#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/29/2012965.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012965_Fobs loop_ _publ_author_name 'Poto\N,N^1^)(dicyanamido-\kN')copper(II) perchlorate and \m-dicyanamido-\k^2^N^1^:N^5^-bis[bis(2,2'-bipyridine-\k^2^N,N')copper(II)] triperchlorate ethanol hemisolvate, complexes with unusual dicyanamide coordination ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m523 _journal_page_last m528 _journal_volume 58 _journal_year 2002 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.7343 _cell_length_b 17.9450 _cell_length_c 28.7230 _exptl_crystal_F_000 2200.00 _reflns_d_resolution_high 0.7556 _[local]_cod_data_source_file bm1508Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' poto19b in Pbca IPDS 193 K mit numer. Absorptionskorr.' _shelx_refln_list_code 4 _shelx_f_calc_maximum 344.49 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 43606.57 45254.57 624.94 o 2 1 0 76.25 7.23 76.79 o 4 1 0 7331.02 6954.13 178.04 o 0 2 0 41333.02 38023.27 617.27 o 2 2 0 100840.70 110129.37 674.38 o 4 2 0 6281.67 6429.05 146.00 o 6 2 0 2986.58 2884.73 176.16 o 4 3 0 3249.59 3830.68 102.95 o 6 3 0 11791.46 12191.25 240.74 o 0 4 0 18806.78 18267.63 436.30 o 2 4 0 20197.44 19703.09 193.58 o 4 4 0 2818.83 2954.16 73.67 o 6 4 0 2072.21 1951.84 92.35 o 8 4 0 2479.34 2444.63 288.58 o 2 5 0 3545.14 3552.29 78.42 o 4 5 0 49739.73 50884.09 872.78 o 6 5 0 5908.40 6148.02 144.44 o 8 5 0 1224.03 1257.33 158.50 o 0 6 0 8482.06 6533.70 116.89 o 2 6 0 16122.32 15246.74 235.23 o 4 6 0 418.38 499.95 49.67 o 6 6 0 1670.47 1619.83 75.45 o 8 6 0 1834.41 1838.34 123.59 o 2 7 0 3.43 43.53 61.29 o 4 7 0 501.09 612.25 51.90 o 6 7 0 1751.68 1649.94 73.20 o 8 7 0 25.71 47.68 76.68 o 0 8 0 71596.13 74243.05 1032.54 o 2 8 0 19346.65 19113.20 241.45 o 4 8 0 22121.45 22175.74 272.05 o 6 8 0 1078.47 890.98 55.54 o 8 8 0 860.67 889.44 77.34 o 10 8 0 28.95 12.72 309.12 o 2 9 0 506.59 511.59 51.19 o 4 9 0 81.34 118.52 44.07 o 6 9 0 7.38 30.33 54.08 o 8 9 0 18.48 16.16 68.76 o 10 9 0 148.22 115.43 267.06 o 0 10 0 4366.07 4303.12 91.99 o 2 10 0 25050.22 25111.85 624.23 o 4 10 0 674.19 698.06 51.58 o 6 10 0 584.28 569.74 62.08 o 8 10 0 94.86 81.81 103.09 o 10 10 0 26.39 -29.60 162.10 o 2 11 0 2170.25 2060.62 60.82 o 4 11 0 2426.14 2302.01 61.19 o 6 11 0 3148.13 3354.92 