#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2013262.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013262_Fobs loop_ _publ_author_name 'Munro, Orde Q.' 'Ntshangase, Mthembeni M.' _publ_section_title ; [Fe(TPP)(4-MePip)~2~]: an axially compressed bis(secondary amine) complex of an iron(II) porphyrin ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m224 _journal_page_last m227 _journal_volume 59 _journal_year 2003 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 93.077 _cell_angle_beta 111.112 _cell_angle_gamma 113.483 _cell_length_a 10.3189 _cell_length_b 11.2427 _cell_length_c 11.8631 _exptl_crystal_F_000 458.00 _reflns_d_resolution_high 0.8747 _[local]_cod_data_source_file fg1690Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' mn1; [Fe(TPP)(4-MePip)2]; triclinic P1-bar' _shelx_refln_list_code 4 _shelx_f_calc_maximum 174.25 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2918.03 3116.77 20.24 o 2 0 0 1891.33 2142.75 6.49 o 3 0 0 169.64 231.66 2.96 o 4 0 0 537.98 664.89 5.53 o 5 0 0 13.32 0.11 1.57 o 6 0 0 830.38 882.89 7.96 o 7 0 0 93.95 78.79 2.29 o 8 0 0 55.15 51.12 1.40 o 9 0 0 4.01 3.46 1.11 o -10 1 0 121.50 135.45 4.24 o -9 1 0 76.55 68.28 2.15 o -8 1 0 131.81 106.04 3.28 o -7 1 0 0.60 -2.02 2.02 o -6 1 0 1.05 3.09 0.74 o -5 1 0 180.00 257.38 3.94 o -4 1 0 3996.07 4276.37 13.08 o -3 1 0 6115.37 6079.28 48.07 o -2 1 0 17.87 8.92 0.36 o -1 1 0 732.01 811.25 2.05 o 0 1 0 7153.98 6389.97 19.22 o 1 1 0 1603.47 1736.54 27.68 o 2 1 0 1966.34 1903.56 7.87 o 3 1 0 12.84 17.66 0.64 o 4 1 0 260.07 248.61 3.72 o 5 1 0 220.37 243.65 4.18 o 6 1 0 352.18 343.68 5.39 o 7 1 0 3.65 2.86 0.93 o 8 1 0 41.44 46.63 1.44 o 9 1 0 106.26 100.20 2.78 o -10 2 0 3.20 8.08 1.17 o -9 2 0 62.40 67.73 2.07 o -8 2 0 728.62 753.69 8.58 o -7 2 0 1127.38 1208.08 9.72 o -6 2 0 773.14 744.95 6.97 o -5 2 0 0.98 0.85 1.48 o -4 2 0 2.60 4.12 0.56 o -3 2 0 491.76 466.23 3.83 o -2 2 0 2734.01 2896.12 20.23 o -1 2 0 259.28 249.91 2.09 o 0 2 0 83.92 119.86 1.29 o 1 2 0 30.39 31.82 0.68 o 2 2 0 0.91 3.47 0.57 o 3 2 0 55.39 60.52 1.82 o 4 2 0 1086.82 1124.25 8.07 o 5 2 0 203.87 210.68 