#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2013229.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013229_Fobs loop_ _publ_author_name 'Harada, Tomoko' 'Wada, Satoko' 'Yuge, Hidetaka' 'Miyamoto, Takeshi Ken' _publ_section_title ; The trans influence of the pyridine ligand on ruthenium(II)--porphyrin--carbene complexes ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m37 _journal_page_last m39 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 99.436 _cell_angle_gamma 90.000 _cell_length_a 12.4428 _cell_length_b 17.3768 _cell_length_c 25.1794 _exptl_crystal_F_000 2360.00 _reflns_d_resolution_high 0.7697 _[local]_cod_data_source_file tr1046IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title '[Ru(ttp){C(3-C6H4CF3)2}(py)]' _shelx_refln_list_code 4 _shelx_f_calc_maximum 451.71 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1617.84 1866.15 24.84 o 3 0 0 5517.39 5724.12 51.67 o 4 0 0 20531.60 20818.68 109.37 o 5 0 0 10793.50 10951.17 90.80 o 6 0 0 11767.56 12865.77 108.78 o 7 0 0 558.25 508.26 35.92 o 8 0 0 12.91 7.21 29.01 o 9 0 0 7318.45 6958.44 106.46 o 10 0 0 5114.25 5290.16 103.45 o 11 0 0 10.53 25.43 39.41 o 12 0 0 40.96 14.02 42.01 o 13 0 0 215.15 247.32 28.74 o 14 0 0 1162.94 1105.47 74.25 o 15 0 0 637.35 653.28 48.27 o 2 1 0 4647.53 4476.43 38.03 o 3 1 0 28878.06 29402.19 112.98 o 4 1 0 8419.99 8261.11 70.81 o 5 1 0 84.13 119.20 13.34 o 6 1 0 8174.41 8568.66 91.01 o 7 1 0 9843.38 9555.91 104.71 o 8 1 0 6608.93 6001.44 92.76 o 9 1 0 1881.02 1879.12 63.95 o 10 1 0 21.86 43.18 20.59 o 11 1 0 46.37 2.94 40.58 o 12 1 0 1496.12 1446.72 73.75 o 13 1 0 2150.09 2078.35 85.23 o 14 1 0 626.65 636.39 44.97 o 15 1 0 64.46 36.98 56.67 o 1 2 0 30203.78 30358.10 85.87 o 2 2 0 489.83 480.10 19.65 o 3 2 0 11666.08 11828.00 76.14 o 4 2 0 18688.07 19189.80 108.52 o 5 2 0 19041.90 18936.99 120.80 o 6 2 0 20613.86 20134.41 137.45 o 7 2 0 3415.85 3439.04 67.51 o 8 2 0 2804.05 2815.30 68.75 o 9 2 0 7162.05 7123.11 110.20 o 10 2 0 4829.29 4990.15 101.18 o 11 2 0 218.48 200.06 25.07 o 12 2 0 67.08 98.03 25.00 o 13 2 0 114.83 36.73 50.66 o 14 2 0 566.21 535.35 43.38 o 15 2 0 539.87 570.72 47.19 o 1 3 0 7708.78 8040.25 53.60 o 2 3 0 15550.56 15705.73 81.76 o 3 3 0 8187.90 7328.25 64.48 o 4 3 0 10288.90 10289.14 83.73 o 5 3 0 803.72 727.86 32.57 o 6 3 0 5142.93 5425.05 75.93 o 7 3 0 6183.35 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507.01 517.19 50.87 o 11 5 0 1187.64 1125.62 67.28 o 12 5 0 1879.56 1985.85 80.61 o 13 5 0 38.11 45.70 26.95 o 14 5 0 214.00 214.02 32.43 o 15 5 0 10.38 17.12 51.09 o 0 6 0 29931.81 30895.89 140.52 o 1 6 0 17821.07 19925.17 115.92 o 2 6 0 15834.72 16287.44 109.44 o 3 6 0 91.23 93.17 12.99 o 4 6 0 3076.45 3319.04 58.90 o 5 6 0 1371.88 1230.01 42.88 o 6 6 0 3200.66 3202.23 66.89 o 7 6 0 23.39 47.28 32.25 o 8 6 0 2.87 12.88 35.69 o 9 6 0 348.66 381.51 32.27 o 10 6 0 924.52 957.60 57.61 o 11 6 0 1218.67 1203.57 67.71 o 12 6 0 536.86 409.03 33.70 o 13 6 0 304.80 281.27 31.52 o 14 6 0 128.86 164.76 29.56 o 15 6 0 245.70 235.66 34.84 o 1 7 0 282.93 384.29 29.29 o 2 7 0 1636.45 1616.57 42.99 o 3 7 0 7891.32 8502.39 89.86 o 4 7 0 2613.88 2938.68 58.76 o 5 7 0 75.19 101.43 15.91 o 6 7 0 2633.02 2978.32 66.47 o 7 7 0 2641.30 2819.57 71.22 o 8 7 0 1340.47 1410.77 61.47 o 9 7 0 1074.38 1096.26 58.00 o 10 7 0 8.20 -9.11 37.37 o 11 7 0 706.45 639.33 62.48 o 12 7 0 718.53 678.07 45.91 o 13 7 0 39.34 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