#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/32/2013245.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013245_Fobs loop_ _publ_author_name 'Anacona, J. R.' 'G\'omez, Jofre' 'Loro\~no, Daniel' _publ_section_title ; Two polymorphs of bis(2-bromophenyl) disulfide ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o277 _journal_page_last o280 _journal_volume 59 _journal_year 2003 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 102.122 _cell_angle_beta 100.393 _cell_angle_gamma 110.001 _cell_length_a 11.8186 _cell_length_b 15.4891 _cell_length_c 15.6529 _exptl_crystal_F_000 1456.00 _reflns_d_resolution_high 0.7376 _[local]_cod_data_source_file bm1522IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' II in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 462.43 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 227.37 276.15 12.84 o 2 0 0 31987.18 35716.20 599.34 o 3 0 0 667.41 711.38 33.33 o 4 0 0 2767.47 2656.47 106.79 o 5 0 0 922.41 946.74 50.09 o 6 0 0 23304.63 24034.33 562.31 o 7 0 0 15544.36 15505.93 395.09 o 8 0 0 3438.38 3313.34 168.19 o 9 0 0 656.04 552.56 79.16 o 10 0 0 228.92 262.42 72.22 o 11 0 0 357.51 264.25 77.52 o 12 0 0 73.49 101.03 66.13 o 13 0 0 1854.19 2016.02 264.06 o -14 1 0 691.45 629.72 198.04 o -13 1 0 621.91 707.79 180.25 o -12 1 0 20.47 32.23 66.63 o -11 1 0 370.88 387.49 85.20 o -10 1 0 315.17 259.39 73.47 o -9 1 0 12.37 14.41 51.89 o -8 1 0 6866.94 6433.53 176.25 o -7 1 0 9894.19 10066.22 268.55 o -6 1 0 6530.91 7124.19 421.92 o -5 1 0 934.75 902.33 47.42 o -4 1 0 3438.45 3623.99 74.85 o -3 1 0 441.59 483.69 29.47 o -2 1 0 65.40 106.54 14.83 o -1 1 0 0.38 27.35 5.55 o 0 1 0 1002.44 994.38 20.64 o 1 1 0 7100.73 7940.32 239.54 o 2 1 0 11939.11 12595.72 138.50 o 3 1 0 10232.88 11049.01 120.61 o 4 1 0 9807.96 10581.17 231.11 o 5 1 0 1274.61 1413.30 61.79 o 6 1 0 1035.22 946.55 57.13 o 7 1 0 5785.31 5454.04 243.16 o 8 1 0 350.54 337.83 66.05 o 9 1 0 12180.67 11191.42 312.28 o 10 1 0 2677.80 2561.08 141.23 o 11 1 0 933.16 817.83 104.07 o 12 1 0 10.57 -17.22 132.60 o 13 1 0 225.81 268.08 160.73 o -14 2 0 248.27 217.56 158.43 o -13 2 0 3662.92 3511.30 186.56 o -12 2 0 2254.87 2095.20 141.20 o -11 2 0 420.17 379.76 82.19 o -10 2 0 897.34 742.30 89.82 o -9 2 0 29.37 24.88 51.57 o -8 2 0 3528.10 3285.02 130.43 o -7 2 0 3655.85 3995.25 181.04 o -6 2 0 26570.18 27590.24 348.34 o -5 2 0 13316.40 13352.14 155.95 o -4 2 0 4638.11 4520.18 146.07 o -3 2 0 12221.17 12729.07 117.57 o -2 2 0 11051.75 11040.18 162.56 o -1 2 0 2682.95 2927.05 76.30 o 0 2 0 19338.50 19034.55 131.11 o 1 2 0 8510.18 9371.02 135.41 o 2 2 0 209115.69 203490.98 1493.89 o 3 2 0 7308.40 7832.19 172.25 o 4 2 0 2943.52 3098.15 79.61 o 5 2 0 537.83 525.23 46.49 o 6 2 0 716.15 715.86 56.28 o 7 2 0 16.52 