74.86 o 8 11 0 472.69 616.92 107.94 o 10 11 0 308.74 373.69 252.39 o 0 12 0 7818.85 7858.87 233.80 o 2 12 0 1.64 8.19 47.18 o 4 12 0 22.89 47.59 44.40 o 6 12 0 1733.15 1841.11 68.35 o 8 12 0 205.22 162.62 80.65 o 2 13 0 4475.17 4160.04 78.51 o 4 13 0 336.81 336.02 57.26 o 6 13 0 2096.46 2174.74 61.08 o 8 13 0 1668.95 1726.51 96.68 o 0 14 0 2817.80 2738.89 78.13 o 2 14 0 179.56 166.47 49.63 o 4 14 0 429.40 523.35 57.46 o 6 14 0 42.40 13.51 58.68 o 8 14 0 8.39 41.00 86.21 o 2 15 0 4203.41 4475.30 76.89 o 4 15 0 81.47 102.56 51.51 o 6 15 0 1937.43 1924.66 72.65 o 8 15 0 133.56 121.32 123.12 o 0 16 0 3820.73 3806.92 114.45 o 2 16 0 2134.86 2241.66 88.95 o 4 16 0 2081.05 2247.91 82.16 o 6 16 0 382.95 336.84 66.78 o 8 16 0 613.11 541.11 89.83 o 2 17 0 45.33 114.62 57.62 o 4 17 0 215.37 158.45 51.26 o 6 17 0 73.77 47.82 64.86 o 8 17 0 3.68 165.32 169.24 o 0 18 0 4888.95 5162.31 98.22 o 2 18 0 3369.71 3660.90 216.88 o 4 18 0 974.82 1082.55 68.13 o 6 18 0 415.36 353.27 68.87 o 2 19 0 101.75 29.73 78.68 o 4 19 0 2472.96 2433.05 73.16 o 6 19 0 2.59 -44.68 84.41 o 0 20 0 7.37 18.07 116.90 o 2 20 0 1343.71 1183.85 71.37 o 4 20 0 90.17 46.56 70.02 o 6 20 0 69.53 55.82 83.66 o 2 21 0 394.81 336.58 68.27 o 4 21 0 267.79 250.67 80.20 o 0 22 0 207.18 100.27 106.53 o 2 22 0 1548.09 1537.05 75.47 o 4 22 0 257.77 140.50 137.11 o 2 23 0 1.90 119.25 97.70 o 1 1 1 37482.09 38354.19 272.87 o 2 1 1 14831.53 15663.24 165.12 o 3 1 1 3602.34 3132.97 84.64 o 4 1 1 2452.44 2339.91 87.85 o 5 1 1 6223.06 6403.14 150.37 o 6 1 1 3781.26 3790.03 163.99 o 0 2 1 46043.45 42315.02 556.03 o 1 2 1 2753.44 3204.10 68.58 o 2 2 1 5767.03 5858.90 87.76 o 3 2 1 4622.21 4590.40 77.02 o 4 2 1 3416.28 3564.16 85.96 o 5 2 1 2122.63 1918.77 81.72 o 6 2 1 2343.79 2405.20 102.99 o 7 2 1 1822.53 1764.43 160.70 o 1 3 1 2085.44 2114.93 55.07 o 2 3 1 4162.24 3990.46 64.15 o 3 3 1 163.60 179.17 36.00 o 4 3 1 2702.83 2769.61 60.71 o 5 3 1 2446.26 2411.00 68.91 o 6 3 1 294.56 250.87 64.85 o 7 3 1 134.55 125.80 92.21 o 0 4 1 36045.70 37142.27 790.99 o 1 4 1 27779.27 28854.42 158.18 o 2 4 1 28425.91 28245.79 157.56 o 3 4 1 17299.22 17070.16 127.68 o 4 4 1 2655.62 2142.68 51.67 o 5 4 1 1629.99 1687.17 56.93 o 6 4 1 4650.19 4692.54 81.99 o 7 4 1 410.03 431.64 65.45 o 8 4 1 78.67 96.85 183.91 o 1 5 1 35.97 42.34 32.66 o 2 5 1 0.78 10.47 30.50 o 3 5 