#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/29/2012939.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012939_Fobs loop_ _publ_author_name 'Karaghiosoff, Konstantin' 'Klap\"otke, Thomas M.' 'Michailovski, Alexej' 'Holl, Gerhard' _publ_section_title ; 4,10-Dinitro-2,6,8,12-tetraoxa-4,10-diazaisowurtzitane (TEX): a nitramine with an exceptionally high density ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o580 _journal_page_last o581 _journal_volume 58 _journal_year 2002 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 82.370 _cell_angle_beta 75.054 _cell_angle_gamma 79.456 _cell_length_a 6.8360 _cell_length_b 7.6404 _cell_length_c 8.7765 _exptl_crystal_F_000 268.00 _reflns_d_resolution_high 0.7550 _[local]_cod_data_source_file gg1130Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' G027 in P -1 (2) SIR97' _shelx_refln_list_code 4 _shelx_f_calc_maximum 59.23 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 820.33 662.04 14.71 o 2 0 0 2635.90 2467.79 31.76 o 3 0 0 1.69 4.61 1.05 o 4 0 0 202.31 224.65 2.91 o 5 0 0 0.33 1.36 1.89 o 6 0 0 0.23 0.76 1.05 o 7 0 0 1.65 1.99 1.16 o 8 0 0 39.62 45.25 2.32 o -8 1 0 78.93 87.89 2.37 o -7 1 0 2.38 1.57 1.63 o -6 1 0 583.40 566.53 22.26 o -5 1 0 55.15 51.80 1.67 o -4 1 0 25.97 24.41 1.36 o -3 1 0 119.72 109.64 1.99 o -2 1 0 13.68 11.51 1.43 o -1 1 0 320.07 268.60 11.43 o 0 1 0 65.29 53.14 2.80 o 1 1 0 798.61 684.42 17.89 o 2 1 0 12.51 8.75 1.25 o 3 1 0 157.68 149.97 2.44 o 4 1 0 239.94 237.50 8.77 o 5 1 0 75.21 75.72 1.59 o 6 1 0 8.72 8.01 0.99 o 7 1 0 3.44 3.16 1.35 o 8 1 0 0.01 0.36 1.58 o -8 2 0 0.38 -0.01 1.96 o -7 2 0 0.17 -0.33 1.58 o -6 2 0 11.88 9.67 1.40 o -5 2 0 70.28 65.50 1.59 o -4 2 0 16.68 13.86 1.23 o -3 2 0 58.30 55.87 2.23 o -2 2 0 1415.56 1450.67 17.45 o -1 2 0 575.86 536.06 4.62 o 0 2 0 3.11 1.69 1.53 o 1 2 0 487.82 409.01 5.44 o 2 2 0 985.13 936.66 15.47 o 3 2 0 360.15 388.30 3.59 o 4 2 0 78.37 90.84 1.78 o 5 2 0 139.87 141.31 3.02 o 6 2 0 121.42 120.62 2.37 o 7 2 0 12.40 11.46 1.66 o 8 2 0 15.66 15.44 1.65 o -7 3 0 23.01 25.54 1.53 o -6 3 0 32.92 32.07 1.54 o -5 3 0 3.39 5.88 1.32 o -4 3 0 