#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/30/2013080.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013080_Fobs loop_ _publ_author_name 'Malathi, R.' 'Rajan, S. S.' 'Gopalakrishnan, Geetha' 'Suresh, G.' _publ_section_title ; Azadirachtol, a tetranortriterpenoid from neem kernels ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o708 _journal_page_last o710 _journal_volume 58 _journal_year 2002 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 14.1425 _cell_length_b 17.2873 _cell_length_c 21.5047 _exptl_crystal_F_000 2464.00 _reflns_d_resolution_high 0.8102 _[local]_cod_data_source_file ln1147Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' AZADIRACHTOL 26.4.00 ORTHORHOMBIC p212121' _shelx_refln_list_code 4 _shelx_f_calc_maximum 223.66 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 40479.41 46806.59 263.59 o 4 0 0 33215.02 37368.83 301.03 o 6 0 0 39.79 -40.81 51.99 o 8 0 0 2245.20 2451.77 80.70 o 10 0 0 2226.37 2355.58 97.59 o 12 0 0 18.55 -32.37 62.70 o 14 0 0 2197.79 2048.24 123.42 o 16 0 0 413.77 154.72 80.44 o 1 1 0 16759.47 18530.66 132.11 o 3 1 0 8170.15 9362.59 129.29 o 4 1 0 4343.53 5582.28 115.53 o 5 1 0 73.24 73.54 27.82 o 6 1 0 1968.77 1877.52 58.27 o 7 1 0 9.73 -32.72 59.05 o 8 1 0 277.61 224.94 46.65 o 9 1 0 46.69 35.45 80.60 o 10 1 0 3784.51 3820.00 118.48 o 11 1 0 65.05 67.26 60.65 o 12 1 0 476.83 458.10 71.88 o 13 1 0 47.04 0.00 111.83 o 14 1 0 202.73 320.10 71.73 o 15 1 0 1571.36 1484.23 117.57 o 16 1 0 41.62 66.80 87.78 o 17 1 0 160.12 -3.99 78.46 o 0 2 0 22716.19 24470.91 213.10 o 1 2 0 37731.12 39799.89 229.42 o 2 2 0 19589.37 19612.98 171.80 o 3 2 0 312.88 300.30 25.69 o 4 2 0 1899.39 2648.37 75.16 o 5 2 0 4407.53 6096.95 140.45 o 6 2 0 4.81 39.55 47.08 o 7 2 0 1241.39 1370.23 60.96 o 8 2 0 242.65 278.30 48.93 o 9 2 0 1608.01 1997.33 86.49 o 10 2 0 20.08 -70.68 99.86 o 11 2 0 49.49 97.47 63.27 o 12 2 0 298.79 251.38 73.22 o 13 2 0 10.31 -123.91 123.91 o 14 2 0 394.33 419.70 78.26 o 15 2 0 5.28 56.31 65.32 o 16 2 0 11.90 -86.86 86.86 o 17 2 0 1.61 -42.06 70.10 o 1 3 0 23995.38 23154.24 195.01 o 2 3 0 6964.13 7231.92 115.32 o 3 3 0 711.80 654.92 31.45 o 4 3 0 814.14 855.18 36.82 o 5 3 0 1904.80 2273.71 67.35 o 6 3 0 1949.81 2065.58 65.01 o 7 3 0 