#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/29/2012956.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012956_Fobs loop_ _publ_author_name 'Rivard, Eric' 'McWilliams, Andrew R.' 'Lough, Alan J.' 'Manners, Ian' _publ_section_title ; Bis(trichlorophosphine)iminium salts, [Cl~3~P=N=PCl~3~]^+^, with transition metal halide counter-ions ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first i114 _journal_page_last i118 _journal_volume 58 _journal_year 2002 _space_group_IT_number 64 _symmetry_space_group_name_Hall '-C 2ac 2' _symmetry_space_group_name_H-M 'C m c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 18.0456 _cell_length_b 11.4295 _cell_length_c 15.7039 _exptl_crystal_F_000 2112.00 _reflns_d_resolution_high 0.7962 _[local]_cod_data_source_file sk1570IVsup5.hkl _[local]_cod_data_source_block IV #BEGIN Tags that were not found in dictionaries: _shelx_title ' k98227a in Cmca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 771.68 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y+1/2, z+1/2' '-x, y+1/2, -z+1/2' 'x, -y, -z' 'x+1/2, y+1/2, z' '-x+1/2, -y+1, z+1/2' '-x+1/2, y+1, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x, y-1/2, -z-1/2' 'x, -y-1/2, z-1/2' '-x, y, z' '-x+1/2, -y+1/2, -z' 'x+1/2, y, -z-1/2' 'x+1/2, -y, z-1/2' '-x+1/2, y+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 72355.30 68355.70 2620.32 o 6 0 0 261499.17 251973.30 8130.23 o 8 0 0 595488.50 570605.50 18999.61 o 10 0 0 38740.77 39877.68 1562.48 o 12 0 0 27101.23 25941.39 994.67 o 14 0 0 44703.53 46958.34 2809.47 o 16 0 0 82964.08 95162.73 3935.30 o 18 0 0 362.19 522.26 170.30 o 20 0 0 19108.34 24007.32 2163.85 o 22 0 0 4386.78 4737.28 590.74 o 2 2 0 135138.36 137292.50 5219.20 o 4 2 0 181.91 227.08 34.06 o 6 2 0 27684.36 27092.73 839.10 o 8 2 0 12333.27 11665.29 330.69 o 10 2 0 1865.08 1919.67 90.87 o 12 2 0 6290.88 6242.58 216.05 o 14 2 0 13464.75 14335.67 557.94 o 16 2 0 629.31 431.46 113.54 o 18 2 0 3456.74 3510.16 215.83 o 20 2 0 323.34 613.08 249.77 o 22 2 0 2395.93 2589.36 397.49 o 2 4 0 69164.42 71419.26 2260.40 o 4 4 0 105.30 -45.41 45.41 o 6 4 0 59134.64 60772.77 1668.82 o 8 4 0 355384.22 364602.16 9719.72 o 10 4 0 4837.95 4660.58 193.24 o 12 4 0 23413.47 24598.52 833.27 o 14 4 0 29949.28 31414.29 1188.03 o 16 4 0 12679.23 13746.83 637.27 o 18 4 0 5010.39 4863.16 284.06 o 20 4 0 1205.41 2021.17 442.84 o 0 6 0 35971.08 35514.26 1447.22 o 2 6 0 34174.36 33683.89 1469.01 o 4 6 0 11564.00 12087.37 375.95 o 6 6 0 144715.92 148980.55 4744.53 o 8 6 0 762.82 794.84 90.84 o 10 6 0 31263.58 31638.23 1166.28 o 12 6 0 1509.78 1533.10 124.92 o 14 6 0 35022.24 37805.77 1771.43 o 16 6 0 4935.31 5067.72 272.70 o 