370.36 363.89 3.70 o -3 3 0 352.65 358.73 5.14 o -2 3 0 1506.74 1636.34 47.34 o -1 3 0 1895.65 2036.42 21.61 o 0 3 0 188.23 146.36 4.72 o 1 3 0 520.09 487.85 15.29 o 2 3 0 244.32 277.37 6.64 o 3 3 0 5.69 7.62 1.37 o 4 3 0 77.52 78.54 3.73 o 5 3 0 161.05 155.43 2.79 o 6 3 0 1.25 2.30 1.09 o 7 3 0 38.95 40.90 1.48 o 8 3 0 13.80 16.18 1.71 o -7 4 0 91.54 95.34 2.05 o -6 4 0 9.23 9.10 1.20 o -5 4 0 28.00 27.76 1.53 o -4 4 0 31.02 31.64 1.90 o -3 4 0 307.98 290.69 4.70 o -2 4 0 173.53 181.44 2.21 o -1 4 0 28.89 31.89 1.75 o 0 4 0 206.24 217.13 2.58 o 1 4 0 443.08 429.63 5.37 o 2 4 0 418.97 472.99 6.38 o 3 4 0 220.24 215.66 2.87 o 4 4 0 23.54 22.05 1.16 o 5 4 0 214.59 209.54 8.79 o 6 4 0 463.59 455.73 14.58 o 7 4 0 45.86 44.58 2.19 o 8 4 0 1.02 1.28 1.58 o -6 5 0 0.20 0.67 1.59 o -5 5 0 2.03 4.06 1.32 o -4 5 0 390.68 380.73 9.33 o -3 5 0 0.05 0.47 1.16 o -2 5 0 0.33 -0.35 0.94 o -1 5 0 35.57 37.21 1.27 o 0 5 0 47.70 58.99 1.46 o 1 5 0 31.33 28.63 1.23 o 2 5 0 110.77 114.48 1.95 o 3 5 0 321.76 323.08 12.77 o 4 5 0 5.89 7.46 1.11 o 5 5 0 75.72 74.03 1.58 o 6 5 0 27.60 23.71 2.52 o 7 5 0 194.25 194.85 2.67 o 8 5 0 14.46 10.85 3.77 o -6 6 0 10.66 9.40 2.13 o -5 6 0 82.11 91.51 1.94 o -4 6 0 0.08 0.25 1.72 o -3 6 0 52.28 47.02 1.61 o -2 6 0 49.25 45.92 1.28 o -1 6 0 111.42 109.84 1.81 o 0 6 0 5.94 4.96 1.36 o 1 6 0 611.61 605.41 10.11 o 2 6 0 6.92 6.93 1.00 o 3 6 0 65.56 61.84 1.42 o 4 6 0 155.01 148.24 2.17 o 5 6 0 64.16 71.10 1.79 o 6 6 0 27.90 31.23 1.50 o 7 6 0 2.28 0.26 2.01 o -5 7 0 7.09 4.79 2.02 o -4 7 0 34.11 33.57 2.96 o -3 7 0 33.85 32.27 1.40 o -2 7 0 31.72 32.49 1.39 o -1 7 0 1.70 2.15 1.15 o 0 7 0 5.81 6.06 1.38 o 1 7 0 461.42 425.55 2.94 o 2 7 0 1.30 1.15 0.92 o 3 7 0 116.67 110.64 1.84 o 4 7 0 8.37 9.23 1.22 o 5 7 0 153.78 149.80 2.94 o 6 7 0 21.61 24.45 1.68 o 7 7 0 6.56 4.80 2.11 o -4 8 0 1.17 2.73 1.38 o -3 8 0 2.38 3.35 1.96 o -2 8 0 7.34 4.94 1.47 o -1 8 0 394.34 399.71 2.90 o 0 8 0 77.38 85.44 1.84 o 1 8 0 106.22 102.14 1.93 o 2 8 0 57.79 58.66 1.54 o 3 8 0 141.94 147.40 4.03 o 4 8 0 32.22 31.47 1.54 o 5 8 0 17.06 18.90 1.94 o 6 8 0 11.47 10.10 2.28 o -2 9 0 7.33 2.92 2.04 