4.19 o 6 2 0 388.28 397.16 6.10 o 7 2 0 77.36 76.08 2.35 o 8 2 0 47.99 45.76 1.53 o -10 3 0 100.17 101.89 2.99 o -9 3 0 276.09 267.92 5.83 o -8 3 0 227.40 220.70 4.88 o -7 3 0 23.79 28.96 1.01 o -6 3 0 69.85 84.03 2.33 o -5 3 0 80.09 59.32 1.76 o -4 3 0 1562.22 1693.88 8.29 o -3 3 0 723.36 799.53 5.12 o -2 3 0 317.72 349.10 2.26 o -1 3 0 1536.87 1442.98 4.22 o 0 3 0 727.25 728.95 3.23 o 1 3 0 79.29 61.85 1.24 o 2 3 0 253.84 255.57 8.26 o 3 3 0 213.96 181.22 3.37 o 4 3 0 101.92 103.53 2.96 o 5 3 0 202.77 200.54 4.35 o 6 3 0 840.12 850.38 9.25 o 7 3 0 92.30 95.80 2.80 o 8 3 0 0.48 2.33 1.13 o -10 4 0 0.25 1.50 1.10 o -9 4 0 0.32 -0.38 2.20 o -8 4 0 1.05 1.81 0.90 o -7 4 0 230.63 225.18 4.45 o -6 4 0 151.03 143.72 3.31 o -5 4 0 122.27 126.09 2.94 o -4 4 0 2459.33 2736.38 10.85 o -3 4 0 785.82 815.03 5.54 o -2 4 0 430.76 445.42 2.81 o -1 4 0 190.94 189.94 5.36 o 0 4 0 577.36 577.25 3.35 o 1 4 0 124.88 95.65 1.71 o 2 4 0 1640.23 1614.40 6.48 o 3 4 0 345.89 313.63 4.73 o 4 4 0 0.57 0.63 1.80 o 5 4 0 132.77 116.60 3.48 o 6 4 0 378.61 386.69 6.90 o 7 4 0 22.92 17.68 1.28 o -10 5 0 133.58 134.39 4.07 o -9 5 0 2.18 2.48 0.95 o -8 5 0 6.78 4.76 0.97 o -7 5 0 81.74 81.71 2.45 o -6 5 0 122.09 127.26 3.38 o -5 5 0 55.64 60.30 1.82 o -4 5 0 740.21 744.67 6.15 o -3 5 0 1474.28 1549.19 8.22 o -2 5 0 738.23 762.97 4.02 o -1 5 0 14.31 3.64 0.41 o 0 5 0 67.17 48.42 1.01 o 1 5 0 15.08 30.21 0.74 o 2 5 0 884.70 901.35 5.35 o 3 5 0 184.12 179.50 4.05 o 4 5 0 312.24 293.84 5.45 o 5 5 0 76.36 70.63 2.10 o 6 5 0 81.93 86.95 2.61 o 7 5 0 76.58 88.21 2.40 o -11 6 0 19.15 24.77 1.42 o -10 6 0 96.16 96.66 2.77 o -9 6 0 107.52 101.11 3.11 o -8 6 0 11.71 11.02 1.01 o -7 6 0 17.75 20.32 1.00 o -6 6 0 347.55 368.73 5.33 o -5 6 0 151.66 140.62 3.32 o -4 6 0 378.97 371.95 4.72 o -3 6 0 637.86 644.77 5.91 o -2 6 0 209.50 193.16 4.58 o -1 6 0 4.87 0.56 1.04 o 0 6 0 3.96 10.28 0.84 o 1 6 0 4.18 1.28 1.20 o 2 6 0 250.82 253.55 4.10 o 3 6 0 189.74 181.10 4.31 o 4 6 0 488.81 500.20 7.46 o 5 6 0 14.80 18.09 1.29 o 6 6 0 144.96 162.96 4.62 o -10 7 0 14.47 16.62 1.22 o -9 7 0 419.24 406.80 6.98 o -8 7 0 90.67 84.37 2.73 o -7 7 