#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2013089.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013089_Fobs loop_ _publ_author_name 'Blake, Alexander J.' 'De, Binod B.' 'Li, Wan-Sheung' 'Thomas, Neil R.' _publ_section_title ; Retroracemization using new forms of Belokon's original ligand: intermediate Ni^II^ complexes of N-({2-[N-(S)-alkylprolylamino]phenyl}phenylmethylene)-(S)-phenylalanine (alkyl is 2-picolyl, 3-picolyl or ethyl) ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m570 _journal_page_last m574 _journal_volume 58 _journal_year 2002 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.7220 _cell_length_b 18.3910 _cell_length_c 25.5280 _exptl_crystal_F_000 2464.00 _reflns_d_resolution_high 0.8392 _[local]_cod_data_source_file sk1578Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' PYO3NI (#211) FOR Binod B.De/NR.Thomas in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 305.45 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 26.88 58.98 44.54 o 4 0 0 10166.36 10319.60 161.77 o 6 0 0 40687.50 39799.98 376.04 o 8 0 0 19027.06 19099.91 309.09 o 10 0 0 2861.47 2998.87 158.79 o 12 0 0 8874.58 8010.10 184.41 o 2 1 0 2630.38 2430.49 66.74 o 3 1 0 7.17 103.05 61.34 o 4 1 0 6455.40 6407.29 134.02 o 5 1 0 2911.26 2823.96 112.01 o 6 1 0 448.62 556.81 83.80 o 7 1 0 3467.97 3828.12 139.48 o 8 1 0 160.93 -38.97 81.82 o 9 1 0 707.35 650.62 105.51 o 10 1 0 1720.63 1980.09 140.54 o 11 1 0 139.04 236.20 108.80 o 12 1 0 96.11 370.01 79.27 o 13 1 0 1731.87 1545.35 113.54 o 1 2 0 6676.79 6422.44 80.87 o 2 2 0 2668.12 2551.50 73.82 o 3 2 0 1291.51 1342.06 76.01 o 4 2 0 213.86 335.49 68.89 o 5 2 0 1348.87 1159.61 87.23 o 6 2 0 11.47 -31.99 77.66 o 7 2 0 2640.67 2538.75 126.61 o 8 2 0 467.29 684.77 95.13 o 9 2 0 1877.10 1875.03 135.17 o 10 2 0 110.16 86.25 96.54 o 11 2 0 535.58 621.34 119.19 o 12 2 0 7.13 36.05 73.23 o 13 2 0 20.01 81.81 75.21 o 1 3 0 7193.66 6151.09 91.40 o 2 3 0 2321.87 2270.13 78.23 o 3 3 0 236.25 300.58 62.10 o 4 3 0 11594.63 10894.50 178.17 o 5 3 0 14147.88 14708.85 224.22 o 6 3 0 168.50 -141.46 77.10 o 7 3 0 1058.85 844.46 99.39 o 8 3 0 2680.42 2716.18 144.07 o 9 3 0 1030.35 1180.79 119.86 o 10 3 0 674.97 391.08 104.75 o 11 3 0 2928.54 2918.91 181.72 o 12 3 0 1002.45 916.11 92.39 o 13 3 0 146.04 137.77 86.63 o 0 4 0 4678.53 4473.36 91.21 o 1 4 0 10386.10 9700.56 122.87 o 2 4 0 2966.03 3019.31 95.25 o 3 4 0 0.40 -44.35 61.71 o 4 4 0 2791.71 2925.34 107.86 o 5 4 0 8265.95 8548.12 177.69 o 6 4 0 2177.90 2356.11 117.54 o 7 4 0 55.69 -154.95 77.47 o 8 4 0 344.33 263.01 95.31 o 9 4 0 686.54 700.64 104.76 o 10 4 0 614.21 579.35 110.98 o 11 4 0 15.04 -121.82 69.45 o 12 4 0 221.83 260.36 73.70 o 13 4 0 1342.07 1192.29 104.10 o 1 5 0 9061.55 8572.51 132.06 o 2 5 0 13.60 -64.36 59.26 o 3 5 0 4568.15 4676.03 122.29 o 4 5 0 3078.54 3378.28 116.55 o 5 5 0 24956.79 25873.45 306.58 o 6 5 0 2466.27 2378.02 121.04 o 7 5 0 14491.15 14813.53 268.84 o 8 5 0 8.08 -132.11 80.78 o 9 5 0 2967.10 2864.73 156.81 o 10 