#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2012977.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012977_Fobs loop_ _publ_author_name 'Sun, Cui Rong' 'Jin, Zhi Min' _publ_section_title ; The 2:1 complex of maleic acid and 1,4-diazabicyclo[2.2.2]octane: hydrogen-bonded sheets linked by C--H···O hydrogen bonds ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o600 _journal_page_last o601 _journal_volume 58 _journal_year 2002 _space_group_IT_number 36 _symmetry_space_group_name_Hall 'C 2c -2' _symmetry_space_group_name_H-M 'C m c 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.7584 _cell_length_b 20.1447 _cell_length_c 11.2549 _exptl_crystal_F_000 728.00 _reflns_d_resolution_high 0.7570 _[local]_cod_data_source_file gd1226Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Y1198 in Cmc2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 343.63 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' 'x, -y, z+1/2' '-x, y, z' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z+1/2' 'x+1/2, -y+1/2, z+1/2' '-x+1/2, y+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 118079.95 133793.63 1017.75 o 4 0 0 25693.23 25118.24 96.99 o 6 0 0 5899.94 5622.23 56.87 o 8 0 0 277.62 262.41 18.78 o 1 1 0 31.35 39.77 2.23 o 3 1 0 323.26 365.45 9.86 o 5 1 0 40.31 23.66 7.59 o 7 1 0 0.78 -0.45 8.48 o 0 2 0 320.38 266.05 3.64 o 2 2 0 7219.57 6997.19 33.62 o 4 2 0 568.88 539.81 13.92 o 6 2 0 2.12 2.23 8.03 o 8 2 0 82.41 68.76 12.06 o 1 3 0 7918.55 7558.53 29.44 o 3 3 0 0.04 3.12 4.02 o 5 3 0 603.55 623.23 17.50 o 7 3 0 17.21 12.50 9.37 o 0 4 0 3567.67 3841.00 19.34 o 2 4 0 3412.44 3593.88 25.10 o 4 4 0 725.33 686.29 15.74 o 6 4 0 104.03 111.66 10.72 o 8 4 0 43.35 48.21 11.16 o 1 5 0 26.74 16.52 3.57 o 3 5 0 1113.60 1202.83 17.66 o 5 5 0 38.37 44.64 8.48 o 7 5 0 15.81 11.60 8.93 o 0 6 0 958.66 992.73 11.85 o 2 6 0 2280.83 2334.33 21.71 o 4 6 0 403.00 445.41 13.44 o 6 6 0 23.85 16.52 8.48 o 8 6 0 28.01 33.92 10.27 o 1 7 0 126.08 116.29 5.37 o 3 7 0 364.61 358.11 10.76 o 5 7 0 0.40 -1.34 6.25 o 7 7 0 17.35 22.32 8.93 o 0 8 0 2968.84 3026.55 24.32 o 2 8 0 619.67 624.09 12.60 o 4 8 0 212.74 215.54 10.73 o 6 8 0 79.81 87.52 10.27 o 8 8 0 0.19 -3.12 10.71 o 1 9 0 179.48 170.01 7.16 o 3 9 0 243.16 228.19 9.84 o 5 9 0 46.83 50.45 8.48 o 7 9 0 11.20 10.27 8.93 o 0 10 0 2747.75 2969.57 26.82 o 2 10 0 1489.94 1559.50 21.79 o 4 10 0 257.48 255.40 12.08 o 6 10 0 20.21 25.44 8.03 o 8 10 0 1.94 -10.26 10.26 o 1 11 0 3694.65 3930.90 