0 7.40 9.30 0.95 o -6 7 0 598.87 585.89 6.83 o -5 7 0 281.19 249.65 4.44 o -4 7 0 92.77 81.28 2.40 o -3 7 0 220.65 190.41 3.68 o -2 7 0 31.01 33.28 2.05 o -1 7 0 29.47 21.03 0.61 o 0 7 0 171.79 165.13 2.69 o 1 7 0 375.68 364.75 3.97 o 2 7 0 601.92 599.71 5.31 o 3 7 0 40.24 40.48 1.27 o 4 7 0 80.77 78.08 2.32 o 5 7 0 87.43 77.60 2.26 o -10 8 0 49.20 51.71 1.59 o -9 8 0 378.72 400.22 7.09 o -8 8 0 2.33 4.53 0.96 o -7 8 0 1.65 5.11 0.91 o -6 8 0 325.43 315.58 5.46 o -5 8 0 67.42 56.95 1.54 o -4 8 0 117.04 105.39 2.83 o -3 8 0 165.88 159.10 3.82 o -2 8 0 263.29 238.92 3.18 o -1 8 0 745.85 747.49 5.51 o 0 8 0 326.63 345.98 7.09 o 1 8 0 2.54 1.75 1.99 o 2 8 0 10.06 8.88 0.72 o 3 8 0 8.96 5.44 1.16 o 4 8 0 0.41 0.69 2.47 o -10 9 0 59.63 55.57 1.69 o -9 9 0 85.17 81.85 2.64 o -8 9 0 13.53 12.24 1.12 o -7 9 0 52.92 43.78 1.32 o -6 9 0 56.09 57.26 1.81 o -5 9 0 170.10 158.29 4.26 o -4 9 0 163.13 175.38 4.30 o -3 9 0 0.43 -0.76 2.01 o -2 9 0 45.75 47.21 1.15 o -1 9 0 55.32 57.95 1.19 o 0 9 0 498.56 491.52 5.16 o 1 9 0 129.79 132.56 2.67 o 2 9 0 62.41 69.85 1.93 o 3 9 0 36.57 39.45 1.50 o -10 10 0 20.20 17.01 1.40 o -9 10 0 63.19 59.35 1.71 o -8 10 0 330.40 306.79 6.49 o -7 10 0 186.74 176.14 4.98 o -6 10 0 7.22 5.16 1.02 o -5 10 0 171.84 172.87 4.57 o -4 10 0 57.78 62.98 1.78 o -3 10 0 196.90 187.56 4.78 o -2 10 0 69.98 75.65 2.74 o -1 10 0 210.74 208.93 3.71 o 0 10 0 246.66 251.54 4.18 o 1 10 0 14.08 9.23 0.86 o 2 10 0 1.30 1.75 1.06 o -9 11 0 2.79 1.33 2.81 o -8 11 0 8.30 9.78 1.21 o -7 11 0 113.87 117.24 3.41 o -6 11 0 176.98 184.53 5.24 o -5 11 0 18.45 25.62 1.30 o -4 11 0 57.59 63.26 1.93 o -3 11 0 98.09 108.17 3.18 o -2 11 0 16.79 17.37 0.89 o -1 11 0 51.42 52.99 3.19 o 0 11 0 66.36 85.87 5.11 o -8 12 0 94.90 133.69 3.97 o -7 12 0 58.30 63.16 1.85 o -6 12 0 7.89 8.77 1.19 o -5 12 0 22.60 30.52 1.42 o -4 12 0 193.27 211.36 5.76 o -3 12 0 110.52 107.03 3.04 o -2 12 0 5.53 5.75 1.40 o 1 -12 1 0.14 1.63 1.09 o 2 -12 1 25.21 28.43 1.01 o 3 -12 1 104.54 98.64 2.88 o 4 -12 1 53.89 53.68 1.60 o 5 -12 1 20.54 24.35 1.38 o 6 -12 1 213.54 197.03 5.75 o 7 -12 1 26.99 26.53 1.45 o -1 -11 1 17.95 