29.79 36.60 o 8 2 0 4182.52 4029.25 153.65 o 9 2 0 3942.60 3565.00 154.13 o 10 2 0 667.51 597.57 110.79 o 11 2 0 45.79 87.25 137.19 o 12 2 0 14.69 30.42 149.82 o 13 2 0 593.56 537.87 198.62 o -14 3 0 62.74 87.47 74.06 o -13 3 0 270.57 277.08 86.00 o -12 3 0 43.95 72.05 67.55 o -11 3 0 293.97 246.84 72.65 o -10 3 0 1103.86 1058.41 100.69 o -9 3 0 7610.30 7010.85 197.53 o -8 3 0 10612.25 10242.09 277.55 o -7 3 0 3050.67 2866.82 88.64 o -6 3 0 215.68 226.92 45.91 o -5 3 0 1748.23 1680.60 61.21 o -4 3 0 6190.95 6478.47 114.03 o -3 3 0 13880.14 13876.35 209.21 o -2 3 0 22153.10 22882.09 147.70 o -1 3 0 483.56 468.72 27.13 o 0 3 0 9.67 42.49 16.29 o 1 3 0 85.55 111.78 20.24 o 2 3 0 24618.04 25997.12 196.73 o 3 3 0 6443.87 6476.20 119.59 o 4 3 0 16540.16 17601.86 192.49 o 5 3 0 13186.92 13479.35 183.49 o 6 3 0 3382.30 3501.10 105.21 o 7 3 0 2305.03 2249.59 94.35 o 8 3 0 13.50 -3.70 50.12 o 9 3 0 182.96 160.32 64.86 o 10 3 0 7.45 -29.85 110.79 o 11 3 0 233.93 237.65 170.49 o 12 3 0 1717.96 1598.12 268.65 o -15 4 0 2809.28 2800.73 216.41 o -14 4 0 902.80 882.80 121.47 o -13 4 0 3.64 -17.70 67.42 o -12 4 0 2363.08 2083.59 141.08 o -11 4 0 841.90 803.31 100.20 o -10 4 0 984.83 842.63 93.09 o -9 4 0 7809.78 7335.46 200.39 o -8 4 0 3015.13 2922.27 125.30 o -7 4 0 722.17 656.55 52.79 o -6 4 0 231.43 300.07 40.49 o -5 4 0 151.98 193.64 31.44 o -4 4 0 12217.72 11653.60 126.83 o -3 4 0 5566.75 5804.59 84.94 o -2 4 0 104224.18 110163.17 468.90 o -1 4 0 16131.19 16842.36 425.77 o 0 4 0 104268.09 101270.38 1095.66 o 1 4 0 29696.71 31887.41 505.54 o 2 4 0 6559.14 6972.81 114.52 o 3 4 0 10261.29 10837.00 150.31 o 4 4 0 177.58 219.82 37.84 o 5 4 0 3751.75 4005.00 109.64 o 6 4 0 13701.75 13898.79 309.89 o 7 4 0 243.87 241.50 51.39 o 8 4 0 93.18 77.05 58.41 o 9 4 0 109.70 91.85 121.70 o 10 4 0 2.41 23.54 111.94 o 11 4 0 17.66 44.20 154.42 o 12 4 0 1538.64 1569.99 258.89 o -15 5 0 232.94 302.52 122.27 o -14 5 0 50.31 38.22 77.10 o -13 5 0 12.05 17.44 73.47 o -12 5 0 40.39 15.11 67.07 o -11 5 0 15.55 8.75 60.15 o -10 5 0 307.63 315.51 73.66 o -9 5 0 138.50 109.25 54.76 o -8 5 0 13227.47 13129.12 248.81 o -7 5 0 4561.51 4311.01 108.77 o -6 5 0 23016.05 24573.64 476.74 o -5 5 0 1763.06 1605.37 59.61 o -4 5 0 6088.21 5985.66 98.20 o -3 5 0 1324.61 1342.67 59.75 o -2 5 0 289.75 270.81 29.42 o -1 5 0 138.00 168.52 27.25 o 0 5 0 16272.27 15743.83 490.94 o 1 5 0 9397.22 9995.52 144.34 o 2 5 0 4201.46 4409.13 102.14 o 3 5 0 2384.19 2529.14 84.66 o 4 5 0 97.17 121.03 37.86 o 5 5 0 513.70 486.61 57.37 o 6 5 0 19746.21 20409.54 261.11 o 7 5 0 25356.60 25500.19 307.26 o 8 5 0 194.82 234.21 126.86 o 9 5 0 3303.75 3440.78 302.52 o 10 5 0 174.12 283.00 160.16 o 12 5 0 43.79 53.96 164.75 o -15 6 0 6.44 -6.53 75.54 o -14 6 0 19.10 27.04 76.66 o -13 6 0 4248.87 