o -1 9 0 13.30 14.34 2.20 o 0 9 0 35.07 37.67 1.63 o 1 9 0 43.66 45.52 2.60 o 2 9 0 56.59 58.22 3.55 o 3 9 0 5.61 5.61 1.42 o 4 9 0 104.41 107.93 2.11 o -4 -9 1 5.98 2.88 1.96 o -3 -9 1 239.45 250.55 4.62 o -2 -9 1 11.80 13.87 2.57 o -1 -9 1 69.85 76.15 1.85 o 0 -9 1 0.40 0.50 1.36 o 1 -9 1 28.83 35.32 1.80 o 2 -9 1 25.72 20.45 8.53 o -5 -8 1 49.67 53.72 2.19 o -4 -8 1 88.24 87.75 1.87 o -3 -8 1 124.44 129.25 2.29 o -2 -8 1 62.81 66.54 1.77 o -1 -8 1 66.80 63.43 2.22 o 0 -8 1 32.27 29.05 1.78 o 1 -8 1 9.83 9.12 2.08 o 2 -8 1 8.87 8.13 2.24 o 3 -8 1 2.00 1.68 1.99 o 4 -8 1 0.00 -0.38 1.36 o -6 -7 1 12.72 11.56 3.29 o -5 -7 1 10.08 12.67 1.66 o -4 -7 1 101.08 97.57 2.13 o -3 -7 1 9.71 10.52 1.22 o -2 -7 1 198.34 199.93 2.64 o -1 -7 1 165.69 163.61 4.59 o 0 -7 1 1014.87 969.76 4.26 o 1 -7 1 127.74 128.60 2.34 o 2 -7 1 29.59 27.19 1.33 o 3 -7 1 26.38 24.04 1.46 o 4 -7 1 1.10 0.90 1.42 o 5 -7 1 29.34 14.57 2.23 o -7 -6 1 3.59 2.79 1.95 o -6 -6 1 25.38 25.51 1.52 o -5 -6 1 7.48 7.53 1.61 o -4 -6 1 51.15 46.30 1.44 o -3 -6 1 5.13 4.88 0.94 o -2 -6 1 114.82 106.04 1.94 o -1 -6 1 99.39 91.72 3.72 o 0 -6 1 271.03 250.07 2.87 o 1 -6 1 0.70 3.37 0.97 o 2 -6 1 39.40 38.95 1.52 o 3 -6 1 100.95 112.22 1.82 o 4 -6 1 55.59 43.65 2.86 o 5 -6 1 15.54 16.23 1.30 o 6 -6 1 16.36 15.78 4.44 o -7 -5 1 16.95 20.42 1.77 o -6 -5 1 121.24 119.60 3.19 o -5 -5 1 86.16 87.20 1.82 o -4 -5 1 12.21 13.15 1.15 o -3 -5 1 8.08 7.24 1.12 o -2 -5 1 930.49 946.46 40.28 o -1 -5 1 42.59 42.54 1.33 o 0 -5 1 279.16 299.95 10.56 o 1 -5 1 47.31 47.74 1.64 o 2 -5 1 145.44 162.45 1.99 o 3 -5 1 131.53 121.93 1.75 o 4 -5 1 11.28 11.31 1.19 o 5 -5 1 7.88 7.65 1.20 o 6 -5 1 4.45 5.13 1.56 o -8 -4 1 20.41 16.92 2.31 o -7 -4 1 114.06 112.31 1.93 o -6 -4 1 106.27 113.32 2.21 o -5 -4 1 95.07 95.83 1.83 o -4 -4 1 154.75 159.51 2.34 o -3 -4 1 34.34 39.69 1.28 o -2 -4 1 82.03 76.23 2.21 o -1 -4 1 401.41 431.79 3.35 o 0 -4 1 334.02 351.14 8.33 o 1 -4 1 415.74 410.96 7.26 o 2 -4 1 30.48 28.07 1.59 o 3 -4 1 85.06 78.34 3.36 o 4 -4 1 37.99 38.30 1.24 o 5 -4 1 0.57 2.02 1.13 o 6 -4 1 2.94 5.71 1.49 o 7 -4 1 3.44 1.89 1.63 o -8 -3 1 1.01 2.26 1.56 