#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/33/2013308.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013308_Fobs loop_ _publ_author_name 'Freire, Eleonora' 'Baggio, Sergio' 'Mu\~noz, Juan Carlos' 'Baggio, Ricardo' _publ_section_title ; Two hydrates of 2,6-bis(1H-benzimidazol-2-yl)pyridine ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o259 _journal_page_last o262 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 104.810 _cell_angle_gamma 90.000 _cell_length_a 18.8126 _cell_length_b 18.4171 _cell_length_c 10.3219 _exptl_crystal_F_000 1416.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file kb1001IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' ef25 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 386.97 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2465.88 2491.13 54.44 o 3 0 0 21694.67 23149.79 213.36 o 4 0 0 14078.96 14500.50 181.87 o 5 0 0 729.65 686.75 50.68 o 6 0 0 4712.51 4985.25 135.14 o 7 0 0 143.00 218.42 41.51 o 8 0 0 2857.38 2884.50 169.48 o 9 0 0 7.54 5.99 26.98 o 10 0 0 763.37 880.20 93.08 o 11 0 0 4.62 -7.75 30.73 o 12 0 0 887.86 889.91 86.29 o 13 0 0 24.91 61.55 42.72 o 14 0 0 50.72 1.76 50.05 o 15 0 0 311.38 232.70 97.47 o 16 0 0 482.62 383.74 127.33 o 17 0 0 31.23 98.35 83.42 o 18 0 0 36.00 39.52 65.86 o 19 0 0 60.95 64.10 75.52 o 20 0 0 18.36 100.11 61.47 o 21 0 0 0.01 1.76 46.54 o 1 1 0 4083.96 3613.51 86.06 o 2 1 0 8609.25 8710.91 148.08 o 3 1 0 71.08 83.19 16.22 o 4 1 0 1074.47 1068.26 41.67 o 5 1 0 9902.92 10468.59 155.48 o 6 1 0 119.71 132.91 25.77 o 7 1 0 1704.69 1747.32 62.73 o 8 1 0 756.97 840.35 48.97 o 9 1 0 147.75 168.61 32.30 o 10 1 0 368.75 405.58 43.23 o 11 1 0 2932.21 3085.85 102.36 o 12 1 0 64.55 78.25 30.52 o 13 1 0 129.61 140.60 38.05 o 14 1 0 12.07 15.17 32.98 o 15 1 0 16.11 29.19 45.84 o 16 1 0 29.44 35.33 44.30 o 17 1 0 10.45 49.79 45.28 o 18 1 0 375.08 367.76 93.81 o 19 1 0 73.43 67.52 46.85 o 20 1 0 8.39 4.82 37.24 o 21 1 0 1.00 -22.13 34.13 o 0 2 0 1385.48 1263.52 40.13 o 1 2 0 51.54 74.84 10.63 o 2 2 0 2664.77 2609.60 42.92 o 3 2 0 2329.38 2373.04 54.14 o 4 2 0 217.63 222.02 25.93 o 5 2 0 1400.61 1320.64 53.11 o 6 2 0 2025.41 1977.60 67.25 o 7 2 0 4064.63 4282.84 119.76 o 8 2 0 1536.56 1565.08 64.08 o 9 2 0 1548.12 1773.39 71.63 o 10 2 0 37.14 53.82 24.88 o 11 2 0 342.96 405.79 45.30 o 12 2 0 874.97 800.97 59.65 o 13 2 0 477.54 551.85 66.72 o 14 2 0 64.20 72.03 39.03 o 15 2 0 0.71 14.44 40.07 o 16 2 0 84.71 88.31 54.95 o 17 2 0 3.40 -2.35 39.03 o 18 2 0 285.81 335.43 90.22 o 19 2 0 17.95 61.10 46.26 o 20 2 0 131.67 127.82 56.08 o 21 2 0 8.96 54.49 40.58 o 1 3 0 420.58 383.25 18.00 o 2 3 0 8083.92 7950.64 81.39 o 3 3 0 7213.53 7130.53 84.92 o 4 3 0 6514.33 6706.83 105.89 o 5 3 0 51.00 57.51 21.45 o 6 3 0 106.84 