#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2013120.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013120_Fobs loop_ _publ_author_name 'Qiu, Li Qin' 'Qi, Jian Ying' 'Ji, Jian Xin' 'Zhou, Zhong Yuan' 'Yeung, Chi Hung' 'Choi, Michael C. K.' 'Chan, Albert S. C.' _publ_section_title ; (R)-(6,6'-Dihydroxybiphenyl-2,2'-diyl)bis(diphenylphosphine oxide) methanol solvate ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o33 _journal_page_last o35 _journal_volume 59 _journal_year 2003 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.9351 _cell_length_b 11.1490 _cell_length_c 27.9770 _exptl_crystal_F_000 1296.00 _reflns_d_resolution_high 0.7687 _[local]_cod_data_source_file de1193Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' QLQ2 in P2(1)2(1)2(1) C36H28O4P2.CH3OH' _shelx_refln_list_code 4 _shelx_f_calc_maximum 178.97 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 18618.58 17514.78 220.97 o 4 0 0 1441.86 1354.54 80.04 o 6 0 0 542.00 565.25 68.93 o 8 0 0 136.93 170.84 49.14 o 10 0 0 683.85 700.67 83.81 o 12 0 0 4.53 -28.62 52.26 o 1 1 0 8769.83 8818.90 89.48 o 2 1 0 1091.58 1105.61 27.19 o 3 1 0 78.52 79.19 13.11 o 4 1 0 717.68 687.61 34.97 o 5 1 0 30.66 18.46 15.79 o 6 1 0 815.40 699.21 44.03 o 7 1 0 19.86 -1.26 21.68 o 8 1 0 273.60 295.92 42.05 o 9 1 0 1576.14 1615.22 79.51 o 10 1 0 34.98 70.71 30.26 o 11 1 0 0.11 15.23 30.84 o 12 1 0 3.08 11.34 42.51 o 0 2 0 3104.34 3152.82 77.36 o 1 2 0 7710.18 7780.35 66.15 o 2 2 0 74.40 80.04 9.80 o 3 2 0 5563.10 5539.86 61.23 o 4 2 0 2.16 -5.44 8.53 o 5 2 0 1182.22 1177.52 42.85 o 6 2 0 103.13 84.02 24.30 o 7 2 0 1110.44 1009.25 56.35 o 8 2 0 0.63 -3.05 22.96 o 9 2 0 0.89 -13.13 25.75 o 10 2 0 67.28 62.77 47.08 o 11 2 0 340.89 435.76 63.70 o 12 2 0 5.97 40.46 42.63 o 1 3 0 4295.02 4325.22 56.18 o 2 3 0 950.84 984.60 30.26 o 3 3 0 135.94 156.27 13.02 o 4 3 0 1309.01 1275.73 53.09 o 5 3 0 1.18 -2.53 10.70 o 6 3 0 3589.65 3529.72 97.62 o 7 3 0 17.90 22.91 27.08 o 8 3 0 809.18 689.82 70.64 o 9 3 0 442.09 464.57 87.51 o 10 3 0 32.20 71.05 62.81 o 11 3 0 4.21 -25.30 45.91 o 12 3 0 51.82 56.13 46.79 o 0 4 0 3906.68 4071.49 117.38 o 1 4 0 1142.17 1139.18 33.19 o 2 4 0 1612.42 1642.92 41.43 o 3 4 0 3739.88 3566.60 65.25 o 4 4 0 982.35 1027.62 39.12 o 5 4 0 197.93 237.13 30.27 o 6 4 0 471.24 458.88 