2211.52 2669.56 81.75 o 8 3 0 2657.70 3176.29 93.62 o 9 3 0 427.23 499.07 58.76 o 10 3 0 150.04 22.12 110.60 o 11 3 0 266.46 414.57 69.46 o 12 3 0 260.77 236.88 79.38 o 13 3 0 181.58 181.76 81.87 o 14 3 0 209.51 233.09 82.79 o 15 3 0 225.74 184.41 76.18 o 16 3 0 213.73 5.59 111.54 o 17 3 0 0.49 -78.20 78.20 o 0 4 0 25345.90 25407.87 252.08 o 1 4 0 5760.19 5668.88 111.61 o 2 4 0 42.32 44.58 40.47 o 3 4 0 24586.48 24524.83 252.64 o 4 4 0 1597.90 1640.47 51.71 o 5 4 0 871.88 818.79 43.44 o 6 4 0 3334.42 4062.98 126.12 o 7 4 0 1103.26 1204.07 63.56 o 8 4 0 2138.49 2774.50 93.83 o 9 4 0 2047.72 2841.83 102.48 o 10 4 0 713.73 754.03 81.62 o 11 4 0 92.73 114.47 106.60 o 12 4 0 52.40 17.67 115.37 o 13 4 0 42.87 87.66 120.84 o 14 4 0 608.23 774.14 96.67 o 15 4 0 1.24 80.13 106.92 o 16 4 0 39.33 -47.88 90.74 o 17 4 0 0.86 10.03 72.72 o 1 5 0 2885.26 2543.21 68.80 o 2 5 0 3400.08 3412.45 101.13 o 3 5 0 11311.63 11784.99 189.32 o 4 5 0 867.15 847.90 47.44 o 5 5 0 962.06 1103.17 49.61 o 6 5 0 6044.09 7169.10 204.48 o 7 5 0 1185.30 1164.86 67.22 o 8 5 0 240.28 336.68 57.37 o 9 5 0 291.16 394.54 62.85 o 10 5 0 46.61 -71.02 118.45 o 11 5 0 73.22 -58.60 115.72 o 12 5 0 39.27 -129.16 129.16 o 13 5 0 113.92 -34.66 111.16 o 14 5 0 302.28 242.49 79.73 o 15 5 0 1.74 20.86 99.97 o 16 5 0 5.29 -4.90 88.23 o 0 6 0 6407.01 6021.98 97.94 o 1 6 0 1696.62 1550.84 49.21 o 2 6 0 2928.06 2703.45 76.71 o 3 6 0 179.51 187.05 31.71 o 4 6 0 6357.61 7227.68 180.90 o 5 6 0 5875.09 6517.89 175.63 o 6 6 0 118.52 63.74 76.05 o 7 6 0 80.45 60.31 75.70 o 8 6 0 1330.79 1472.45 81.40 o 9 6 0 88.86 176.37 62.82 o 10 6 0 2.54 -103.62 103.62 o 11 6 0 162.02 231.36 75.48 o 12 6 0 93.50 35.80 127.12 o 13 6 0 1022.26 1151.93 103.14 o 14 6 0 18.64 30.55 108.64 o 15 6 0 126.47 170.46 70.81 o 16 6 0 36.74 -36.14 88.92 o 1 7 0 1249.26 1263.38 46.47 o 2 7 0 1570.99 1490.83 53.61 o 3 7 0 2408.36 2351.08 72.33 o 4 7 0 16494.00 19714.34 313.51 o 5 7 0 41.10 47.99 61.22 o 6 7 0 3623.97 3816.01 115.23 o 7 7 0 3.90 0.00 71.47 o 8 7 0 2431.08 2834.01 104.74 o 9 7 0 1038.51 1373.00 91.05 o 10 7 0 14.99 -25.65 101.57 o 11 7 0 716.59 803.51 87.90 o 12 7 0 465.45 651.48 87.17 o 13 7 0 639.57 815.61 101.47 o 14 7 0 7.09 115.70 104.30 o 15 7 0 11.20 -96.55 96.55 o 16 7 