#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:41:11 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180799 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/30/2013014.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013014_Fobs loop_ _publ_author_name 'Malathy Sony, S. M.' 'Kuppayee, M.' 'Ponnuswamy, M. N.' 'Bhasker Reddy, D.' 'Padmavathi, V.' 'Fun, Hoong-Kun' _publ_section_title ; 9,9-Dimethoxy-7,11-diphenyl-2,4-diazaspiro[5.5]undecane-1,3,5-trione monohydrate ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o678 _journal_page_last o680 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 114.100 _cell_angle_gamma 90.000 _cell_length_a 14.5590 _cell_length_b 10.7550 _cell_length_c 15.3460 _exptl_crystal_F_000 896.00 _reflns_d_resolution_high 0.7697 _cod_data_source_file de1191Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' MNP3 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 151.96 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 19003.93 17474.31 205.10 o 3 0 0 56.67 156.98 28.16 o 4 0 0 5320.03 4890.82 189.70 o 5 0 0 5534.93 5621.28 215.29 o 6 0 0 5778.74 5769.34 232.47 o 7 0 0 3661.27 3063.36 184.13 o 8 0 0 2378.00 2207.68 145.15 o 9 0 0 3.24 7.36 47.42 o 10 0 0 218.34 192.86 54.74 o 11 0 0 35.67 39.95 57.04 o 12 0 0 52.14 11.99 56.52 o 13 0 0 6.08 -38.25 57.63 o 14 0 0 5.47 -20.35 62.03 o 15 0 0 4.01 3.73 65.82 o 1 1 0 23090.40 21722.37 332.68 o 2 1 0 90.88 128.91 17.51 o 3 1 0 3101.34 3120.87 105.65 o 4 1 0 2978.41 3008.41 94.79 o 5 1 0 54.32 25.07 22.14 o 6 1 0 4.86 10.34 23.93 o 7 1 0 4575.07 4416.85 143.60 o 8 1 0 14.22 19.92 29.75 o 9 1 0 16.17 33.47 34.13 o 10 1 0 2.02 -20.67 37.79 o 11 1 0 15.98 72.32 40.29 o 12 1 0 7.22 -4.22 40.31 o 13 1 0 55.12 16.37 42.60 o 14 1 0 55.46 65.91 44.30 o 15 1 0 0.17 -5.00 45.97 o 0 2 0 1078.79 791.60 29.87 o 1 2 0 209.94 189.15 22.05 o 2 2 0 15.33 149.96 34.68 o 3 2 0 7067.48 6476.13 221.88 o 5 2 0 13.99 11.65 34.12 o 6 2 0 303.38 344.83 38.34 o 7 2 0 148.23 166.76 41.07 o 8 2 0 1127.13 1137.97 54.53 o 9 2 0 8.52 -12.13 50.67 o 11 2 0 36.44 11.11 59.55 o 12 2 0 8.49 -29.90 58.44 o 13 2 0 59.45 65.19 60.29 o 14 2 0 70.37 112.54 63.90 o 15 2 0 27.99 79.76 70.29 o 1 3 0 10210.69 10423.04 302.39 o 2 3 0 1236.83 1121.74 53.65 o 3 3 0 201.19 190.20 40.92 o 4 3 0 396.59 367.30 39.99 o 5 3 0 