41.51 o 7 4 0 896.39 846.08 53.58 o 8 4 0 209.78 215.73 49.18 o 9 4 0 915.53 868.15 80.97 o 10 4 0 1.72 -22.39 45.19 o 11 4 0 36.35 51.01 52.84 o 12 4 0 19.57 -9.96 70.85 o 1 5 0 3.84 -4.84 10.08 o 2 5 0 18.96 5.97 10.85 o 3 5 0 9713.22 9536.96 115.57 o 4 5 0 230.55 173.15 22.79 o 5 5 0 81.53 71.22 20.05 o 6 5 0 771.18 741.99 43.65 o 7 5 0 301.89 301.21 36.17 o 8 5 0 346.95 299.27 38.91 o 9 5 0 50.60 63.42 34.50 o 10 5 0 139.30 147.24 61.51 o 11 5 0 11.97 9.35 53.68 o 12 5 0 3.75 56.90 64.28 o 0 6 0 6434.58 6336.65 139.40 o 1 6 0 331.61 378.46 28.16 o 2 6 0 2934.94 2764.84 62.44 o 3 6 0 272.42 286.82 27.16 o 4 6 0 1606.72 1577.63 54.09 o 5 6 0 1544.84 1469.08 54.92 o 6 6 0 906.94 904.40 47.29 o 7 6 0 512.38 530.70 44.99 o 8 6 0 0.01 -21.27 21.27 o 9 6 0 56.32 63.82 45.62 o 10 6 0 23.36 44.78 46.70 o 11 6 0 0.08 -33.91 51.10 o 1 7 0 87.73 95.51 19.10 o 2 7 0 1198.40 1090.97 43.62 o 3 7 0 1040.70 981.29 43.11 o 4 7 0 1500.62 1479.58 57.21 o 5 7 0 167.59 149.83 27.54 o 6 7 0 839.33 827.24 50.94 o 7 7 0 0.73 4.18 26.23 o 8 7 0 49.83 69.71 35.74 o 9 7 0 154.42 154.23 44.74 o 10 7 0 145.54 184.36 66.61 o 11 7 0 47.67 67.66 62.09 o 0 8 0 1621.79 1575.40 78.35 o 1 8 0 368.32 396.42 34.11 o 2 8 0 7.02 -5.18 15.88 o 3 8 0 234.76 286.83 31.18 o 4 8 0 152.88 156.98 26.77 o 5 8 0 1.49 -8.48 22.03 o 6 8 0 754.97 767.70 67.49 o 7 8 0 12.56 7.10 29.37 o 8 8 0 31.11 65.51 38.40 o 9 8 0 85.63 93.44 54.21 o 10 8 0 97.32 133.30 66.36 o 1 9 0 404.36 416.55 37.62 o 2 9 0 1.66 3.76 17.51 o 3 9 0 436.52 578.61 44.13 o 4 9 0 27.70 29.31 27.77 o 5 9 0 10.46 15.68 27.24 o 6 9 0 125.28 146.49 38.73 o 7 9 0 137.35 145.82 41.85 o 8 9 0 16.07 22.40 48.47 o 9 9 0 50.96 50.70 57.03 o 10 9 0 132.47 171.36 72.92 o 0 10 0 29.93 -9.31 26.44 o 1 10 0 488.18 506.15 42.81 o 2 10 0 26.73 -3.04 24.18 o 3 10 0 174.75 187.99 39.20 o 4 10 0 1.54 -7.35 25.77 o 5 10 0 11.18 3.22 29.09 o 6 10 0 1.32 14.94 31.33 o 7 10 0 115.72 69.23 49.61 o 8 10 0 1.63 20.47 47.30 o 9 10 0 27.09 -15.55 56.23 o 1 11 0 84.76 27.80 30.74 o 2 11 0 77.90 43.08 31.97 o 3 11 0 19.84 35.48 31.73 o 4 11 0 24.10 19.83 32.74 o 5 11 0 31.33 44.09 36.39 o 6 11 0 162.93 132.43 58.78 o 7 11 0 0.08 15.36 48.79 o 8 11 0 1.67 10.96 54.55 o 0 12 0 346.12 217.52 81.95 o 1 12 0 23.35 10.06 41.53 o 2 12 0 113.50 138.85 54.82 o 3 12 0 0.09 -28.96 