#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2013157.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013157_Fobs loop_ _publ_author_name 'Low, John N.' 'Cobo, Justo' 'Nogueras, Manuel' 'S\'anchez, Adolfo' 'Quiroga, Jairo' 'Cisneros, Carlos' _publ_section_title ; 2-Amino-4-(4-chlorophenyl)-7,7-dimethyl-5-oxo-5,6,7,8-tetrahydro-4H-chromene-3-carbonitrile ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o38 _journal_page_last o39 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 118.118 _cell_angle_gamma 90.000 _cell_length_a 9.3867 _cell_length_b 16.5328 _cell_length_c 11.3189 _exptl_crystal_F_000 688.00 _reflns_d_resolution_high 0.7710 _[local]_cod_data_source_file gd1236Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 254 - SHELXL' _shelx_refln_list_code 4 _shelx_f_calc_maximum 189.08 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1542.30 1426.66 47.84 o 3 0 0 337.73 336.42 15.51 o 4 0 0 4240.84 4644.02 161.00 o 5 0 0 296.48 292.99 30.20 o 6 0 0 433.55 447.01 25.40 o 7 0 0 3017.22 3252.55 175.66 o 8 0 0 1158.39 1216.65 84.19 o 9 0 0 175.87 154.99 14.56 o 10 0 0 3.25 0.00 30.42 o 2 1 0 337.94 326.28 8.49 o 3 1 0 1607.28 1625.18 38.18 o 4 1 0 844.96 876.94 24.29 o 5 1 0 104.39 98.12 8.59 o 6 1 0 1083.56 1067.41 33.68 o 7 1 0 71.98 60.92 8.13 o 8 1 0 54.98 52.04 15.74 o 9 1 0 0.37 0.00 13.61 o 10 1 0 12.53 15.21 21.51 o 1 2 0 113.97 113.63 6.82 o 2 2 0 5047.15 4610.71 113.61 o 3 2 0 442.89 424.10 15.21 o 4 2 0 231.56 251.12 9.63 o 5 2 0 138.47 114.85 7.62 o 6 2 0 997.48 1015.26 35.73 o 7 2 0 529.78 534.16 37.74 o 8 2 0 39.83 67.59 22.06 o 9 2 0 156.25 175.27 21.51 o 10 2 0 183.86 264.24 76.13 o 1 3 0 3099.40 2864.89 71.49 o 2 3 0 1094.57 1072.14 26.52 o 3 3 0 431.58 446.58 10.80 o 4 3 0 1208.13 1424.74 43.84 o 5 3 0 78.75 65.44 7.64 o 6 3 0 2.05 3.81 7.62 o 7 3 0 94.82 94.11 11.51 o 8 3 0 139.94 147.63 16.43 o 9 3 0 3.81 10.14 15.21 o 10 3 0 1.65 20.28 17.56 o 0 4 0 1822.13 1608.84 59.01 o 1 4 0 2082.42 1992.24 55.85 o 2 4 0 553.30 517.25 13.02 o 3 4 0 1045.91 1057.36 26.46 o 4 4 0 105.34 92.20 6.80 o 5 4 0 3.57 -3.05 6.83 o 6 4 0 20.47 15.25 7.64 o 7 4 0 147.70 128.01 15.27 o 8 4 0 547.29 537.08 29.48 o 9 4 0 51.20 52.17 22.15 o 10 4 0 178.35 227.72 28.82 o 1 5 0 2632.58 2385.50 60.55 o 2 5 0 986.55 1052.28 22.56 