33.50 o 3 11 0 2094.62 2170.04 28.67 o 5 11 0 336.50 340.92 15.21 o 7 11 0 38.76 30.80 11.16 o 0 12 0 2461.71 2416.24 27.05 o 2 12 0 1277.62 1260.60 21.24 o 4 12 0 319.14 337.37 13.87 o 6 12 0 37.98 34.37 9.37 o 1 13 0 216.76 217.37 9.84 o 3 13 0 20.71 28.12 7.14 o 5 13 0 0.47 -1.79 7.59 o 7 13 0 1.34 4.91 9.82 o 0 14 0 356.60 361.39 12.54 o 2 14 0 507.09 497.17 15.24 o 4 14 0 230.41 251.24 13.41 o 6 14 0 12.26 8.93 8.93 o 1 15 0 2479.39 2463.02 31.92 o 3 15 0 741.47 741.56 19.30 o 5 15 0 405.49 440.33 18.35 o 7 15 0 62.93 64.29 12.50 o 0 16 0 2218.51 2168.29 31.37 o 2 16 0 539.90 575.51 17.48 o 4 16 0 222.28 229.30 14.30 o 6 16 0 260.06 263.27 17.88 o 1 17 0 76.43 72.34 8.93 o 3 17 0 96.11 93.78 10.27 o 5 17 0 23.10 26.78 9.82 o 0 18 0 46.51 49.11 8.04 o 2 18 0 91.85 92.44 9.82 o 4 18 0 11.67 12.94 8.93 o 6 18 0 27.64 29.46 11.16 o 1 19 0 606.38 627.53 19.72 o 3 19 0 75.78 63.85 9.82 o 5 19 0 222.77 230.14 16.98 o 0 20 0 155.53 146.99 11.62 o 2 20 0 289.49 298.25 15.65 o 4 20 0 83.73 71.00 12.06 o 1 21 0 3.13 4.46 7.59 o 3 21 0 161.97 156.36 13.40 o 5 21 0 2.61 7.59 10.26 o 0 22 0 2.16 -0.45 8.03 o 2 22 0 14.71 13.39 8.93 o 4 22 0 7.12 14.73 9.82 o 1 23 0 129.28 121.93 12.51 o 3 23 0 15.86 14.73 9.82 o 0 24 0 610.35 663.82 24.19 o 2 24 0 239.92 244.46 16.98 o 1 25 0 5.57 -0.89 9.82 o 3 25 0 0.09 -4.46 9.37 o 0 26 0 5.90 11.60 9.82 o 1 1 1 1998.86 1800.05 8.78 o 3 1 1 1279.85 1303.82 13.41 o 5 1 1 169.19 167.16 7.74 o 7 1 1 0.83 3.43 5.52 o 0 2 1 499.95 619.79 4.52 o 2 2 1 8151.10 7798.73 32.16 o 4 2 1 947.57 970.35 12.75 o 6 2 1 16.05 17.54 6.10 o 8 2 1 77.35 83.94 12.50 o 1 3 1 12722.89 11891.12 34.04 o 3 3 1 1803.67 1816.45 14.71 o 5 3 1 783.89 791.20 13.66 o 7 3 1 94.50 93.00 7.89 o 0 4 1 3927.64 3807.82 17.36 o 2 4 1 1464.86 1377.16 11.01 o 4 4 1 86.77 87.10 5.37 o 6 4 1 120.64 110.17 7.56 o 8 4 1 21.44 26.78 10.71 o 1 5 1 163.37 169.39 4.12 o 3 5 1 476.67 490.46 8.53 o 5 5 1 4.94 9.06 4.88 o 7 5 1 1.00 -0.48 5.83 o 0 6 1 514.43 429.80 7.44 o 2 6 1 559.76 601.79 7.96 o 4 6 1 39.36 48.49 4.74 o 6 6 1 21.59 17.39 5.46 o 8 6 1 28.13 25.00 10.71 o 1 7 1 2318.80 2349.88 14.75 o 3 7 1 1809.95 1857.26 16.43 o 5 7 1 47.93 44.90 5.83 o 7 7 1 21.37 23.66 9.37 o 0 8 1 95.63 89.78 7.38 o 2 8 1 378.98 356.62 7.13 o 4 8 1 49.66 47.26 5.02 o 6 8 1 7.43 5.28 5.34 o 8 8 1 14.54 11.60 11.16 o 1 9 1 1634.66 1691.73 20.30 o 3 9 1 199.56 188.67 6.48 o 5 9 1 114.41 117.62 11.61 o 7 9 1 0.24 0.00 7.59 o 0 10 1 2234.77 2322.21 37.42 o 2 10 1 