18 6 0 23.38 -181.64 204.35 o 20 6 0 3562.99 3498.54 454.36 o 0 8 0 31699.12 32758.85 1270.08 o 2 8 0 10712.79 11200.54 421.16 o 4 8 0 8087.71 7177.37 409.49 o 6 8 0 11938.78 12043.68 398.42 o 8 8 0 512.98 522.28 90.83 o 10 8 0 358.52 295.19 102.18 o 12 8 0 2989.04 2578.50 159.03 o 14 8 0 3692.85 3669.29 215.84 o 16 8 0 664.65 692.59 193.02 o 18 8 0 2679.45 2600.84 318.01 o 0 10 0 4141.70 4715.34 318.14 o 2 10 0 44801.24 48271.24 2073.35 o 4 10 0 3717.64 3237.90 272.67 o 6 10 0 27998.15 30930.46 2568.03 o 8 10 0 18078.29 18099.36 774.55 o 10 10 0 1381.92 987.93 124.91 o 12 10 0 9325.80 9653.47 477.56 o 14 10 0 13909.59 13357.53 955.73 o 16 10 0 732.12 635.82 227.08 o 0 12 0 17918.66 20179.49 1844.85 o 2 12 0 1938.88 2055.53 158.99 o 4 12 0 11476.88 12410.02 546.00 o 6 12 0 2261.40 2294.11 181.71 o 8 12 0 2167.38 2350.84 227.13 o 10 12 0 11499.00 13283.91 705.14 o 12 12 0 944.79 885.64 181.67 o 0 14 0 11469.42 13317.39 1046.29 o 2 14 0 2256.59 2453.03 215.78 o 4 14 0 1416.47 1226.36 170.33 o 3 1 1 73585.87 70141.84 1626.16 o 5 1 1 444.45 420.16 22.71 o 7 1 1 42424.56 41055.93 670.21 o 9 1 1 15946.63 15750.71 273.93 o 11 1 1 2913.78 2897.30 79.53 o 13 1 1 4131.83 3977.39 125.00 o 15 1 1 9976.34 10091.07 295.79 o 17 1 1 3155.51 3237.46 124.95 o 19 1 1 197.32 215.71 113.53 o 21 1 1 546.42 579.04 215.72 o 2 2 1 18485.84 18321.69 437.60 o 4 2 1 653.68 749.57 34.07 o 6 2 1 110256.02 104888.50 1927.83 o 8 2 1 21.69 22.71 34.06 o 10 2 1 921.29 760.84 56.78 o 12 2 1 6409.50 6174.50 170.57 o 14 2 1 29140.13 30152.18 776.94 o 16 2 1 29.30 56.76 90.82 o 18 2 1 276.76 386.01 90.83 o 20 2 1 1952.49 1794.30 181.70 o 22 2 1 2892.31 3850.27 386.16 o 1 3 1 34714.80 35358.94 892.67 o 3 3 1 1026.90 999.59 34.08 o 5 3 1 9530.89 8402.07 250.81 o 7 3 1 13846.39 13497.59 285.24 o 9 3 1 24209.33 24701.94 480.32 o 11 3 1 2826.72 3010.69 90.89 o 13 3 1 18.51 -11.35 56.76 o 15 3 1 25033.45 26997.06 741.68 o 17 3 1 2442.74 2192.06 136.29 o 19 3 1 12.57 45.41 124.88 o 21 3 1 3258.29 4145.85 318.04 o 0 4 1 139411.73 141170.52 8255.80 o 2 4 1 22819.63 23801.80 573.54 o 4 4 1 1114.53 1124.43 45.43 o 6 4 1 7655.17 7478.84 170.75 o 8 4 1 51396.34 51267.82 945.35 o 10 4 1 9664.92 9708.56 227.63 o 12 4 1 2295.27 2067.30 90.87 o 14 4 1 841.69 726.70 79.48 o 16 4 1 4188.98 4158.37 159.06 o 18 4 1 3232.04 3816.64 170.39 o 20 4 1 554.61 442.79 204.37 o 1 5 1 640.68 840.31 56.78 o 3 5 1 2679.66 3000.03 79.55 o 5 5 1 5760.73 5800.88 147.87 o 7 5 1 102.11 102.18 45.41 o 9 5 1 355.87 295.20 56.77 o 11 5 1 4491.60 4250.36 113.65 o 13 5 1 1684.84 1680.80 102.21 o 15 5 1 2756.02 2498.91 124.95 o 17 5 1 11.85 11.35 102.17 o 19 5 1 2.31 -45.41 136.23 o 21 5 1 18.62 22.71 