1 218.79 283.00 36.82 o 4 5 1 227.40 212.17 38.87 o 5 5 1 2.22 7.04 42.18 o 6 5 1 207.94 244.15 47.46 o 7 5 1 117.47 127.19 58.15 o 8 5 1 342.22 378.56 97.73 o 9 5 1 26.31 18.05 232.74 o 0 6 1 183.01 215.65 44.52 o 1 6 1 11.30 -6.40 34.72 o 2 6 1 7164.88 6563.55 72.33 o 3 6 1 377.58 451.79 40.82 o 4 6 1 601.94 616.49 39.10 o 5 6 1 564.74 469.84 38.98 o 6 6 1 26.46 30.37 41.56 o 7 6 1 8.68 11.41 57.42 o 8 6 1 2481.59 2685.15 90.96 o 9 6 1 483.47 610.45 185.29 o 1 7 1 4308.63 4312.03 50.51 o 2 7 1 943.48 761.38 43.21 o 3 7 1 16589.22 16543.29 199.66 o 4 7 1 4464.09 4734.92 95.10 o 5 7 1 158.49 160.76 36.94 o 6 7 1 4015.42 4189.52 64.32 o 7 7 1 2613.12 2729.51 64.73 o 8 7 1 8.87 15.22 62.55 o 9 7 1 479.52 412.32 119.86 o 10 7 1 444.22 531.19 426.51 o 0 8 1 23553.77 23034.64 386.88 o 1 8 1 8489.52 8607.75 65.08 o 2 8 1 2183.84 2102.58 44.94 o 3 8 1 1763.81 1689.55 45.12 o 4 8 1 388.24 429.29 38.00 o 5 8 1 1372.29 1265.56 37.53 o 6 8 1 49.04 64.98 32.24 o 7 8 1 1284.19 1374.61 56.80 o 8 8 1 396.58 426.26 52.46 o 9 8 1 369.88 319.18 112.01 o 10 8 1 259.11 262.10 233.93 o 1 9 1 14929.48 14537.15 146.14 o 2 9 1 126.45 97.56 34.04 o 3 9 1 5499.93 5315.88 51.82 o 4 9 1 3400.26 3195.51 43.95 o 5 9 1 1043.73 1062.71 34.29 o 6 9 1 956.27 987.51 42.39 o 7 9 1 1280.85 1324.17 52.46 o 8 9 1 913.57 1008.38 51.34 o 9 9 1 249.84 259.50 78.25 o 10 9 1 334.09 427.29 172.00 o 0 10 1 5669.34 4803.56 66.64 o 1 10 1 241.27 287.64 40.51 o 2 10 1 1230.15 1276.56 42.81 o 3 10 1 470.02 483.82 43.07 o 4 10 1 2411.61 2490.09 40.33 o 5 10 1 80.92 89.92 30.98 o 6 10 1 41.41 45.47 36.28 o 7 10 1 14.05 27.44 40.72 o 8 10 1 29.77 70.89 67.29 o 9 10 1 98.14 108.24 67.49 o 10 10 1 162.75 103.56 119.17 o 1 11 1 130.37 164.70 33.58 o 2 11 1 3578.24 3409.13 44.40 o 3 11 1 5334.01 5134.82 51.31 o 4 11 1 450.11 443.01 33.57 o 5 11 1 1027.95 932.65 34.75 o 6 11 1 1248.08 1466.26 45.54 o 7 11 1 890.91 993.66 47.90 o 8 11 1 3.27 -9.09 63.41 o 9 11 1 57.38 50.53 80.58 o 10 11 1 4.12 20.74 155.63 o 0 12 1 4204.70 4390.20 100.25 o 1 12 1 4227.04 4115.64 45.46 o 2 12 1 8143.95 7675.69 134.17 o 3 12 1 1296.04 1312.87 40.11 o 4 12 1 89.45 120.06 32.82 o 5 12 1 81.09 82.26 36.44 o 6 12 1 1106.68 1193.78 44.47 o 7 12 1 1486.77 1506.20 45.72 o 8 12 1 335.07 350.78 55.80 o 9 12 1 13.14 30.66 92.68 o 1 13 1 313.75 316.49 36.36 o 2 13 1 137.23 