5 0 675.86 898.25 117.50 o 11 5 0 319.62 385.40 75.78 o 12 5 0 134.02 157.87 77.66 o 13 5 0 2790.39 2651.85 138.67 o 0 6 0 3472.97 3233.40 103.18 o 1 6 0 1272.75 1105.52 72.51 o 2 6 0 2.85 71.62 58.13 o 3 6 0 1477.50 1374.93 86.29 o 4 6 0 434.00 391.75 74.08 o 5 6 0 8583.68 9155.85 193.46 o 6 6 0 2247.77 2393.91 117.82 o 7 6 0 1.65 136.26 76.62 o 8 6 0 27.11 -50.30 88.04 o 9 6 0 513.25 484.41 102.11 o 10 6 0 262.84 175.52 111.64 o 11 6 0 4569.17 3958.99 141.44 o 12 6 0 1023.37 835.51 95.32 o 13 6 0 207.96 194.68 92.48 o 1 7 0 3479.78 3654.24 111.95 o 2 7 0 3198.81 2904.65 103.24 o 3 7 0 3286.35 3537.76 117.97 o 4 7 0 5154.93 4475.19 139.84 o 5 7 0 1994.01 1902.84 112.63 o 6 7 0 864.05 713.70 94.95 o 7 7 0 320.00 17.93 85.97 o 8 7 0 774.99 738.68 102.87 o 9 7 0 2108.15 2150.30 145.74 o 10 7 0 200.48 90.88 106.54 o 11 7 0 4.44 194.20 78.89 o 12 7 0 162.81 -11.61 79.83 o 13 7 0 152.21 397.47 96.54 o 0 8 0 21463.99 21606.67 260.52 o 1 8 0 21010.98 21572.71 270.24 o 2 8 0 65.00 -47.47 60.49 o 3 8 0 9020.72 8412.24 179.22 o 4 8 0 780.05 901.53 87.87 o 5 8 0 1878.74 2013.10 114.70 o 6 8 0 3007.82 2872.56 137.00 o 7 8 0 1186.02 994.33 107.69 o 8 8 0 882.90 998.23 114.57 o 9 8 0 10536.68 10792.76 279.47 o 10 8 0 1679.79 1788.33 152.34 o 11 8 0 767.97 1041.13 95.22 o 12 8 0 469.93 429.76 88.33 o 1 9 0 8.42 -118.52 59.26 o 2 9 0 1816.46 2153.77 101.58 o 3 9 0 338.92 547.26 74.93 o 4 9 0 6.17 159.95 71.15 o 5 9 0 4445.50 4638.24 159.99 o 6 9 0 253.78 305.28 83.23 o 7 9 0 326.72 466.85 91.44 o 8 9 0 606.05 634.00 109.85 o 9 9 0 1535.61 1896.00 139.78 o 10 9 0 57.69 12.55 70.49 o 11 9 0 135.73 288.57 80.49 o 12 9 0 1174.03 1003.70 102.02 o 0 10 0 17491.71 17140.20 259.98 o 1 10 0 3646.71 4108.54 136.38 o 2 10 0 4417.39 4312.96 137.43 o 3 10 0 1017.00 1149.51 92.69 o 4 10 0 1676.11 1578.76 109.59 o 5 10 0 522.12 488.95 86.45 o 6 10 0 5962.92 5880.62 196.57 o 7 10 0 2.15 -170.80 85.40 o 8 10 0 3930.62 4251.51 191.20 o 9 10 0 573.28 759.98 113.72 o 10 10 0 121.50 77.29 72.57 o 11 10 0 9.96 -110.97 73.60 o 12 10 0 477.64 740.33 95.50 o 1 11 0 3412.90 3134.84 129.84 o 2 11 0 3570.84 3510.91 135.04 o 3 11 0 166.40 270.55 76.53 o 4 11 0 8416.23 8883.60 216.90 o 5 11 0 4120.83 4617.99 168.65 o 6 11 0 139.48 239.60 88.70 o 7 11 0 2857.43 3068.36 159.73 o 8 11 0 7.95 -78.79 97.20 o 9 11 0 207.08 230.73 74.64 o 10 11 0 916.25 881.84 95.51 o 11 11 0 1735.98 1543.46 114.11 o 12 11 0 51.23 -130.41 78.79 o 0 12 0 317.97 308.68 76.35 o 1 12 0 2.91 62.66 70.87 o 2 12 0 948.11 1167.87 95.04 o 3 12 0 293.10 437.78 85.12 o 4 12 0 1483.53 1656.05 116.19 o 5 12 0 12.86 22.46 77.76 o 6 12 0 379.93 570.84 93.90 o 7 12 0 22.97 104.56 94.18 o 8 12 0 318.67 235.92 95.50 o 9 12 0 870.98 785.95 92.11 o 10 12 0 1253.43 1416.34 102.12 o 11 12 0 30.27 -13.87 86.15 o 1 13 0 1530.41 1145.42 105.43 o 2 13 0 6571.94 6850.88 194.14 o 3 13 0 212.36 309.43 95.50 o 4 13 0 30354.32 31841.24 428.82 o 5 13 0 4660.72 4735.80 186.50 o 6 13 0 17.07 61.24 92.38 o 7 13 0 3969.34 4520.49 195.73 o 8 13 