#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2013202.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013202_Fobs loop_ _publ_author_name 'Low, John N.' 'Arranz, Paloma' 'Cuesta, Rafael' 'Guti\'errez, M. Dolores' 'Glidewell, Christopher' _publ_section_title ; Bis[\m-6-amino-3-methyl-5-nitrosopyrimidine-2,4(1H,3H)-dionato-\k^3^O^4^,N^5^:O^5^]-di-\m-aqua-bis{diaqua[6-amino-3-methyl-5-nitrosopyrimidine-2,4(1H,3H)-dionato-\k^2^N^1^,O^2^]strontium(II)}: centrosymmetric dimers containing nine-coordinate Sr, linked by multiple hydrogen bonds into a three-dimensional framework ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m21 _journal_page_last m24 _journal_volume 59 _journal_year 2003 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 69.965 _cell_angle_beta 77.518 _cell_angle_gamma 72.361 _cell_length_a 6.9388 _cell_length_b 9.8852 _cell_length_c 14.1962 _exptl_crystal_F_000 484.00 _reflns_d_resolution_high 0.7708 _[local]_cod_data_source_file sk1602IIIsup2.hkl _[local]_cod_data_source_block III #BEGIN Tags that were not found in dictionaries: _shelx_title ' amnalk-sr P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 170.48 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 8654.43 7654.30 174.89 o 2 0 0 78.77 70.94 3.63 o 3 0 0 916.04 860.31 17.89 o 4 0 0 58.09 57.91 2.93 o 5 0 0 162.94 160.49 5.79 o 6 0 0 554.38 587.88 14.29 o 7 0 0 696.14 717.38 25.11 o 8 0 0 407.81 408.57 28.86 o -8 1 0 419.02 429.09 26.00 o -7 1 0 431.91 461.57 32.50 o -6 1 0 577.64 587.41 18.11 o -5 1 0 205.11 196.57 6.32 o -4 1 0 391.05 406.49 9.09 o -3 1 0 247.86 237.70 4.80 o -2 1 0 34.28 38.17 3.61 o -1 1 0 2432.35 2276.07 50.14 o 1 1 0 6149.02 5715.01 121.36 o 2 1 0 1058.55 1042.00 19.51 o 3 1 0 408.43 327.21 6.47 o 4 1 0 173.66 180.20 8.17 o 5 1 0 385.98 380.73 9.54 o 6 1 0 1055.29 1127.44 24.26 o 7 1 0 594.31 608.51 18.77 o 8 1 0 239.03 217.57 12.79 o -8 2 0 262.87 252.29 26.89 o -7 2 0 646.77 638.45 65.02 o -6 2 0 563.86 587.78 21.17 o -5 2 0 7.29 16.88 4.68 o -4 2 0 82.10 84.24 3.55 o -3 2 0 1082.21 1147.32 24.69 o -2 2 0 109.34 119.69 3.22 o -1 2 0 1799.74 1796.93 44.39 o 0 2 0 3599.39 3303.54 76.45 o 1 2 0 332.66 350.35 7.23 o 2 2 0 4507.56 4357.26 107.92 o 3 2 0 91.44 115.83 3.23 o 4 2 0 17.75 16.58 3.81 o 5 2 0 52.21 48.92 4.19 o 6 2 0 1156.63 1211.23 44.68 o 7 2 0 1537.90 1570.72 51.78 o 8 2 0 59.98 54.42 6.83 o -7 3 0 375.43 346.26 23.78 o -6 3 0 893.98 921.18 36.31 o -5 3 0 565.27 574.23 19.03 o -4 3 0 1262.17 1359.32 29.71 o -3 3 0 