33.32 o 4 12 0 28.71 13.25 35.19 o 5 12 0 66.77 81.78 52.67 o 6 12 0 11.26 -1.31 47.06 o 7 12 0 14.34 48.76 59.67 o 1 13 0 7.56 -4.53 46.27 o 2 13 0 104.18 102.31 57.03 o 3 13 0 5.60 -24.46 48.93 o 4 13 0 14.06 -15.70 61.66 o 5 13 0 15.28 90.38 79.66 o 0 14 0 155.59 225.56 107.61 o 1 14 0 40.57 -40.25 48.46 o 2 14 0 0.02 -3.55 53.06 o 3 14 0 23.00 -18.00 72.38 o 1 0 1 3959.43 3586.78 49.76 o 2 0 1 4028.32 3964.87 69.04 o 3 0 1 5235.25 5220.86 133.08 o 4 0 1 539.22 498.18 37.09 o 5 0 1 57.46 99.18 25.05 o 6 0 1 200.62 218.10 36.33 o 7 0 1 782.52 742.00 49.95 o 8 0 1 845.08 866.14 59.33 o 9 0 1 399.64 402.93 44.15 o 10 0 1 369.35 469.08 51.36 o 11 0 1 160.93 152.46 40.65 o 12 0 1 2.80 -6.01 34.31 o -12 1 1 60.49 63.02 40.02 o -11 1 1 210.05 186.62 40.62 o -10 1 1 261.52 298.64 39.78 o -9 1 1 632.18 718.34 50.53 o -8 1 1 1939.61 1858.77 79.35 o -7 1 1 24.91 5.75 21.17 o -6 1 1 218.82 189.00 29.58 o -5 1 1 197.37 213.31 46.72 o -4 1 1 727.95 681.67 61.66 o -3 1 1 1523.41 1634.87 78.89 o -2 1 1 17392.26 17425.36 157.15 o -1 1 1 4173.54 4244.40 65.34 o 0 1 1 2856.92 2824.18 142.84 o 1 1 1 4163.02 4149.59 39.20 o 2 1 1 17292.20 17334.49 252.30 o 3 1 1 1550.69 1568.83 33.45 o 4 1 1 752.06 727.40 30.51 o 5 1 1 206.32 179.25 23.38 o 6 1 1 226.50 223.55 31.41 o 7 1 1 24.69 14.20 21.04 o 8 1 1 1954.27 1887.77 80.53 o 9 1 1 635.80 771.53 81.03 o 10 1 1 262.41 350.74 45.64 o 11 1 1 210.03 165.50 39.95 o 12 1 1 62.09 51.92 43.96 o -12 2 1 55.19 82.61 47.04 o -11 2 1 169.80 214.23 43.04 o -10 2 1 38.33 14.31 31.92 o -9 2 1 81.44 124.70 37.34 o -8 2 1 95.29 75.74 28.73 o -7 2 1 130.46 132.75 29.72 o -6 2 1 459.66 470.20 53.78 o -5 2 1 237.03 223.32 27.31 o -4 2 1 143.22 134.23 17.37 o -3 2 1 906.05 888.68 22.37 o -2 2 1 1735.70 1763.19 34.97 o -1 2 1 6886.20 6772.00 70.48 o 0 2 1 2964.50 3098.17 37.59 o 1 2 1 6888.46 6641.29 62.61 o 2 2 1 1729.80 1769.92 37.88 o 3 2 1 916.00 956.49 27.52 o 4 2 1 136.77 128.19 15.65 o 5 2 1 226.65 216.38 21.16 o 6 2 1 465.92 455.50 30.05 o 7 2 1 133.28 142.18 23.53 o 8 2 1 91.47 33.42 34.28 o 9 2 1 82.27 94.53 42.64 o 10 2 1 39.97 11.12 41.53 o 11 2 1 171.26 180.38 83.10 o 12 2 1 55.90 70.18 46.10 o -12 3 1 11.30 1.54 38.39 o -11 3 1 69.13 116.46 53.91 o -10 3 1 64.74 94.94 46.64 o -9 3 1 643.12 756.65 79.75 o -8 3 1 102.28 81.02 43.27 o -7 