35.67 99.83 39.07 o 6 3 0 93.30 75.42 40.31 o 7 3 0 607.19 590.76 46.95 o 8 3 0 20.38 37.26 50.06 o 9 3 0 43.48 74.52 54.87 o 10 3 0 72.88 95.07 60.13 o 11 3 0 22.20 -17.12 61.60 o 12 3 0 0.21 65.39 60.56 o 13 3 0 1.79 -28.29 63.86 o 14 3 0 37.07 34.30 65.58 o 15 3 0 2.68 9.30 69.84 o 0 4 0 2.86 -22.85 38.23 o 1 4 0 452.07 476.14 28.41 o 2 4 0 837.74 898.23 42.20 o 3 4 0 4529.66 4628.73 223.57 o 4 4 0 14.54 75.31 42.45 o 5 4 0 268.65 402.39 45.91 o 6 4 0 135.61 195.12 46.81 o 7 4 0 450.25 483.10 53.63 o 8 4 0 107.98 144.61 57.31 o 9 4 0 217.91 162.45 60.79 o 10 4 0 384.82 348.47 64.42 o 11 4 0 146.28 112.88 62.96 o 12 4 0 1.52 -13.46 62.30 o 13 4 0 25.74 66.23 67.97 o 14 4 0 6.32 -28.93 67.11 o 15 4 0 1.73 -6.35 72.62 o 1 5 0 1217.74 1353.66 44.85 o 2 5 0 418.24 403.59 42.90 o 3 5 0 2925.39 3254.72 146.87 o 4 5 0 220.28 163.78 48.53 o 5 5 0 265.48 215.76 51.19 o 6 5 0 268.83 378.62 55.78 o 7 5 0 2.15 30.51 58.42 o 8 5 0 84.50 53.58 62.73 o 9 5 0 207.95 218.95 65.08 o 10 5 0 95.38 12.10 63.57 o 11 5 0 55.49 119.50 65.58 o 12 5 0 4.90 4.61 64.94 o 13 5 0 0.70 -43.54 66.66 o 14 5 0 2.58 59.86 69.44 o 15 5 0 12.35 66.32 74.04 o 0 6 0 225.55 170.64 47.37 o 1 6 0 22.20 -9.51 32.48 o 2 6 0 120.11 92.54 48.73 o 3 6 0 373.22 287.55 52.00 o 4 6 0 459.54 538.31 56.61 o 5 6 0 9.05 33.69 58.08 o 6 6 0 182.98 156.98 62.84 o 7 6 0 140.05 97.21 68.62 o 8 6 0 166.64 138.72 70.32 o 9 6 0 184.68 134.52 70.23 o 10 6 0 52.84 5.33 66.03 o 11 6 0 0.06 -24.61 68.24 o 12 6 0 10.17 64.92 68.74 o 13 6 0 0.43 -24.95 71.29 o 14 6 0 1.83 -16.19 74.77 o 15 6 0 0.01 12.28 81.65 o 1 7 0 46.89 12.51 37.98 o 2 7 0 130.48 155.27 55.91 o 3 7 0 188.39 201.33 60.49 o 4 7 0 297.50 219.06 63.79 o 5 7 0 14.84 73.16 66.03 o 6 7 0 35.84 79.94 68.99 o 7 7 0 84.98 98.57 69.50 o 8 7 0 14.69 37.98 70.43 o 9 7 0 57.49 -54.51 70.86 o 10 7 0 87.27 191.85 70.20 o 11 7 0 18.09 -2.82 74.54 o 12 7 0 3.19 -31.23 72.39 o 13 7 0 8.40 -15.02 77.09 o 14 7 0 4.76 -23.80 80.91 o 0 8 0 230.27 195.26 62.87 o 1 8 0 49.59 40.18 45.11 o 2 8 0 11.91 -30.10 63.93 o 3 8 0 6.92 6.80 67.16 o 4 8 0 392.67 406.10 69.69 o 5 8 0 0.48 43.65 69.23 o 6 8 0 17.90 -8.45 70.72 o 7 8 0 24.03 -24.93 69.75 o 8 8 0 18.11 38.23 71.18 o 9 8 0 60.57 139.05 74.40 o 10 8 0 5.83 69.98 74.13 o 11 8 0 3.05 -38.79 77.32 o 12 8 0 5.24 37.69 80.84 o 13 8 0 39.91 2.33 82.35 