1139.70 1164.55 30.05 o -2 3 0 3317.28 3434.97 67.84 o -1 3 0 12999.31 12645.37 240.56 o 0 3 0 3171.12 3155.98 67.57 o 1 3 0 867.91 874.90 20.14 o 2 3 0 2425.30 2502.34 53.91 o 3 3 0 52.84 45.69 3.29 o 4 3 0 28.31 33.27 5.17 o 5 3 0 366.18 360.09 12.30 o 6 3 0 962.60 1018.14 28.92 o 7 3 0 285.90 261.57 21.85 o 8 3 0 431.29 440.33 31.09 o -7 4 0 201.26 196.77 21.08 o -6 4 0 625.58 644.84 43.49 o -5 4 0 309.09 305.16 14.35 o -4 4 0 236.22 245.72 10.25 o -3 4 0 10.23 5.67 3.17 o -2 4 0 4658.95 4844.79 97.03 o -1 4 0 9308.18 9445.13 173.75 o 0 4 0 8289.35 8368.97 183.07 o 1 4 0 2883.81 2758.51 62.52 o 2 4 0 1257.78 1266.99 23.64 o 3 4 0 3.46 4.30 3.20 o 4 4 0 32.88 42.23 4.16 o 5 4 0 1346.44 1449.59 33.08 o 6 4 0 1763.10 1851.38 66.10 o 7 4 0 678.69 654.33 23.87 o 8 4 0 201.65 192.31 30.65 o -6 5 0 422.72 383.68 44.34 o -5 5 0 27.20 27.69 7.99 o -4 5 0 43.12 26.59 6.44 o -3 5 0 133.74 152.65 6.05 o -2 5 0 447.36 429.99 11.29 o -1 5 0 1977.27 2107.19 42.90 o 0 5 0 830.11 859.27 16.52 o 1 5 0 2243.39 2190.87 42.20 o 2 5 0 5.48 7.16 3.58 o 3 5 0 16.37 20.31 3.57 o 4 5 0 372.46 407.41 15.97 o 5 5 0 1398.43 1448.70 38.55 o 6 5 0 829.84 838.77 27.93 o 7 5 0 551.07 546.42 25.09 o 8 5 0 116.80 122.45 20.41 o -6 6 0 148.66 122.20 19.14 o -5 6 0 8.81 -3.43 9.71 o -4 6 0 542.16 504.48 18.07 o -3 6 0 1489.42 1499.80 39.56 o -2 6 0 267.99 264.54 12.20 o -1 6 0 438.14 467.82 11.07 o 0 6 0 600.16 599.58 14.22 o 1 6 0 223.35 245.24 6.37 o 2 6 0 206.62 225.66 6.37 o 3 6 0 73.89 69.62 3.44 o 4 6 0 309.76 333.35 9.47 o 5 6 0 649.73 623.70 18.81 o 6 6 0 283.67 285.16 12.70 o 7 6 0 558.64 522.08 41.26 o 8 6 0 76.32 108.59 20.36 o -5 7 0 13.73 13.61 9.63 o -4 7 0 553.13 490.81 26.29 o -3 7 0 550.62 591.52 18.85 o -2 7 0 814.10 888.07 39.51 o -1 7 0 4773.34 4974.21 114.13 o 0 7 0 570.04 582.45 18.06 o 1 7 0 25.66 26.85 7.62 o 2 7 0 20.52 11.32 3.17 o 3 7 0 19.77 18.95 3.15 o 4 7 0 622.83 638.80 19.33 o 5 7 0 486.81 493.40 16.36 o 6 7 0 265.71 249.44 15.36 o 7 7 0 369.62 390.80 21.36 o 8 7 0 239.65 229.85 27.05 o -4 8 0 89.94 88.50 14.45 o -3 8 0 446.90 461.33 19.03 o -2 8 0 204.49 262.40 37.40 o -1 8 0 47.64 50.41 5.10 o 0 8 0 3919.59 4106.54 110.78 o 1 8 0 631.53 680.24 18.23 o 2 8 0 25.07 30.39 5.12 o 3 8 0 42.04 37.96 4.50 o 4 8 0 561.05 538.99 17.48 o 5 8 0 564.65 566.23 34.03 o 6 8 0 287.61 308.76 20.52 o 7 8 0 238.24 230.74 20.38 o -4 9 0 8.10 -3.36 23.53 o -3 9 0 311.72 291.71 21.19 o -1 9 0 894.33 933.63 31.40 o 0 9 0 866.65 935.88 34.31 o 1 9 0 302.82 276.39 12.02 o 2 9 