227.05 o 0 6 1 2659.16 2692.92 113.63 o 2 6 1 4589.23 5184.41 170.54 o 4 6 1 6500.58 6642.96 170.62 o 6 6 1 14463.52 14737.90 307.75 o 8 6 1 447.65 442.81 56.77 o 10 6 1 161.31 136.24 68.12 o 12 6 1 266.73 193.01 79.47 o 14 6 1 5115.29 5022.80 170.46 o 16 6 1 446.13 465.50 102.18 o 18 6 1 29.28 113.53 113.53 o 20 6 1 413.53 465.49 261.13 o 1 7 1 2317.47 2465.14 79.52 o 3 7 1 1828.40 1942.28 102.23 o 5 7 1 2217.37 2158.25 79.51 o 7 7 1 6500.91 6913.24 193.30 o 9 7 1 7330.20 7197.97 204.68 o 11 7 1 751.80 692.62 79.48 o 13 7 1 948.91 953.80 90.84 o 15 7 1 3255.57 3350.97 147.67 o 17 7 1 2283.78 2271.39 159.00 o 19 7 1 81.52 45.41 181.65 o 0 8 1 76568.42 79764.15 2926.38 o 2 8 1 1229.72 1362.74 68.14 o 4 8 1 2138.60 2612.45 124.94 o 6 8 1 2675.96 2680.86 79.52 o 8 8 1 28287.52 30037.03 776.62 o 10 8 1 2455.06 2464.74 102.22 o 12 8 1 1554.61 1453.57 102.20 o 14 8 1 369.68 340.60 102.18 o 16 8 1 5218.08 4999.45 215.89 o 18 8 1 841.12 885.63 204.38 o 1 9 1 8755.20 8508.36 216.12 o 3 9 1 143.15 56.77 68.12 o 5 9 1 4959.31 5318.64 227.29 o 7 9 1 3225.06 3226.27 124.96 o 9 9 1 3024.40 3067.01 113.59 o 11 9 1 278.35 215.71 79.47 o 13 9 1 998.67 840.24 113.55 o 15 9 1 2764.69 2669.08 147.65 o 17 9 1 331.08 227.07 170.30 o 0 10 1 4921.99 5420.65 227.28 o 2 10 1 837.63 806.18 68.13 o 4 10 1 3258.10 3646.56 193.12 o 6 10 1 0.07 -34.06 102.17 o 8 10 1 291.46 227.07 79.47 o 10 10 1 85.63 22.71 68.12 o 12 10 1 198.51 306.53 113.53 o 14 10 1 57.68 11.35 113.53 o 16 10 1 9.48 -79.47 170.29 o 1 11 1 429.55 329.26 79.48 o 3 11 1 467.67 386.03 79.48 o 7 11 1 21.02 -45.41 113.53 o 9 11 1 1316.33 1101.46 136.26 o 11 11 1 28.75 56.76 102.17 o 13 11 1 149.82 215.71 136.24 o 0 12 1 3449.66 3589.60 249.91 o 2 12 1 23.10 -22.71 79.47 o 4 12 1 0.23 68.12 79.47 o 6 12 1 24.18 34.06 79.47 o 8 12 1 3062.99 2953.17 170.38 o 10 12 1 306.76 363.30 147.59 o 12 12 1 123.12 215.71 147.59 o 1 13 1 3960.98 4146.40 204.48 o 3 13 1 2164.86 2328.12 124.92 o 5 13 1 868.42 828.86 102.19 o 7 13 1 5500.83 5669.85 215.89 o 9 13 1 2146.63 1873.81 170.35 o 0 14 1 221.56 227.06 170.30 o 2 14 1 496.68 544.97 124.89 o 4 14 1 499.20 465.50 113.54 o 2 0 2 61808.80 63371.48 2503.56 o 4 0 2 63082.75 59283.73 1571.92 o 6 0 2 48603.34 47059.71 1289.15 o 8 0 2 47248.04 43937.63 1027.98 o 10 0 2 5208.97 4514.15 136.45 o 12 0 2 25379.02 25835.60 834.14 o 14 0 2 31020.99 33482.41 1223.15 o 16 0 2 1605.23 1680.74 136.28 o 18 0 2 169.16 147.59 136.24 o 20 0 2 489.91 397.38 238.43 o 22 0 2 7172.41 9285.36 966.04 o 1 1 2 41351.23 40650.50 1537.55 o 3 1 2 40337.41 37384.86 783.23 o 5 1 2 9557.61 9402.49 205.39 o 7 1 2 12104.12 11180.68 216.77 o 9 1 2 49916.92 49694.23 842.28 o 11 1 2 