541.58 552.39 12.80 o 4 10 1 186.22 184.09 7.74 o 6 10 1 74.29 90.31 12.50 o 8 10 1 5.93 9.82 10.26 o 1 11 1 132.57 141.69 5.59 o 3 11 1 289.21 312.61 8.95 o 5 11 1 8.44 13.61 5.36 o 7 11 1 3.07 7.59 8.93 o 0 12 1 198.74 186.16 6.16 o 2 12 1 208.92 221.82 7.27 o 4 12 1 36.45 34.16 5.37 o 6 12 1 13.60 17.69 5.97 o 1 13 1 183.43 203.67 6.64 o 3 13 1 312.33 309.67 9.18 o 5 13 1 8.74 8.06 5.97 o 7 13 1 10.61 12.05 9.37 o 0 14 1 1439.99 1469.22 16.63 o 2 14 1 1387.45 1388.12 17.09 o 4 14 1 427.97 419.25 19.92 o 6 14 1 49.17 53.12 11.61 o 1 15 1 536.57 509.76 12.11 o 3 15 1 5.09 7.50 5.02 o 5 15 1 85.31 97.23 15.41 o 7 15 1 13.99 9.82 9.82 o 0 16 1 77.37 75.12 5.84 o 2 16 1 41.53 38.27 5.68 o 4 16 1 34.59 32.55 6.46 o 6 16 1 26.84 34.82 11.61 o 1 17 1 1699.88 1618.19 32.79 o 3 17 1 1685.02 1638.25 23.04 o 5 17 1 228.59 208.71 15.64 o 0 18 1 252.36 241.84 9.32 o 2 18 1 506.59 496.98 15.01 o 4 18 1 303.88 284.37 11.22 o 6 18 1 40.89 55.35 10.71 o 1 19 1 256.26 234.98 9.48 o 3 19 1 182.46 190.79 9.15 o 5 19 1 96.87 79.48 12.50 o 0 20 1 155.10 175.72 8.51 o 2 20 1 163.12 155.21 9.00 o 4 20 1 60.68 68.31 12.05 o 1 21 1 55.52 45.52 7.10 o 3 21 1 36.89 37.50 9.82 o 5 21 1 13.42 10.27 10.71 o 0 22 1 202.58 211.37 14.30 o 2 22 1 24.39 32.58 9.82 o 4 22 1 24.43 28.57 10.71 o 1 23 1 62.84 75.00 11.61 o 3 23 1 19.09 21.87 10.27 o 0 24 1 133.40 127.29 13.40 o 2 24 1 22.93 11.60 10.71 o 1 25 1 11.98 8.93 10.71 o 3 25 1 23.01 21.42 11.16 o 0 26 1 136.77 132.65 15.63 o 0 0 2 2996.05 3153.31 16.76 o 2 0 2 8873.19 8710.05 39.74 o 4 0 2 1131.51 1129.25 19.42 o 6 0 2 84.18 82.61 10.27 o 8 0 2 78.42 78.14 12.50 o 1 1 2 6057.65 5638.54 26.30 o 3 1 2 1315.05 1237.00 17.26 o 5 1 2 455.99 451.67 15.23 o 7 1 2 75.63 62.06 10.72 o 0 2 2 9579.82 8880.17 31.76 o 2 2 2 2456.67 2328.98 20.03 o 4 2 2 483.63 519.00 13.91 o 6 2 2 276.04 283.08 14.31 o 8 2 2 6.65 8.48 9.82 o 1 3 2 970.08 1003.31 11.41 o 3 3 2 963.81 966.22 15.82 o 5 3 2 107.54 100.95 9.38 o 7 3 2 13.68 16.51 8.48 o 0 4 2 6919.61 7007.54 30.99 o 2 4 2 6779.56 6608.14 36.54 o 4 4 2 1398.28 1418.66 22.63 o 6 4 2 158.09 152.36 12.06 o 8 4 2 35.95 26.78 10.71 o 1 5 2 1882.83 1959.91 18.03 o 3 5 2 39.09 43.31 5.36 o 5 5 2 243.50 232.54 12.52 o 7 5 2 10.35 4.46 8.48 o 0 6 2 12346.99 12036.83 47.57 o 2 6 2 2307.44 2073.79 21.66 o 4 6 2 815.49 804.74 17.99 o 6 6 2 321.23 313.12 15.66 o 8 6 2 19.38 12.50 10.71 o 1 7 2 5544.09 5810.68 34.83 o 3 7 2 2306.42 2258.45 26.09 o 5 7 2 203.89 192.67 11.62 o 7 7 2 