3 1 107.50 82.76 32.49 o -6 3 1 622.92 599.40 29.02 o -5 3 1 1252.20 1234.50 44.84 o -4 3 1 1979.41 2079.38 59.29 o -3 3 1 2225.05 2175.89 46.83 o -2 3 1 6301.64 5995.48 69.54 o -1 3 1 2135.02 2004.41 37.35 o 0 3 1 1588.22 1614.82 33.49 o 1 3 1 2157.49 1999.79 47.98 o 2 3 1 6280.89 5840.38 83.53 o 3 3 1 2217.30 2258.19 42.16 o 4 3 1 2000.26 2049.57 43.98 o 5 3 1 1257.80 1303.69 39.97 o 6 3 1 614.84 631.24 32.42 o 7 3 1 105.80 101.12 32.74 o 8 3 1 99.16 96.46 36.86 o 9 3 1 640.39 716.20 79.99 o 10 3 1 63.29 80.10 46.95 o 11 3 1 70.54 88.83 50.09 o 12 3 1 11.61 10.79 46.17 o -12 4 1 30.98 29.85 47.30 o -11 4 1 151.97 229.78 95.74 o -10 4 1 32.77 54.37 45.96 o -9 4 1 2.98 26.79 34.95 o -8 4 1 107.92 117.19 41.16 o -7 4 1 805.55 810.65 52.01 o -6 4 1 12.58 9.08 19.07 o -5 4 1 658.69 625.04 35.96 o -4 4 1 759.31 773.97 34.32 o -3 4 1 348.91 324.02 23.55 o -2 4 1 1787.83 1764.90 41.66 o -1 4 1 35.10 30.33 10.85 o 0 4 1 199.30 199.70 17.68 o 1 4 1 38.79 36.32 11.34 o 2 4 1 1749.75 1744.35 43.35 o 3 4 1 349.72 370.79 26.40 o 4 4 1 772.30 767.47 35.32 o 5 4 1 657.85 709.34 41.84 o 6 4 1 12.71 12.82 18.47 o 7 4 1 804.52 804.78 54.74 o 8 4 1 109.21 97.48 40.61 o 9 4 1 3.43 -13.31 33.85 o 10 4 1 31.88 72.24 46.89 o 11 4 1 153.95 151.39 61.25 o 12 4 1 29.20 1.53 82.72 o -12 5 1 10.90 2.37 62.22 o -11 5 1 13.03 14.86 54.38 o -10 5 1 61.21 51.91 63.00 o -9 5 1 13.02 30.38 31.86 o -8 5 1 246.46 247.94 42.52 o -7 5 1 13.24 -15.38 18.95 o -6 5 1 325.38 291.54 33.23 o -5 5 1 1638.17 1514.38 52.38 o -4 5 1 443.24 437.34 31.60 o -3 5 1 61.91 69.54 16.20 o -2 5 1 91.95 83.15 15.72 o -1 5 1 1462.61 1460.34 40.84 o 0 5 1 694.80 724.35 29.84 o 1 5 1 1464.09 1476.24 42.19 o 2 5 1 101.13 104.83 20.46 o 3 5 1 66.35 72.96 16.86 o 4 5 1 433.50 436.89 32.55 o 5 5 1 1646.78 1554.91 54.36 o 6 5 1 328.51 316.30 33.94 o 7 5 1 13.37 10.36 20.86 o 8 5 1 248.48 226.95 39.89 o 9 5 1 12.58 4.21 35.87 o 10 5 1 61.89 59.21 79.66 o 11 5 1 12.78 3.05 59.63 o 12 5 1 10.79 24.35 64.07 o -11 6 1 48.35 88.76 64.31 o -10 6 1 142.90 114.80 57.79 o -9 6 1 85.28 91.21 48.56 o -8 6 1 305.92 332.18 49.12 o -7 6 1 704.56 723.83 49.07 o -6 6 1 503.33 535.74 42.12 o -5 6 1 1044.72 1004.53 47.25 o -4 6 1 860.63 854.46 40.12 o -3 6 1 1398.39 1391.02 46.59 o -2 6 1 247.33 263.08 24.35 o -1 6 1 1406.01 1422.35 44.22 o 