140.37 33.00 o 3 13 1 5.77 40.14 33.10 o 4 13 1 833.22 854.63 46.34 o 5 13 1 21.34 61.57 36.64 o 6 13 1 408.35 379.89 40.16 o 7 13 1 162.62 183.95 51.62 o 8 13 1 27.24 16.43 51.65 o 9 13 1 31.66 39.15 71.68 o 0 14 1 6847.01 6169.58 72.15 o 1 14 1 0.17 41.14 32.36 o 2 14 1 320.21 328.13 36.90 o 3 14 1 41.72 63.68 42.20 o 4 14 1 1206.79 1252.58 49.09 o 5 14 1 271.71 288.95 38.58 o 6 14 1 441.66 426.95 39.61 o 7 14 1 7.03 6.08 48.19 o 8 14 1 5.73 1.33 61.21 o 9 14 1 143.12 129.08 74.39 o 1 15 1 2765.54 2621.18 48.25 o 2 15 1 1010.39 995.07 44.15 o 3 15 1 316.32 249.06 39.57 o 4 15 1 424.66 485.67 39.53 o 5 15 1 1413.14 1443.22 42.42 o 6 15 1 37.33 33.34 45.89 o 7 15 1 78.65 32.94 48.17 o 8 15 1 407.73 390.51 65.92 o 0 16 1 546.17 724.10 53.30 o 1 16 1 33.13 45.43 39.04 o 2 16 1 311.96 352.00 44.07 o 3 16 1 100.09 56.93 40.09 o 4 16 1 141.65 201.56 39.19 o 5 16 1 305.74 228.63 46.99 o 6 16 1 0.74 -18.97 43.85 o 7 16 1 144.21 137.53 61.94 o 8 16 1 25.97 10.21 58.67 o 1 17 1 1104.61 1154.44 42.09 o 2 17 1 239.23 260.74 40.30 o 3 17 1 1992.54 2177.95 44.90 o 4 17 1 109.35 66.62 38.51 o 5 17 1 146.99 101.41 46.15 o 6 17 1 588.41 506.81 47.04 o 7 17 1 12.11 -32.78 55.81 o 8 17 1 19.57 2.90 122.41 o 0 18 1 945.86 1110.06 81.19 o 1 18 1 87.99 48.17 42.98 o 2 18 1 480.53 516.99 40.29 o 3 18 1 0.63 10.04 49.36 o 4 18 1 34.09 79.90 43.55 o 5 18 1 51.93 23.98 40.35 o 6 18 1 186.91 162.82 64.78 o 7 18 1 1.76 -18.47 62.71 o 1 19 1 433.77 405.75 55.60 o 2 19 1 17.71 38.28 46.74 o 3 19 1 728.97 707.85 46.53 o 4 19 1 83.38 49.48 45.45 o 5 19 1 185.38 178.33 58.06 o 6 19 1 117.04 98.48 55.30 o 0 20 1 375.41 387.30 87.43 o 1 20 1 0.44 2.23 47.80 o 2 20 1 2257.13 2271.65 50.99 o 3 20 1 220.15 187.40 43.62 o 4 20 1 845.87 802.10 56.05 o 5 20 1 439.29 411.58 54.65 o 6 20 1 9.86 -13.94 57.49 o 1 21 1 6.35 -13.47 48.32 o 2 21 1 8.26 52.84 54.51 o 3 21 1 35.97 68.70 54.45 o 4 21 1 1.42 25.24 58.38 o 5 21 1 58.33 136.80 69.00 o 0 22 1 1396.82 1472.18 180.09 o 1 22 1 53.70 73.00 60.05 o 2 22 1 486.86 471.39 57.32 o 3 22 1 44.39 48.34 54.27 o 4 22 1 499.03 360.59 71.61 o 1 23 1 461.90 322.19 53.37 o 2 23 1 36.75 -59.42 63.28 o 1 0 2 68.43 24.03 77.05 o 2 0 2 4344.66 4464.23 187.42 o 3 0 2 10814.68 10921.53 235.04 o 4 0 2 796.98 735.49 121.56 o 5 0 2 997.09 827.67 93.16 o 6 0 2 0.12 0.04 85.06 o 7 0 2 145.31 159.14 