0 1.75 43.89 78.08 o 0 8 0 2808.27 2652.97 62.76 o 1 8 0 1162.94 1143.67 49.98 o 2 8 0 14873.65 15861.75 268.36 o 3 8 0 9611.25 9746.14 222.45 o 4 8 0 3510.15 4326.53 132.40 o 5 8 0 2675.91 2729.08 85.14 o 6 8 0 1656.65 1964.30 84.56 o 7 8 0 1455.63 1604.89 85.08 o 8 8 0 64.95 57.80 58.26 o 9 8 0 4.95 -119.80 119.80 o 10 8 0 2031.34 2430.04 111.02 o 11 8 0 271.89 284.90 74.93 o 12 8 0 60.73 174.08 71.48 o 13 8 0 418.37 494.56 86.36 o 14 8 0 122.90 93.95 115.50 o 15 8 0 155.25 71.16 96.01 o 16 8 0 7.68 -72.16 72.16 o 1 9 0 2654.81 2705.04 80.59 o 2 9 0 647.68 520.21 51.84 o 3 9 0 59.60 19.15 62.70 o 4 9 0 3188.94 3288.31 100.74 o 5 9 0 173.94 169.00 47.55 o 6 9 0 194.31 211.88 54.62 o 7 9 0 190.09 234.00 58.16 o 8 9 0 347.10 361.38 71.18 o 9 9 0 26.09 -65.55 95.53 o 10 9 0 561.24 584.27 81.36 o 11 9 0 306.43 395.44 77.79 o 12 9 0 4.89 -8.32 102.25 o 13 9 0 14.82 101.57 67.03 o 14 9 0 131.97 -24.40 97.03 o 15 9 0 62.89 90.75 58.60 o 0 10 0 6196.73 5494.50 113.95 o 1 10 0 857.69 860.15 53.23 o 2 10 0 136.88 150.63 48.12 o 3 10 0 936.15 928.32 60.21 o 4 10 0 3271.26 3474.33 101.41 o 5 10 0 1764.49 1864.26 85.48 o 6 10 0 219.21 217.93 63.41 o 7 10 0 239.51 302.22 64.66 o 8 10 0 2364.16 2250.95 108.01 o 9 10 0 1768.83 1658.55 103.98 o 10 10 0 69.12 79.35 73.65 o 11 10 0 23.97 53.92 112.17 o 12 10 0 0.44 -87.32 108.52 o 13 10 0 26.12 -54.26 97.69 o 14 10 0 4.91 0.00 84.12 o 15 10 0 82.38 -3.65 69.21 o 1 11 0 28.43 -28.50 73.98 o 2 11 0 0.96 -78.08 78.08 o 3 11 0 168.02 214.38 48.92 o 4 11 0 300.61 329.99 52.36 o 5 11 0 206.93 201.39 61.12 o 6 11 0 76.81 -52.67 95.42 o 7 11 0 670.15 735.20 71.45 o 8 11 0 581.15 607.47 85.13 o 9 11 0 1555.57 1750.08 101.19 o 10 11 0 158.11 174.12 77.76 o 11 11 0 136.76 85.97 116.53 o 12 11 0 4.86 58.59 90.28 o 13 11 0 220.16 234.93 64.21 o 14 11 0 227.35 243.74 62.62 o 0 12 0 323.71 342.77 44.42 o 1 12 0 2478.77 2261.37 90.31 o 2 12 0 1.84 56.20 83.10 o 3 12 0 1324.75 1239.24 78.76 o 4 12 0 1045.55 1003.24 73.68 o 5 12 0 21.18 7.64 96.10 o 6 12 0 237.17 274.27 69.22 o 7 12 0 172.93 110.27 115.97 o 8 12 0 34.98 112.51 69.65 o 9 12 0 403.39 319.54 74.15 o 10 12 0 3.71 113.99 105.55 o 11 12 0 866.75 821.73 85.99 o 12 12 0 104.27 -19.61 96.80 o 13 12 0 59.25 137.03 54.49 o 14 12 0 