2987.17 2976.86 79.53 o 13 1 2 1484.43 1374.16 79.50 o 15 1 2 9971.50 10068.14 284.41 o 17 1 2 8010.47 8254.49 261.51 o 19 1 2 5.86 -34.06 102.17 o 21 1 2 1600.22 1328.60 204.40 o 0 2 2 71463.18 69926.98 2645.76 o 2 2 2 9082.12 8716.87 182.79 o 4 2 2 6200.81 5923.48 125.30 o 6 2 2 655.30 533.73 34.07 o 8 2 2 3.27 34.06 34.06 o 10 2 2 7996.89 7840.19 182.07 o 12 2 2 3451.16 3306.48 102.26 o 14 2 2 97.06 102.18 68.12 o 16 2 2 2515.98 2532.90 113.58 o 18 2 2 278.23 113.53 102.18 o 20 2 2 496.75 283.84 147.60 o 22 2 2 16.04 22.71 249.76 o 1 3 2 544.93 613.24 34.07 o 3 3 2 0.97 0.00 22.71 o 5 3 2 2940.23 2830.35 68.20 o 7 3 2 3963.39 4263.23 90.95 o 9 3 2 7733.46 7919.74 170.68 o 11 3 2 765.10 669.94 56.77 o 13 3 2 753.21 647.21 68.13 o 15 3 2 7.84 -34.06 79.47 o 17 3 2 2148.06 2044.29 113.57 o 19 3 2 568.54 431.44 124.89 o 21 3 2 14.70 249.76 295.17 o 0 4 2 102254.70 103043.06 3253.12 o 2 4 2 67.07 102.18 22.71 o 4 4 2 39288.73 38467.39 876.09 o 6 4 2 34886.10 33189.52 746.74 o 8 4 2 5441.17 5333.06 125.08 o 10 4 2 4960.34 5285.83 136.41 o 12 4 2 4675.81 4659.63 159.11 o 14 4 2 10953.50 11787.97 284.46 o 16 4 2 6169.30 6398.95 227.32 o 18 4 2 966.59 885.66 113.55 o 20 4 2 3209.91 3759.67 318.04 o 1 5 2 56101.98 57882.85 1772.99 o 3 5 2 62323.51 63605.51 1484.86 o 5 5 2 32940.71 34671.04 745.74 o 7 5 2 31969.95 32446.85 721.80 o 9 5 2 45998.88 47164.03 964.88 o 11 5 2 11473.56 11564.86 284.57 o 13 5 2 4519.35 4363.54 147.72 o 15 5 2 21124.14 22021.07 649.69 o 17 5 2 7372.32 7400.10 272.81 o 19 5 2 202.39 136.24 215.71 o 21 5 2 2640.52 2930.17 533.79 o 0 6 2 11120.76 10549.84 330.39 o 2 6 2 21089.21 21769.11 662.79 o 4 6 2 16803.10 16942.45 376.50 o 6 6 2 600.08 601.79 45.42 o 8 6 2 32451.72 33509.18 881.22 o 10 6 2 533.45 556.35 68.12 o 12 6 2 160.24 102.18 68.12 o 14 6 2 729.33 624.49 90.83 o 16 6 2 1255.86 1010.61 113.55 o 18 6 2 3027.49 3316.63 181.73 o 20 6 2 104.87 22.71 215.70 o 1 7 2 7600.88 7815.67 193.40 o 3 7 2 3491.09 3681.73 136.36 o 5 7 2 2850.32 2897.04 90.89 o 7 7 2 12529.99 12217.74 273.28 o 9 7 2 259.60 317.89 56.77 o 11 7 2 1383.31 1237.79 79.49 o 13 7 2 2983.09 2930.65 113.59 o 15 7 2 2034.88 2169.14 124.92 o 17 7 2 6.72 158.94 136.23 o 19 7 2 772.41 579.06 306.56 o 0 8 2 2303.65 2851.14 590.68 o 2 8 2 6416.53 6822.24 159.19 o 4 8 2 40.27 0.00 79.47 o 6 8 2 99.88 102.18 56.76 o 8 8 2 11567.17 12245.35 341.41 o 10 8 2 138.69 113.53 56.77 o 12 8 2 1926.58 1680.80 102.21 o 14 8 2 372.98 227.07 90.83 o 16 8 2 28.32 56.76 113.53 o 18 8 2 780.95 840.20 181.67 o 1 9 2 10941.65 10993.16 295.88 o 3 9 2 21819.24 23474.17 627.35 o 5 9 2 6864.18 6957.87 272.86 o 7 9 2 10942.94 11013.56 295.82 o 9 9 2 11012.04 11410.66 352.67 