148.88 o 1 1 2 28433.83 28003.49 222.41 o 2 1 2 3679.13 3775.55 95.36 o 3 1 2 2757.31 2434.78 77.58 o 4 1 2 2576.75 2626.50 91.18 o 5 1 2 11131.19 11209.63 143.56 o 6 1 2 60.35 85.14 70.85 o 7 1 2 360.38 409.38 118.75 o 0 2 2 11266.30 10953.62 192.53 o 1 2 2 28986.98 30427.55 239.37 o 2 2 2 98450.94 111191.21 865.54 o 3 2 2 309.27 249.48 39.55 o 4 2 2 1268.73 1471.71 65.98 o 5 2 2 4715.36 4713.82 100.12 o 6 2 2 1808.76 1857.83 97.62 o 7 2 2 4813.18 5071.95 136.87 o 1 3 2 27604.46 30617.83 290.01 o 2 3 2 1443.65 1365.31 46.22 o 3 3 2 13560.63 11415.02 186.89 o 4 3 2 193.26 222.27 48.16 o 5 3 2 343.52 416.36 52.43 o 6 3 2 1067.66 1126.19 68.00 o 7 3 2 8128.94 8437.09 154.40 o 8 3 2 22.03 12.60 154.57 o 0 4 2 55980.23 54555.40 770.79 o 1 4 2 22814.68 22219.98 197.86 o 2 4 2 32850.27 34691.64 323.76 o 3 4 2 26.48 37.14 31.21 o 4 4 2 54.15 58.47 39.29 o 5 4 2 35.56 49.24 45.40 o 6 4 2 10.90 -8.02 50.30 o 7 4 2 487.31 530.47 67.02 o 8 4 2 136.13 64.64 80.05 o 1 5 2 20806.11 19580.13 200.91 o 2 5 2 2034.67 1866.60 40.50 o 3 5 2 35973.07 38250.36 268.19 o 4 5 2 7073.05 7296.09 86.57 o 5 5 2 10656.92 10148.79 94.06 o 6 5 2 20.54 32.72 42.44 o 7 5 2 269.30 273.44 70.38 o 8 5 2 334.15 318.48 81.14 o 9 5 2 1581.72 1638.81 186.21 o 0 6 2 1664.22 1660.01 56.26 o 1 6 2 1149.61 1323.49 38.57 o 2 6 2 986.83 1044.00 35.88 o 3 6 2 2870.35 2886.34 47.52 o 4 6 2 5.72 0.18 39.62 o 5 6 2 2228.75 1905.91 48.57 o 6 6 2 25.66 47.68 37.69 o 7 6 2 146.43 169.15 58.86 o 8 6 2 2150.32 2309.77 96.00 o 9 6 2 1603.91 1812.88 186.35 o 1 7 2 5411.20 4687.15 53.13 o 2 7 2 8733.56 8998.73 146.69 o 3 7 2 8260.33 8000.33 73.01 o 4 7 2 2180.04 2425.99 46.56 o 5 7 2 3215.81 3367.84 50.04 o 6 7 2 0.31 19.68 36.46 o 7 7 2 572.86 612.68 54.05 o 8 7 2 137.27 107.44 61.00 o 9 7 2 561.99 622.14 99.34 o 10 7 2 39.40 51.85 306.19 o 0 8 2 1877.99 1986.39 66.99 o 1 8 2 8878.87 9709.72 87.80 o 2 8 2 1.42 5.04 35.77 o 3 8 2 148.35 76.32 32.30 o 4 8 2 352.86 320.15 34.22 o 5 8 2 7249.65 7558.73 97.63 o 6 8 2 1238.73 1209.89 43.79 o 7 8 2 38.01 26.39 53.87 o 8 8 2 3.19 8.37 61.55 o 9 8 2 1172.83 1223.38 88.58 o 10 8 2 51.67 64.19 198.18 o 1 9 2 2270.31 2182.12 43.70 o 2 9 2 872.04 977.59 36.17 o 3 9 2 375.67 354.44 34.29 o 4 9 2 224.24 213.89 37.62 o 5 9 2 45.30 65.82 32.86 o 6 9 2 328.07 386.32 46.20 o 7 9 2 148.44 156.98 49.86 o 8 9 