o 3 5 0 4281.30 4390.90 110.34 o 4 5 0 4156.70 4481.51 101.33 o 5 5 0 10.65 15.29 7.64 o 6 5 0 438.79 460.38 18.26 o 7 5 0 175.73 156.05 13.65 o 8 5 0 14.58 10.88 9.18 o 9 5 0 37.46 -0.03 25.10 o 10 5 0 280.24 238.32 32.92 o 0 6 0 1522.59 1338.54 51.10 o 1 6 0 356.78 340.59 12.44 o 2 6 0 12.09 19.05 7.61 o 3 6 0 8.87 19.03 7.64 o 4 6 0 119.55 112.25 8.84 o 5 6 0 333.94 333.15 13.60 o 6 6 0 68.21 55.30 8.19 o 7 6 0 212.52 223.25 15.44 o 8 6 0 911.87 879.27 43.25 o 9 6 0 25.88 20.32 17.59 o 10 6 0 16.41 32.34 19.47 o 1 7 0 179.63 168.99 7.64 o 2 7 0 4602.78 4566.71 94.31 o 3 7 0 3768.26 4018.95 109.65 o 4 7 0 662.69 740.55 21.39 o 5 7 0 2362.09 2561.37 75.53 o 6 7 0 80.24 79.93 7.40 o 7 7 0 58.31 57.91 13.65 o 8 7 0 31.71 17.93 9.91 o 9 7 0 11.75 -3.79 19.47 o 10 7 0 14.14 -3.81 19.50 o 0 8 0 39.61 45.94 10.86 o 1 8 0 1644.99 1597.52 45.92 o 2 8 0 65.56 64.10 6.84 o 3 8 0 40.13 30.46 7.61 o 4 8 0 55.43 38.12 7.62 o 5 8 0 0.12 0.00 6.82 o 6 8 0 1055.16 1033.60 36.36 o 7 8 0 375.59 382.09 22.50 o 8 8 0 38.67 15.24 17.59 o 9 8 0 9.75 25.38 26.38 o 1 9 0 81.55 60.15 7.64 o 2 9 0 23.94 15.31 8.81 o 3 9 0 371.15 348.40 13.67 o 4 9 0 67.60 54.94 7.61 o 5 9 0 0.54 0.00 7.62 o 6 9 0 20.71 10.88 8.44 o 7 9 0 199.58 181.04 15.46 o 8 9 0 45.73 66.05 17.59 o 9 9 0 54.50 48.48 28.54 o 0 10 0 0.13 0.00 15.36 o 1 10 0 44.14 43.61 7.64 o 2 10 0 177.65 165.84 10.33 o 3 10 0 2.13 3.04 6.80 o 4 10 0 8.29 9.13 6.80 o 5 10 0 123.59 122.87 15.25 o 6 10 0 15.01 7.64 15.25 o 7 10 0 0.79 -12.51 12.51 o 8 10 0 8.18 7.66 21.57 o 9 10 0 1.28 -7.59 32.32 o 1 11 0 592.43 588.20 22.97 o 2 11 0 34.99 33.61 6.86 o 3 11 0 2.49 9.18 8.54 o 4 11 0 242.66 244.52 13.67 o 5 11 0 63.28 61.03 15.25 o 6 11 0 0.02 -2.54 9.62 o 7 11 0 60.77 76.36 45.78 o 8 11 0 6.17 6.10 25.40 o 9 11 0 171.90 137.37 43.18 o 0 12 0 52.54 22.97 10.86 o 1 12 0 514.44 555.36 20.92 o 2 12 0 137.65 133.08 11.59 o 3 12 0 0.08 -7.61 8.83 o 4 12 0 22.70 20.33 7.38 o 5 12 0 228.47 209.88 17.98 o 6 12 0 186.70 175.64 37.85 o 7 12 0 8.83 22.84 22.89 o 8 12 0 22.51 53.39 32.37 o 1 13 0 178.53 165.69 11.52 o 2 13 0 286.73 285.99 18.34 o 3 13 0 731.81 723.02 33.35 o 4 13 0 7.22 5.70 8.14 o 5 13 0 628.17 668.69 43.28 o 6 13 0 564.34 519.31 43.42 o 7 13 0 232.45 199.58 32.37 o 8 13 0 45.98 61.07 32.37 o 0 14 0 579.28 672.61 