#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2013007.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013007_Fobs loop_ _publ_author_name 'Chantrapromma, Suchada' 'Usman, Anwar' 'Fun, Hoong-Kun' _publ_section_title ; A ternary complex of aqua(18-crown-6)bis(o-nitrophenolato)barium(II), the triaqua(18-crown-6)(o-nitrophenolato)barium(II) cation and the o-nitrophenolate anion ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m531 _journal_page_last m533 _journal_volume 58 _journal_year 2002 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 97.936 _cell_angle_beta 109.755 _cell_angle_gamma 108.864 _cell_length_a 13.7492 _cell_length_b 14.9672 _cell_length_c 16.8669 _exptl_crystal_F_000 1448.00 _reflns_d_resolution_high 0.7504 _[local]_cod_data_source_file av1117Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title 'av1117r in P-1 (R.T.)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 364.02 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 22022.09 20358.28 2922.07 o 4 0 0 64342.46 66162.23 9479.84 o 5 0 0 19927.03 19152.11 2752.54 o 6 0 0 13383.72 15915.14 1610.55 o 7 0 0 15007.25 15753.15 1591.27 o 8 0 0 3640.75 3682.16 382.24 o 9 0 0 761.00 1016.81 117.02 o 10 0 0 665.28 633.17 119.08 o 11 0 0 47.71 56.35 48.00 o 15 0 0 43.13 69.18 69.40 o -16 1 0 992.90 1219.52 250.40 o -15 1 0 763.52 931.57 200.92 o -14 1 0 1240.24 1723.88 313.21 o -13 1 0 1237.38 1662.15 301.08 o -12 1 0 187.13 119.63 57.07 o -11 1 0 107.93 167.92 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28317.67 2856.84 o -5 2 0 23026.19 21736.41 2191.56 o -4 2 0 25978.34 24358.73 2062.90 o -3 2 0 16313.28 17476.44 1476.31 o -2 2 0 38883.39 39973.54 6222.13 o 0 2 0 26748.96 29508.11 2968.09 o 1 2 0 15732.84 18416.38 2646.99 o 2 2 0 4420.86 3899.64 567.80 o 3 2 0 3464.15 2989.33 439.48 o 4 2 0 1543.91 1208.97 185.76 o 5 2 0 1023.93 434.40 76.21 o 6 2 0 75.29 40.99 21.35 o 7 2 0 651.39 601.16 103.02 o 8 2 0 22.58 27.17 27.75 o 9 2 0 3.13 -5.98 31.08 o 10 2 0 319.87 302.72 81.33 o 11 2 0 4.29 34.98 48.58 o 14 2 0 69.78 116.57 80.68 o -16 3 0 0.64 -8.02 63.53 o -15 3 0 3.12 33.89 56.80 o -14 3 0 64.36 96.92 67.61 o -12 3 0 1275.20 1086.72 204.34 o -11 3 0 5712.99 6690.06 1069.94 o -10 3 0 1193.62 1365.75 160.08 o -9 3 0 16.61 8.18 12.01 o -8 3 0 1439.78 1289.72 117.56 o -7 3 0 248.16 214.42 26.91 o -6 3 0 2854.07 2845.70 247.05 o -5 3 0 885.58 1079.06 97.69 o -4 3 0 1563.52 1367.69 120.83 o -3 3 0 2974.05 3387.57 298.10 o -2 3 0 612.64 413.80 141.52 o -1 3 0 5183.88 2645.49 1748.22 o 0 3 0 11175.94 12391.36 1784.15 o 1 3 0 5562.78 4289.46 624.77 o 2 3 0 11530.18 13100.41 1889.57 o 3 3 0 32310.18 39166.99 5619.54 o 4 3 0 37578.05 52030.44 7462.25 o 5 3 0 25027.04 32010.26 4597.74 o 6 3 0 5490.81 5782.20 844.26 o 7 3 0 13862.76 8259.24 1201.50 o 8 3 0 11800.65 3518.45 522.48 o 9 3 0 10805.57 11012.06 1596.68 o 10 3 0 9316.74 10954.74 1582.16 o 11 3 0 1890.49 3145.27 481.36 o 12 3 0 1614.60 2613.48 414.25 o -16 4 0 51.08 19.63 51.99 o -15 4 0 376.45 415.37 121.51 o -14 4 0 718.15 715.20 154.78 o -13 4 0 1677.01 1689.61 302.02 o -12 4 0 2546.77 3332.96 553.11 o -11 4 0 3203.07 3576.00 586.76 o -10 4 0 5069.78 5436.24 872.42 o -9 4 0 6031.05 6928.65 591.48 o -8 4 0 4398.17 5231.64 449.77 o -7 4 0 9273.57 8997.74 766.05 o -6 4 0 12184.02 14137.44 1201.11 o -5 4 0 9830.86 10770.14 915.39 o -4 4 0 58236.46 63978.59 5403.40 o -3 4 0 35285.04 27475.56 2324.05 o -2 4 0 125520.21 122864.87 10383.23 o -1 4 0 99971.28 92146.03 9214.99 o 0 4 0 65456.11 63580.50 9114.71 o 1 4 0 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18500.09 16470.50 2377.00 o 5 5 0 9326.72 8409.92 1224.52 o 6 5 0 11136.59 10545.03 1533.06 o 7 5 0 5607.78 4836.19 717.61 o 8 5 0 1094.92 1159.67 196.62 o 9 5 0 1094.92 1738.20 280.30 o 10 5 0 2698.33 3688.49 561.99 o 11 5 0 786.92 1157.67 213.71 o 12 5 0 193.44 177.39 83.78 o -17 6 0 101.04 55.69 66.69 o -16 6 0 55.08 83.86 77.07 o -15 6 0 166.40 153.35 74.61 o -14 6 0 326.48 267.86 87.70 o -13 6 0 781.22 864.69 172.75 o -12 6 0 104.03 179.97 67.80 o -11 6 0 12.73 -4.04 34.10 o -10 6 0 325.00 338.95 85.09 o -9 6 0 1.67 30.71 22.73 o -8 6 0 3015.37 3242.72 282.53 o -7 6 0 106.54 148.24 22.30 o -6 6 0 631.13 734.60 87.19 o -5 6 0 255.86 294.44 39.83 o -4 6 0 4054.97 3315.09 550.31 o -3 6 0 18087.15 18618.65 1578.21 o -2 6 0 8169.89 4668.54 2266.17 o -1 6 0 10505.28 9934.59 1007.29 o 0 6 0 758.40 697.05 114.87 o 1 6 0 2063.58 1598.68 245.45 o 2 6 0 484.18 551.48 97.87 o 3 6 0 319.37 428.52 83.67 o 4 6 0 171.27 216.55 55.66 o 5 6 0 2.55 -6.88 23.53 o 6 6 0 381.32 445.89 91.30 o 7 6 0 710.46 605.04 118.25 o 8 6 0 4875.00 4691.28 702.99 o 9 6 0 3610.46 4912.54 739.18 o 10 6 0 1418.96 2479.06 401.99 o 12 6 0 2284.81 3259.68 518.14 o -17 7 0 628.27 649.99 159.22 o -16 7 0 852.92 990.97 204.03 o -15 7 0 1499.45 1451.65 269.40 o -14 7 0 792.25 898.62 181.22 o -13 7 0 76.41 16.85 42.29 o -12 7 0 14.68 17.36 42.37 o -11 7 0 214.42 304.61 79.63 o -10 7 0 25.18 28.37 41.30 o -9 7 0 96.89 113.99 50.07 o -8 7 0 978.34 875.82 82.46 o -7 7 0 6373.13 6612.24 854.43 o -6 7 0 2791.61 2953.37 256.73 o -5 7 0 5940.63 5583.91 525.02 o -4 7 0 862.37 820.37 77.13 o -3 7 0 10437.56 10315.00 874.42 o -2 7 0 3429.20 2915.18 253.77 o -1 7 0 12928.36 14090.65 2031.47 o 0 7 0 12715.06 15508.62 2237.05 o 1 7 0 2848.43 2896.33 433.62 o 2 7 0 531.44 448.10 84.89 o 3 7 0 390.80 589.37 109.92 o 4 7 0 4405.85 5645.69 830.76 o 5 7 0 829.41 941.78 165.47 o 6 7 0 186.06 249.00 76.48 o 7 7 0 156.26 197.33 69.97 o 8 7 0 447.70 419.02 95.63 o 9 7 0 57.76 97.80 68.01 o 10 7 0 108.82 56.79 71.00 o -15 8 0 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0 265.88 206.64 75.71 o -12 13 0 513.42 380.34 98.98 o -11 13 0 804.37 707.46 142.29 o -10 13 0 1290.42 1191.17 216.17 o -9 13 0 2390.02 2038.31 341.68 o -8 13 0 3870.72 3838.53 421.80 o -7 13 0 3142.17 3028.16 287.58 o -6 13 0 2245.14 2257.94 202.59 o -5 13 0 3028.45 1902.25 792.99 o -4 13 0 6029.14 5834.85 857.93 o -3 13 0 3001.20 3418.21 518.10 o -2 13 0 1516.08 1336.94 216.10 o -1 13 0 1283.32 1189.15 196.50 o 0 13 0 905.99 1168.59 203.56 o 1 13 0 1160.46 1179.72 200.74 o 2 13 0 670.08 637.06 131.06 o 3 13 0 32.99 31.44 47.02 o 4 13 0 91.89 52.26 50.89 o 5 13 0 52.89 65.83 59.31 o 6 13 0 15.10 24.66 56.73 o 7 13 0 390.36 378.97 114.10 o -15 14 0 673.74 580.26 134.52 o -14 14 0 1085.36 1193.08 228.88 o -13 14 0 1044.93 960.79 186.00 o -12 14 0 416.72 359.16 98.28 o -11 14 0 98.03 48.11 51.30 o -10 14 0 30.18 27.06 41.01 o -9 14 0 6.21 6.78 36.29 o -8 14 0 84.66 24.59 22.52 o -7 14 0 249.38 227.87 45.38 o -6 14 0 362.58 251.64 57.37 o -5 14 0 92.06 88.34 41.60 o -4 14 0 69.73 72.17 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