32.99 32.14 9.37 o 0 8 2 1381.13 1486.82 17.77 o 2 8 2 278.56 266.91 9.40 o 4 8 2 101.59 100.06 8.49 o 6 8 2 34.01 29.02 8.48 o 8 8 2 6.55 1.79 10.71 o 1 9 2 3007.43 3348.13 28.74 o 3 9 2 703.90 750.64 16.63 o 5 9 2 430.68 421.35 16.12 o 7 9 2 57.09 50.45 11.16 o 0 10 2 1053.44 1055.32 16.73 o 2 10 2 358.13 390.69 11.65 o 4 10 2 99.09 109.43 9.38 o 6 10 2 47.80 53.12 8.93 o 8 10 2 14.08 8.48 10.71 o 1 11 2 1637.28 1706.33 22.72 o 3 11 2 560.95 573.31 15.70 o 5 11 2 134.37 133.57 11.17 o 7 11 2 30.68 25.44 10.27 o 0 12 2 449.78 457.40 12.56 o 2 12 2 769.53 703.65 16.64 o 4 12 2 226.48 214.15 12.07 o 6 12 2 10.82 15.62 8.48 o 1 13 2 297.75 281.98 11.64 o 3 13 2 366.18 339.33 13.43 o 5 13 2 31.63 29.46 8.93 o 7 13 2 8.58 7.59 10.26 o 0 14 2 1207.50 1171.60 21.66 o 2 14 2 276.42 246.49 12.08 o 4 14 2 125.25 121.95 11.17 o 6 14 2 69.47 72.78 11.61 o 1 15 2 43.89 42.41 7.59 o 3 15 2 13.73 10.27 7.59 o 5 15 2 24.64 16.52 8.93 o 7 15 2 2.01 8.48 10.71 o 0 16 2 120.36 114.81 9.38 o 2 16 2 385.87 390.79 14.77 o 4 16 2 157.01 142.07 12.06 o 6 16 2 0.81 -8.93 8.93 o 1 17 2 494.05 476.68 17.02 o 3 17 2 138.96 150.99 11.61 o 5 17 2 131.11 146.95 13.85 o 0 18 2 890.66 882.37 22.46 o 2 18 2 228.87 262.85 14.30 o 4 18 2 107.84 97.36 12.06 o 6 18 2 76.73 81.26 13.39 o 1 19 2 392.35 394.27 16.56 o 3 19 2 47.80 43.75 10.27 o 5 19 2 82.22 84.39 12.50 o 0 20 2 10.36 8.48 7.59 o 2 20 2 61.85 45.09 9.38 o 4 20 2 15.16 13.39 8.93 o 1 21 2 90.98 98.69 11.16 o 3 21 2 7.07 -4.91 8.03 o 5 21 2 34.68 28.12 11.61 o 0 22 2 25.58 46.87 9.82 o 2 22 2 3.65 10.26 8.03 o 4 22 2 0.03 4.02 8.48 o 1 23 2 11.35 12.05 8.93 o 3 23 2 33.90 39.28 10.27 o 0 24 2 104.32 107.62 12.95 o 2 24 2 22.74 17.41 10.27 o 1 25 2 44.69 60.26 12.05 o 0 26 2 17.39 17.41 11.16 o 1 1 3 1816.85 1841.05 16.21 o 3 1 3 700.20 754.61 14.41 o 5 1 3 268.89 264.36 12.52 o 7 1 3 40.28 32.59 9.37 o 0 2 3 1888.64 1722.90 15.35 o 2 2 3 193.51 190.70 6.71 o 4 2 3 108.31 100.97 8.49 o 6 2 3 69.17 58.94 9.38 o 8 2 3 3.53 -5.36 9.82 o 1 3 3 1234.97 1094.98 13.25 o 3 3 3 241.80 260.95 9.40 o 5 3 3 88.07 87.09 8.93 o 7 3 3 16.64 11.60 9.82 o 0 4 3 438.98 449.68 9.00 o 2 4 3 158.92 165.51 6.71 o 4 4 3 16.72 23.66 6.25 o 6 4 3 20.11 25.89 8.48 o 8 4 3 10.01 10.27 10.27 o 1 5 3 3879.69 4046.29 27.51 o 3 5 3 202.31 204.87 8.50 o 5 5 3 363.02 367.05 15.22 o 7 5 3 46.81 40.62 10.27 o 0 6 3 4828.23 4815.89 30.75 o 2 6 3 849.32 897.17 14.89 o 4 6 3 222.13 220.92 10.73 o 6 6 3 155.31 142.07 12.51 o 8 6 3 28.62 