0 143.65 123.96 9.07 o 3 9 0 270.63 254.87 10.42 o 4 9 0 60.55 34.34 13.74 o 5 9 0 338.93 334.43 18.57 o 6 9 0 753.52 723.49 43.19 o 7 9 0 166.32 168.46 20.24 o 0 10 0 195.08 157.19 20.52 o 1 10 0 110.66 101.97 9.98 o 2 10 0 33.00 30.55 9.01 o 3 10 0 315.90 294.42 18.26 o 4 10 0 232.85 232.08 31.82 o 5 10 0 80.45 65.89 10.15 o 6 10 0 334.70 363.35 33.67 o -1 11 0 743.11 694.48 40.09 o 0 11 0 486.58 457.35 30.71 o 1 11 0 175.25 162.22 15.95 o 2 11 0 224.12 194.84 29.70 o 3 11 0 151.16 160.66 16.90 o 4 11 0 138.28 118.72 14.29 o 5 11 0 75.35 87.14 20.11 o 2 12 0 6.12 6.68 14.17 o -4 -11 1 790.01 803.29 47.01 o -3 -11 1 551.73 585.99 47.18 o -2 -11 1 1160.51 1233.84 92.96 o -1 -11 1 4.85 0.00 14.30 o 0 -11 1 89.69 60.48 14.26 o -6 -10 1 27.89 20.15 13.44 o -5 -10 1 233.74 219.86 14.33 o -4 -10 1 224.27 205.65 20.36 o -3 -10 1 306.63 276.83 15.78 o -2 -10 1 505.33 486.15 38.15 o -1 -10 1 151.08 126.73 12.77 o 0 -10 1 120.54 103.95 8.71 o 1 -10 1 122.53 121.54 27.10 o 2 -10 1 359.61 343.93 37.03 o -7 -9 1 26.11 26.91 13.46 o -6 -9 1 379.43 385.74 33.87 o -5 -9 1 912.90 904.00 50.43 o -4 -9 1 190.43 195.18 11.48 o -3 -9 1 288.68 290.17 12.65 o -2 -9 1 418.87 422.46 17.74 o -1 -9 1 13.17 7.90 5.45 o 0 -9 1 7.19 5.17 6.89 o 1 -9 1 30.45 10.28 12.12 o 2 -9 1 41.03 35.14 13.64 o 3 -9 1 502.19 480.92 33.51 o -7 -8 1 91.09 81.26 13.54 o -6 -8 1 672.17 662.72 43.40 o -5 -8 1 643.34 650.38 44.96 o -4 -8 1 912.06 925.15 28.01 o -3 -8 1 437.22 429.61 13.51 o -2 -8 1 130.80 133.98 6.37 o -1 -8 1 177.99 184.96 17.29 o 0 -8 1 782.61 826.57 22.61 o 1 -8 1 82.19 81.24 21.02 o 2 -8 1 270.53 227.34 19.55 o 3 -8 1 758.88 741.37 32.51 o 4 -8 1 848.39 886.71 95.16 o -7 -7 1 49.87 54.52 13.63 o -6 -7 1 1215.29 1167.78 55.90 o -5 -7 1 491.72 462.21 14.59 o -4 -7 1 1642.53 1792.24 48.19 o -3 -7 1 908.23 965.82 26.32 o -2 -7 1 383.36 399.27 17.41 o -1 -7 1 92.67 95.65 6.31 o 0 -7 1 1.05 -2.64 3.76 o 1 -7 1 1707.71 1800.56 42.38 o 2 -7 1 2194.73 2225.74 66.85 o 3 -7 1 154.32 166.31 10.08 o 4 -7 1 784.96 844.33 34.59 o -8 -6 1 2.68 6.78 13.56 o -7 -6 1 132.75 110.14 9.70 o -6 -6 1 1145.69 1210.02 46.08 o -5 -6 1 386.36 360.46 18.36 o -4 -6 1 655.71 682.46 17.43 o -3 -6 1 1352.16 1423.20 34.69 o -2 -6 1 1170.97 1204.73 25.33 o -1 -6 1 400.83 400.98 9.54 o 0 -6 1 48.99 60.01 9.14 o 1 -6 1 27.15 28.27 4.24 o 2 -6 1 133.06 138.69 8.12 o 3 -6 1 2522.14 2746.83 64.20 o 4 -6 1 418.18 479.99 19.05 o 5 -6 1 265.22 298.53 19.41 o 6 -6 1 17.54 28.40 11.25 o -8 -5 1 2.76 0.00 13.60 o -7 -5 1 