173.44 91.47 74.47 o 1 13 0 241.94 135.03 111.77 o 2 13 0 0.13 23.60 87.20 o 3 13 0 0.40 62.12 95.75 o 4 13 0 15.79 -71.70 92.56 o 5 13 0 1103.44 1200.11 81.80 o 6 13 0 9.54 0.00 109.09 o 7 13 0 18.42 -34.88 105.33 o 8 13 0 81.61 54.50 117.66 o 9 13 0 8.08 92.22 100.31 o 10 13 0 153.56 297.38 68.64 o 11 13 0 30.53 -28.61 99.52 o 12 13 0 21.54 28.16 82.53 o 13 13 0 88.99 71.37 75.48 o 0 14 0 1451.80 1557.50 85.69 o 1 14 0 3867.09 3746.10 128.32 o 2 14 0 277.43 267.34 71.40 o 3 14 0 671.41 794.66 81.04 o 4 14 0 253.43 328.00 62.95 o 5 14 0 408.27 434.65 70.27 o 6 14 0 434.58 548.64 72.79 o 7 14 0 8.92 -117.18 117.18 o 8 14 0 274.93 370.33 72.19 o 9 14 0 183.62 85.75 107.65 o 10 14 0 4.20 0.00 97.92 o 11 14 0 89.66 85.96 97.82 o 12 14 0 178.34 173.46 51.89 o 13 14 0 73.80 -25.20 59.17 o 1 15 0 6.00 87.43 101.91 o 2 15 0 1873.89 1792.27 104.80 o 3 15 0 10.55 -26.22 110.46 o 4 15 0 4.98 52.21 100.08 o 5 15 0 1086.92 1114.35 83.96 o 6 15 0 337.60 315.39 71.52 o 7 15 0 185.99 8.21 111.07 o 8 15 0 217.88 138.56 68.08 o 9 15 0 203.91 275.74 62.26 o 10 15 0 127.29 112.20 61.00 o 11 15 0 66.91 105.00 53.24 o 12 15 0 3.18 59.16 42.52 o 0 16 0 2428.27 2335.04 108.81 o 1 16 0 149.89 183.12 64.31 o 2 16 0 2.54 18.24 114.67 o 3 16 0 134.57 107.86 60.20 o 4 16 0 0.26 -17.10 94.84 o 5 16 0 41.99 70.11 56.32 o 6 16 0 38.48 -23.94 90.86 o 7 16 0 35.94 51.18 59.51 o 8 16 0 0.84 13.45 81.27 o 9 16 0 3.26 57.45 47.65 o 10 16 0 28.31 103.17 47.65 o 11 16 0 55.64 63.84 66.24 o 1 17 0 194.33 105.59 63.86 o 2 17 0 264.93 310.10 70.03 o 3 17 0 11.73 24.74 93.47 o 4 17 0 159.27 175.26 60.55 o 5 17 0 65.41 116.63 60.88 o 6 17 0 54.16 84.48 91.32 o 7 17 0 9.96 102.02 86.52 o 8 17 0 26.71 11.06 69.65 o 9 17 0 37.77 32.15 62.70 o 10 17 0 3.21 33.28 58.93 o 0 18 0 13.09 7.87 92.22 o 1 18 0 142.40 123.14 99.09 o 2 18 0 1.41 -15.62 100.31 o 3 18 0 46.91 -7.30 95.65 o 4 18 0 1.43 80.36 75.12 o 5 18 0 58.30 43.66 81.17 o 6 18 0 57.05 11.63 74.44 o 7 18 0 257.50 246.48 51.78 o 8 18 0 17.30 29.52 61.33 o 9 18 0 118.47 48.81 52.00 o 1 19 0 53.09 158.01 54.49 o 2 19 0 33.70 -81.17 81.17 o 3 19 0 8.31 15.39 49.02 o 4 19 0 133.67 -21.66 79.82 o 5 19 0 375.63 387.69 58.99 o 6 19 0 1.95 39.78 63.61 o 7 19 0 2.52 -56.99 56.99 o 0 20 0 32.71 76.83 