16.52 11.61 o 1 7 3 2619.88 2690.00 24.52 o 3 7 3 718.97 750.11 15.74 o 5 7 3 134.06 115.26 10.28 o 7 7 3 38.18 32.59 10.27 o 0 8 3 11.65 11.61 4.02 o 2 8 3 1532.11 1475.07 20.44 o 4 8 3 180.32 186.84 10.73 o 6 8 3 41.74 43.75 8.93 o 8 8 3 26.38 32.58 11.16 o 1 9 3 52.83 44.66 4.91 o 3 9 3 81.19 84.86 7.59 o 5 9 3 17.25 9.37 7.59 o 7 9 3 16.84 24.10 9.37 o 0 10 3 1516.84 1600.13 21.35 o 2 10 3 169.27 147.53 8.49 o 4 10 3 49.23 50.45 8.48 o 6 10 3 56.98 52.68 9.38 o 8 10 3 14.52 12.94 11.60 o 1 11 3 1.75 1.34 4.91 o 3 11 3 331.03 320.49 12.53 o 5 11 3 12.36 17.41 8.03 o 7 11 3 8.45 12.50 9.82 o 0 12 3 767.40 820.40 17.09 o 2 12 3 660.02 688.38 16.61 o 4 12 3 335.77 354.82 15.21 o 6 12 3 81.03 75.91 12.06 o 1 13 3 274.83 252.80 11.19 o 3 13 3 155.68 157.29 10.72 o 5 13 3 81.24 91.09 10.72 o 7 13 3 1.70 -1.79 10.26 o 0 14 3 2054.30 2096.70 28.63 o 2 14 3 781.86 798.28 19.77 o 4 14 3 350.31 360.62 15.21 o 6 14 3 205.18 188.12 15.64 o 1 15 3 66.22 59.39 8.04 o 3 15 3 84.35 69.22 9.38 o 5 15 3 19.49 21.87 9.82 o 7 15 3 3.69 8.48 10.26 o 0 16 3 10.44 17.41 7.14 o 2 16 3 41.86 41.96 8.48 o 4 16 3 2.28 -5.80 8.93 o 6 16 3 18.80 24.99 10.27 o 1 17 3 1406.15 1314.39 26.61 o 3 17 3 1028.09 1011.81 25.17 o 5 17 3 170.50 184.95 14.30 o 0 18 3 1864.26 1759.37 32.12 o 2 18 3 877.63 823.11 22.90 o 4 18 3 404.98 418.35 18.79 o 6 18 3 175.00 181.82 16.98 o 1 19 3 262.06 270.50 14.75 o 3 19 3 52.94 45.54 9.38 o 5 19 3 50.13 54.46 11.61 o 0 20 3 255.86 221.29 14.31 o 2 20 3 46.00 48.66 8.93 o 4 20 3 13.45 18.75 9.37 o 1 21 3 165.10 202.38 13.40 o 3 21 3 60.03 62.06 11.16 o 5 21 3 30.62 28.57 11.61 o 0 22 3 7.25 2.68 8.48 o 2 22 3 61.58 77.24 11.16 o 4 22 3 19.31 12.05 10.71 o 1 23 3 61.41 54.02 10.71 o 3 23 3 25.13 18.75 10.71 o 0 24 3 79.35 70.99 12.95 o 2 24 3 10.82 5.80 9.82 o 1 25 3 6.08 10.71 10.71 o 0 26 3 37.29 44.19 11.61 o 0 0 4 1172.51 1199.32 14.13 o 2 0 4 776.00 698.90 13.08 o 4 0 4 107.83 117.94 8.49 o 6 0 4 11.76 6.69 8.03 o 8 0 4 14.53 10.71 9.82 o 1 1 4 387.10 406.97 8.98 o 3 1 4 389.54 397.64 11.21 o 5 1 4 69.08 75.46 8.93 o 7 1 4 48.22 36.61 9.82 o 0 2 4 766.96 791.58 12.21 o 2 2 4 800.04 858.71 14.44 o 4 2 4 120.25 128.23 8.94 o 6 2 4 26.06 22.32 8.03 o 8 2 4 10.07 10.71 9.82 o 1 3 4 9755.50 9516.67 44.97 o 3 3 4 4104.95 4032.57 34.99 o 5 3 4 520.93 523.92 17.03 o 7 3 4 91.21 111.64 12.06 o 0 4 4 10619.35 10744.25 48.10 o 2 4 4 1355.29 1317.53 18.17 o 4 4 4 482.21 487.74 15.24 o 6 4 4 211.89 209.17 13.41 o 8 4 4 14.81 13.39 