47.77 o 1 14 0 0.09 5.15 12.04 o 2 14 0 1.80 -8.70 10.04 o 3 14 0 0.86 6.54 13.32 o 4 14 0 116.25 134.00 17.13 o 5 14 0 248.39 264.43 33.50 o 6 14 0 1.14 15.29 32.37 o 7 14 0 4.40 0.00 30.57 o 8 14 0 195.87 226.67 47.73 o 1 15 0 71.10 70.19 15.52 o 2 15 0 4.34 1.70 7.40 o 3 15 0 268.52 274.41 30.87 o 4 15 0 525.97 564.55 40.54 o 5 15 0 11.99 30.57 30.57 o 6 15 0 277.59 310.37 53.39 o 7 15 0 99.13 99.25 32.37 o 0 16 0 1442.95 1488.78 106.43 o 1 16 0 337.44 334.48 25.94 o 2 16 0 3.63 12.74 9.67 o 3 16 0 130.49 115.83 31.13 o 4 16 0 34.09 0.00 30.50 o 5 16 0 0.49 -9.13 25.45 o 6 16 0 215.64 193.97 36.62 o 7 16 0 146.23 137.48 53.47 o 1 17 0 21.59 49.25 29.71 o 2 17 0 61.11 61.14 21.62 o 3 17 0 12.68 24.43 25.39 o 4 17 0 7.03 12.18 25.36 o 5 17 0 50.39 30.50 21.57 o 6 17 0 291.92 301.66 47.69 o 0 18 0 0.13 0.00 30.57 o 1 18 0 155.66 138.27 32.37 o 2 18 0 197.49 221.81 32.43 o 3 18 0 10.33 -7.64 21.62 o 4 18 0 311.36 297.24 44.58 o 5 18 0 35.20 7.59 22.89 o 1 19 0 249.48 376.66 59.94 o 2 19 0 14.29 22.93 38.10 o 3 19 0 17.45 61.07 21.62 o 4 19 0 16.92 33.60 25.39 o 0 20 0 803.18 1069.01 152.72 o 1 20 0 182.63 203.66 36.60 o 2 20 0 173.94 182.94 36.64 o 3 20 0 92.46 43.66 36.70 o 1 21 0 18.34 -13.05 36.60 o 2 21 0 2.48 52.37 36.64 o -11 1 1 48.52 -3.04 25.31 o -10 1 1 47.40 42.59 25.31 o -9 1 1 98.23 106.48 17.93 o -8 1 1 61.70 47.20 9.21 o -7 1 1 5.56 -4.35 8.44 o -6 1 1 0.14 11.47 11.00 o -5 1 1 1588.46 1593.23 36.44 o -4 1 1 1820.55 1811.66 43.46 o -3 1 1 671.70 626.36 16.46 o -2 1 1 10931.08 9828.33 188.39 o 1 1 1 1436.51 1310.13 30.89 o 2 1 1 8593.69 8106.13 192.39 o 3 1 1 154.13 119.51 7.62 o 4 1 1 1869.51 1911.21 48.59 o 5 1 1 493.50 489.08 15.27 o 6 1 1 367.36 361.73 16.45 o 7 1 1 25.61 35.55 9.63 o 8 1 1 24.23 26.76 15.25 o 9 1 1 186.78 177.28 36.54 o 10 1 1 72.49 48.74 25.31 o -11 2 1 39.06 36.94 36.51 o -10 2 1 31.17 -7.61 32.27 o -9 2 1 88.53 83.74 21.51 o -8 2 1 703.33 677.39 33.65 o -7 2 1 2059.68 2274.81 79.72 o -6 2 1 293.36 285.89 10.44 o -5 2 1 226.22 217.71 7.41 o -4 2 1 33.94 46.89 7.64 o -3 2 1 2426.34 2341.45 54.14 o -2 2 1 1713.77 1679.39 39.66 o -1 2 1 200.93 194.85 6.82 o 0 2 1 5439.10 4506.38 195.43 o 1 2 1 1761.11 1505.88 33.83 o 2 2 1 1431.04 1329.87 35.68 o 3 2 1 382.16 382.75 13.66 o 4 2 1 855.35 974.59 23.88 o 5 2 1 