0 1230.14 1173.80 96.46 o 9 13 0 539.19 550.09 92.48 o 10 13 0 587.35 716.56 91.73 o 11 13 0 481.93 562.73 94.46 o 0 14 0 3793.65 3539.02 156.08 o 1 14 0 33.78 14.91 73.60 o 2 14 0 1086.01 1172.68 108.16 o 3 14 0 1299.50 1179.33 122.13 o 4 14 0 1436.13 1860.24 131.67 o 5 14 0 77.85 177.12 95.40 o 6 14 0 2448.44 2279.69 154.43 o 7 14 0 150.30 45.48 59.46 o 8 14 0 26.65 -14.63 70.68 o 9 14 0 21.08 -69.74 77.66 o 10 14 0 9.69 -160.80 80.40 o 1 15 0 3660.74 4130.80 173.45 o 2 15 0 296.11 286.41 86.72 o 3 15 0 4079.35 4205.67 176.85 o 4 15 0 978.32 853.08 118.07 o 5 15 0 154.14 63.32 97.10 o 6 15 0 363.98 109.66 113.15 o 7 15 0 1173.43 1351.89 76.76 o 8 15 0 462.83 743.35 87.48 o 9 15 0 1195.28 1217.94 112.50 o 10 15 0 229.47 137.68 86.44 o 0 16 0 627.92 537.83 100.51 o 1 16 0 89.86 -52.28 87.85 o 2 16 0 203.26 207.61 87.20 o 3 16 0 2113.10 2446.94 164.15 o 4 16 0 30.05 -124.56 94.74 o 5 16 0 2102.94 2372.63 96.99 o 6 16 0 98.27 175.47 44.98 o 7 16 0 1848.70 1879.94 143.80 o 8 16 0 1012.10 1118.45 104.10 o 9 16 0 3517.21 3737.03 154.73 o 1 17 0 212.80 60.77 92.76 o 2 17 0 29.68 126.64 88.61 o 3 17 0 4.63 -161.74 95.12 o 4 17 0 97.04 121.96 66.33 o 5 17 0 6.46 26.40 70.14 o 6 17 0 288.47 352.82 122.22 o 7 17 0 231.24 194.71 63.07 o 8 17 0 76.97 67.28 82.95 o 1 18 0 641.01 802.26 104.47 o 2 18 0 494.95 485.91 96.73 o 3 18 0 3104.84 3040.23 151.99 o 4 18 0 80.41 129.88 52.41 o 5 18 0 690.58 927.55 139.57 o 6 18 0 354.39 371.56 78.92 o 7 18 0 33.17 -23.89 174.01 o 1 19 0 1678.95 1214.82 126.66 o 3 19 0 94.58 159.10 108.24 o 4 19 0 27.14 56.38 81.93 o 5 19 0 855.28 926.53 65.46 o 6 19 0 590.97 607.53 119.57 o 0 20 0 1041.26 1027.66 121.27 o 1 20 0 275.90 145.33 102.58 o 3 20 0 29.35 -163.35 114.46 o 4 20 0 0.90 163.84 78.70 o 5 20 0 3.14 -16.30 161.64 o 1 21 0 280.48 302.26 104.37 o 3 21 0 936.38 464.23 156.76 o 2 0 1 15406.62 15584.50 137.73 o 3 0 1 10380.66 9916.39 141.96 o 4 0 1 7904.54 7495.87 143.27 o 5 0 1 5326.73 5392.27 140.06 o 6 0 1 3.02 -154.57 77.28 o 7 0 1 173.66 133.44 76.44 o 8 0 1 4616.35 4292.43 166.41 o 9 0 1 1.84 120.50 81.44 o 10 0 1 1028.29 1140.38 123.92 o 11 0 1 12.94 33.22 94.18 o 12 0 1 924.97 1055.40 88.81 o 13 0 1 441.78 369.64 87.39 o 2 1 1 3246.54 2987.56 75.56 o 3 1 1 11425.41 12234.22 154.44 o 4 1 1 8034.79 8153.38 148.86 o 5 1 1 4435.37 4399.40 128.50 o 6 1 1 1662.46 1585.58 106.58 o 7 1 1 9656.92 9146.20 206.04 o 8 1 1 2244.22 2395.01 130.75 o 9 1 1 4688.60 4215.51 175.56 o 10 1 1 783.18 510.00 113.53 o 11 1 1 1168.89 1139.44 133.92 o 12 1 1 212.02 213.36 79.55 o 13 1 1 558.22 503.94 92.86 o 1 2 1 55308.60 51627.00 241.60 o 2 2 1 16301.01 15620.93 152.83 o 3 2 1 1988.79 1917.74 84.72 o 4 2 1 5368.81 5831.13 130.18 o 5 2 1 12714.90 12715.30 202.85 o 6 2 1 1599.15 1814.94 106.86 o 7 2 1 14457.41 14787.81 260.84 o 8 2 1 1301.25 1571.73 122.14 o 9 2 1 1696.37 1843.54 136.68 o 10 2 1 1104.30 1184.09 127.70 o 11 2 1 8.37 -20.95 101.06 o 12 2 1 249.46 195.15 77.10 o 13 2 1 535.82 472.51 97.96 o 1 3 1 36143.54 32313.66 240.37 