o 14 8 0 10.30 -17.55 88.95 o 1 9 0 877.15 833.81 67.04 o 2 9 0 60.51 78.15 68.22 o 3 9 0 4.26 -21.54 70.23 o 4 9 0 35.39 -40.08 69.73 o 5 9 0 0.59 -55.32 70.63 o 6 9 0 4.12 19.33 70.97 o 7 9 0 163.84 181.98 72.71 o 8 9 0 17.71 42.34 75.10 o 9 9 0 40.97 -11.90 78.85 o 10 9 0 7.49 -24.97 77.68 o 11 9 0 0.20 -49.25 83.44 o 12 9 0 1.06 -38.82 87.82 o 13 9 0 0.02 -1.60 89.56 o 0 10 0 136.68 80.37 68.29 o 1 10 0 2.11 -5.69 48.24 o 2 10 0 258.09 245.23 69.89 o 3 10 0 15.25 45.95 68.83 o 4 10 0 72.88 25.45 70.54 o 5 10 0 40.54 55.84 73.00 o 6 10 0 34.29 0.52 74.65 o 7 10 0 17.17 -29.69 75.87 o 8 10 0 17.18 -4.43 78.24 o 9 10 0 33.00 59.18 81.07 o 10 10 0 2.49 40.98 85.76 o 11 10 0 7.16 37.26 87.59 o 12 10 0 0.15 29.69 90.50 o 1 11 0 4.35 -1.86 50.60 o 2 11 0 77.38 60.52 72.46 o 3 11 0 0.43 13.30 74.20 o 4 11 0 29.14 9.05 75.92 o 5 11 0 37.32 4.47 76.41 o 6 11 0 78.83 30.60 77.02 o 7 11 0 53.65 -16.33 79.96 o 8 11 0 42.47 38.84 82.69 o 9 11 0 2.63 -60.97 83.37 o 10 11 0 10.52 22.51 88.29 o 0 12 0 0.88 16.87 73.25 o 1 12 0 22.55 11.71 53.48 o 2 12 0 79.89 1.69 74.02 o 3 12 0 5.27 -12.83 76.50 o 4 12 0 0.01 -74.38 80.73 o 5 12 0 0.58 -80.34 80.34 o 6 12 0 115.74 63.84 85.88 o 7 12 0 24.86 -22.60 86.28 o 8 12 0 2.78 -1.72 88.65 o 1 13 0 6.72 -26.69 58.82 o 2 13 0 18.42 -4.47 85.02 o 3 13 0 2.50 32.40 86.82 o 4 13 0 8.34 1.22 85.24 o 5 13 0 11.90 27.30 87.10 o -15 1 1 0.01 27.13 46.25 o -14 1 1 36.81 16.96 42.33 o -13 1 1 46.75 33.32 41.99 o -12 1 1 3.80 -22.73 40.65 o -11 1 1 1.38 41.32 40.98 o -10 1 1 2.61 -21.29 40.71 o -9 1 1 253.70 262.85 33.71 o -8 1 1 338.36 289.74 30.56 o -7 1 1 8.74 21.20 25.78 o -6 1 1 22.26 16.54 26.43 o -5 1 1 730.68 720.41 27.90 o -4 1 1 111.24 140.70 33.98 o -3 1 1 10161.82 10510.83 152.28 o -2 1 1 9592.03 7676.02 114.29 o -1 1 1 56.68 103.71 8.86 o 0 1 1 910.93 1172.98 27.55 o 1 1 1 30.68 -6.87 11.95 o 2 1 1 1054.08 986.19 30.52 o 3 1 1 775.21 1102.52 52.79 o 4 1 1 1313.25 1730.32 60.63 o 5 1 1 2.16 6.27 22.85 o 6 1 1 39.14 43.09 25.32 o 7 1 1 136.54 134.85 27.97 o 8 1 1 375.02 430.56 33.58 o 9 1 1 1.59 27.04 35.18 o 10 1 1 58.88 63.12 38.93 o 11 1 1 135.35 125.78 40.73 o 12 1 1 4.31 20.89 41.99 o 13 1 1 2.54 29.67 42.06 o 14 1 1 0.20 -21.96 43.69 o 15 1 1 18.87 13.18 47.87 o -15 2 1 1.62 -56.63 64.54 o -14 2 1 1.97 46.27 63.11 o -13 2 1 7.27 5.26 59.82 