17.06 0.97 o 0 -11 1 173.27 190.70 7.30 o 1 -11 1 4.10 2.62 0.79 o 2 -11 1 33.67 29.58 0.98 o 3 -11 1 68.57 74.81 2.22 o 4 -11 1 11.23 13.28 1.16 o 5 -11 1 11.00 12.29 1.14 o 6 -11 1 87.45 84.89 2.48 o 7 -11 1 0.71 1.41 2.57 o 8 -11 1 71.14 73.67 2.22 o -2 -10 1 0.71 1.42 1.03 o -1 -10 1 169.66 185.02 4.91 o 0 -10 1 454.43 471.92 5.43 o 1 -10 1 53.08 52.14 1.10 o 2 -10 1 15.90 17.62 1.72 o 3 -10 1 139.39 132.64 3.57 o 4 -10 1 5.06 4.95 0.98 o 5 -10 1 72.07 76.31 2.31 o 6 -10 1 364.34 404.69 6.92 o 7 -10 1 85.34 95.76 2.81 o 8 -10 1 56.93 53.16 1.58 o 9 -10 1 0.26 0.58 2.51 o -3 -9 1 51.89 52.14 1.61 o -2 -9 1 30.79 34.64 0.97 o -1 -9 1 57.68 62.78 1.97 o 0 -9 1 23.38 20.10 0.78 o 1 -9 1 49.05 50.31 1.35 o 2 -9 1 278.57 291.15 3.79 o 3 -9 1 264.28 260.41 5.03 o 4 -9 1 645.98 648.27 7.68 o 5 -9 1 25.62 27.15 1.12 o 6 -9 1 0.55 1.42 0.92 o 7 -9 1 63.92 61.83 1.72 o 8 -9 1 37.72 40.45 1.39 o 9 -9 1 79.61 80.80 2.60 o 10 -9 1 63.51 53.67 1.69 o -4 -8 1 30.37 24.64 1.41 o -3 -8 1 60.04 60.76 1.70 o -2 -8 1 56.87 53.01 1.10 o -1 -8 1 662.69 673.34 5.67 o 0 -8 1 513.49 487.14 4.71 o 1 -8 1 300.23 295.63 3.57 o 2 -8 1 97.30 95.81 6.04 o 3 -8 1 5.85 5.55 0.80 o 4 -8 1 74.14 74.20 2.25 o 5 -8 1 141.72 147.26 3.91 o 6 -8 1 177.90 161.37 4.31 o 7 -8 1 147.23 156.16 4.33 o 8 -8 1 163.62 159.85 4.58 o 9 -8 1 302.77 302.21 6.44 o 10 -8 1 72.37 65.44 1.86 o -5 -7 1 37.29 36.49 1.51 o -4 -7 1 120.67 124.64 3.81 o -3 -7 1 65.98 62.32 1.91 o -2 -7 1 133.89 129.90 3.22 o -1 -7 1 24.50 24.19 0.70 o 0 -7 1 7.98 10.28 0.58 o 1 -7 1 118.99 102.40 3.29 o 2 -7 1 1085.50 1055.86 5.74 o 3 -7 1 0.79 -0.34 1.58 o 4 -7 1 183.69 184.87 3.86 o 5 -7 1 622.22 591.49 6.62 o 6 -7 1 241.83 237.29 4.72 o 7 -7 1 2.95 4.67 0.95 o 8 -7 1 587.92 553.29 7.69 o 9 -7 1 73.95 73.06 2.32 o 10 -7 1 50.05 47.73 1.58 o -6 -6 1 141.52 148.88 4.28 o -5 -6 1 59.78 64.38 2.01 o -4 -6 1 20.53 22.42 1.09 o -3 -6 1 184.16 188.05 4.38 o -2 -6 1 91.07 93.20 6.25 o -1 -6 1 103.28 90.12 1.72 o 0 -6 1 0.85 0.84 0.57 o 1 -6 1 66.01 50.85 1.30 o 2 -6 1 1510.89 1529.81 7.95 o 3 -6 1 8.33 12.76 0.71 o 4 -6 1 238.09 196.02 3.69 o 5 -6 1 523.82 483.72 