4133.57 197.00 o -12 6 0 101.03 86.15 70.82 o -11 6 0 1.60 -11.55 59.26 o -10 6 0 400.82 379.05 77.78 o -9 6 0 329.89 287.09 67.78 o -8 6 0 142.91 166.47 54.95 o -7 6 0 6905.80 6909.33 255.64 o -6 6 0 11361.37 11342.70 164.46 o -5 6 0 1570.43 1659.12 62.56 o -4 6 0 1699.05 1694.57 60.03 o -3 6 0 16959.56 17477.79 175.51 o -2 6 0 2867.94 2755.92 75.26 o -1 6 0 5278.69 5324.59 138.05 o 0 6 0 25385.52 26420.79 830.66 o 1 6 0 2624.45 2451.15 82.90 o 2 6 0 25108.07 28184.60 355.45 o 3 6 0 355.65 386.93 49.74 o 4 6 0 6807.04 7182.68 212.34 o 5 6 0 6483.40 6726.65 151.33 o 6 6 0 3110.69 3162.88 116.46 o 7 6 0 12.57 6.89 71.09 o 8 6 0 806.08 912.14 183.12 o 9 6 0 0.14 32.15 130.88 o 10 6 0 6.62 53.39 137.19 o -15 7 0 97.02 74.10 80.67 o -14 7 0 2566.64 2572.54 175.12 o -13 7 0 1040.74 1040.98 119.13 o -12 7 0 2157.14 2131.41 146.45 o -11 7 0 1275.55 1243.78 115.27 o -10 7 0 50.30 50.19 57.48 o -9 7 0 2269.78 2111.81 120.05 o -8 7 0 2570.60 2607.52 123.19 o -7 7 0 14245.51 14244.93 306.10 o -6 7 0 18609.00 18083.79 202.43 o -5 7 0 6473.77 6212.73 123.55 o -4 7 0 947.61 921.28 53.72 o -3 7 0 355.90 350.49 40.57 o -2 7 0 134.94 140.54 32.24 o -1 7 0 2755.95 2811.70 88.35 o 0 7 0 24244.05 24988.05 281.75 o 1 7 0 23134.09 24363.61 261.37 o 2 7 0 9721.06 10103.41 174.35 o 3 7 0 8628.90 9240.27 255.04 o 4 7 0 13.90 57.38 41.30 o 5 7 0 34.99 25.04 43.83 o 6 7 0 58.81 63.83 75.88 o 7 7 0 12.12 7.65 72.76 o 8 7 0 7625.16 7840.20 430.53 o 9 7 0 3947.32 3953.39 330.07 o 10 7 0 34.97 16.07 138.34 o -15 8 0 805.38 861.11 129.42 o -14 8 0 1694.44 1685.94 148.01 o -13 8 0 139.23 148.58 83.29 o -12 8 0 3194.29 3209.99 169.21 o -11 8 0 219.49 260.01 77.23 o -10 8 0 4275.19 4312.44 190.01 o -9 8 0 71.43 63.46 57.57 o -8 8 0 741.88 687.24 78.52 o -7 8 0 1319.61 1233.89 68.59 o -6 8 0 1512.31 1577.52 72.15 o -5 8 0 2252.60 2263.27 81.29 o -4 8 0 12439.31 12506.47 172.30 o -3 8 0 2368.24 2215.01 81.95 o -2 8 0 3492.67 3166.01 98.08 o -1 8 0 3965.78 3502.79 104.61 o 0 8 0 1895.82 1795.61 82.26 o 1 8 0 7541.39 7920.78 324.13 o 2 8 0 862.30 911.63 70.11 o 3 8 0 1626.43 1562.78 86.63 o 4 8 0 1938.70 1966.52 97.26 o 5 8 0 2004.42 2010.68 144.88 o 6 8 0 85.45 136.14 80.81 o 7 8 0 59.12 70.07 80.40 o 8 8 0 371.16 409.29 165.32 o 9 8 0 4.80 48.79 134.32 o 10 8 0 249.62 279.56 177.95 o -15 9 0 9.14 46.04 82.68 o -14 9 0 235.72 333.14 98.07 o -13 9 0 157.69 169.89 83.67 o -12 9 0 6179.60 6259.60 230.53 o -11 9 0 325.57 330.44 79.56 o -10 9 0 872.22 924.14 102.23 o -9 9 0 933.80 891.84 95.78 o -8 9 0 1240.68 1405.13 102.63 o -7 9 0 6011.44 6327.95 140.66 o -6 9 0 1338.19 1265.01 72.46 o -5 9 0 26783.24 27512.45 891.91 o -4 9 0 4354.51 4315.51 115.03 o -3 9 0 4775.89 4483.09 118.93 o -2 9 0 8431.14 7837.09 159.41 o -1 9 0 2867.76 2695.87 124.39 o 0 9 0 