o 2 3 1 10573.75 10312.69 136.53 o 3 3 1 5887.93 5758.55 122.87 o 4 3 1 2579.05 2693.44 103.79 o 5 3 1 1470.11 1702.26 98.74 o 6 3 1 13507.18 13344.33 232.39 o 7 3 1 1497.73 1614.40 112.23 o 8 3 1 4259.58 4043.79 166.68 o 9 3 1 294.54 379.46 100.13 o 10 3 1 842.69 935.17 124.67 o 11 3 1 1322.24 1306.62 139.87 o 12 3 1 1572.09 1503.43 105.80 o 13 3 1 515.25 788.08 91.35 o 0 4 1 2390.66 2208.89 71.34 o 2 4 1 27281.15 26502.87 231.96 o 3 4 1 906.27 1006.26 77.97 o 4 4 1 4152.13 4212.09 124.62 o 5 4 1 11718.93 11772.12 209.37 o 6 4 1 7214.80 6844.94 175.33 o 7 4 1 1024.03 925.52 98.91 o 8 4 1 8600.82 8289.77 220.96 o 9 4 1 1381.32 1197.94 122.51 o 10 4 1 1379.41 1331.75 133.17 o 11 4 1 592.05 632.39 79.74 o 12 4 1 429.32 530.73 86.82 o 13 4 1 54.97 74.36 83.70 o 0 5 1 5122.70 4838.69 105.36 o 2 5 1 8558.84 8118.38 144.85 o 3 5 1 8256.55 7545.01 152.15 o 4 5 1 8849.90 8731.97 174.54 o 5 5 1 729.62 608.10 90.98 o 6 5 1 416.61 192.52 73.33 o 7 5 1 79.27 71.25 76.25 o 8 5 1 2761.25 2960.87 143.97 o 9 5 1 7562.38 6785.21 216.82 o 10 5 1 2187.57 2049.30 154.52 o 11 5 1 2105.25 1876.49 110.34 o 12 5 1 1191.12 1017.68 97.78 o 13 5 1 19.73 113.14 79.08 o 0 6 1 954.86 764.25 68.91 o 1 6 1 6817.78 6178.80 130.07 o 2 6 1 5813.75 5523.29 131.61 o 3 6 1 3956.17 4308.09 123.29 o 4 6 1 6987.29 6842.16 159.20 o 5 6 1 4969.12 4970.80 148.70 o 6 6 1 1762.82 1901.19 110.73 o 7 6 1 407.67 375.50 83.24 o 8 6 1 5053.73 4595.96 184.73 o 9 6 1 1493.52 1402.10 132.33 o 10 6 1 2514.35 2543.65 170.67 o 11 6 1 291.17 306.60 76.91 o 12 6 1 402.81 414.47 87.95 o 13 6 1 89.12 -163.06 81.53 o 0 7 1 6055.55 5364.16 125.75 o 1 7 1 1607.25 1536.75 80.63 o 2 7 1 2582.56 2167.89 95.85 o 3 7 1 1536.88 1579.37 93.55 o 4 7 1 4874.69 5011.59 147.19 o 5 7 1 265.68 306.51 76.91 o 6 7 1 342.47 274.71 81.06 o 7 7 1 117.86 14.34 84.17 o 8 7 1 3337.95 2991.56 158.15 o 9 7 1 82.77 181.28 97.67 o 10 7 1 1566.07 1769.53 148.75 o 11 7 1 207.21 -4.72 76.53 o 12 7 1 1632.74 1579.59 111.75 o 13 7 1 347.51 356.90 89.18 o 0 8 1 33.04 62.00 61.53 o 1 8 1 6813.06 6235.74 146.73 o 2 8 1 2152.59 1971.83 99.33 o 3 8 1 3529.49 3043.54 121.65 o 4 8 1 1784.36 1867.94 108.09 o 5 8 1 10555.41 10509.60 219.78 o 6 8 1 193.51 284.14 83.14 o 7 8 1 3084.62 3055.34 144.55 o 8 8 1 724.57 765.95 104.19 o 9 8 1 354.19 279.62 104.37 o 10 8 1 660.63 862.19 120.33 o 11 8 1 820.87 886.08 92.77 o 12 8 1 71.65 110.03 76.91 o 0 9 1 1792.54 2033.34 98.18 o 1 9 1 15947.25 16178.59 241.30 o 2 9 1 6900.76 6572.41 166.17 o 3 9 1 2802.61 2916.95 121.33 o 4 9 1 4783.48 5029.86 157.65 o 5 9 1 1090.89 902.12 99.48 o 6 9 1 101.58 30.10 80.87 o 7 9 1 1765.94 1764.84 132.62 o 8 9 1 301.40 426.55 101.73 o 9 9 1 49.50 236.01 100.03 o 10 9 1 1002.65 993.32 94.09 o 11 9 1 7.15 113.33 76.81 o 12 9 1 627.35 716.66 93.81 o 0 10 1 3018.90 3053.48 124.84 o 1 10 1 3870.95 3668.23 132.04 o 2 10 1 11133.07 10885.88 209.24 o 3 10 1 5599.03 5821.81 167.41 o 4 10 1 8603.40 8526.68 203.32 o 5 10 1 2411.49 2339.66 128.68 o 6 10 1 1837.96 1983.97 126.39 