167.41 128.99 18.20 o -6 -5 1 840.38 874.17 34.73 o -5 -5 1 1148.06 1198.87 32.48 o -4 -5 1 29.63 39.06 5.35 o -3 -5 1 255.50 230.25 7.46 o -2 -5 1 2749.63 2938.13 56.21 o -1 -5 1 157.76 151.50 10.28 o 0 -5 1 251.01 284.21 8.65 o 1 -5 1 77.50 94.02 3.81 o 2 -5 1 1360.75 1362.38 31.62 o 3 -5 1 1254.20 1332.32 32.09 o 4 -5 1 155.83 159.16 8.23 o 5 -5 1 578.81 571.87 28.16 o 6 -5 1 100.05 85.36 14.47 o -8 -4 1 3.18 -6.80 6.80 o -7 -4 1 65.07 66.65 6.92 o -6 -4 1 377.83 366.02 11.66 o -5 -4 1 991.43 1007.26 25.21 o -4 -4 1 222.41 217.50 9.76 o -3 -4 1 820.81 837.96 17.78 o -2 -4 1 132.75 157.49 4.93 o -1 -4 1 24.40 12.93 3.21 o 0 -4 1 2008.64 2066.14 42.53 o 1 -4 1 135.06 108.72 3.70 o 2 -4 1 613.36 588.70 14.27 o 3 -4 1 1648.57 1734.72 39.83 o 4 -4 1 750.09 731.39 23.18 o 5 -4 1 782.98 792.07 34.30 o 6 -4 1 44.15 34.33 7.93 o 7 -4 1 0.51 -2.70 11.24 o -8 -3 1 60.42 39.46 11.32 o -7 -3 1 8.85 6.16 3.36 o -6 -3 1 697.50 701.00 18.84 o -5 -3 1 1179.27 1184.45 34.77 o -4 -3 1 1084.59 1092.27 21.74 o -3 -3 1 1900.09 1890.71 39.02 o -2 -3 1 5610.22 5400.38 102.42 o -1 -3 1 37.02 40.31 3.33 o 0 -3 1 2575.62 2507.86 53.72 o 1 -3 1 3322.73 3230.64 66.37 o 2 -3 1 3093.52 2982.32 59.59 o 3 -3 1 1526.02 1605.28 30.70 o 4 -3 1 1376.46 1396.21 44.21 o 5 -3 1 48.88 45.69 8.09 o 6 -3 1 129.49 123.32 17.17 o 7 -3 1 34.97 27.17 9.61 o -8 -2 1 14.15 23.12 11.32 o -7 -2 1 683.85 687.54 19.65 o -6 -2 1 1174.55 1248.66 32.37 o -5 -2 1 859.67 860.36 20.56 o -4 -2 1 1057.11 1023.12 22.77 o -3 -2 1 4556.37 4547.13 78.00 o -2 -2 1 1287.13 1275.49 27.01 o -1 -2 1 1437.19 1427.17 26.57 o 0 -2 1 33.35 55.31 3.24 o 1 -2 1 2526.40 2450.13 53.01 o 2 -2 1 2772.87 2727.54 53.60 o 3 -2 1 4885.31 4889.33 108.01 o 4 -2 1 2016.96 2081.15 46.47 o 5 -2 1 880.28 930.87 24.26 o 6 -2 1 79.86 74.40 10.39 o 7 -2 1 195.84 184.12 19.46 o 8 -2 1 115.94 105.57 20.16 o -8 -1 1 4.70 13.61 9.62 o -7 -1 1 107.10 90.99 7.03 o -6 -1 1 462.32 483.38 12.22 o -5 -1 1 1160.34 1187.85 26.56 o -4 -1 1 91.62 93.81 3.20 o -3 -1 1 2110.66 1960.19 41.08 o -2 -1 1 512.16 442.20 8.89 o -1 -1 1 209.19 223.12 4.63 o 0 -1 1 1544.66 1497.24 27.56 o 1 -1 1 5275.54 4886.44 114.36 o 2 -1 1 531.88 533.13 10.17 o 3 -1 1 4103.04 3928.67 67.73 o 4 -1 1 3384.28 3397.54 57.52 o 5 -1 1 15.81 7.77 3.33 o 6 -1 1 12.18 11.34 3.73 o 7 -1 1 44.35 34.75 8.05 o 8 -1 1 504.03 497.52 33.50 o -8 0 1 46.65 27.19 13.60 o -7 0 1 168.54 189.29 11.04 o -6 0 1 587.89 599.61 16.81 o -5 0 1 1173.21 1209.04 26.06 o -4 0 1 1688.11 1690.92 30.13 o -3 0 1 