0 6 1 1509.61 1537.98 46.02 o 1 6 1 1390.96 1442.28 45.40 o 2 6 1 250.23 265.42 30.57 o 3 6 1 1398.06 1366.49 47.54 o 4 6 1 845.30 789.01 41.05 o 5 6 1 1065.49 1044.49 47.65 o 6 6 1 510.64 512.18 42.29 o 7 6 1 715.28 707.68 51.76 o 8 6 1 305.53 296.67 39.77 o 9 6 1 89.70 139.90 42.85 o 10 6 1 145.57 51.70 51.16 o 11 6 1 49.66 40.49 57.29 o -11 7 1 73.04 78.98 65.49 o -10 7 1 76.87 66.43 58.05 o -9 7 1 0.33 -18.51 32.39 o -8 7 1 211.88 269.69 47.76 o -7 7 1 345.69 369.16 48.27 o -6 7 1 682.98 689.49 46.92 o -5 7 1 1239.43 1173.31 50.23 o -4 7 1 153.36 191.74 26.22 o -3 7 1 3.58 5.23 14.79 o -2 7 1 3.14 6.55 14.24 o -1 7 1 196.82 198.81 23.93 o 0 7 1 521.54 597.14 39.17 o 1 7 1 190.75 188.29 23.95 o 2 7 1 2.65 19.76 14.50 o 3 7 1 2.74 2.00 15.52 o 4 7 1 155.62 148.20 24.88 o 5 7 1 1232.33 1140.85 52.96 o 6 7 1 690.58 668.54 48.82 o 7 7 1 345.92 295.11 38.54 o 8 7 1 218.61 272.34 49.17 o 9 7 1 0.19 -8.16 34.41 o 10 7 1 79.14 98.84 59.46 o 11 7 1 72.74 73.11 63.72 o -10 8 1 22.78 -2.28 57.72 o -9 8 1 72.43 100.02 58.58 o -8 8 1 74.73 46.72 35.76 o -7 8 1 268.68 215.18 44.35 o -6 8 1 440.34 420.84 55.88 o -5 8 1 290.89 259.90 47.24 o -4 8 1 297.38 290.66 32.51 o -3 8 1 330.27 343.50 45.66 o -2 8 1 498.87 581.66 38.31 o -1 8 1 173.82 172.57 24.97 o 0 8 1 1195.37 1199.93 47.80 o 1 8 1 170.21 165.98 27.32 o 2 8 1 499.23 560.38 39.41 o 3 8 1 326.09 349.48 38.53 o 4 8 1 302.79 250.24 31.48 o 5 8 1 296.82 303.02 34.95 o 6 8 1 442.66 455.01 52.62 o 7 8 1 270.63 320.10 50.01 o 8 8 1 74.43 44.49 35.35 o 9 8 1 71.02 55.30 41.76 o 10 8 1 22.59 44.69 58.47 o -10 9 1 2.35 10.71 58.61 o -9 9 1 6.76 -27.93 51.50 o -8 9 1 81.51 99.86 54.52 o -7 9 1 54.31 41.84 34.91 o -6 9 1 184.49 178.72 47.42 o -5 9 1 40.81 21.21 27.12 o -4 9 1 45.95 29.14 26.84 o -3 9 1 66.75 28.60 24.21 o -2 9 1 665.12 692.29 43.84 o -1 9 1 617.42 536.22 42.95 o 0 9 1 35.81 26.11 19.86 o 1 9 1 620.51 586.60 42.38 o 2 9 1 661.86 650.62 44.15 o 3 9 1 69.41 58.87 23.07 o 4 9 1 50.27 30.73 26.83 o 5 9 1 43.08 0.90 27.47 o 6 9 1 178.55 196.66 41.90 o 7 9 1 53.42 46.03 35.08 o 8 9 1 81.37 50.82 35.27 o 9 9 1 6.64 38.37 55.35 o 10 9 1 2.34 -17.59 59.66 o -9 10 1 45.01 8.64 56.32 o -8 10 1 11.13 23.27 51.67 o -7 10 1 72.20 110.93 53.02 o -6 10 1 24.12 9.56 31.26 o -5 10 1 102.01 135.22 37.77 o -4 10 1 91.45 69.60 