487.16 484.23 60.15 o 1 9 0 57.76 35.59 40.96 o 2 9 0 48.59 76.73 45.91 o 3 9 0 5080.50 5244.83 147.24 o 4 9 0 1799.45 1755.72 138.40 o 5 9 0 266.76 288.45 90.31 o 6 9 0 1677.96 1669.59 153.86 o 7 9 0 1775.57 1901.91 249.13 o 8 9 0 23.11 58.55 144.66 o 9 9 0 170.96 98.73 146.38 o 10 9 0 428.06 338.68 177.95 o -15 10 0 39.68 46.22 77.62 o -14 10 0 1039.16 1025.49 130.49 o -13 10 0 739.86 894.05 121.77 o -12 10 0 14.55 42.53 72.84 o -11 10 0 1244.40 1141.64 112.52 o -10 10 0 944.93 892.49 104.35 o -9 10 0 1296.41 1489.49 114.90 o -8 10 0 634.51 678.25 88.68 o -7 10 0 732.82 723.48 66.74 o -6 10 0 4.14 20.20 35.70 o -5 10 0 3983.07 3961.28 133.24 o -4 10 0 2265.72 2143.69 112.23 o -3 10 0 3247.63 2950.11 106.71 o -2 10 0 4929.33 4617.59 133.31 o -1 10 0 24.07 27.93 40.47 o 0 10 0 117.93 110.03 48.02 o 1 10 0 2868.80 2980.37 117.54 o 2 10 0 747.83 822.96 78.65 o 3 10 0 4371.80 4456.51 198.67 o 4 10 0 3245.83 3089.55 180.42 o 5 10 0 1162.80 1293.59 159.30 o 6 10 0 208.90 273.94 103.10 o 7 10 0 5440.32 5729.86 267.71 o 8 10 0 45.13 -12.63 133.18 o 9 10 0 586.99 601.59 202.06 o -15 11 0 0.18 91.85 120.55 o -14 11 0 98.71 118.47 87.04 o -13 11 0 0.18 -11.14 73.38 o -12 11 0 2806.95 3033.48 176.71 o -11 11 0 326.31 431.28 89.82 o -10 11 0 4615.16 4950.78 199.87 o -9 11 0 1227.32 1311.78 110.99 o -8 11 0 555.32 578.78 89.79 o -7 11 0 5548.77 5739.88 168.84 o -6 11 0 8974.16 9066.67 286.24 o -5 11 0 2495.66 2312.81 101.89 o -4 11 0 80.57 106.53 45.28 o -3 11 0 8989.85 7602.39 375.97 o -2 11 0 363.81 332.04 56.70 o -1 11 0 3773.64 3619.95 130.16 o 0 11 0 28069.49 28874.05 793.95 o 1 11 0 3392.16 3481.06 139.47 o 2 11 0 622.08 612.17 101.75 o 3 11 0 1119.13 1226.56 131.45 o 4 11 0 0.42 20.21 78.60 o 5 11 0 7.32 24.92 82.73 o 6 11 0 3723.54 3806.04 226.68 o 7 11 0 609.65 680.35 135.97 o 8 11 0 1045.96 1220.40 230.76 o -14 12 0 749.71 878.15 127.09 o -13 12 0 497.02 577.96 110.42 o -12 12 0 4.07 22.80 77.17 o -11 12 0 313.79 326.84 88.76 o -10 12 0 2230.42 2408.66 230.19 o -9 12 0 152.36 263.07 80.42 o -8 12 0 1604.47 1587.19 123.08 o -7 12 0 1406.14 1410.56 88.34 o -6 12 0 1.48 37.00 42.00 o -5 12 0 12144.68 11531.99 262.39 o -4 12 0 24.39 13.05 42.23 o -3 12 0 2293.63 2083.48 104.03 o -2 12 0 116.29 141.35 53.12 o -1 12 0 218.15 167.91 55.63 o 0 12 0 3166.66 3634.29 174.96 o 1 12 0 720.78 682.63 105.16 o 2 12 0 3279.26 3578.84 189.26 o 3 12 0 670.68 695.75 117.10 o 4 12 0 1526.57 1672.48 156.63 o 5 12 0 87.01 62.00 136.62 o 6 12 0 210.87 241.67 156.14 o 7 12 0 877.21 1045.32 230.19 o -14 13 0 1480.05 1618.78 231.91 o -13 13 0 303.47 351.88 161.88 o -12 13 0 1306.41 1541.86 219.28 o -11 13 0 166.11 398.96 147.53 o -10 13 0 6181.56 6722.55 356.48 o -9 13 0 90.77 140.07 120.55 o -8 13 0 406.04 567.15 141.79 o -7 13 0 4459.01 4538.63 