2 0.00 -12.70 51.40 o 9 9 2 48.77 32.11 79.52 o 10 9 2 14.52 -5.84 161.59 o 0 10 2 2512.64 2968.65 61.45 o 1 10 2 1408.11 1222.41 40.86 o 2 10 2 347.60 407.16 36.75 o 3 10 2 393.45 365.25 33.90 o 4 10 2 352.43 307.72 33.48 o 5 10 2 314.19 329.75 34.77 o 6 10 2 19.50 8.07 40.84 o 7 10 2 1265.34 1407.02 46.31 o 8 10 2 119.96 108.74 63.95 o 9 10 2 343.73 391.70 72.01 o 10 10 2 17.42 13.72 117.87 o 1 11 2 1462.65 1278.62 36.44 o 2 11 2 53.20 34.93 35.86 o 3 11 2 8092.72 8080.45 87.93 o 4 11 2 1338.14 1306.12 37.89 o 5 11 2 350.75 361.02 36.41 o 6 11 2 29.56 32.83 37.29 o 7 11 2 1370.59 1320.99 46.80 o 8 11 2 0.98 4.05 59.15 o 9 11 2 179.52 171.04 89.03 o 10 11 2 0.50 -15.31 137.17 o 0 12 2 6153.01 6250.91 99.67 o 1 12 2 3457.36 3560.06 46.21 o 2 12 2 410.51 419.03 34.07 o 3 12 2 952.73 1054.20 35.36 o 4 12 2 162.49 162.92 31.55 o 5 12 2 117.59 100.90 36.91 o 6 12 2 49.82 71.19 43.09 o 7 12 2 8.06 33.21 40.72 o 8 12 2 124.03 105.02 51.68 o 9 12 2 399.94 337.28 85.57 o 1 13 2 8294.37 8133.60 74.27 o 2 13 2 940.39 942.62 40.09 o 3 13 2 679.92 708.11 36.07 o 4 13 2 32.44 15.92 40.40 o 5 13 2 3812.83 3965.10 94.99 o 6 13 2 19.24 5.80 35.66 o 7 13 2 480.67 602.64 49.10 o 8 13 2 0.75 -2.49 53.66 o 9 13 2 28.01 3.88 68.75 o 0 14 2 636.80 613.19 46.83 o 1 14 2 127.01 114.96 34.04 o 2 14 2 128.09 145.47 36.04 o 3 14 2 101.15 163.40 39.65 o 4 14 2 20.11 13.70 41.69 o 5 14 2 224.28 221.04 36.37 o 6 14 2 398.06 377.13 37.85 o 7 14 2 37.50 37.64 46.70 o 8 14 2 10.43 -16.51 70.87 o 9 14 2 134.66 107.26 69.48 o 1 15 2 901.00 868.57 35.47 o 2 15 2 237.45 268.71 45.48 o 3 15 2 1139.88 1283.16 43.64 o 4 15 2 88.56 99.20 41.69 o 5 15 2 4.75 34.54 35.80 o 6 15 2 8.48 -2.09 44.31 o 7 15 2 509.51 360.97 46.39 o 8 15 2 30.15 24.04 75.40 o 0 16 2 233.36 251.55 60.75 o 1 16 2 2811.29 2991.46 48.84 o 2 16 2 79.94 74.69 43.78 o 3 16 2 14.76 13.52 35.53 o 4 16 2 92.53 81.21 40.20 o 5 16 2 521.30 541.49 45.88 o 6 16 2 40.94 41.18 45.75 o 7 16 2 1108.20 1185.08 57.24 o 8 16 2 38.76 48.97 60.53 o 1 17 2 127.69 131.55 43.31 o 2 17 2 695.24 682.25 40.59 o 3 17 2 62.11 80.38 37.92 o 4 17 2 422.37 393.61 37.68 o 5 17 2 20.38 28.61 41.32 o 6 17 2 190.03 196.39 44.76 o 7 17 2 73.71 5.70 54.22 o 8 17 2 46.52 37.17 165.32 o 0 18 2 26.58 -3.93 53.72 o 1 18 2 41.25 23.40 38.04 o 2 18 2 122.87 131.19 36.49 o 3 18 2 851.96 908.90 