1248.17 1221.05 27.53 o -2 0 1 662.26 631.18 12.23 o -1 0 1 732.52 700.55 13.02 o 1 0 1 425.49 383.77 8.43 o 2 0 1 1851.28 1809.56 40.82 o 3 0 1 1247.81 1153.89 21.61 o 4 0 1 1223.39 1233.00 25.40 o 5 0 1 19.43 22.29 4.52 o 6 0 1 101.70 110.86 7.63 o 7 0 1 45.52 39.93 4.89 o 8 0 1 326.84 318.16 16.76 o -8 1 1 21.42 20.28 16.91 o -7 1 1 289.41 279.87 12.59 o -6 1 1 967.77 1021.37 30.84 o -5 1 1 792.45 791.91 20.13 o -4 1 1 2714.46 2697.20 52.31 o -3 1 1 1448.20 1380.32 29.56 o -2 1 1 430.65 422.26 8.06 o -1 1 1 1375.20 1310.64 22.57 o 1 1 1 3011.09 2693.43 59.23 o 2 1 1 29061.88 26231.63 537.92 o 3 1 1 1334.69 1216.87 24.96 o 4 1 1 2312.68 2196.07 52.26 o 5 1 1 116.74 100.49 5.39 o 6 1 1 103.32 109.07 6.35 o 7 1 1 212.63 214.92 9.31 o 8 1 1 149.80 146.92 14.49 o -7 2 1 228.15 242.81 19.35 o -6 2 1 1153.94 1216.42 41.86 o -5 2 1 910.35 933.26 23.57 o -4 2 1 1330.23 1338.61 29.85 o -3 2 1 338.74 338.75 7.27 o -2 2 1 307.54 337.34 7.76 o -1 2 1 1946.58 1854.41 41.51 o 0 2 1 3826.73 3639.27 88.46 o 1 2 1 6853.23 6530.36 136.33 o 2 2 1 16728.93 15327.29 332.21 o 3 2 1 9443.18 9022.92 194.66 o 4 2 1 1279.84 1292.81 24.53 o 5 2 1 299.74 324.59 9.56 o 6 2 1 0.49 2.64 3.77 o 7 2 1 383.51 362.50 14.59 o 8 2 1 129.60 111.41 7.38 o -7 3 1 260.53 285.43 19.21 o -6 3 1 395.30 397.27 18.30 o -5 3 1 1406.65 1417.13 42.61 o -4 3 1 357.63 372.46 10.62 o -3 3 1 351.29 380.38 9.34 o -2 3 1 2138.14 2346.60 37.50 o -1 3 1 9.44 7.21 3.60 o 0 3 1 1004.48 978.77 22.95 o 1 3 1 70.29 85.00 3.60 o 2 3 1 6312.66 5939.62 130.03 o 3 3 1 4046.47 4019.86 77.13 o 4 3 1 95.26 88.91 5.36 o 5 3 1 74.19 61.35 4.01 o 6 3 1 251.06 233.88 7.15 o 7 3 1 186.41 187.12 10.43 o 8 3 1 248.99 232.27 16.41 o -7 4 1 368.80 327.16 23.85 o -6 4 1 803.31 806.81 48.69 o -5 4 1 1055.82 1153.27 47.94 o -4 4 1 402.50 424.41 14.23 o -3 4 1 387.28 413.76 9.53 o -2 4 1 14.55 11.93 4.13 o -1 4 1 101.96 142.19 7.18 o 0 4 1 2162.07 2292.52 47.38 o 1 4 1 2652.45 2539.56 57.04 o 2 4 1 4081.55 4089.83 85.20 o 3 4 1 142.59 129.23 3.59 o 4 4 1 659.60 675.92 15.12 o 5 4 1 72.41 80.94 4.29 o 6 4 1 367.64 347.48 11.52 o 7 4 1 110.25 104.53 8.11 o 8 4 1 187.58 191.33 19.30 o -6 5 1 682.08 617.08 87.36 o -5 5 1 601.41 615.17 21.85 o -4 5 1 1046.76 1080.83 29.53 o -3 5 1 151.40 146.80 6.54 o -2 5 1 156.13 160.13 6.73 o -1 5 1 173.95 182.59 7.14 o 0 5 1 2922.03 3085.80 65.85 o 1 5 1 6188.08 6106.54 134.83 o 2 5 1 5405.42 5509.65 121.11 o 3 5 1 615.05 619.24 14.28 o 4 5 1 1303.22 1328.09 28.35 o 5 5 1 4.74 4.23 3.15 o 6 5 1 