o -12 2 1 138.61 124.35 60.00 o -11 2 1 58.36 84.16 60.47 o -10 2 1 37.43 18.49 54.96 o -9 2 1 0.00 11.49 49.09 o -8 2 1 175.33 152.15 44.51 o -7 2 1 6.76 2.71 38.68 o -6 2 1 1185.14 1165.41 63.81 o -5 2 1 841.82 864.70 61.13 o -4 2 1 92.06 58.30 35.97 o -3 2 1 5657.75 4928.63 203.48 o -2 2 1 2336.67 3202.17 138.67 o -1 2 1 618.34 667.83 22.83 o 0 2 1 16956.25 16078.81 529.68 o 1 2 1 4370.56 4416.20 281.74 o 3 2 1 1279.84 1078.45 53.22 o 4 2 1 1235.57 1205.67 51.42 o 5 2 1 12.77 -3.39 35.23 o 6 2 1 368.55 318.17 39.90 o 7 2 1 142.01 122.91 42.59 o 8 2 1 31.39 16.46 47.42 o 9 2 1 15.37 36.81 52.30 o 11 2 1 73.00 98.97 59.07 o 12 2 1 26.68 53.58 60.38 o 13 2 1 4.60 -3.18 62.68 o 14 2 1 2.23 -5.01 64.85 o 15 2 1 4.17 26.01 69.64 o -15 3 1 5.45 -28.90 66.77 o -14 3 1 1.30 -14.11 63.70 o -13 3 1 10.50 13.41 61.47 o -12 3 1 83.48 54.49 60.00 o -11 3 1 16.31 36.11 60.88 o -10 3 1 3.82 12.56 58.35 o -9 3 1 19.12 -9.60 52.61 o -8 3 1 65.49 65.58 46.99 o -7 3 1 147.67 181.08 42.88 o -6 3 1 629.26 576.40 42.75 o -5 3 1 1.51 -26.22 38.59 o -4 3 1 20.71 -31.46 38.82 o -1 3 1 3255.70 3105.77 101.54 o 0 3 1 1378.89 1545.78 152.77 o 1 3 1 8454.65 7972.78 169.88 o 2 3 1 24.03 -34.98 38.84 o 3 3 1 603.63 581.76 40.17 o 4 3 1 188.83 175.36 39.90 o 5 3 1 126.98 118.62 40.24 o 6 3 1 9.24 37.46 42.23 o 7 3 1 122.07 169.40 47.37 o 8 3 1 165.16 198.65 53.70 o 9 3 1 42.77 10.03 58.28 o 10 3 1 142.32 167.91 60.47 o 11 3 1 118.57 109.90 62.05 o 12 3 1 97.72 60.45 61.33 o 13 3 1 24.46 14.59 63.77 o 14 3 1 1.73 -27.89 64.85 o 15 3 1 2.66 60.83 71.20 o -15 4 1 18.52 -69.69 69.69 o -14 4 1 20.93 31.00 67.49 o -13 4 1 2.92 5.28 64.15 o -12 4 1 32.31 40.65 61.19 o -11 4 1 0.76 -26.28 62.68 o -9 4 1 0.08 3.16 59.23 o -8 4 1 1075.40 1222.69 69.21 o -7 4 1 95.89 90.48 49.61 o -6 4 1 58.40 42.43 46.34 o -5 4 1 79.86 84.00 44.35 o -4 4 1 129.74 162.61 44.17 o -3 4 1 5851.92 5333.39 253.49 o -2 4 1 1646.87 1826.35 93.21 o -1 4 1 2009.46 2107.93 66.49 o 0 4 1 958.49 1177.42 48.25 o 1 4 1 1913.91 1888.18 65.05 o 2 4 1 2727.21 2885.67 132.10 o 3 4 1 2496.60 2386.45 116.36 o 4 4 1 181.00 222.45 43.81 o 5 4 1 410.73 417.75 49.36 o 6 4 1 1169.50 1181.48 55.84 o 7 4 1 19.03 54.04 53.77 o 8 4 1 163.20 131.72 58.73 o 9 4 1 143.86 140.12 61.80 o 10 4 1 120.40 202.03 63.23 o 11 4 1 43.70 -6.30 62.05 o 12 4 1 40.82 13.80 