65.78 o 1 20 0 1.83 -65.09 72.38 o 2 20 0 147.02 285.87 46.75 o 3 20 0 2.90 -13.56 64.86 o 4 20 0 253.23 250.26 50.53 o 5 20 0 214.76 230.74 44.60 o 6 20 0 52.37 2.96 49.14 o 1 21 0 139.14 160.79 41.17 o 2 21 0 58.01 125.52 38.65 o 2 0 1 170.76 175.35 20.66 o 3 0 1 10994.61 10438.54 135.23 o 4 0 1 1270.26 1342.23 40.82 o 5 0 1 205.70 193.70 26.24 o 6 0 1 2045.06 2398.19 69.64 o 7 0 1 213.24 224.81 41.74 o 8 0 1 234.42 203.02 44.03 o 9 0 1 15.37 -5.93 76.15 o 10 0 1 0.27 -34.77 83.67 o 11 0 1 2813.70 3123.36 117.97 o 12 0 1 29.30 69.20 102.37 o 13 0 1 439.07 534.16 78.72 o 14 0 1 59.20 76.84 111.72 o 15 0 1 28.37 -108.07 108.07 o 16 0 1 17.76 -73.07 84.36 o 17 0 1 9.26 -23.82 62.92 o 1 1 1 13006.09 13178.51 114.51 o 2 1 1 5179.80 4631.59 81.77 o 3 1 1 488.33 613.74 27.89 o 4 1 1 1157.36 1355.51 39.30 o 5 1 1 7517.94 8943.73 163.15 o 6 1 1 240.62 310.97 34.56 o 7 1 1 2348.52 2149.60 70.33 o 8 1 1 1197.74 1146.05 63.11 o 9 1 1 491.82 452.13 55.80 o 10 1 1 32.49 -97.47 97.47 o 11 1 1 372.70 410.33 64.80 o 12 1 1 247.90 78.01 122.94 o 13 1 1 150.49 116.42 110.03 o 14 1 1 79.25 198.14 65.67 o 15 1 1 9.55 70.22 96.55 o 16 1 1 30.17 42.29 81.39 o 17 1 1 42.80 -68.97 68.97 o 0 2 1 2944.12 2827.11 103.91 o 1 2 1 989.60 843.19 27.26 o 2 2 1 3688.06 3575.00 75.84 o 3 2 1 8944.31 9886.18 140.88 o 4 2 1 4095.88 5397.94 120.61 o 5 2 1 8344.90 10988.81 186.34 o 6 2 1 160.56 130.70 35.92 o 7 2 1 890.00 977.43 57.25 o 8 2 1 698.54 747.12 59.15 o 9 2 1 463.17 524.33 62.30 o 10 2 1 401.81 462.74 68.00 o 11 2 1 416.55 376.14 72.22 o 12 2 1 875.42 955.52 90.21 o 13 2 1 176.41 0.00 127.83 o 14 2 1 60.53 66.58 68.86 o 15 2 1 173.17 -119.62 119.62 o 16 2 1 23.17 -11.86 77.74 o 17 2 1 56.44 -66.01 66.01 o 1 3 1 858.38 718.25 27.86 o 2 3 1 26.35 -13.22 52.10 o 3 3 1 7089.09 7090.74 126.11 o 4 3 1 3077.53 3396.35 92.41 o 5 3 1 3833.79 4879.72 130.25 o 6 3 1 298.56 421.56 39.93 o 7 3 1 687.64 882.86 56.98 o 8 3 1 142.33 252.23 50.51 o 9 3 1 1169.49 1372.84 77.95 o 10 3 1 250.25 207.00 67.63 o 11 3 1 201.28 183.60 71.96 o 12 3 1 58.59 131.67 124.49 o 13 3 1 624.56 582.06 85.48 o 14 3 1 821.99 738.62 100.25 o 15 3 1 61.24 -67.72 121.53 o 16 3 1 14.38 61.33 90.40 o 17 3 1 10.71 -50.27 78.08 o 0 4 1 1141.03 1180.91 24.12 o 1 4 1 8996.29 