o 11 9 2 3915.18 3578.63 159.05 o 13 9 2 1897.83 1567.18 124.92 o 15 9 2 6935.84 6978.34 272.77 o 17 9 2 2015.36 1873.77 193.06 o 0 10 2 28591.68 30885.50 1210.30 o 2 10 2 5961.20 6353.73 193.23 o 4 10 2 14.74 -11.35 102.17 o 6 10 2 13671.18 14603.33 591.87 o 8 10 2 5260.41 5193.17 170.45 o 10 10 2 9658.13 10018.58 363.90 o 12 10 2 125.27 124.88 90.82 o 14 10 2 3237.31 2873.71 181.74 o 16 10 2 4156.34 4214.50 261.28 o 1 11 2 4320.66 4022.08 136.34 o 3 11 2 370.28 476.85 79.47 o 5 11 2 1437.86 1203.70 90.85 o 7 11 2 3731.16 3601.15 181.76 o 9 11 2 1200.31 1214.99 136.26 o 11 11 2 620.90 510.92 113.54 o 13 11 2 712.76 431.45 124.89 o 0 12 2 414.02 272.48 136.24 o 2 12 2 620.74 476.86 90.83 o 4 12 2 2008.83 1794.34 102.21 o 6 12 2 2.17 79.47 79.47 o 8 12 2 941.79 828.87 147.61 o 10 12 2 532.93 431.44 147.60 o 12 12 2 1233.09 851.61 136.26 o 1 13 2 103.95 147.59 102.18 o 3 13 2 469.34 283.84 102.18 o 5 13 2 164.99 79.47 79.47 o 7 13 2 50.67 79.47 102.18 o 9 13 2 261.46 181.65 136.24 o 0 14 2 2570.87 2316.86 238.50 o 2 14 2 4854.92 5407.88 227.22 o 4 14 2 1322.40 1180.92 124.90 o 1 1 3 22045.53 21580.30 519.59 o 3 1 3 129292.57 129684.02 2817.09 o 5 1 3 2060.96 1613.71 56.82 o 7 1 3 461.36 363.35 45.42 o 9 1 3 87.67 102.18 45.41 o 11 1 3 286.74 317.90 56.77 o 13 1 3 5590.35 5399.58 159.15 o 15 1 3 4081.60 4158.60 136.35 o 17 1 3 810.47 692.62 90.84 o 19 1 3 119.45 90.82 102.18 o 21 1 3 770.68 817.49 238.44 o 0 2 3 97391.96 97134.15 4364.22 o 2 2 3 26094.78 23786.48 553.44 o 4 2 3 362148.34 361419.47 8148.14 o 6 2 3 78109.75 75908.63 1592.16 o 8 2 3 23728.28 23217.04 480.59 o 10 2 3 1296.69 1260.61 68.14 o 12 2 3 16614.01 16756.28 387.56 o 14 2 3 19921.57 21126.95 513.07 o 16 2 3 1758.64 1555.85 102.21 o 18 2 3 975.24 1067.34 113.55 o 20 2 3 38.32 -22.71 147.59 o 22 2 3 2600.53 2532.65 374.79 o 1 3 3 445.53 579.12 22.71 o 3 3 3 5952.89 6853.33 148.00 o 5 3 3 47275.82 46078.50 1098.76 o 7 3 3 21104.46 20249.37 400.19 o 9 3 3 2292.09 2283.42 68.16 o 11 3 3 17482.74 16944.48 364.89 o 13 3 3 6518.66 6776.05 204.65 o 15 3 3 1188.93 1192.32 90.84 o 17 3 3 6.82 22.71 90.82 o 19 3 3 22.45 0.00 124.88 o 21 3 3 81.69 34.06 295.17 o 0 4 3 48907.78 47998.33 1518.05 o 2 4 3 3717.93 3899.96 90.96 o 4 4 3 63340.63 65035.76 1371.13 o 6 4 3 3386.82 3023.21 90.92 o 8 4 3 19404.48 19111.18 422.41 o 10 4 3 3409.05 3033.81 90.90 o 12 4 3 15536.65 15721.88 410.14 o 14 4 3 5254.96 5682.44 159.11 o 16 4 3 4419.68 4078.96 159.07 o 18 4 3 413.98 408.73 113.54 o 20 4 3 1707.04 1794.21 227.12 o 1 5 3 1395.34 1635.60 79.51 o 3 5 3 2564.53 2590.67 68.18 o 5 5 3 16662.78 16786.57 388.00 o 7 5 3 14135.19 14406.87 307.74 o 9 5 3 679.20 465.54 56.77 o 11 5 