63.93 o 13 4 1 8.32 21.52 66.18 o 14 4 1 23.63 67.54 68.49 o 15 4 1 0.23 -53.47 75.40 o -15 5 1 8.81 -40.26 74.49 o -14 5 1 40.56 50.15 70.77 o -13 5 1 139.03 141.74 68.60 o -12 5 1 54.83 43.02 65.19 o -11 5 1 29.74 61.96 63.25 o -10 5 1 147.39 136.93 65.12 o -9 5 1 161.74 128.37 64.67 o -8 5 1 0.15 6.73 61.83 o -7 5 1 32.84 73.07 57.31 o -6 5 1 72.41 8.83 52.57 o -5 5 1 0.82 -43.13 50.47 o -4 5 1 688.55 698.09 51.21 o -3 5 1 1045.82 1209.21 59.09 o -2 5 1 2066.77 2224.77 131.40 o -1 5 1 225.08 255.96 29.34 o 0 5 1 223.02 208.55 29.13 o 1 5 1 470.00 492.29 31.11 o 2 5 1 3266.21 3151.91 148.49 o 3 5 1 88.35 137.20 45.30 o 4 5 1 104.85 121.64 48.17 o 5 5 1 125.70 149.67 52.09 o 6 5 1 291.47 319.68 57.99 o 7 5 1 0.43 -9.44 60.56 o 9 5 1 286.72 302.74 67.22 o 10 5 1 118.47 61.04 66.23 o 11 5 1 18.79 -12.71 65.89 o 12 5 1 1.21 3.48 65.98 o 13 5 1 14.12 -8.02 70.11 o 14 5 1 2.11 -17.43 74.47 o 15 5 1 1.66 11.49 79.08 o -15 6 1 0.60 31.75 78.33 o -14 6 1 0.00 -42.18 72.62 o -13 6 1 9.86 -15.78 70.20 o -12 6 1 26.81 29.97 68.71 o -11 6 1 5.24 9.24 65.10 o -10 6 1 4.74 8.13 66.61 o -9 6 1 74.27 51.80 69.71 o -8 6 1 45.16 34.10 67.77 o -7 6 1 3.17 20.07 65.64 o -6 6 1 45.56 71.04 61.35 o -5 6 1 10.21 94.89 58.24 o -4 6 1 218.53 237.64 54.96 o -3 6 1 3.29 -49.41 49.41 o -2 6 1 103.54 160.17 48.26 o -1 6 1 988.21 1030.41 40.54 o 0 6 1 691.45 626.63 35.14 o 1 6 1 32.93 12.05 32.82 o 2 6 1 222.04 194.83 48.01 o 3 6 1 45.04 24.91 51.21 o 4 6 1 3.72 -5.80 55.01 o 5 6 1 21.88 73.46 58.51 o 6 6 1 26.02 42.02 62.21 o 7 6 1 232.50 273.77 67.90 o 8 6 1 62.64 131.51 69.10 o 9 6 1 19.79 -34.93 68.58 o 10 6 1 84.09 64.45 67.09 o 11 6 1 7.89 83.64 71.24 o 12 6 1 7.58 35.88 69.14 o 13 6 1 21.90 -33.49 73.48 o 14 6 1 0.17 -32.79 76.55 o 15 6 1 2.98 23.82 84.54 o -15 7 1 0.02 35.07 89.06 o -14 7 1 5.18 34.68 80.32 o -13 7 1 10.75 -14.56 76.01 o -12 7 1 2.91 -41.89 71.85 o -11 7 1 43.16 -16.46 71.97 o -10 7 1 23.01 32.79 70.09 o -9 7 1 58.13 49.34 72.30 o -8 7 1 10.69 15.13 72.49 o -7 7 1 2.20 65.60 70.11 o -6 7 1 33.06 26.01 69.28 o -5 7 1 7.38 50.94 66.28 o -4 7 1 287.16 289.53 62.46 o -3 7 1 461.95 507.46 60.47 o -2 7 1 73.56 63.72 55.93 o -1 7 1 728.93 771.99 51.59 o 0 7 1 300.66 303.02 39.53 o 1 7 1 153.37 188.46 39.02 o 2 7 1 7.61 53.81 54.76 o 3 7 1 1.34 -27.77 58.64 o 4 7 1 2.77 -39.92 63.02 o 5 7 