o -7 -3 1 39.06 37.99 1.42 o -6 -3 1 102.42 100.93 1.95 o -5 -3 1 250.45 260.49 8.59 o -4 -3 1 227.48 232.79 5.10 o -3 -3 1 151.69 138.44 2.03 o -2 -3 1 62.21 66.51 1.92 o -1 -3 1 223.79 224.79 2.68 o 0 -3 1 511.62 488.67 16.40 o 1 -3 1 75.16 69.58 1.84 o 2 -3 1 1501.43 1640.12 27.56 o 3 -3 1 110.51 127.94 4.29 o 4 -3 1 113.83 116.60 2.27 o 5 -3 1 149.59 150.78 2.58 o 6 -3 1 210.86 214.88 5.74 o 7 -3 1 6.90 5.63 1.41 o -8 -2 1 100.28 101.08 15.73 o -7 -2 1 4.75 1.21 1.32 o -6 -2 1 0.01 0.12 1.05 o -5 -2 1 8.28 7.74 1.14 o -4 -2 1 433.33 435.82 4.50 o -3 -2 1 4.36 5.47 1.12 o -2 -2 1 41.01 38.28 1.69 o -1 -2 1 2209.71 1920.65 103.88 o 0 -2 1 154.46 122.96 2.47 o 1 -2 1 268.76 203.73 2.90 o 2 -2 1 1695.17 1872.00 55.19 o 3 -2 1 777.79 835.18 4.82 o 4 -2 1 58.26 56.03 1.48 o 5 -2 1 142.29 137.46 5.62 o 6 -2 1 1.75 1.72 1.14 o 7 -2 1 22.22 22.89 1.48 o 8 -2 1 77.79 66.60 2.16 o -8 -1 1 32.02 35.73 1.79 o -7 -1 1 124.53 122.34 2.13 o -6 -1 1 7.42 7.42 1.12 o -5 -1 1 90.01 80.66 1.57 o -4 -1 1 17.55 15.05 1.24 o -3 -1 1 0.08 0.19 1.33 o -2 -1 1 2228.99 2112.02 8.24 o -1 -1 1 340.34 267.34 10.29 o 0 -1 1 1301.93 1105.78 40.42 o 1 -1 1 39.84 34.65 2.44 o 2 -1 1 22.27 18.76 1.57 o 3 -1 1 75.42 72.64 1.79 o 4 -1 1 376.83 398.39 10.68 o 5 -1 1 121.84 122.00 3.44 o 6 -1 1 40.46 41.18 1.44 o 7 -1 1 37.87 34.45 2.06 o 8 -1 1 0.58 1.47 1.58 o -8 0 1 5.17 5.40 1.41 o -7 0 1 48.98 49.34 3.81 o -6 0 1 1008.15 991.01 44.01 o -5 0 1 3.24 3.99 1.26 o -4 0 1 0.05 -0.40 1.93 o -3 0 1 8.77 8.23 1.55 o -2 0 1 679.63 603.57 10.62 o -1 0 1 684.69 633.72 8.65 o 0 0 1 260.61 191.21 5.38 o 1 0 1 981.32 847.25 15.91 o 2 0 1 638.81 559.14 12.46 o 3 0 1 724.00 778.55 5.37 o 4 0 1 463.09 516.67 4.71 o 5 0 1 329.65 330.75 15.02 o 6 0 1 2.20 1.49 1.93 o 7 0 1 70.83 74.15 1.70 o 8 0 1 0.01 -0.07 1.21 o -8 1 1 6.51 5.78 1.42 o -7 1 1 36.24 33.81 1.61 o -6 1 1 5.07 3.74 1.72 o -5 1 1 354.65 342.29 9.58 o -4 1 1 8.74 9.26 1.18 o -3 1 1 266.66 251.34 8.33 o -2 1 1 248.62 241.27 4.43 o 2 1 1 374.88 363.07 4.92 o 3 1 1 1078.49 1117.85 28.84 o 4 1 1 0.84 -0.27 1.31 o 5 1 1 1.28 0.26 0.93 o 6 1 1 201.99 198.24 5.05 o 7 1 1 54.63 