3 3531.31 3294.93 113.62 o 13 5 3 3950.26 4169.83 136.34 o 15 5 3 1632.71 1601.22 113.56 o 17 5 3 710.39 476.87 113.54 o 19 5 3 90.06 90.82 170.29 o 0 6 3 66786.57 67364.24 2293.74 o 2 6 3 5810.36 5788.70 181.96 o 4 6 3 9567.58 8890.87 193.53 o 6 6 3 33120.01 32812.31 664.26 o 8 6 3 22072.10 21892.01 570.70 o 10 6 3 12.29 -11.35 68.12 o 12 6 3 3.11 -45.41 68.12 o 14 6 3 11762.40 12856.92 420.98 o 16 6 3 2934.77 2532.95 136.30 o 18 6 3 6.77 -102.17 136.23 o 20 6 3 435.41 601.73 227.07 o 1 7 3 2951.94 2919.97 79.53 o 3 7 3 23187.61 23437.18 651.03 o 5 7 3 5761.49 6298.45 147.80 o 7 7 3 0.65 -45.41 45.41 o 9 7 3 665.05 488.24 68.13 o 11 7 3 73.52 158.94 68.12 o 13 7 3 304.03 272.48 68.12 o 15 7 3 3667.95 3816.94 147.68 o 17 7 3 976.60 1135.45 136.25 o 19 7 3 96.44 56.76 158.94 o 0 8 3 30620.73 31392.58 1075.01 o 2 8 3 376.02 431.44 56.77 o 4 8 3 24980.66 24069.53 856.36 o 6 8 3 6727.56 7447.07 204.65 o 8 8 3 16168.25 16983.91 558.16 o 10 8 3 199.10 238.42 79.47 o 12 8 3 11456.57 12298.04 352.67 o 14 8 3 6820.57 7126.49 238.69 o 16 8 3 3237.73 3169.06 181.74 o 18 8 3 8.07 11.35 215.70 o 1 9 3 2860.72 2578.67 102.24 o 3 9 3 1925.49 1771.75 102.22 o 5 9 3 6320.30 6445.42 238.72 o 7 9 3 339.49 420.08 68.12 o 9 9 3 531.89 465.51 68.12 o 11 9 3 792.42 669.90 90.83 o 13 9 3 772.33 851.56 102.19 o 15 9 3 1016.05 1044.62 136.25 o 17 9 3 45.38 -102.18 204.35 o 0 10 3 10951.17 10455.88 477.85 o 2 10 3 702.13 760.74 68.13 o 4 10 3 2091.50 2180.61 90.86 o 6 10 3 5678.61 5421.03 250.03 o 8 10 3 4886.38 4465.56 170.44 o 10 10 3 483.53 465.50 90.83 o 12 10 3 1582.40 1544.37 136.27 o 14 10 3 2707.19 2544.09 147.65 o 1 11 3 6.67 102.17 79.47 o 3 11 3 725.62 522.29 68.13 o 5 11 3 1006.05 828.90 90.84 o 7 11 3 3421.70 3385.11 181.75 o 9 11 3 161.97 147.59 136.24 o 11 11 3 600.77 431.44 90.83 o 13 11 3 2279.55 2112.35 170.35 o 0 12 3 8609.92 9322.94 477.52 o 2 12 3 370.44 261.13 79.47 o 4 12 3 1917.57 1817.02 102.21 o 6 12 3 1993.90 2282.64 124.92 o 8 12 3 3541.69 3793.96 227.18 o 10 12 3 202.09 124.88 136.24 o 1 13 3 75.46 90.82 90.82 o 3 13 3 1471.82 1498.91 102.20 o 5 13 3 361.12 272.48 90.83 o 7 13 3 374.41 329.25 102.18 o 0 14 3 61.59 215.70 147.59 o 2 14 3 537.27 556.33 102.18 o 0 0 4 16906.52 15784.96 941.36 o 2 0 4 72762.70 73939.44 2523.49 o 4 0 4 4587.10 4483.31 170.68 o 6 0 4 3867.48 3763.68 136.45 o 8 0 4 769.56 772.18 68.13 o 10 0 4 39624.43 38376.93 918.38 o 12 0 4 8845.21 8658.15 295.81 o 14 0 4 3475.77 3476.54 193.14 o 16 0 4 1520.63 1328.66 147.63 o 18 0 4 3362.74 4146.20 261.27 o 20 0 4 1956.62 1680.74 454.25 o 22 0 4 146.85 -124.88 340.59 o 1 1 4 42089.52 42315.39 978.12 o 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