0.03 11.44 7.62 o 6 2 1 255.48 302.78 19.52 o 7 2 1 328.06 286.78 19.97 o 8 2 1 124.29 134.12 22.25 o 9 2 1 2.77 30.42 25.31 o 10 2 1 5.44 22.89 38.10 o -10 3 1 45.28 45.63 45.63 o -9 3 1 69.64 117.83 45.48 o -8 3 1 24.65 10.15 9.63 o -7 3 1 514.72 500.48 19.95 o -6 3 1 42.53 50.50 7.62 o -5 3 1 224.27 210.89 11.51 o -4 3 1 1035.84 990.86 22.85 o -3 3 1 2885.74 2795.17 51.66 o -1 3 1 1063.50 961.28 24.34 o 1 3 1 4989.44 4630.00 117.46 o 2 3 1 572.33 557.54 13.78 o 3 3 1 620.79 643.57 22.14 o 4 3 1 3533.19 3759.66 87.57 o 5 3 1 371.80 392.88 15.25 o 6 3 1 70.13 75.67 13.09 o 7 3 1 0.03 -7.62 7.62 o 8 3 1 47.59 63.49 22.07 o 9 3 1 0.57 -10.19 19.15 o 10 3 1 35.08 30.42 22.14 o -10 4 1 128.75 179.84 28.54 o -9 4 1 72.65 76.08 17.59 o -8 4 1 523.28 497.24 25.86 o -7 4 1 1069.10 1135.21 44.77 o -6 4 1 254.83 269.16 18.57 o -5 4 1 418.77 429.96 25.57 o -4 4 1 305.96 351.11 13.24 o -3 4 1 487.68 539.52 15.46 o -2 4 1 4661.30 4593.71 96.26 o -1 4 1 26020.15 23153.56 563.87 o 0 4 1 3446.88 3175.42 103.71 o 1 4 1 3685.98 3632.18 81.25 o 2 4 1 317.58 312.93 10.07 o 3 4 1 187.75 199.38 6.80 o 4 4 1 69.95 85.08 6.96 o 5 4 1 231.68 233.86 10.81 o 6 4 1 155.33 136.14 9.18 o 7 4 1 222.61 215.09 14.26 o 8 4 1 654.08 592.65 32.35 o 9 4 1 8.89 15.21 14.38 o 10 4 1 92.20 189.15 35.16 o -10 5 1 396.84 401.78 43.94 o -9 5 1 14.20 25.39 17.59 o -8 5 1 93.28 93.85 11.16 o -7 5 1 669.63 697.71 30.63 o -6 5 1 1.01 6.08 8.53 o -5 5 1 6.51 9.16 6.83 o -4 5 1 472.24 411.12 12.42 o -3 5 1 937.76 934.02 20.42 o -2 5 1 1520.47 1520.30 35.65 o -1 5 1 1890.10 1867.03 55.68 o 0 5 1 15.66 15.21 15.21 o 1 5 1 285.76 279.15 7.66 o 2 5 1 528.93 440.15 12.93 o 3 5 1 47.33 43.71 6.83 o 4 5 1 362.32 408.19 13.60 o 5 5 1 112.46 110.90 8.68 o 6 5 1 0.84 0.00 6.83 o 7 5 1 184.26 173.82 16.22 o 8 5 1 47.62 30.51 13.66 o 9 5 1 1.22 10.16 17.59 o 10 5 1 85.54 73.36 28.54 o -10 6 1 32.82 15.21 23.44 o -9 6 1 17.35 15.24 17.59 o -8 6 1 13.49 9.87 14.71 o -7 6 1 337.63 311.80 21.05 o -6 6 1 401.08 402.01 16.63 o -5 6 1 64.97 74.80 6.83 o -4 6 1 19.42 18.30 6.83 o -3 6 1 136.97 125.89 6.83 o -2 6 1 1.57 0.00 15.36 o -1 6 1 2256.26 2055.79 57.37 o 0 6 1 29.04 15.29 10.81 o 1 6 1 1908.48 1777.61 48.94 o 2 6 1 427.23 407.74 13.63 o 3 6 1 706.55 738.46 17.01 o 4 6 1 10.87 0.00 6.83 o 5 6 1 692.33 