53.94 1.68 o 8 1 1 143.89 145.79 8.64 o -7 2 1 2.36 2.87 1.25 o -6 2 1 15.56 19.96 1.43 o -5 2 1 44.51 46.20 1.98 o -4 2 1 378.80 383.99 8.97 o -3 2 1 115.65 120.81 2.97 o -2 2 1 188.14 221.27 4.87 o -1 2 1 113.40 117.29 2.38 o 0 2 1 206.00 190.14 3.56 o 1 2 1 15.93 17.66 1.58 o 2 2 1 2730.67 2736.84 16.00 o 3 2 1 235.64 226.76 5.09 o 4 2 1 46.11 48.13 1.79 o 5 2 1 19.81 21.02 1.15 o 6 2 1 0.27 1.71 0.88 o 7 2 1 10.96 8.45 1.19 o 8 2 1 28.53 27.06 1.39 o -7 3 1 32.80 31.92 2.42 o -6 3 1 25.47 29.78 2.30 o -5 3 1 28.43 26.56 1.14 o -4 3 1 158.11 151.58 2.95 o -3 3 1 28.15 36.16 1.59 o -2 3 1 56.76 51.09 1.58 o -1 3 1 83.60 68.43 2.28 o 0 3 1 44.47 52.52 1.63 o 1 3 1 430.58 377.05 5.55 o 2 3 1 232.53 237.32 3.17 o 3 3 1 693.33 724.59 11.20 o 4 3 1 53.79 45.00 1.67 o 5 3 1 259.99 265.42 6.65 o 6 3 1 118.64 113.99 1.97 o 7 3 1 13.02 12.11 1.24 o 8 3 1 57.45 62.11 4.47 o -7 4 1 17.23 12.96 1.77 o -6 4 1 3.11 3.79 1.70 o -5 4 1 2.47 2.11 1.36 o -4 4 1 141.00 137.24 7.38 o -3 4 1 346.78 357.79 2.79 o -2 4 1 6.10 5.40 1.17 o -1 4 1 123.76 134.08 3.76 o 0 4 1 1392.63 1427.16 29.92 o 1 4 1 83.92 97.05 1.91 o 2 4 1 350.67 344.24 10.69 o 3 4 1 47.62 51.15 1.61 o 4 4 1 17.38 17.98 1.11 o 5 4 1 101.76 98.51 3.36 o 6 4 1 199.66 188.52 2.82 o 7 4 1 13.10 15.35 1.48 o 8 4 1 0.10 0.54 1.57 o -6 5 1 4.28 3.43 1.38 o -5 5 1 0.02 0.78 1.59 o -4 5 1 328.67 339.57 2.84 o -3 5 1 2.70 3.38 1.08 o -2 5 1 37.61 37.58 1.41 o -1 5 1 158.94 170.76 2.30 o 0 5 1 83.12 86.35 1.77 o 1 5 1 665.34 640.68 9.26 o 2 5 1 5.59 4.04 0.98 o 3 5 1 17.01 20.72 1.27 o 4 5 1 201.56 208.75 7.78 o 5 5 1 1.83 1.24 0.89 o 6 5 1 0.60 1.39 1.57 o 7 5 1 1.06 1.25 1.35 o 8 5 1 20.76 17.11 1.62 o -5 6 1 31.32 31.58 2.68 o -4 6 1 1.41 -0.21 1.64 o -3 6 1 0.60 0.62 1.12 o -2 6 1 245.26 234.13 2.24 o -1 6 1 1179.77 1109.00 4.68 o 0 6 1 0.00 0.78 1.06 o 1 6 1 98.67 94.51 1.77 o 2 6 1 177.10 189.53 2.28 o 3 6 1 56.28 59.33 1.56 o 4 6 1 61.15 64.01 2.10 o 5 6 1 0.43 -0.86 1.32 o 6 6 1 123.03 120.94 6.56 o 7 6 1 0.30 -1.35 1.93 o -5 7 1 38.55 23.08 2.67 o -4 7 1 0.02 0.48 1.58 o -3 7 1 9.47 7.23 1.34 o -2 7 1 5.86 4.54 1.22 o -1 7 1 0.15 -0.37 