 34.88 -6.89 189.18 o 8 8 1 146.51 287.14 356.89 o 9 8 1 418.04 532.61 373.78 o -9 9 1 6.90 522.32 581.59 o -8 9 1 1994.04 2744.49 365.99 o -7 9 1 30.71 126.12 194.44 o -6 9 1 949.25 984.27 158.10 o -5 9 1 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