1 0.16 -40.17 65.78 o 6 7 1 3.58 38.88 68.29 o 7 7 1 21.78 53.90 68.29 o 8 7 1 0.01 -63.86 69.46 o 9 7 1 0.94 5.85 70.63 o 10 7 1 9.01 52.88 70.88 o 11 7 1 24.82 69.28 72.60 o 12 7 1 22.04 139.39 75.47 o 13 7 1 8.06 23.98 79.35 o 14 7 1 1.46 43.94 84.36 o -14 8 1 0.93 96.26 87.05 o -13 8 1 12.17 7.70 81.81 o -12 8 1 18.99 -7.29 77.27 o -11 8 1 0.09 17.64 76.80 o -10 8 1 12.38 -25.38 75.22 o -9 8 1 35.80 29.83 71.85 o -8 8 1 0.09 -37.89 72.96 o -7 8 1 1.14 1.42 70.86 o -6 8 1 116.39 137.61 71.97 o -4 8 1 52.93 88.90 69.01 o -3 8 1 127.20 123.86 67.00 o -2 8 1 1.11 4.81 65.51 o -1 8 1 162.61 133.85 45.82 o 0 8 1 100.24 132.60 45.88 o 1 8 1 355.81 367.67 47.09 o 2 8 1 2.05 -59.16 64.27 o 3 8 1 10.74 10.75 66.73 o 4 8 1 10.86 52.14 68.94 o 5 8 1 122.56 188.08 70.09 o 6 8 1 27.59 19.83 69.59 o 7 8 1 13.95 -14.99 70.07 o 8 8 1 47.94 45.68 71.20 o 9 8 1 4.32 20.98 71.51 o 10 8 1 79.91 0.29 76.73 o 11 8 1 22.32 -36.40 78.47 o 12 8 1 35.36 4.45 82.24 o 13 8 1 50.14 28.72 84.79 o -13 9 1 5.24 -47.47 87.91 o -12 9 1 0.43 95.31 86.19 o -11 9 1 23.70 -6.84 82.01 o -10 9 1 22.00 -10.75 76.98 o -9 9 1 18.59 45.55 77.43 o -8 9 1 0.25 -0.38 73.30 o -7 9 1 1.74 33.51 70.70 o -6 9 1 25.52 121.49 72.42 o -5 9 1 133.56 42.20 71.18 o -3 9 1 85.62 50.65 71.31 o -2 9 1 634.77 541.85 71.79 o -1 9 1 229.73 195.10 49.27 o 0 9 1 313.46 285.54 49.17 o 1 9 1 325.01 338.57 50.15 o 2 9 1 59.47 46.45 66.41 o 3 9 1 43.97 -64.45 70.34 o 4 9 1 0.03 -63.00 70.02 o 5 9 1 3.24 -59.95 69.14 o 6 9 1 13.73 -19.49 70.20 o 7 9 1 125.60 136.66 72.10 o 8 9 1 56.51 51.82 74.18 o 9 9 1 0.00 16.39 75.29 o 10 9 1 10.84 15.11 78.11 o 11 9 1 55.89 96.47 85.58 o 12 9 1 52.98 160.80 88.68 o -12 10 1 38.74 -51.76 91.57 o -11 10 1 13.78 42.00 86.51 o -10 10 1 6.31 -10.97 83.50 o -9 10 1 13.06 67.72 80.70 o -8 10 1 316.52 137.56 81.29 o -7 10 1 32.66 72.24 76.98 o -6 10 1 170.12 160.08 74.02 o -5 10 1 34.92 35.38 72.33 o -4 10 1 0.35 36.24 70.97 o -3 10 1 608.25 500.12 73.86 o -2 10 1 17.14 46.38 68.96 o -1 10 1 120.02 33.59 60.82 o 0 10 1 15.17 20.21 48.41 o 1 10 1 58.28 72.25 49.61 o 2 10 1 409.33 332.12 70.43 o 3 10 1 4.81 13.32 70.43 o 4 10 1 1.56 19.83 69.32 o 5 10 1 1.15 -48.82 71.51 o 6 10 1 74.39 37.12 72.24 o 7 10 1 0.04 22.15 75.99 o 8 10 1 215.36 282.08 78.69 o 9 10 1 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