5.69 o 6 -6 1 0.71 -1.48 1.82 o 7 -6 1 275.67 272.65 5.15 o 8 -6 1 307.67 301.70 5.76 o 9 -6 1 2.88 3.72 1.08 o 10 -6 1 107.27 102.85 3.11 o -7 -5 1 7.86 6.72 1.20 o -6 -5 1 74.54 77.56 2.31 o -5 -5 1 38.66 42.66 1.30 o -4 -5 1 235.58 226.87 4.75 o -3 -5 1 709.72 729.70 7.33 o -2 -5 1 80.11 72.16 1.76 o -1 -5 1 392.28 408.06 3.39 o 0 -5 1 225.43 204.66 2.56 o 1 -5 1 85.33 62.19 1.89 o 2 -5 1 154.73 165.15 2.07 o 3 -5 1 1067.70 995.53 6.78 o 4 -5 1 2345.38 2273.95 10.76 o 5 -5 1 623.48 665.07 6.39 o 6 -5 1 236.76 214.72 4.12 o 7 -5 1 52.43 49.28 1.47 o 8 -5 1 13.48 17.45 1.05 o 9 -5 1 6.29 0.60 2.46 o 10 -5 1 26.57 26.26 1.38 o -8 -4 1 0.24 -2.61 2.61 o -7 -4 1 9.30 6.64 1.19 o -6 -4 1 202.78 215.02 5.11 o -5 -4 1 204.47 204.16 4.68 o -4 -4 1 322.70 315.81 5.05 o -3 -4 1 743.20 740.03 6.70 o -2 -4 1 0.79 0.57 1.37 o -1 -4 1 279.84 246.76 2.41 o 0 -4 1 370.21 307.94 3.01 o 1 -4 1 391.20 364.66 4.02 o 2 -4 1 1773.71 1675.37 19.87 o 3 -4 1 1702.48 1606.10 7.92 o 4 -4 1 83.69 106.06 2.60 o 5 -4 1 918.04 984.50 7.50 o 6 -4 1 303.45 299.21 4.70 o 7 -4 1 3.78 2.61 0.86 o 8 -4 1 59.71 55.31 1.61 o 9 -4 1 23.58 19.88 1.19 o 10 -4 1 6.13 6.53 1.16 o -8 -3 1 26.22 31.58 1.39 o -7 -3 1 1.28 -1.05 2.33 o -6 -3 1 228.49 241.21 5.05 o -5 -3 1 373.91 378.12 5.58 o -4 -3 1 567.86 562.01 6.05 o -3 -3 1 453.14 448.21 4.86 o -2 -3 1 178.39 156.16 1.95 o -1 -3 1 68.22 48.21 1.01 o 0 -3 1 243.79 262.35 5.94 o 1 -3 1 1019.96 927.43 17.66 o 2 -3 1 935.84 857.31 11.67 o 3 -3 1 10.26 11.69 0.58 o 4 -3 1 518.58 582.35 5.15 o 5 -3 1 210.84 218.51 3.73 o 6 -3 1 211.24 245.24 4.35 o 7 -3 1 751.60 772.07 8.06 o 8 -3 1 1147.25 1086.40 10.34 o 9 -3 1 0.93 1.85 1.10 o 10 -3 1 0.69 0.73 1.13 o -9 -2 1 121.49 125.36 3.82 o -8 -2 1 90.02 94.15 2.66 o -7 -2 1 0.39 -1.31 2.06 o -6 -2 1 95.44 101.59 3.02 o -5 -2 1 1132.77 1204.64 9.00 o -4 -2 1 805.30 837.64 6.77 o -3 -2 1 339.89 348.74 3.94 o -2 -2 1 96.64 89.71 1.66 o -1 -2 1 80.35 86.23 1.33 o 0 -2 1 8.75 9.37 0.37 o 1 -2 1 471.64 589.71 8.56 o 2 -2 1 268.56 232.79 3.12 o 3 -2 1 254.29 356.63 3.63 o 4 -2 1 1.26 1.47 0.57 o 5 -2 1 1969.45 2146.72 10.88 o 6 -2 1 494.80 