1.16 o 0 7 1 30.98 32.27 2.07 o 1 7 1 24.63 23.40 1.28 o 2 7 1 0.01 0.13 1.04 o 3 7 1 11.79 11.79 1.36 o 4 7 1 8.70 6.14 1.18 o 5 7 1 72.96 70.55 1.82 o 6 7 1 20.72 22.54 1.87 o 7 7 1 1.68 0.20 2.71 o -3 8 1 78.74 75.53 17.83 o -2 8 1 31.00 40.62 1.73 o -1 8 1 5.86 5.97 1.36 o 0 8 1 11.62 13.29 1.25 o 1 8 1 115.81 116.09 2.02 o 2 8 1 18.73 17.96 1.28 o 3 8 1 10.80 12.89 1.82 o 4 8 1 1.12 1.16 1.28 o 5 8 1 10.05 11.64 1.21 o 6 8 1 3.36 3.15 1.58 o -2 9 1 38.77 36.17 14.78 o -1 9 1 15.64 16.43 1.68 o 0 9 1 14.94 17.16 1.34 o 1 9 1 17.04 17.27 1.27 o 2 9 1 55.34 55.81 1.56 o 3 9 1 29.84 32.02 1.61 o 4 9 1 44.52 45.27 3.15 o 5 9 1 1.31 -0.03 1.39 o 1 10 1 0.36 2.28 2.85 o 2 10 1 0.09 0.79 1.37 o -3 -9 2 100.99 94.47 4.40 o -2 -9 2 32.35 22.98 8.62 o -1 -9 2 13.32 10.03 2.13 o 0 -9 2 63.75 77.28 7.34 o 1 -9 2 1.27 2.21 1.43 o 2 -9 2 99.24 101.92 2.99 o -5 -8 2 49.01 52.90 4.44 o -4 -8 2 2.94 3.08 2.44 o -3 -8 2 44.49 43.29 1.45 o -2 -8 2 84.10 84.72 1.72 o -1 -8 2 31.63 31.63 1.50 o 0 -8 2 25.03 23.77 1.52 o 1 -8 2 12.32 13.77 1.44 o 2 -8 2 7.79 9.79 1.19 o 3 -8 2 10.82 9.32 1.49 o -6 -7 2 25.97 21.01 4.12 o -5 -7 2 44.51 44.25 3.37 o -4 -7 2 0.00 -0.05 1.27 o -3 -7 2 142.00 144.98 2.11 o -2 -7 2 65.65 65.92 1.94 o -1 -7 2 28.07 25.14 1.49 o 0 -7 2 63.36 57.39 1.71 o 1 -7 2 0.97 1.24 1.34 o 2 -7 2 32.11 31.73 1.51 o 3 -7 2 1.58 4.20 1.13 o 4 -7 2 8.74 11.57 1.43 o 5 -7 2 65.53 61.57 9.49 o -7 -6 2 0.24 0.71 1.96 o -6 -6 2 2.48 2.24 1.34 o -5 -6 2 5.77 6.86 1.30 o -4 -6 2 73.41 74.35 1.78 o -3 -6 2 0.03 -0.46 1.26 o -2 -6 2 186.36 178.78 2.02 o -1 -6 2 231.52 229.35 3.48 o 0 -6 2 347.29 342.90 3.29 o 1 -6 2 10.43 11.01 1.01 o 2 -6 2 130.38 141.79 3.76 o 3 -6 2 105.40 122.83 4.43 o 4 -6 2 126.78 117.51 2.81 o 5 -6 2 0.03 0.01 1.12 o 6 -6 2 22.20 22.01 2.22 o -7 -5 2 50.57 45.25 14.28 o -6 -5 2 61.42 63.73 2.77 o -5 -5 2 42.27 45.58 1.58 o -4 -5 2 63.49 60.08 1.48 o -3 -5 2 1.17 2.91 1.02 o -2 -5 2 38.14 37.40 1.25 o -1 -5 2 16.35 19.08 1.21 o 0 -5 2 2.09 2.28 0.95 o 1 -5 2 0.02 0.34 0.92 o 2 -5 2 368.61 367.93 10.64 o 3 -5 2 316.34 315.93 2.76 o 4 -5 2 42.13 51.83 1.66 o 5 -5 2 2.53 2.06 