127.58 27.50 o 7 3 0 2393.66 2558.01 83.98 o 8 3 0 119.13 126.13 31.39 o 9 3 0 1402.24 1490.02 85.69 o 10 3 0 355.30 400.89 42.93 o 11 3 0 439.03 448.07 46.01 o 12 3 0 125.84 139.29 36.99 o 13 3 0 3.38 -18.38 31.63 o 14 3 0 154.35 162.79 53.10 o 15 3 0 138.80 169.83 54.56 o 16 3 0 3.72 35.52 43.46 o 17 3 0 39.87 76.95 54.36 o 18 3 0 40.84 38.25 41.10 o 19 3 0 101.10 88.04 53.07 o 20 3 0 3.62 16.06 39.38 o 21 3 0 51.74 49.69 44.99 o 0 4 0 324.58 286.07 22.66 o 1 4 0 31.96 40.71 12.38 o 2 4 0 12068.13 12366.51 113.00 o 3 4 0 5257.71 5281.53 78.75 o 4 4 0 1527.41 1518.27 46.94 o 5 4 0 2.96 8.04 16.88 o 6 4 0 30.78 46.76 20.95 o 7 4 0 2.92 12.97 21.00 o 8 4 0 24.61 60.76 26.94 o 9 4 0 164.73 181.68 38.59 o 10 4 0 298.46 367.57 56.75 o 11 4 0 5.52 5.57 30.09 o 12 4 0 33.07 87.59 44.54 o 13 4 0 52.02 106.89 49.07 o 14 4 0 63.63 118.67 43.91 o 15 4 0 488.15 611.75 76.26 o 16 4 0 127.91 106.13 55.45 o 17 4 0 214.22 162.76 63.30 o 18 4 0 81.82 101.35 58.01 o 19 4 0 66.35 64.70 46.51 o 20 4 0 69.39 129.21 61.50 o 21 4 0 35.86 46.12 46.54 o 1 5 0 1524.91 1487.95 35.30 o 2 5 0 2278.54 2106.89 50.63 o 3 5 0 7756.67 7594.81 99.72 o 4 5 0 223.62 200.22 23.95 o 5 5 0 0.27 9.07 14.14 o 6 5 0 394.89 417.16 38.93 o 7 5 0 7.02 18.06 19.44 o 8 5 0 3645.16 3852.79 114.92 o 9 5 0 68.13 67.02 29.82 o 10 5 0 609.05 665.64 58.00 o 11 5 0 121.78 157.57 46.84 o 12 5 0 326.92 301.82 61.84 o 13 5 0 30.60 46.05 40.02 o 14 5 0 1.65 16.89 37.94 o 15 5 0 154.93 179.70 55.41 o 16 5 0 172.72 218.96 58.25 o 17 5 0 166.39 175.85 64.51 o 18 5 0 1.24 24.83 43.15 o 19 5 0 0.35 27.01 37.13 o 20 5 0 108.52 119.83 60.15 o 21 5 0 62.62 32.19 44.08 o 0 6 0 4454.33 4327.75 92.33 o 1 6 0 522.54 506.84 24.35 o 2 6 0 651.83 698.29 33.88 o 3 6 0 512.99 520.16 31.52 o 4 6 0 3371.02 3451.35 77.29 o 5 6 0 1275.67 1236.32 49.52 o 6 6 0 4744.93 4884.42 100.59 o 7 6 0 9.06 16.42 22.25 o 8 6 0 69.64 100.07 31.22 o 9 6 0 405.69 426.37 48.96 o 10 6 0 506.00 520.28 54.29 o 11 6 0 329.51 332.26 56.20 o 12 6 0 7.68 3.71 36.55 o 13 6 0 173.36 135.82 51.01 o 14 6 0 0.18 2.28 37.20 o 15 6 0 17.44 15.92 40.66 o 16 6 0 65.18 89.40 48.17 o 17 6 0 4.40 -3.77 41.56 o 18 6 0 7.69 48.58 48.23 o 19 6 0 21.30 41.43 47.26 o 20 6 0 21.85 53.71 46.88 o 1 7 0 4.05 0.64 11.17 o 2 7 0 2.89 25.19 14.09 o 3 7 0 546.87 561.48 34.31 o 4 7 0 3273.98 3347.71 78.66 o 5 7 0 1746.14 1803.64 62.99 o 6 7 0 580.61 534.29 38.62 o 7 7 0 308.85 308.53 34.56 o 8 7 0 50.53 61.45 28.53 o 9 7 0 12.54 9.09 24.50 o 10 7 0 53.37 46.08 30.97 o 11 7 0 1855.83 1823.78 97.54 o 12 7 0 142.64 104.05 39.85 o 13 7 0 258.12 306.53 71.01 o 14 7 0 443.77 459.24 72.64 o 15 7 0 580.46 569.63 81.64 o 16 7 0 19.57 54.48 42.04 o 17 7 0 24.31 46.89 44.42 o 18 7 0 125.10 118.70 64.43 o 19 7 0 20.11 21.95 77.28 o 20 7 0 