8209.89 128.62 o 2 4 1 2604.21 2442.07 68.09 o 3 4 1 879.96 802.45 34.09 o 4 4 1 322.30 235.89 34.92 o 5 4 1 1160.20 1332.66 50.00 o 6 4 1 3386.59 4366.91 127.05 o 7 4 1 1527.62 1953.23 70.49 o 8 4 1 773.91 906.85 62.35 o 9 4 1 530.74 681.54 68.02 o 10 4 1 18.22 83.90 96.78 o 11 4 1 594.49 796.60 75.78 o 12 4 1 369.18 588.04 80.31 o 13 4 1 248.65 193.99 75.50 o 14 4 1 341.73 361.60 82.59 o 15 4 1 35.27 -114.91 114.91 o 16 4 1 177.04 74.12 99.10 o 17 4 1 116.08 13.23 78.00 o 0 5 1 699.08 714.18 22.68 o 1 5 1 9328.07 7765.61 133.85 o 2 5 1 3973.84 3771.06 103.08 o 3 5 1 19473.56 20401.77 253.97 o 4 5 1 3400.27 3563.10 109.74 o 5 5 1 3881.42 4051.47 118.30 o 6 5 1 765.87 950.93 56.88 o 7 5 1 823.53 942.79 62.82 o 8 5 1 216.97 306.67 57.48 o 9 5 1 578.25 787.17 70.88 o 10 5 1 122.59 23.72 107.06 o 11 5 1 60.44 138.40 63.16 o 12 5 1 60.47 97.02 73.65 o 13 5 1 100.12 17.33 124.39 o 14 5 1 10.58 -87.43 121.86 o 15 5 1 44.86 90.06 108.87 o 16 5 1 70.49 -96.57 96.57 o 0 6 1 34177.77 33455.52 550.82 o 1 6 1 9158.56 7594.29 145.64 o 2 6 1 7890.76 7105.39 153.81 o 3 6 1 4586.44 4619.99 133.99 o 4 6 1 4564.72 5147.46 135.21 o 5 6 1 2703.94 2719.58 81.54 o 6 6 1 71.19 112.64 41.27 o 7 6 1 1959.45 2326.07 88.30 o 8 6 1 364.49 450.74 64.68 o 9 6 1 140.14 142.07 60.09 o 10 6 1 384.52 426.54 68.56 o 11 6 1 117.93 51.42 109.23 o 12 6 1 131.70 116.30 137.16 o 13 6 1 150.30 280.72 74.46 o 14 6 1 115.44 -106.83 123.48 o 15 6 1 127.64 161.45 67.39 o 16 6 1 25.39 -67.37 81.28 o 0 7 1 2433.34 2198.14 94.80 o 1 7 1 4956.90 4548.60 129.38 o 2 7 1 4010.81 3910.44 111.15 o 3 7 1 3044.28 3295.03 97.08 o 4 7 1 7007.14 7877.74 204.87 o 5 7 1 7895.26 8300.61 211.71 o 6 7 1 3398.70 3754.67 118.61 o 7 7 1 447.42 527.97 59.68 o 8 7 1 1868.67 1987.71 92.36 o 9 7 1 418.52 440.27 68.45 o 10 7 1 484.88 617.63 79.19 o 11 7 1 759.21 968.31 90.99 o 12 7 1 749.20 885.52 93.38 o 13 7 1 79.19 74.22 74.79 o 14 7 1 31.93 -36.02 110.58 o 15 7 1 41.90 -16.87 100.09 o 16 7 1 45.02 67.49 81.28 o 0 8 1 3577.09 3129.06 93.30 o 1 8 1 946.50 1021.42 49.61 o 2 8 1 46.19 81.17 33.18 o 3 8 1 444.22 443.84 45.19 o 4 8 1 2006.04 2077.60 77.69 o 5 8 1 5345.95 5820.55 163.98 o 6 8 1 2662.01 3012.57 102.08 o 7 8 1 1020.29 1204.96 75.52 o 8 8 1 1279.19 1509.65 83.55 