45.52 o 4 18 2 58.22 95.68 46.05 o 5 18 2 320.27 266.40 48.47 o 6 18 2 53.64 32.84 47.24 o 7 18 2 157.50 122.94 60.67 o 1 19 2 2019.74 2047.13 51.70 o 2 19 2 20.13 2.47 50.66 o 3 19 2 282.04 246.46 44.32 o 4 19 2 58.40 46.51 44.94 o 5 19 2 717.29 615.23 52.05 o 6 19 2 0.06 39.32 46.37 o 0 20 2 1202.13 1166.75 65.53 o 1 20 2 18.46 -0.22 44.78 o 2 20 2 0.17 1.03 50.67 o 3 20 2 0.99 19.50 58.18 o 4 20 2 49.00 54.07 52.56 o 5 20 2 109.88 77.43 49.24 o 6 20 2 56.37 107.15 63.59 o 1 21 2 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49.87 o 4 2 29 610.81 699.41 52.06 o 5 2 29 1.32 -54.40 54.40 o 6 2 29 143.30 115.51 68.34 o 7 2 29 25.84 9.89 62.55 o 1 3 29 360.01 324.97 46.05 o 2 3 29 86.88 99.48 41.69 o 3 3 29 8.41 42.10 59.37 o 4 3 29 256.57 214.29 54.74 o 5 3 29 779.51 695.63 54.08 o 6 3 29 130.84 179.68 57.72 o 7 3 29 42.12 42.11 67.47 o 0 4 29 6336.78 6518.40 144.59 o 1 4 29 34.91 11.14 43.03 o 2 4 29 7064.18 7009.79 107.30 o 3 4 29 156.86 80.49 48.57 o 4 4 29 2078.82 2102.13 64.10 o 5 4 29 160.54 137.77 47.33 o 6 4 29 195.07 180.90 64.05 o 7 4 29 12.49 23.90 73.90 o 1 5 29 39.06 0.27 43.67 o 2 5 29 159.25 115.08 54.74 o 3 5 29 31.55 7.70 50.11 o 4 5 29 391.10 399.25 53.22 o 5 5 29 11.50 4.45 51.57 o 6 5 29 77.22 93.77 64.28 o 7 5 29 23.41 79.38 103.50 o 0 6 29 999.26 904.72 111.40 o 1 6 29 24.70 16.12 56.51 o 2 6 29 5096.45 5658.53 70.20 o 3 6 29 9.44 0.66 45.42 o 4 6 29 1430.02 1449.13 60.27 o 5 6 29 105.10 107.13 56.74 o 6 6 29 12.37 71.52 56.96 o 1 7 29 106.55 98.98 45.56 o 2 7 29 320.60 308.41 50.92 o 3 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736.54 733.01 52.03 o 2 3 31 14.05 66.15 46.38 o 3 3 31 354.63 276.30 51.36 o 4 3 31 197.18 152.59 48.58 o 5 3 31 412.84 368.95 69.18 o 6 3 31 78.21 57.74 59.70 o 0 4 31 600.94 643.40 77.99 o 1 4 31 268.83 279.25 54.33 o 2 4 31 25.88 51.82 58.85 o 3 4 31 616.10 666.71 54.96 o 4 4 31 303.26 323.76 62.96 o 5 4 31 1057.71 1126.34 61.19 o 6 4 31 0.91 48.01 67.73 o 1 5 31 701.13 617.33 53.66 o 2 5 31 0.04 42.88 50.90 o 3 5 31 117.09 82.35 49.93 o 4 5 31 3.61 -29.77 57.66 o 5 5 31 183.06 181.00 58.17 o 6 5 31 65.43 25.80 68.75 o 0 6 31 133.18 -4.91 83.89 o 1 6 31 424.73 399.28 52.99 o 2 6 31 310.26 212.88 54.12 o 3 6 31 5.25 -4.42 44.12 o 4 6 31 13.96 6.09 61.88 o 5 6 31 129.70 130.50 67.02 o 6 6 31 38.68 -47.93 130.02 o 1 7 31 