o 7 10 1 505.20 798.57 103.53 o 8 10 1 5077.44 5207.91 207.29 o 9 10 1 429.26 158.45 105.60 o 10 10 1 485.47 166.28 83.71 o 11 10 1 1080.11 864.59 98.25 o 12 10 1 446.72 401.16 90.50 o 0 11 1 1684.97 1540.00 99.50 o 1 11 1 5596.94 5738.26 166.37 o 2 11 1 6277.90 5995.58 165.16 o 3 11 1 4869.85 4488.80 156.51 o 4 11 1 1060.85 1354.86 106.18 o 5 11 1 455.51 536.97 95.98 o 6 11 1 3730.00 3692.73 170.81 o 7 11 1 998.18 966.15 122.03 o 8 11 1 905.92 727.74 120.24 o 9 11 1 1723.48 1682.62 106.47 o 10 11 1 17.92 228.55 77.38 o 11 11 1 366.54 229.79 84.65 o 12 11 1 914.32 887.49 105.13 o 0 12 1 91.26 106.26 67.85 o 1 12 1 474.43 364.94 80.97 o 2 12 1 1376.30 1399.59 106.85 o 3 12 1 3486.12 3104.27 142.49 o 4 12 1 5923.45 5964.63 191.47 o 5 12 1 1608.32 1851.16 126.58 o 6 12 1 139.13 392.09 93.71 o 7 12 1 4396.88 4072.64 189.23 o 8 12 1 1019.01 977.00 126.37 o 9 12 1 231.49 384.17 86.44 o 10 12 1 464.72 415.79 91.07 o 11 12 1 1373.82 1371.99 113.07 o 0 13 1 1178.83 800.28 98.16 o 1 13 1 1019.73 1217.80 107.03 o 2 13 1 4830.17 5538.85 175.95 o 3 13 1 11176.95 11843.10 256.21 o 4 13 1 295.41 274.90 92.76 o 5 13 1 884.66 1123.56 113.25 o 6 13 1 1669.62 1646.78 132.33 o 7 13 1 264.11 551.30 105.60 o 8 13 1 961.59 1007.56 94.28 o 9 13 1 1819.15 1874.79 113.26 o 10 13 1 147.98 160.14 76.06 o 11 13 1 545.80 681.16 100.98 o 0 14 1 2562.68 2552.42 140.47 o 1 14 1 82.41 21.04 78.13 o 2 14 1 2797.73 3011.22 153.88 o 3 14 1 193.78 210.72 88.14 o 4 14 1 3013.91 3094.70 157.10 o 5 14 1 172.94 73.61 101.82 o 6 14 1 3152.04 3254.28 182.87 o 7 14 1 169.97 349.32 98.38 o 8 14 1 2022.73 1798.86 117.51 o 9 14 1 277.18 224.88 84.65 o 10 14 1 559.79 558.39 97.01 o 0 15 1 901.52 959.91 112.12 o 1 15 1 1717.44 1816.62 131.20 o 2 15 1 42.94 55.58 78.98 o 3 15 1 4994.15 5037.46 193.88 o 4 15 1 7474.39 7832.95 242.21 o 5 15 1 1224.25 1345.77 131.38 o 6 15 1 1869.26 1868.85 128.32 o 7 15 1 289.29 159.25 59.91 o 8 15 1 1156.08 1197.37 105.33 o 9 15 1 1267.32 1193.98 107.40 o 10 15 1 891.77 1024.15 108.25 o 0 16 1 164.28 210.15 88.99 o 1 16 1 150.80 89.84 87.76 o 2 16 1 1024.73 918.77 112.50 o 3 16 1 1133.68 1042.61 121.94 o 4 16 1 3485.97 4112.69 189.39 o 5 16 1 135.18 209.46 204.35 o 6 16 1 1388.03 1441.20 62.44 o 7 16 1 796.17 947.58 73.27 o 8 16 1 815.48 1067.36 104.57 o 9 16 1 39.26 112.77 84.93 o 0 17 1 48.00 171.08 90.78 o 1 17 1 31.49 67.57 84.74 o 2 17 1 256.59 581.96 97.01 o 3 17 1 1086.33 934.16 136.28 o 4 17 1 922.40 968.14 82.91 o 5 17 1 296.15 314.07 48.81 o 6 17 1 2.56 -92.19 104.49 o 7 17 1 1143.27 1277.34 144.26 o 8 17 1 14.61 -155.32 77.66 o 0 18 1 584.11 562.55 95.60 o 1 18 1 694.24 784.15 101.26 o 2 18 1 26.38 -177.03 88.51 o 3 18 1 241.90 253.19 109.37 o 4 18 1 1313.68 1584.07 84.95 o 5 18 1 1419.40 1499.97 67.46 o 6 18 1 586.72 606.08 118.67 o 7 18 1 697.65 700.71 75.50 o 0 19 1 9.85 -70.77 91.72 o 1 19 1 1280.72 1583.22 124.01 o 2 19 1 476.63 338.32 99.75 o 3 19 1 2818.05 2693.63 150.94 o 4 19 1 154.26 88.77 67.88 o 5 19 1 556.73 538.57 68.44 o 6 19 1 278.95 