703.51 22.52 o 6 6 1 1929.68 2046.19 73.09 o 7 6 1 1015.85 1092.59 49.95 o 8 6 1 2.92 -3.04 11.52 o 9 6 1 21.62 59.53 28.52 o -10 7 1 10.12 15.21 30.57 o -9 7 1 0.75 20.92 19.47 o -8 7 1 88.60 71.66 24.30 o -7 7 1 124.87 107.26 18.45 o -6 7 1 421.63 452.90 21.55 o -5 7 1 1258.31 1303.53 33.04 o -4 7 1 7.01 0.00 6.83 o -3 7 1 1090.45 1243.48 30.82 o -2 7 1 4.12 -3.06 6.84 o -1 7 1 1.08 -5.09 8.81 o 0 7 1 20.98 15.36 15.36 o 1 7 1 2298.38 2270.17 60.85 o 2 7 1 54.94 46.77 6.82 o 3 7 1 351.84 367.22 10.86 o 4 7 1 150.80 154.38 6.75 o 5 7 1 0.23 -5.09 7.40 o 6 7 1 77.58 74.84 10.80 o 7 7 1 192.05 190.94 20.37 o 8 7 1 143.85 126.27 19.48 o 9 7 1 3.92 12.21 53.31 o -10 8 1 5.43 -10.16 19.15 o -9 8 1 7.09 2.21 22.19 o -8 8 1 158.10 173.91 19.48 o -7 8 1 335.32 320.61 19.54 o -6 8 1 41.26 45.78 21.69 o -5 8 1 176.60 159.99 7.62 o -4 8 1 7.26 25.40 8.78 o -3 8 1 1211.81 1258.98 38.71 o -2 8 1 842.50 848.93 23.91 o -1 8 1 8.76 22.97 7.64 o 0 8 1 633.35 662.07 23.52 o 1 8 1 3589.12 3596.08 92.68 o 2 8 1 40.36 42.77 6.82 o 3 8 1 87.00 74.94 6.83 o 4 8 1 496.73 547.29 18.31 o 5 8 1 480.79 478.73 20.51 o 6 8 1 514.03 471.31 23.81 o 7 8 1 14.83 23.94 16.11 o 8 8 1 31.05 40.63 17.59 o 9 8 1 32.88 39.20 22.19 o -10 9 1 30.47 28.57 19.50 o -9 9 1 20.94 15.36 30.57 o -8 9 1 27.97 49.52 12.43 o -7 9 1 89.87 91.93 15.12 o -6 9 1 0.05 22.94 12.43 o -5 9 1 468.37 454.03 24.22 o -4 9 1 43.70 36.57 6.80 o -3 9 1 251.44 274.22 10.84 o -2 9 1 317.09 311.31 12.52 o -1 9 1 2.78 0.00 8.84 o 0 9 1 67.33 78.01 7.66 o 1 9 1 320.31 302.72 15.32 o 2 9 1 126.35 141.92 8.12 o 3 9 1 591.03 632.48 20.50 o 4 9 1 110.10 108.25 9.10 o 5 9 1 29.90 34.35 7.62 o 6 9 1 348.89 340.12 24.27 o 7 9 1 28.91 32.87 15.46 o 8 9 1 2.47 7.63 12.43 o 9 9 1 16.66 14.06 23.45 o -9 10 1 170.54 166.42 26.40 o -8 10 1 1.83 30.50 30.57 o -7 10 1 89.35 87.72 19.52 o -6 10 1 212.56 209.61 17.94 o -5 10 1 28.13 22.91 8.83 o -4 10 1 91.69 90.44 9.27 o -3 10 1 372.03 393.16 13.67 o -2 10 1 84.22 78.01 7.64 o -1 10 1 442.39 371.80 15.32 o 0 10 1 564.48 591.27 41.18 o 1 10 1 117.64 138.53 7.64 o 2 10 1 11.17 3.07 6.86 o 3 10 1 399.33 428.38 17.98 o 4 10 1 20.15 38.11 7.61 o 5 10 1 131.71 128.65 10.82 o 6 10 1 176.62 165.12 16.44 o 7 10 1 79.86 58.69 24.73 o 8 10 1 14.56 22.87 21.57 o 9 10 1 36.43 25.44 38.10 o -9 11 