2179.73 2296.47 58.80 o 2 7 31 95.65 75.27 46.48 o 3 7 31 1523.68 1565.09 61.46 o 4 7 31 29.46 58.05 59.70 o 5 7 31 209.22 166.63 57.54 o 0 8 31 0.78 -38.95 58.87 o 1 8 31 9.40 30.12 42.47 o 2 8 31 2.67 49.67 48.65 o 3 8 31 11.52 13.34 57.78 o 4 8 31 51.96 37.45 51.15 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49.20 o 2 4 33 1448.15 1439.71 62.87 o 3 4 33 2.11 51.46 63.41 o 4 4 33 1817.50 1646.27 62.54 o 5 4 33 114.17 114.31 68.60 o 1 5 33 231.98 222.98 51.88 o 2 5 33 40.18 27.36 70.24 o 3 5 33 365.31 477.50 71.01 o 4 5 33 222.63 184.23 60.57 o 5 5 33 112.74 105.86 63.97 o 0 6 33 882.47 1046.32 97.35 o 1 6 33 3.97 45.53 61.14 o 2 6 33 2767.58 2879.41 100.06 o 3 6 33 99.79 97.68 54.28 o 4 6 33 825.01 824.02 64.43 o 1 7 33 184.65 158.27 64.75 o 2 7 33 18.70 -50.23 62.45 o 3 7 33 208.94 125.37 56.96 o 4 7 33 9.25 20.49 62.28 o 0 8 33 110.77 104.94 74.14 o 1 8 33 0.18 72.22 52.06 o 2 8 33 9.16 -9.33 54.34 o 3 8 33 85.56 73.87 59.04 o 4 8 33 1.65 7.41 71.29 o 1 9 33 209.74 219.79 62.32 o 2 9 33 97.07 8.17 56.22 o 3 9 33 3.23 68.40 61.67 o 0 10 33 1600.19 1521.50 80.86 o 1 10 33 10.43 -36.33 54.25 o 2 10 33 12.13 -66.43 66.43 o 1 11 33 88.91 144.42 69.56 o 0 0 34 917.85 794.38 98.20 o 1 0 34 19.29 49.10 75.48 o 2 0 34 1000.51 879.21 113.47 o 3 0 34 1691.67 1809.06 97.37 o 4 0 34 270.28 286.24 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35 1481.48 1393.99 192.71 o 0 0 36 480.95 464.07 157.37 o 1 0 36 9.28 61.13 89.88 o 2 0 36 442.27 411.08 79.85 o 3 0 36 103.30 -60.57 97.79 o 1 1 36 51.82 114.39 63.96 o 2 1 36 0.40 3.69 57.07 o 3 1 36 45.89 123.21 67.07 o 0 2 36 91.55 266.64 89.72 o 1 2 36 277.81 235.01 62.67 o 2 2 36 913.54 614.81 66.33 o 3 2 36 4.09 11.02 70.82 o 1 3 36 340.76 334.43 62.24 o 2 3 36 66.69 63.74 66.94 o 3 3 36 603.41 634.91 82.86 o 0 4 36 0.39 -75.47 111.00 o 1 4 36 4.44 -17.23 64.19 o 2 4 36 57.46 34.56 70.08 o 3 4 36 15.68 -18.24 80.90 o 1 5 36 908.69 884.39 61.66 o 2 5 36 39.45 104.21 73.95 o 0 6 36 712.47 513.81 99.66 o 1 6 36 74.87 152.18 68.30 o 2 6 36 623.40 440.63 92.66 o 1 7 36 643.53 500.69 76.83 o 1 1 37 337.23 272.08 67.64 o 2 1 37 19.74 24.12 80.95 o 0 2 37 588.76 599.82 94.60 o 1 2 37 5.86 -54.41 68.13 o 2 2 37 435.71 285.81 75.64 o 1 3 37 128.14 212.45 70.47 o 2 3 37 1.26 68.73 110.15 o 0 4 37 955.49 701.45 98.60 o 1 4 37 116.15 161.63 70.40 o