1.34 o 6 -5 2 3.08 3.98 2.11 o -7 -4 2 94.71 107.97 2.56 o -6 -4 2 96.36 101.19 2.82 o -5 -4 2 0.08 0.16 1.22 o -4 -4 2 21.59 20.58 1.06 o -3 -4 2 179.25 172.21 3.20 o -2 -4 2 51.45 51.36 1.38 o -1 -4 2 157.53 154.32 4.37 o 0 -4 2 137.74 128.77 3.82 o 1 -4 2 9.60 5.90 1.00 o 2 -4 2 276.97 273.09 2.61 o 3 -4 2 52.72 60.51 1.48 o 4 -4 2 7.92 7.37 1.36 o 5 -4 2 20.91 24.23 2.57 o 6 -4 2 101.85 95.03 1.95 o 7 -4 2 123.88 127.69 2.44 o -8 -3 2 9.68 6.79 1.69 o -7 -3 2 34.33 33.45 2.06 o -6 -3 2 2.91 3.47 1.31 o -5 -3 2 5.22 6.91 1.66 o -4 -3 2 408.32 423.53 12.97 o -3 -3 2 24.10 24.46 1.45 o -2 -3 2 25.22 24.18 1.33 o -1 -3 2 110.32 108.77 2.01 o 0 -3 2 83.89 78.79 1.75 o 1 -3 2 3116.89 3443.90 29.31 o 2 -3 2 495.09 516.61 5.82 o 3 -3 2 0.83 2.40 0.95 o 4 -3 2 19.87 19.90 1.71 o 5 -3 2 126.64 121.65 5.10 o 6 -3 2 95.23 102.14 2.40 o 7 -3 2 3.00 3.60 1.37 o -8 -2 2 2.71 1.60 1.42 o -7 -2 2 10.91 11.89 1.37 o -6 -2 2 0.35 0.81 1.15 o -5 -2 2 246.54 253.37 7.25 o -4 -2 2 1237.58 1265.41 16.37 o -3 -2 2 141.02 146.31 5.34 o -2 -2 2 156.39 160.47 2.24 o -1 -2 2 864.26 835.35 5.03 o 0 -2 2 1118.52 1011.01 17.82 o 1 -2 2 2351.33 2324.45 102.72 o 2 -2 2 367.92 399.05 3.67 o 3 -2 2 23.54 19.94 1.37 o 4 -2 2 10.80 10.96 1.32 o 5 -2 2 207.15 196.73 2.30 o 6 -2 2 100.85 101.58 4.01 o 7 -2 2 10.11 8.32 1.42 o 8 -2 2 77.35 78.27 2.80 o -8 -1 2 97.79 100.50 2.09 o -7 -1 2 23.14 22.04 1.49 o -6 -1 2 44.22 44.10 1.43 o -5 -1 2 37.87 38.15 1.24 o -4 -1 2 0.00 1.22 1.10 o -3 -1 2 0.52 0.28 0.94 o -2 -1 2 2175.08 2197.31 39.51 o -1 -1 2 578.05 534.70 4.41 o 1 -1 2 429.33 380.07 6.68 o 2 -1 2 287.09 247.10 3.51 o 3 -1 2 0.80 0.44 1.39 o 4 -1 2 336.22 367.37 8.35 o 5 -1 2 440.22 458.60 10.74 o 6 -1 2 198.76 185.14 2.90 o 7 -1 2 48.02 48.25 1.54 o 8 -1 2 139.66 152.91 3.99 o -8 0 2 9.52 8.24 3.57 o -7 0 2 3.79 0.70 1.33 o -6 0 2 286.10 297.48 4.29 o -5 0 2 2.22 3.66 1.07 o -4 0 2 5.22 4.52 1.11 o -3 0 2 398.73 420.51 3.30 o -2 0 2 533.40 575.22 25.37 o -1 0 2 288.64 229.29 5.24 o 0 0 2 567.73 479.08 7.15 o 1 0 2 306.64 280.39 6.16 o 2 0 2 2.29 2.70 1.66 o 3 0 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