43.21 o -3 10 1 53.98 34.22 32.23 o -2 10 1 545.19 666.96 58.35 o -1 10 1 93.84 89.26 30.76 o 0 10 1 602.32 570.88 42.99 o 1 10 1 95.64 90.97 25.55 o 2 10 1 545.46 593.02 57.20 o 3 10 1 54.67 62.16 30.55 o 4 10 1 90.11 70.44 30.71 o 5 10 1 102.14 117.59 37.46 o 6 10 1 24.13 11.91 31.22 o 7 10 1 72.25 78.32 39.32 o 8 10 1 11.01 -12.83 45.63 o 9 10 1 44.61 5.08 60.50 o -8 11 1 3.70 -48.19 48.19 o -7 11 1 29.93 -27.34 56.30 o -6 11 1 51.97 33.17 48.24 o -5 11 1 41.73 29.58 34.87 o -4 11 1 21.86 18.33 32.52 o -3 11 1 397.78 498.44 58.13 o -2 11 1 767.32 821.95 80.36 o -1 11 1 157.67 110.04 36.81 o 0 11 1 77.85 74.27 32.50 o 1 11 1 159.76 153.85 51.16 o 2 11 1 774.97 864.32 67.47 o 3 11 1 401.32 468.43 56.18 o 4 11 1 21.52 17.13 30.04 o 5 11 1 43.94 57.94 36.53 o 6 11 1 53.15 38.23 37.81 o 7 11 1 29.44 37.19 48.90 o 8 11 1 3.73 15.77 61.08 o -7 12 1 8.56 -26.52 54.84 o -6 12 1 20.78 4.01 57.09 o -5 12 1 42.54 29.26 48.27 o -4 12 1 152.09 68.74 40.15 o -3 12 1 18.52 -10.17 33.56 o -2 12 1 537.01 799.25 73.63 o -1 12 1 137.86 151.83 54.09 o 0 12 1 38.59 29.32 42.38 o 1 12 1 140.70 114.09 53.61 o 2 12 1 542.68 735.14 90.94 o 3 12 1 18.71 -24.89 40.08 o 4 12 1 154.10 179.14 46.84 o 5 12 1 43.22 82.38 41.39 o 6 12 1 20.17 32.41 49.13 o 7 12 1 8.98 -4.25 50.63 o -5 13 1 103.11 81.74 60.66 o -4 13 1 58.12 63.19 75.83 o -3 13 1 3.71 9.96 72.38 o -2 13 1 27.21 17.52 48.56 o -1 13 1 336.65 302.61 101.87 o 0 13 1 47.46 41.77 48.25 o 1 13 1 333.92 360.63 72.78 o 2 13 1 27.13 34.72 51.37 o 3 13 1 4.19 -20.58 48.58 o 4 13 1 56.95 44.62 54.30 o 5 13 1 105.09 111.06 83.87 o -3 14 1 29.27 9.96 78.12 o -2 14 1 15.86 30.25 75.06 o -1 14 1 3.22 10.18 53.75 o 0 14 1 45.10 80.25 61.06 o 1 14 1 3.28 -10.56 51.50 o 2 14 1 15.70 4.55 56.08 o 3 14 1 28.35 36.35 57.80 o 0 0 2 37.62 1.35 2.75 o 1 0 2 15460.84 15512.13 92.66 o 2 0 2 509.56 505.20 22.08 o 3 0 2 3117.78 2929.26 70.12 o 4 0 2 8.86 11.48 13.67 o 5 0 2 2455.86 2679.75 67.77 o 6 0 2 622.33 590.73 42.53 o 7 0 2 297.15 289.94 38.06 o 8 0 2 394.27 410.75 47.77 o 9 0 2 2494.66 2419.57 76.10 o 10 0 2 79.07 102.15 31.87 o 11 0 2 34.87 -20.20 29.94 o 12 0 2 64.02 46.91 37.02 o -12 1 2 180.22 233.68 50.30 o -11 1 2 98.10 120.83 37.93 o -10 1 2 136.43 121.24 29.91 o -9 1 2 5.63 14.08 21.54 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