561.75 6.31 o 7 -2 1 44.83 48.21 1.43 o 8 -2 1 10.64 13.21 1.05 o 9 -2 1 1.33 3.84 1.11 o 10 -2 1 95.78 90.50 2.91 o -9 -1 1 20.09 21.96 1.29 o -8 -1 1 162.44 169.81 4.83 o -7 -1 1 73.66 86.78 2.64 o -6 -1 1 109.37 110.44 2.87 o -5 -1 1 281.76 310.38 4.46 o -4 -1 1 214.87 212.59 3.40 o -3 -1 1 1.24 -0.39 1.25 o -2 -1 1 1305.12 1403.43 8.49 o -1 -1 1 860.28 947.90 3.02 o 0 -1 1 4628.34 4488.93 24.07 o 1 -1 1 7033.65 7238.57 75.63 o 2 -1 1 2996.00 3489.20 30.57 o 3 -1 1 51.77 49.81 1.54 o 4 -1 1 829.13 1034.94 6.87 o 5 -1 1 131.73 158.51 3.33 o 6 -1 1 226.82 216.12 4.30 o 7 -1 1 133.29 139.24 3.92 o 8 -1 1 18.71 16.99 1.07 o 9 -1 1 81.49 79.96 2.47 o -10 0 1 25.82 25.20 1.45 o -9 0 1 38.57 35.39 1.43 o -8 0 1 228.53 234.16 5.27 o -7 0 1 508.14 508.86 6.65 o -6 0 1 2.78 4.55 0.75 o -5 0 1 445.00 520.69 5.41 o -4 0 1 1.24 1.54 0.57 o -3 0 1 844.42 838.59 5.03 o -2 0 1 2633.73 2588.71 18.09 o -1 0 1 6076.71 6173.87 59.50 o 1 0 1 541.73 618.55 7.33 o 2 0 1 64.53 70.09 1.29 o 3 0 1 2980.02 2830.08 10.11 o 4 0 1 458.52 431.86 4.75 o 5 0 1 204.34 185.23 3.68 o 6 0 1 53.62 52.02 1.63 o 7 0 1 58.59 57.08 1.90 o 8 0 1 112.51 104.78 3.22 o 9 0 1 68.87 64.09 2.04 o -10 1 1 0.79 -1.72 2.68 o -9 1 1 0.40 -1.78 2.36 o -8 1 1 535.79 499.94 7.03 o -7 1 1 677.51 703.16 7.47 o -6 1 1 276.90 270.78 4.39 o -5 1 1 29.20 6.56 0.65 o -4 1 1 344.00 326.44 3.68 o -3 1 1 137.42 178.72 2.45 o -2 1 1 1749.98 1832.74 30.39 o -1 1 1 2391.03 2372.18 13.50 o 0 1 1 2424.32 2233.21 19.49 o 1 1 1 4940.04 4959.18 27.09 o 2 1 1 2400.23 2288.26 7.43 o 3 1 1 1226.87 1269.97 7.33 o 4 1 1 0.56 0.06 0.62 o 5 1 1 66.70 62.50 1.87 o 6 1 1 7.93 8.72 0.93 o 7 1 1 154.23 142.51 3.73 o 8 1 1 193.67 190.90 5.27 o 9 1 1 103.95 101.52 3.05 o -10 2 1 35.35 37.25 1.43 o -9 2 1 1084.70 1050.84 10.68 o -8 2 1 1165.30 1094.66 9.94 o -7 2 1 341.74 378.63 5.48 o -6 2 1 138.44 194.25 3.68 o -5 2 1 760.66 872.12 6.53 o -4 2 1 587.47 608.60 4.87 o -3 2 1 1514.93 1581.55 6.62 o -2 2 1 12954.73 12283.77 53.35 o -1 2 1 1325.83 1249.39 3.39 o 0 2 1 5289.08 5015.96 60.46 o 1 2 1 1612.05 1687.45 4.94 o 2 2 1 564.90 571.86 6.01 o 3 2 1 116.77 148.63 