10.27 o 1 5 4 1921.09 2019.09 21.09 o 3 5 4 842.88 902.87 17.11 o 5 5 4 65.25 48.67 8.04 o 7 5 4 32.17 37.94 9.37 o 0 6 4 899.72 932.40 14.46 o 2 6 4 818.63 832.84 15.32 o 4 6 4 125.02 117.95 8.94 o 6 6 4 8.49 5.36 7.14 o 8 6 4 20.73 24.10 11.16 o 1 7 4 3839.39 3978.36 31.80 o 3 7 4 3351.78 3227.55 33.66 o 5 7 4 168.84 153.72 11.17 o 7 7 4 15.18 11.16 8.93 o 0 8 4 896.65 985.04 16.24 o 2 8 4 227.60 238.46 9.40 o 4 8 4 87.00 108.08 8.49 o 6 8 4 42.15 41.96 9.82 o 8 8 4 9.85 12.05 10.71 o 1 9 4 901.04 915.12 16.68 o 3 9 4 377.80 378.88 12.99 o 5 9 4 200.23 197.99 12.96 o 7 9 4 7.12 3.57 8.03 o 0 10 4 1281.75 1302.26 20.36 o 2 10 4 1658.48 1576.05 24.04 o 4 10 4 419.06 388.23 15.22 o 6 10 4 31.80 32.59 9.37 o 1 11 4 90.38 84.42 7.15 o 3 11 4 151.83 171.15 10.28 o 5 11 4 8.18 6.25 8.03 o 7 11 4 17.84 13.39 10.27 o 0 12 4 190.65 186.44 9.84 o 2 12 4 446.39 468.22 14.79 o 4 12 4 122.59 114.35 10.72 o 6 12 4 23.47 30.35 9.82 o 1 13 4 72.48 94.23 8.04 o 3 13 4 37.83 33.48 7.14 o 5 13 4 18.74 22.32 8.03 o 7 13 4 2.97 -4.46 8.93 o 0 14 4 426.86 413.44 14.33 o 2 14 4 1244.16 1175.22 24.34 o 4 14 4 361.50 384.34 16.11 o 6 14 4 24.42 20.53 10.27 o 1 15 4 782.14 787.74 19.76 o 3 15 4 583.45 553.97 18.82 o 5 15 4 161.33 174.23 14.30 o 0 16 4 208.61 212.78 12.52 o 2 16 4 24.52 23.66 8.03 o 4 16 4 9.82 17.41 8.93 o 6 16 4 23.92 23.21 10.71 o 1 17 4 81.40 85.74 9.82 o 3 17 4 33.71 31.25 9.37 o 5 17 4 45.75 38.84 11.16 o 0 18 4 369.32 335.60 15.21 o 2 18 4 379.89 377.65 17.00 o 4 18 4 143.24 165.27 12.95 o 6 18 4 36.75 42.85 12.05 o 1 19 4 407.73 413.07 17.90 o 3 19 4 228.10 266.37 15.64 o 5 19 4 148.72 167.95 15.63 o 0 20 4 44.21 43.75 8.48 o 2 20 4 50.08 45.54 10.27 o 4 20 4 29.10 24.55 9.37 o 1 21 4 63.28 65.18 10.72 o 3 21 4 9.94 8.48 8.93 o 0 22 4 31.55 33.48 10.27 o 2 22 4 59.18 63.39 11.61 o 4 22 4 35.33 31.69 11.61 o 1 23 4 122.87 120.58 12.95 o 3 23 4 141.14 131.31 14.74 o 0 24 4 0.06 0.45 8.93 o 2 24 4 4.59 4.91 8.03 o 1 25 4 35.12 35.26 11.16 o 1 1 5 50.25 34.39 4.91 o 3 1 5 14.58 18.75 5.80 o 5 1 5 7.76 4.46 7.14 o 7 1 5 3.12 8.48 8.48 o 0 2 5 3399.26 3554.46 28.07 o 2 2 5 1045.98 1097.79 17.17 o 4 2 5 353.52 376.52 13.43 o 6 2 5 96.19 109.86 11.16 o 8 2 5 7.32 8.48 10.71 o 1 3 5 561.00 584.08 12.14 o 3 3 5 64.36 61.63 6.70 o 5 3 5 60.37 67.87 9.38 o 7 3 5 3.65 4.46 8.93 o 0 4 5 171.80 178.03 7.16 o 2 4 5 37.79 37.50 5.36 o 4 4 5 20.94 22.32 7.14 o 6 4 5 8.11 0.89 7.59 o 8 4 5 0.34 -0.45 8.93 o 1 5 5 666.09 747.87 14.40 o 3 5 5 31.14 