396.45 89.74 o 0 20 1 119.52 -12.64 95.59 o 1 20 1 324.46 85.21 109.28 o 2 20 1 148.93 160.89 100.03 o 3 20 1 666.61 311.99 124.19 o 4 20 1 355.86 117.58 71.20 o 5 20 1 849.76 1071.36 108.76 o 0 21 1 2331.89 2488.12 153.20 o 1 21 1 740.43 503.19 119.29 o 2 21 1 1632.75 1142.12 134.97 o 3 21 1 182.01 -55.77 125.22 o 2 0 2 889.66 738.08 55.90 o 3 0 2 46266.29 47143.57 298.42 o 4 0 2 29.95 -103.90 64.17 o 5 0 2 1468.30 1257.46 91.57 o 6 0 2 310.28 514.32 83.80 o 7 0 2 3467.10 3573.61 149.49 o 8 0 2 1313.19 1430.44 111.85 o 9 0 2 9705.96 9763.30 246.02 o 10 0 2 1056.55 1041.00 138.83 o 11 0 2 616.15 628.99 120.42 o 12 0 2 1512.86 1505.21 107.22 o 13 0 2 99.41 238.18 82.48 o 1 1 2 40429.39 40087.48 185.45 o 2 1 2 18376.18 18690.68 159.12 o 3 1 2 851.59 778.52 76.18 o 4 1 2 13293.20 13574.12 189.32 o 5 1 2 20072.45 20643.74 252.63 o 6 1 2 3901.62 4098.40 137.71 o 7 1 2 2656.45 2496.65 128.50 o 8 1 2 4317.27 4390.48 165.65 o 9 1 2 5976.98 6384.38 205.54 o 10 1 2 3732.39 3740.62 188.55 o 11 1 2 2974.76 3145.70 180.40 o 12 1 2 782.21 723.37 93.34 o 13 1 2 514.35 588.68 92.11 o 0 2 2 14009.55 13549.40 106.94 o 1 2 2 29855.56 28893.24 180.98 o 2 2 2 22078.76 20912.74 176.27 o 3 2 2 8405.61 8482.73 140.44 o 4 2 2 4703.49 4834.78 122.96 o 5 2 2 5148.82 5301.51 141.56 o 6 2 2 5029.55 5212.55 155.51 o 7 2 2 8511.84 8795.87 206.36 o 8 2 2 1772.83 1894.88 125.26 o 9 2 2 1343.57 1340.46 125.82 o 10 2 2 4162.13 3944.80 186.96 o 11 2 2 500.12 319.54 115.89 o 12 2 2 253.86 155.89 84.08 o 13 2 2 1901.36 1745.66 114.58 o 0 3 2 3548.17 3301.73 70.94 o 1 3 2 9133.27 8644.34 114.35 o 2 3 2 15382.36 15025.77 164.78 o 3 3 2 9519.37 9400.67 151.17 o 4 3 2 3607.26 3664.63 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0 4 12 6575.20 6293.12 153.87 o 1 4 12 6438.70 6462.90 160.38 o 2 4 12 4404.27 4259.38 138.86 o 3 4 12 6219.47 5942.49 165.83 o 4 4 12 7296.02 7303.37 189.67 o 5 4 12 7544.59 7441.09 211.02 o 6 4 12 2017.10 1957.43 136.88 o 7 4 12 3304.43 3414.32 175.33 o 8 4 12 5560.21 5974.20 216.18 o 9 4 12 2729.37 2647.08 177.57 o 10 4 12 4099.54 4111.03 144.64 o 11 4 12 1202.32 1323.09 106.36 o 12 4 12 721.20 513.48 97.58 o 0 5 12 2.04 -33.97 62.66 o 1 5 12 2137.56 2005.93 106.59 o 2 5 12 6391.93 6595.24 166.79 o 3 5 12 2482.60 2485.90 123.02 o 4 5 12 467.68 250.09 89.18 o 5 5 12 1845.12 1922.19 133.85 o 6 5 12 272.19 549.98 103.81 o 7 5 12 414.47 566.51 117.68 o 8 5 12 2111.29 2350.03 166.51 o 9 5 12 214.97 293.01 113.71 o 10 5 12 1323.12 1150.31 100.70 o 11 5 12 623.54 571.23 90.31 o 12 5 12 168.67 152.21 88.52 o 0 6 12 17698.35 17132.30 256.24 o 1 6 12 1429.41 1312.16 96.66 o 2 6 12 1910.08 1739.64 110.83 o 3 6 12 269.63 295.00 81.82 o 4 6 12 3163.64 3377.34 147.96 o 5 6 12 3821.48 3793.85 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19.20 10.66 63.98 o 1 9 12 3650.55 3445.96 137.20 o 2 9 12 1949.78 2116.21 118.75 o 3 9 12 5717.16 5190.89 177.39 o 4 9 12 4366.13 4497.30 173.95 o 5 9 12 3979.20 3993.96 178.37 o 6 9 12 1705.25 1766.67 145.45 o 7 9 12 