1 8.66 -25.34 25.34 o -8 11 1 1.96 7.59 21.57 o -7 11 1 47.88 30.46 21.57 o -6 11 1 152.98 156.10 16.44 o -5 11 1 0.44 0.00 11.51 o -4 11 1 74.26 64.84 15.29 o -3 11 1 108.86 99.61 8.47 o -2 11 1 771.48 800.54 29.11 o -1 11 1 17.09 15.32 7.68 o 0 11 1 302.17 291.50 22.26 o 1 11 1 904.19 977.72 33.81 o 2 11 1 397.36 417.67 16.76 o 3 11 1 1157.78 1241.54 54.36 o 4 11 1 106.67 78.72 9.63 o 5 11 1 604.54 643.25 26.29 o 6 11 1 47.34 42.70 11.51 o 7 11 1 91.65 61.07 21.57 o 8 11 1 1.64 0.00 21.57 o -9 12 1 4.63 -22.89 32.37 o -8 12 1 97.82 148.17 25.43 o -7 12 1 81.70 92.62 21.57 o -6 12 1 42.02 50.83 19.15 o -5 12 1 1100.02 1160.87 54.14 o -4 12 1 7.40 17.40 9.19 o -3 12 1 0.89 12.24 6.84 o -2 12 1 842.09 838.02 33.80 o -1 12 1 929.72 962.56 35.84 o 0 12 1 535.32 519.91 32.55 o 1 12 1 1223.86 1270.87 50.58 o 2 12 1 308.46 314.30 20.02 o 3 12 1 153.72 168.11 13.67 o 4 12 1 20.00 25.46 10.78 o 5 12 1 911.94 1007.15 40.29 o 6 12 1 45.29 26.37 13.05 o 7 12 1 441.86 574.13 58.71 o 8 12 1 38.98 7.64 32.43 o -8 13 1 17.13 7.68 22.89 o -7 13 1 57.70 22.89 21.62 o -6 13 1 276.80 267.16 32.37 o -5 13 1 476.03 475.13 32.98 o -4 13 1 8.65 9.51 8.14 o -3 13 1 27.28 15.34 8.21 o -2 13 1 9.48 6.53 8.47 o -1 13 1 544.85 545.21 22.93 o 0 13 1 2.11 -2.20 8.52 o 1 13 1 495.05 483.94 35.35 o 2 13 1 251.06 237.22 22.12 o 3 13 1 61.54 61.22 9.25 o 4 13 1 488.77 515.32 28.35 o 5 13 1 416.94 383.56 22.52 o 6 13 1 2.43 39.69 45.78 o 7 13 1 1.41 6.09 30.57 o 8 13 1 198.74 218.41 43.24 o -8 14 1 89.23 117.82 36.62 o -7 14 1 426.07 495.93 60.69 o -6 14 1 19.90 7.62 21.57 o -5 14 1 189.15 180.81 22.23 o -4 14 1 10.27 7.62 8.41 o -3 14 1 90.41 82.62 10.78 o -2 14 1 15.71 10.19 15.46 o -1 14 1 245.79 245.09 17.65 o 0 14 1 332.81 397.79 24.33 o 1 14 1 185.08 166.00 15.31 o 2 14 1 60.71 76.51 15.32 o 3 14 1 18.33 12.75 10.84 o 4 14 1 0.50 11.11 16.47 o 5 14 1 346.22 354.09 25.90 o 6 14 1 159.14 178.69 32.37 o 7 14 1 0.08 12.24 25.43 o -8 15 1 85.93 96.03 36.65 o -7 15 1 22.14 36.66 30.57 o -6 15 1 281.64 290.90 32.37 o -5 15 1 71.12 38.18 22.97 o -4 15 1 306.89 320.39 28.61 o -3 15 1 45.28 28.05 10.83 o -2 15 1 1339.30 1467.58 63.30 o -1 15 1 247.39 236.03 20.02 o 0 15 1 9.94 -0.03 11.52 o 1 15 1 21.94 10.94 8.83 o 2 15 1 30.17 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