313.42 o -6 13 0 496.82 434.75 81.16 o -5 13 0 5057.88 4482.71 178.97 o -4 13 0 1235.52 1131.28 107.69 o -3 13 0 16656.72 15393.51 323.30 o -2 13 0 662.35 597.86 92.95 o -1 13 0 78.92 118.38 68.79 o 0 13 0 78.86 21.81 102.75 o 1 13 0 2443.89 2564.22 252.00 o 2 13 0 3022.99 3079.13 272.67 o 3 13 0 3233.96 3220.92 296.20 o 4 13 0 1476.41 1425.33 235.93 o 5 13 0 409.93 365.09 175.66 o 6 13 0 63.52 87.83 155.56 o 7 13 0 199.41 254.87 155.56 o -13 14 0 1199.69 1503.98 229.61 o -12 14 0 134.99 170.49 138.92 o -11 14 0 3740.82 4261.08 315.15 o -10 14 0 272.81 349.59 144.08 o -9 14 0 1678.66 1858.16 221.00 o -8 14 0 5029.45 5049.23 308.26 o -7 14 0 52.18 79.22 88.40 o -6 14 0 4103.91 3725.79 172.45 o -5 14 0 7212.02 6714.30 224.25 o -4 14 0 142.10 187.07 74.25 o -3 14 0 7241.12 7023.65 235.61 o -2 14 0 1702.00 1583.53 128.06 o -1 14 0 34.72 71.18 109.07 o 0 14 0 394.49 331.79 133.18 o 1 14 0 2947.26 2763.41 264.63 o 2 14 0 5662.41 5628.43 359.35 o 3 14 0 569.57 595.28 182.54 o 4 14 0 894.80 971.27 214.12 o 5 14 0 461.61 444.30 184.84 o 6 14 0 599.85 802.50 214.12 o -13 15 0 438.39 603.31 187.14 o -12 15 0 1124.16 1532.68 236.50 o -11 15 0 377.07 567.72 168.77 o -10 15 0 92.87 187.71 139.49 o -9 15 0 111.70 109.64 124.57 o -7 15 0 507.80 550.21 98.21 o -6 15 0 16.13 -3.34 63.00 o -5 15 0 2115.75 2061.92 146.51 o -4 15 0 1331.80 1261.37 145.23 o -3 15 0 205.17 222.96 79.35 o -2 15 0 1436.10 1320.28 185.41 o -1 15 0 946.73 948.31 191.73 o 0 15 0 451.63 519.50 159.58 o 1 15 0 59.54 72.90 132.60 o 2 15 0 284.31 235.93 146.95 o 3 15 0 8.96 31.00 144.08 o 4 15 0 67.47 70.61 159.58 o -12 16 0 137.68 113.66 153.27 o -11 16 0 172.17 295.05 160.16 o -10 16 0 216.38 284.15 148.68 o -8 16 0 594.43 571.17 157.29 o -7 16 0 114.59 121.01 79.52 o -6 16 0 350.49 412.56 90.72 o -5 16 0 925.77 835.85 115.20 o -4 16 0 4436.17 4091.81 195.54 o -3 16 0 119.36 102.75 122.84 o -2 16 0 226.47 188.28 132.60 o -1 16 0 1022.22 1086.65 206.08 o 0 16 0 3185.23 3061.34 299.07 o 1 16 0 1559.15 1669.87 254.87 o 2 16 0 961.34 1099.85 220.43 o 3 16 0 285.65 316.29 177.38 o -12 17 0 1928.42 2261.71 277.26 o -11 17 0 395.51 517.21 179.10 o -10 17 0 41.42 13.78 123.42 o -9 17 0 58.80 68.88 121.70 o -8 17 0 61.88 13.78 113.09 o -7 17 0 8.17 36.45 73.47 o -6 17 0 27.51 43.72 70.99 o -5 17 0 816.07 762.32 171.64 o -4 17 0 1.60 48.79 110.79 o -3 17 0 1309.46 1208.92 206.65 o -2 17 0 747.57 726.16 188.86 o -1 17 0 57.23 58.55 138.92 o 0 17 0 15.31 -26.98 129.16 o 1 17 0 69.51 57.40 141.21 o -11 18 0 983.66 1032.69 212.39 o -10 18 0 557.06 518.36 175.08 o -9 18 0 17.01 80.37 117.68 o -8 18 0 40.84 25.26 119.40 o -7 18 0 2408.55 2261.93 164.84 o -6 18 0 1334.11 1218.68 188.86 o -5 18 0 3506.24 3248.47 282.43 o 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