38.39 6.25 o 5 5 5 165.90 145.23 10.72 o 7 5 5 13.20 4.46 8.93 o 0 6 5 1692.91 1737.48 21.41 o 2 6 5 75.65 68.78 6.70 o 4 6 5 28.55 25.89 7.59 o 6 6 5 53.44 53.13 9.38 o 8 6 5 8.11 16.96 10.26 o 1 7 5 2216.52 2238.68 25.62 o 3 7 5 230.69 249.12 11.18 o 5 7 5 198.50 196.21 12.51 o 7 7 5 11.99 15.62 8.93 o 0 8 5 2015.11 1972.72 24.64 o 2 8 5 172.70 167.65 8.94 o 4 8 5 57.01 52.24 8.48 o 6 8 5 142.68 140.71 12.95 o 1 9 5 815.95 846.96 17.10 o 3 9 5 205.40 175.26 10.73 o 5 9 5 52.61 47.77 8.93 o 7 9 5 7.59 16.51 8.93 o 0 10 5 1839.19 1787.86 25.00 o 2 10 5 50.53 62.51 7.59 o 4 10 5 64.09 41.97 8.93 o 6 10 5 102.89 115.22 12.50 o 1 11 5 214.41 232.53 10.73 o 3 11 5 657.40 664.94 18.40 o 5 11 5 11.65 12.05 8.03 o 7 11 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32.95 o 2 4 8 1278.03 1260.89 23.91 o 4 4 8 584.75 579.95 19.27 o 6 4 8 227.68 232.84 16.54 o 1 5 8 73.56 76.81 7.59 o 3 5 8 89.82 83.51 9.38 o 5 5 8 37.96 33.03 9.82 o 7 5 8 1.14 8.48 11.16 o 0 6 8 1003.36 966.57 20.71 o 2 6 8 851.12 812.52 19.77 o 4 6 8 300.57 321.56 14.76 o 6 6 8 84.39 106.27 12.50 o 1 7 8 192.54 166.73 10.73 o 3 7 8 501.73 497.25 17.47 o 5 7 8 16.73 12.05 8.03 o 7 7 8 21.09 8.48 11.16 o 0 8 8 16.32 20.98 7.59 o 2 8 8 54.49 60.72 8.04 o 4 8 8 21.83 22.76 8.48 o 6 8 8 4.09 -8.48 8.48 o 1 9 8 314.95 306.92 13.87 o 3 9 8 367.48 392.43 15.66 o 5 9 8 26.42 23.21 9.37 o 0 10 8 46.19 36.61 7.59 o 2 10 8 198.59 185.04 11.17 o 4 10 8 99.41 108.52 10.72 o 6 10 8 21.69 20.53 10.27 o 1 11 8 202.77 181.02 12.07 o 3 11 8 85.32 96.90 10.27 o 5 11 8 46.35 54.46 10.71 o 0 12 8 1706.15 1681.10 30.73 o 2 12 8 677.58 679.37 21.08 o 4 12 8 309.31 343.42 16.99 o 6 12 8 110.17 104.50 14.74 o 1 13 8 193.71 213.62 12.96 o 3 13 8 13.15 8.48 8.03 o 5 13 8 20.79 21.42 10.71 o 0 14 8 270.35 294.65 14.76 o 2 14 8 197.18 196.18 13.85 o 4 14 8 54.40 65.18 11.61 o 1 15 8 255.00 216.82 13.41 o 3 15 8 43.41 37.94 9.82 o 5 15 8 57.49 46.43 12.05 o 0 16 8 264.81 235.60 15.20 o 2 16 8 129.82 129.98 12.51 o 4 16 8 37.26 37.05 11.61 o 1 17 8 35.20 33.03 9.82 o 3 17 8 22.50 20.09 8.93 o 0 18 8 9.94 17.85 7.59 o 2 18 8 132.64 138.46 13.40 o 4 18 8 39.63 59.37 12.05 o 1 19 8 64.02 65.63 11.16 o 3 19 8 40.03 41.96 11.16 o 0 20 8 21.53 26.78 9.82 o 2 20 8 70.61 84.38 12.50 o 1 21 8 21.75 28.57 9.82 o 0 22 8 50.64 53.57 12.05 o 1 1 9 91.11 91.11 8.93 o 3 1 9 268.23 258.47 13.42 o 5 1 9 34.95 34.37 10.27 o 7 1 9 1.16 10.71 9.82 o 0 2 9 158.85 140.77 10.28 o 2 2 9 6.22 21.42 7.14 o 4 2 9 