196.44 186.29 7.54 o 7 5 1 116.07 105.00 7.99 o 8 5 1 184.13 204.32 20.45 o -6 6 1 895.05 897.41 57.48 o -5 6 1 228.44 204.06 36.11 o -4 6 1 426.51 401.51 19.33 o -3 6 1 462.95 442.49 13.01 o -2 6 1 116.46 107.43 7.05 o -1 6 1 9.21 1.18 4.48 o 0 6 1 2790.37 2977.21 62.51 o 1 6 1 7222.10 7438.91 175.54 o 2 6 1 1618.91 1751.91 45.28 o 3 6 1 827.23 880.70 20.86 o 4 6 1 5.87 4.70 5.53 o 5 6 1 12.06 12.63 3.64 o 6 6 1 4.92 2.32 4.41 o 7 6 1 391.51 412.13 15.93 o 8 6 1 356.11 373.60 33.99 o -5 7 1 462.36 378.80 26.17 o -4 7 1 127.13 141.57 10.02 o -3 7 1 68.32 69.56 9.02 o -2 7 1 109.39 100.37 9.08 o -1 7 1 884.94 914.24 22.08 o 0 7 1 213.51 223.62 6.32 o 1 7 1 1603.98 1729.17 39.29 o 2 7 1 325.66 378.82 14.60 o 3 7 1 309.44 316.37 10.63 o 4 7 1 185.09 184.57 8.54 o 5 7 1 31.95 35.01 4.22 o 6 7 1 105.76 88.08 6.92 o 7 7 1 235.00 287.55 19.36 o 8 7 1 304.99 318.02 27.09 o -4 8 1 49.57 34.09 9.64 o -3 8 1 27.23 28.47 15.97 o -2 8 1 591.84 527.85 34.97 o -1 8 1 137.05 127.62 8.72 o 0 8 1 3420.27 3622.37 98.96 o 1 8 1 4926.82 5132.24 134.47 o 2 8 1 24.80 31.37 4.52 o 3 8 1 194.06 211.06 9.19 o 4 8 1 123.77 114.34 6.63 o 5 8 1 9.05 10.40 4.02 o 6 8 1 185.76 184.84 12.57 o 7 8 1 301.30 316.04 47.56 o 8 8 1 204.51 255.79 26.95 o -4 9 1 244.97 236.28 30.33 o -3 9 1 0.33 0.00 9.61 o -2 9 1 169.02 111.24 14.52 o -1 9 1 875.85 915.21 39.39 o 0 9 1 862.74 947.95 51.30 o 1 9 1 557.49 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1343.20 74.75 o -1 -10 2 589.01 608.32 54.88 o 1 -10 2 141.62 119.21 20.27 o 2 -10 2 16.36 26.86 14.25 o -6 -9 2 36.85 40.52 13.51 o -5 -9 2 294.67 270.36 21.23 o -4 -9 2 38.81 37.10 5.58 o -3 -9 2 1038.32 1044.69 39.56 o -2 -9 2 1429.81 1432.48 87.45 o -1 -9 2 757.58 761.83 25.65 o 0 -9 2 526.27 551.42 23.15 o 1 -9 2 311.37 301.24 51.54 o 2 -9 2 147.65 136.37 14.43 o 3 -9 2 59.80 57.39 14.32 o -7 -8 2 280.26 263.52 27.05 o -6 -8 2 275.12 271.95 20.43 o -5 -8 2 61.07 41.50 6.42 o -4 -8 2 47.75 30.15 6.97 o -3 -8 2 853.46 824.31 25.19 o -2 -8 2 257.87 286.67 9.36 o -1 -8 2 367.15 371.92 11.60 o 0 -8 2 540.30 551.29 17.20 o 1 -8 2 157.74 141.55 17.05 o 2 -8 2 8.69 10.32 17.20 o 3 -8 2 248.51 243.11 19.34 o 4 -8 2 246.88 222.79 23.73 o -7 -7 2 43.13 33.99 6.80 o -6 -7 2 1.11 2.28 5.40 o -5 -7 2 30.69 23.56 4.39 o -4 -7 2 93.09 86.98 7.10 o -3 -7 2 1222.24 1278.89 31.57 o -2 -7 2 1262.75 1324.22 31.38 o -1 -7 2 249.70 250.07 9.56 o 0 -7 2 590.88 600.15 17.20 o 1 -7 2 7.66 6.99 3.50 o 2 -7 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