2.96 o 4 2 1 13.50 11.04 0.73 o 5 2 1 247.37 254.23 4.63 o 6 2 1 30.24 25.96 1.12 o 7 2 1 54.82 51.12 1.49 o 8 2 1 90.40 93.97 2.81 o -11 3 1 14.68 12.97 1.33 o -10 3 1 30.43 30.59 1.39 o -9 3 1 10.96 11.87 1.06 o -8 3 1 9.43 11.66 0.99 o -7 3 1 315.52 301.26 4.93 o -6 3 1 853.33 873.44 7.33 o -5 3 1 794.37 836.09 6.43 o -4 3 1 343.61 376.21 3.96 o -3 3 1 597.55 565.37 4.29 o -2 3 1 4953.65 4772.14 28.72 o -1 3 1 111.45 145.88 1.63 o 0 3 1 544.29 475.17 2.80 o 1 3 1 86.47 88.47 1.55 o 2 3 1 366.24 409.42 4.00 o 3 3 1 183.88 158.57 3.31 o 4 3 1 96.25 93.81 2.69 o 5 3 1 499.12 499.74 6.76 o 6 3 1 33.89 38.13 1.25 o 7 3 1 0.64 1.95 1.07 o 8 3 1 26.93 32.10 1.52 o -11 4 1 60.99 66.94 2.05 o -10 4 1 34.89 36.43 1.44 o -9 4 1 1.44 -1.27 2.22 o -8 4 1 13.38 12.47 0.96 o -7 4 1 7.91 4.67 0.77 o -6 4 1 584.25 655.76 6.41 o -5 4 1 810.15 860.64 6.61 o -4 4 1 597.00 595.05 5.16 o -3 4 1 477.25 506.30 4.43 o -2 4 1 99.39 120.61 1.66 o -1 4 1 752.20 819.41 3.87 o 0 4 1 9.23 12.97 0.54 o 1 4 1 273.79 248.18 2.61 o 2 4 1 540.17 529.17 3.94 o 3 4 1 15.54 11.71 0.81 o 4 4 1 148.50 146.66 3.92 o 5 4 1 313.32 291.82 5.73 o 6 4 1 3.88 1.62 2.57 o 7 4 1 149.20 151.70 4.42 o -11 5 1 114.88 106.11 3.20 o -10 5 1 8.72 9.45 1.16 o -9 5 1 65.24 72.02 2.08 o -8 5 1 8.74 9.44 0.94 o -7 5 1 5.33 8.01 0.83 o -6 5 1 430.27 456.75 5.52 o -5 5 1 7.84 5.31 0.64 o -4 5 1 311.71 304.23 4.01 o -3 5 1 1936.63 2142.68 9.64 o -2 5 1 188.80 169.91 2.13 o -1 5 1 19.00 31.08 0.67 o 0 5 1 288.95 404.46 3.34 o 1 5 1 88.13 76.43 1.58 o 2 5 1 266.95 265.59 4.29 o 3 5 1 495.45 488.83 6.43 o 4 5 1 499.37 492.97 7.04 o 5 5 1 148.18 147.91 3.84 o 6 5 1 14.62 16.49 1.31 o -11 6 1 35.25 34.52 1.50 o -10 6 1 33.44 35.36 1.40 o -9 6 1 159.03 141.34 3.82 o -8 6 1 21.70 28.41 1.09 o -7 6 1 135.91 129.87 3.71 o -6 6 1 1043.99 1070.60 8.58 o -5 6 1 20.43 28.92 0.91 o -4 6 1 53.09 61.20 1.79 o -3 6 1 444.73 507.46 5.24 o -2 6 1 70.45 53.51 1.18 o -1 6 1 98.23 85.00 2.47 o 0 6 1 101.69 83.30 1.66 o 1 6 1 108.86 104.20 2.55 o 2 6 1 65.10 63.27 1.30 o 3 6 1 341.41 347.40 5.97 o 4 6 1 100.95 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