o 9 8 1 1114.35 1369.05 91.97 o 10 8 1 808.53 976.75 93.74 o 11 8 1 655.94 719.63 86.40 o 12 8 1 88.66 88.58 68.41 o 13 8 1 106.49 134.08 118.80 o 14 8 1 13.75 0.00 101.00 o 15 8 1 36.77 -87.67 87.67 o 16 8 1 47.64 -75.81 75.81 o 0 9 1 119.74 78.06 49.77 o 1 9 1 565.58 487.12 43.50 o 2 9 1 3799.64 3840.10 108.55 o 3 9 1 722.18 762.03 54.47 o 4 9 1 4316.43 4272.58 119.56 o 5 9 1 842.22 862.30 64.30 o 6 9 1 1919.48 2221.41 93.98 o 7 9 1 154.40 48.12 99.89 o 8 9 1 733.99 769.68 81.74 o 9 9 1 363.73 338.79 73.69 o 10 9 1 332.20 430.59 81.21 o 11 9 1 203.24 309.38 73.89 o 12 9 1 433.60 404.90 77.81 o 13 9 1 310.76 386.44 78.48 o 14 9 1 20.84 -12.08 92.45 o 15 9 1 17.23 -4.45 80.59 o 0 10 1 1006.66 974.85 41.84 o 1 10 1 798.17 699.66 52.20 o 2 10 1 4775.08 4885.96 144.01 o 3 10 1 1459.70 1527.34 70.34 o 4 10 1 68.81 -5.81 78.66 o 5 10 1 1276.90 1252.97 74.19 o 6 10 1 877.20 954.17 79.14 o 7 10 1 736.98 890.25 76.26 o 8 10 1 74.14 37.96 66.58 o 9 10 1 212.63 211.31 66.94 o 10 10 1 7.38 -46.05 115.36 o 11 10 1 701.15 950.05 89.61 o 12 10 1 17.99 -23.71 105.33 o 13 10 1 306.96 315.84 72.09 o 14 10 1 51.10 53.47 80.37 o 15 10 1 80.52 -69.55 70.46 o 0 11 1 0.13 49.69 42.46 o 1 11 1 846.23 783.48 61.90 o 2 11 1 744.80 691.14 65.08 o 3 11 1 849.28 683.06 61.67 o 4 11 1 831.69 908.65 69.32 o 5 11 1 365.55 325.46 59.55 o 6 11 1 1358.72 1626.97 90.19 o 7 11 1 124.53 104.55 100.79 o 8 11 1 988.52 947.86 89.09 o 9 11 1 355.50 405.51 72.89 o 10 11 1 1508.66 1501.95 103.01 o 11 11 1 382.29 551.67 77.46 o 12 11 1 362.64 316.33 73.92 o 13 11 1 150.72 138.89 61.69 o 14 11 1 7.92 -81.05 81.05 o 0 12 1 2799.49 2761.61 69.09 o 1 12 1 64.14 45.72 83.45 o 2 12 1 282.59 301.57 57.94 o 3 12 1 522.28 514.43 63.68 o 4 12 1 907.71 975.43 78.69 o 5 12 1 363.82 415.46 69.93 o 6 12 1 798.29 736.41 77.18 o 7 12 1 226.17 50.98 115.75 o 8 12 1 732.15 806.16 81.73 o 9 12 1 121.63 86.88 113.90 o 10 12 1 139.22 266.01 69.89 o 11 12 1 6.22 -15.96 114.79 o 12 12 1 40.66 103.40 56.09 o 13 12 1 11.53 -71.93 86.86 o 14 12 1 10.41 -58.14 67.94 o 0 13 1 221.16 295.31 43.73 o 1 13 1 999.42 796.62 75.50 o 2 13 1 637.29 716.34 77.50 o 3 13 1 619.57 780.79 67.80 o 4 13 1 111.05 -71.83 114.81 o 5 13 1 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