1.03 46.54 71.13 o 0 8 0 1165.11 1163.10 58.47 o 1 8 0 89.02 104.71 18.93 o 2 8 0 25.52 42.87 14.25 o 3 8 0 67.62 81.88 22.14 o 4 8 0 279.95 324.44 31.39 o 5 8 0 14.34 7.42 16.30 o 6 8 0 988.59 1017.27 51.38 o 7 8 0 599.96 642.91 43.96 o 8 8 0 0.13 2.41 17.04 o 9 8 0 461.63 494.03 52.40 o 10 8 0 2.45 2.51 27.63 o 11 8 0 96.03 112.64 41.81 o 12 8 0 51.97 38.24 33.25 o 13 8 0 327.28 336.62 62.88 o 14 8 0 34.01 32.63 37.41 o 15 8 0 23.73 25.79 36.52 o 16 8 0 362.77 373.55 99.23 o 17 8 0 19.74 46.97 55.87 o 18 8 0 89.94 93.08 94.84 o 19 8 0 37.06 76.40 86.93 o 20 8 0 16.10 69.37 82.54 o 1 9 0 712.80 739.36 36.64 o 2 9 0 23.78 34.28 15.08 o 3 9 0 552.88 519.37 36.28 o 4 9 0 310.78 289.44 34.91 o 5 9 0 2029.89 2022.94 70.58 o 6 9 0 5.25 10.89 18.42 o 7 9 0 1279.65 1325.20 63.24 o 8 9 0 121.89 135.58 30.30 o 9 9 0 75.98 89.91 31.70 o 10 9 0 110.31 126.14 39.86 o 11 9 0 0.96 3.92 27.55 o 12 9 0 15.24 15.54 31.74 o 13 9 0 22.31 34.93 39.14 o 14 9 0 2.41 12.36 48.25 o 15 9 0 224.59 254.84 87.31 o 16 9 0 27.12 48.50 61.03 o 17 9 0 0.03 18.12 51.85 o 18 9 0 45.42 89.57 86.93 o 19 9 0 35.02 63.23 79.91 o 0 10 0 81.28 110.74 31.60 o 1 10 0 7.98 6.35 13.71 o 2 10 0 8.21 21.71 16.32 o 3 10 0 331.92 334.81 28.19 o 4 10 0 471.76 525.10 41.50 o 5 10 0 151.84 183.06 33.67 o 6 10 0 57.21 71.87 25.09 o 7 10 0 42.96 67.46 25.68 o 8 10 0 409.84 429.77 43.52 o 9 10 0 0.08 -20.23 23.67 o 10 10 0 113.94 101.18 46.54 o 11 10 0 416.18 380.54 76.31 o 12 10 0 545.00 578.00 87.07 o 13 10 0 33.71 36.31 43.12 o 14 10 0 207.49 205.57 65.99 o 15 10 0 6.38 34.88 54.44 o 16 10 0 12.23 47.19 58.33 o 17 10 0 2.42 48.93 61.39 o 18 10 0 34.17 32.04 58.05 o 19 10 0 20.48 81.67 90.45 o 1 11 0 156.44 162.24 25.14 o 2 11 0 1482.98 1476.46 54.26 o 3 11 0 1207.03 1175.92 46.73 o 4 11 0 470.88 487.75 50.58 o 5 11 0 197.16 213.84 44.05 o 6 11 0 92.87 105.52 34.47 o 7 11 0 101.31 135.90 39.32 o 8 11 0 15.55 20.62 29.35 o 9 11 0 461.19 436.82 71.64 o 10 11 0 166.12 134.30 52.69 o 11 11 0 153.07 135.88 53.26 o 12 11 0 1097.23 982.38 101.26 o 13 11 0 0.26 19.89 42.54 o 14 11 0 102.14 59.85 49.23 o 15 11 0 85.01 79.43 65.39 o 16 11 0 10.33 55.80 57.13 o 17 11 0 19.57 82.08 63.01 o 18 11 0 10.34 23.06 57.18 o 0 12 0 338.55 344.00 45.37 o 1 12 0 110.69 122.22 24.13 o 2 12 0 750.12 757.57 51.39 o 3 12 0 42.09 57.54 32.13 o 4 12 0 31.45 18.06 26.15 o 5 12 0 98.40 107.56 35.70 o 6 12 0 25.16 39.06 29.36 o 7 12 0 7.71 17.72 27.79 o 8 12 0 206.40 249.37 54.32 o 9 12 0 275.45 229.72 63.56 o 10 12 0 50.54 68.84 44.97 o 11 12 0 208.88 237.58 67.46 o 12 12 0 24.69 7.36 39.25 o 13 12 0 132.29 102.02 54.10 o 14 12 0 131.75 184.29 61.87 o 15 12 0 453.92 474.30 93.46 o 16 12 0 97.85 119.49 70.10 o 17 12 0 1.83 8.36 47.08 o 18 12 0 38.31 83.03 64.72 o 1 13 0 22.81 20.19 