1056.04 1089.69 141.76 o 8 9 12 1507.61 1567.43 155.54 o 9 9 12 846.74 628.91 96.26 o 10 9 12 1151.67 1104.59 107.02 o 11 9 12 409.81 481.19 91.44 o 0 10 12 116.33 235.54 72.57 o 1 10 12 900.73 1050.63 94.85 o 2 10 12 2305.77 2182.10 132.45 o 3 10 12 2430.79 2803.85 138.11 o 4 10 12 1881.83 1894.28 134.98 o 5 10 12 213.69 183.45 104.28 o 6 10 12 22.26 -35.58 110.78 o 7 10 12 1494.09 1325.53 155.92 o 8 10 12 1782.12 1598.72 106.56 o 9 10 12 1295.62 1468.17 113.92 o 10 10 12 458.19 585.85 87.57 o 11 10 12 101.59 -162.40 87.00 o 0 11 12 1422.17 1415.42 111.85 o 1 11 12 3096.24 2958.81 142.09 o 2 11 12 140.01 172.41 87.38 o 3 11 12 1248.42 1354.87 120.81 o 4 11 12 966.53 623.37 112.78 o 5 11 12 3214.31 2995.89 167.86 o 6 11 12 484.45 410.14 111.07 o 7 11 12 638.55 614.26 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12 19.15 -30.48 74.93 o 1 19 12 979.67 889.01 103.62 o 2 19 12 764.11 877.57 101.17 o 3 19 12 1026.79 1353.82 118.91 o 4 19 12 835.76 917.63 66.14 o 0 20 12 1909.36 1856.46 126.19 o 1 20 12 911.47 993.19 105.70 o 1 0 13 6.34 51.62 69.45 o 2 0 13 5551.29 5918.25 158.45 o 3 0 13 2266.36 2412.21 120.00 o 4 0 13 6772.09 7295.62 184.64 o 5 0 13 569.16 887.78 103.34 o 6 0 13 6222.37 5982.82 194.32 o 7 0 13 1267.91 1030.77 132.61 o 8 0 13 2291.23 2209.17 149.24 o 9 0 13 1497.59 1429.64 149.60 o 10 0 13 156.01 382.09 84.36 o 11 0 13 11.23 10.10 72.09 o 12 0 13 574.16 389.85 96.73 o 0 1 13 624.76 371.10 75.41 o 1 1 13 3026.36 3388.26 126.35 o 2 1 13 6919.64 7341.31 173.34 o 3 1 13 4905.68 5160.28 157.66 o 4 1 13 1385.73 1303.63 109.30 o 5 1 13 2807.23 2766.35 140.11 o 6 1 13 2847.64 2941.86 146.72 o 7 1 13 336.00 232.71 104.18 o 8 1 13 2165.59 2419.63 158.68 o 9 1 13 15.18 -23.59 100.97 o 10 1 13 449.92 384.09 82.48 o 11 1 13 2233.02 2466.61 120.16 o 12 1 13 573.14 525.36 94.37 o 0 2 13 539.64 593.34 74.18 o 1 2 13 2879.32 3394.99 126.25 o 2 2 13 4400.95 3849.31 134.32 o 3 2 13 271.66 232.90 78.70 o 4 2 13 4632.30 5290.77 164.82 o 5 2 13 277.18 366.53 91.44 o 6 2 13 5376.18 5595.28 198.92 o 7 2 13 39.32 27.37 102.20 o 8 2 13 3235.00 3167.55 170.03 o 9 2 13 39.27 354.91 109.27 o 10 2 13 1212.00 1353.97 100.99 o 11 2 13 585.85 589.16 87.86 o 12 2 13 2399.82 2106.71 126.96 o 0 3 13 402.98 428.74 72.48 o 1 3 13 6853.97 6622.39 164.45 o 2 3 13 666.91 451.32 82.20 o 3 3 13 219.07 197.04 74.17 o 4 3 13 1189.21 1424.95 109.11 o 5 3 13 2664.12 2684.10 142.56 o 6 3 13 233.46 128.91 98.80 o 7 3 13 3105.55 3205.35 169.56 o 8 3 13 604.65 452.05 117.68 o 9 3 13 258.17 457.02 129.28 o 10 3 13 552.94 555.09 89.65 o 11 3 13 2145.07 1880.23 118.46 o 12 3 13 122.43 -19.82 84.93 o 0 4 13 4162.88 3805.99 128.65 o 1 4 13 8755.70 8324.19 182.39 o 2 4 13 528.85 523.78 80.50 o 3 4 13 2118.73 2058.98 117.63 o 4 4 13 4182.70 4046.41 153.28 o 5 4 13 5597.22 5928.03 189.58 o 6 4 13 2331.80 2071.64 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7 13 9334.39 9307.17 201.75 o 1 7 13 847.43 614.32 90.13 o 2 7 13 3256.62 2984.44 134.18 o 3 7 13 9763.27 9968.57 