3.18 -0.45 8.48 o 6 2 9 20.90 23.66 9.82 o 1 3 9 743.62 685.18 17.96 o 3 3 9 281.27 279.51 13.86 o 5 3 9 159.95 166.63 13.40 o 7 3 9 25.17 29.01 12.05 o 0 4 9 117.15 100.96 8.93 o 2 4 9 611.64 604.46 18.38 o 4 4 9 195.39 219.42 13.85 o 6 4 9 4.81 3.57 10.71 o 1 5 9 1160.96 1122.01 23.42 o 3 5 9 708.31 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20.60 o 5 7 10 95.60 98.24 13.40 o 0 8 10 164.94 146.55 11.17 o 2 8 10 168.82 146.55 12.06 o 4 8 10 54.84 44.20 11.16 o 6 8 10 9.45 4.46 12.05 o 1 9 10 44.54 54.02 8.93 o 3 9 10 43.09 63.84 9.82 o 5 9 10 6.58 17.85 11.16 o 0 10 10 357.53 354.77 16.11 o 2 10 10 257.42 246.32 15.20 o 4 10 10 99.32 96.90 12.50 o 1 11 10 8.87 7.59 8.03 o 3 11 10 10.44 12.50 8.03 o 5 11 10 4.23 7.59 9.82 o 0 12 10 1.89 7.14 7.14 o 2 12 10 9.55 7.59 8.48 o 4 12 10 14.20 15.17 8.93 o 1 13 10 129.87 121.49 12.06 o 3 13 10 7.09 13.39 8.93 o 0 14 10 21.85 29.46 8.93 o 2 14 10 7.36 1.79 8.93 o 4 14 10 7.07 8.93 10.26 o 1 15 10 43.86 61.60 10.27 o 3 15 10 83.34 71.44 12.50 o 0 16 10 12.52 11.60 8.93 o 2 16 10 164.46 154.56 14.29 o 1 17 10 25.43 26.78 11.61 o 3 17 10 31.23 34.37 11.16 o 0 18 10 74.73 72.33 12.50 o 2 18 10 4.35 4.02 10.26 o 1 19 10 115.04 131.29 16.08 o 1 1 11 102.40 126.39 11.17 o 3 1 11 58.25 56.70 11.16 o 5 1 11 73.14 84.83 12.50 o 0 2 11 308.20 325.60 15.21 o 2 2 11 94.00 92.44 11.16 o 4 2 11 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14 12 73.26 74.11 13.39 o 2 14 12 76.13 90.19 13.39 o 1 15 12 47.18 49.10 12.95 o 1 1 13 74.36 82.60 11.16 o 3 1 13 1.04 2.23 8.93 o 0 2 13 128.08 113.44 12.95 o 2 2 13 37.80 23.66 9.82 o 4 2 13 18.65 29.90 11.16 o 1 3 13 49.68 45.09 9.82 o 3 3 13 19.89 22.32 9.82 o 0 4 13 267.58 267.31 16.54 o 2 4 13 103.12 101.37 12.50 o 4 4 13 71.67 87.06 13.39 o 1 5 13 8.46 4.46 9.37 o 3 5 13 3.98 -0.89 9.82 o 0 6 13 30.91 33.48 9.37 o 2 6 13 2.33 4.46 9.82 o 1 7 13 69.26 52.24 12.50 o 3 7 13 10.17 12.94 10.27 o 0 8 13 221.06 214.49 15.64 o 2 8 13 86.44 62.51 11.61 o 1 9 13 64.86 58.48 12.05 o 3 9 13 37.25 34.37 11.16 o 0 10 13 144.37 182.23 16.53 o 2 10 13 45.05 59.37 12.05 o 1 11 13 181.24 195.67 16.98 o 0 12 13 21.19 26.33 10.27 o 0 0 14 122.94 140.68 14.29 o 1 1 14 66.57 84.83 12.50 o 0 2 14 43.23 49.10 11.16 o 2 2 14 30.31 48.65 12.05 o 1 3 14 24.78 42.85 10.27 o 0 4 14 124.50 119.24 14.29 o 2 4 14 30.51 41.51 11.61 o 1 5 14 65.23 56.25 11.61 o 0 6 14 95.27 83.50 12.50 o 2 6 14 86.54 104.93 12.95 o 1 7 14 13.03 20.53 12.05 o 0 8 14 168.43 201.02 16.53 o