228.40 o 4 7 13 3305.41 3470.09 154.28 o 5 7 13 515.43 528.58 102.68 o 6 7 13 785.80 796.53 119.20 o 7 7 13 906.98 540.87 126.75 o 8 7 13 1297.13 1053.39 144.88 o 9 7 13 1284.61 1090.56 99.38 o 10 7 13 946.97 1091.36 92.49 o 11 7 13 1424.40 1405.51 111.93 o 0 8 13 12227.77 11777.26 233.24 o 1 8 13 677.43 506.80 83.90 o 2 8 13 3198.79 3152.77 139.17 o 3 8 13 1157.47 1108.54 107.88 o 4 8 13 1575.67 1268.41 129.22 o 5 8 13 1861.69 2001.22 137.25 o 6 8 13 1824.01 1887.53 141.77 o 7 8 13 1446.68 1535.91 144.12 o 8 8 13 1038.41 1023.43 141.94 o 9 8 13 810.48 993.19 96.26 o 10 8 13 19.22 49.35 75.30 o 11 8 13 636.04 793.47 96.73 o 0 9 13 4297.48 4325.79 151.85 o 1 9 13 5809.27 5634.19 176.36 o 2 9 13 3413.95 3151.01 140.59 o 3 9 13 1177.23 1256.99 108.35 o 4 9 13 991.94 1351.51 118.16 o 5 9 13 743.97 865.70 120.71 o 6 9 13 4712.00 4333.87 197.17 o 7 9 13 3224.69 3368.63 188.63 o 9 9 13 393.77 377.76 88.80 o 10 9 13 642.22 674.76 91.82 o 11 9 13 725.36 557.27 103.43 o 0 10 13 26.59 -17.08 71.15 o 1 10 13 136.20 1.51 78.42 o 2 10 13 1123.92 928.25 101.65 o 3 10 13 2171.62 2223.53 135.27 o 4 10 13 66.50 -54.54 89.46 o 5 10 13 35.20 271.96 98.04 o 6 10 13 1848.19 2102.90 146.49 o 7 10 13 1748.48 1731.15 161.68 o 8 10 13 793.79 687.04 94.19 o 9 10 13 94.79 144.00 77.85 o 10 10 13 63.19 27.46 79.55 o 0 11 13 191.05 242.33 77.85 o 1 11 13 747.93 593.43 96.45 o 2 11 13 1283.96 1231.61 112.98 o 3 11 13 1353.63 1315.81 120.81 o 4 11 13 376.73 304.63 106.92 o 5 11 13 1079.78 886.79 130.43 o 6 11 13 848.32 1138.17 139.20 o 7 11 13 425.37 349.25 86.73 o 8 11 13 1044.14 1158.10 100.61 o 9 11 13 358.16 247.81 88.42 o 10 11 13 363.24 195.06 89.74 o 0 12 13 169.29 388.51 81.16 o 1 12 13 1873.93 1968.35 125.16 o 2 12 13 2497.76 2400.60 140.75 o 3 12 13 482.17 647.95 105.03 o 4 12 13 871.10 1020.11 125.05 o 5 12 13 60.93 -66.90 100.97 o 6 12 13 610.18 513.75 86.93 o 7 12 13 188.21 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28 280.10 239.62 68.48 o 4 5 28 54.11 83.98 90.21 o 0 6 28 5.87 123.05 82.47 o 1 6 28 303.30 455.51 91.06 o 2 6 28 941.93 1067.85 109.00 o 3 6 28 222.29 262.81 68.90 o 0 7 28 1665.23 1698.04 113.73 o 1 7 28 8.68 33.03 87.00 o 2 7 28 1585.54 1960.21 121.75 o 3 7 28 302.64 300.63 68.17 o 0 8 28 29.82 -119.09 74.45 o 1 8 28 354.82 535.16 93.52 o 1 0 29 13.90 -108.80 83.80 o 2 0 29 1590.65 1768.15 124.77 o 3 0 29 624.17 729.87 260.70 o 4 0 29 4499.45 4387.57 125.11 o 0 1 29 74.78 142.59 84.36 o 1 1 29 51.62 147.30 86.91 o 2 1 29 653.31 876.33 102.68 o 3 1 29 86.72 255.66 163.49 o 4 1 29 283.56 207.91 209.21 o 0 2 29 38.12 130.22 84.83 o 1 2 29 1744.78 2102.58 127.32 o 2 2 29 588.96 607.84 100.32 o 3 2 29 563.55 639.91 113.86 o 0 3 29 1507.51 1730.85 116.37 o 1 3 29 226.07 219.31 90.59 o 2 3 29 716.76 808.58 100.13 o 3 3 29 241.07 359.50 146.27 o 0 4 29 160.17 347.55 82.48 o 1 4 29 122.80 139.38 91.91 o 2 4 29 137.54 301.12 87.95 o 3 4 29 146.35 163.21 64.73 o 0 5 29 184.01 153.53 87.95 o 1 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