24.39 o 2 13 0 45.35 45.63 27.17 o 3 13 0 0.10 19.42 23.30 o 4 13 0 215.20 208.91 46.91 o 5 13 0 24.07 43.79 32.52 o 6 13 0 106.34 92.80 38.43 o 7 13 0 568.99 510.78 62.85 o 8 13 0 471.67 463.60 72.94 o 9 13 0 143.52 147.27 54.65 o 10 13 0 919.93 792.75 88.14 o 11 13 0 109.62 120.25 53.55 o 12 13 0 946.35 799.66 106.52 o 13 13 0 27.33 31.77 45.78 o 14 13 0 23.83 159.33 75.84 o 15 13 0 308.93 448.12 85.73 o 16 13 0 22.35 38.31 56.37 o 17 13 0 10.30 -9.29 79.47 o 0 14 0 69.11 55.82 47.62 o 1 14 0 26.77 61.41 31.89 o 2 14 0 67.37 83.98 36.52 o 3 14 0 556.38 579.14 60.65 o 4 14 0 18.09 58.33 31.26 o 5 14 0 163.70 207.46 50.49 o 6 14 0 4.15 11.62 30.26 o 7 14 0 96.28 88.06 39.77 o 8 14 0 214.03 202.95 57.16 o 9 14 0 2.29 19.85 39.03 o 10 14 0 365.61 375.83 78.22 o 11 14 0 54.40 59.52 45.63 o 12 14 0 64.84 64.83 50.75 o 13 14 0 326.04 307.72 76.76 o 14 14 0 31.83 42.13 44.27 o 15 14 0 8.34 50.02 46.18 o 16 14 0 33.01 66.60 65.45 o 1 15 0 131.98 98.15 39.15 o 2 15 0 549.20 577.73 63.71 o 3 15 0 36.12 41.81 29.57 o 4 15 0 28.51 18.66 34.06 o 5 15 0 585.82 539.09 75.82 o 6 15 0 23.61 26.25 39.13 o 7 15 0 28.18 22.16 36.67 o 8 15 0 762.94 656.96 78.26 o 9 15 0 385.58 341.54 73.81 o 10 15 0 6.57 18.01 38.01 o 11 15 0 27.75 22.70 41.94 o 12 15 0 112.98 95.56 51.07 o 13 15 0 85.39 58.02 47.74 o 14 15 0 0.63 17.48 41.98 o 15 15 0 11.84 37.66 43.38 o 0 16 0 486.07 383.77 92.70 o 1 16 0 5.57 50.39 39.00 o 2 16 0 101.59 101.39 43.59 o 3 16 0 156.24 192.52 58.12 o 4 16 0 274.48 276.17 65.88 o 5 16 0 381.51 408.63 72.14 o 6 16 0 151.54 123.06 48.11 o 7 16 0 159.34 168.70 70.10 o 8 16 0 7.70 4.61 50.52 o 9 16 0 31.31 72.80 61.86 o 10 16 0 47.59 75.30 58.21 o 11 16 0 351.67 261.67 68.29 o 12 16 0 4.42 36.42 39.50 o 13 16 0 13.55 15.18 42.95 o 14 16 0 7.87 11.87 43.75 o 1 17 0 37.10 33.93 33.09 o 2 17 0 20.87 35.75 40.57 o 3 17 0 243.92 186.76 57.88 o 4 17 0 286.82 228.09 59.13 o 5 17 0 11.44 27.95 42.04 o 6 17 0 43.34 20.58 51.41 o 7 17 0 22.52 24.45 48.10 o 8 17 0 18.68 38.61 51.05 o 9 17 0 18.16 59.23 60.87 o 10 17 0 20.87 36.89 58.15 o 11 17 0 0.53 -15.08 51.49 o 12 17 0 9.10 42.41 57.81 o 13 17 0 12.79 -2.49 49.11 o 0 18 0 101.43 130.84 83.42 o 1 18 0 0.07 22.63 40.72 o 2 18 0 302.53 275.45 81.74 o 3 18 0 2.57 42.23 46.84 o 4 18 0 12.55 36.72 42.05 o 5 18 0 0.61 4.40 32.69 o 6 18 0 40.42 58.52 57.67 o 7 18 0 79.69 154.32 68.06 o 8 18 0 52.07 40.66 49.03 o 9 18 0 4.73 -12.10 69.37 o 10 18 0 165.69 130.52 68.08 o 11 18 0 2.23 23.52 55.26 o 12 18 0 105.26 154.17 75.37 o 1 19 0 12.80 -8.74 36.82 o 2 19 0 0.80 18.18 46.23 o 3 19 0 11.30 49.97 36.70 o 4 19 0 99.42 118.75 57.59 o 5 19 0 5.61 2.63 60.59 o 6 19 0 73.94 56.81 54.31 o 7 19 0 21.28 -2.97 47.68 o 8 19 0 0.34 18.44 55.99 o 9 19 0 67.09 95.85 66.43 o 10 19 0 27.78 74.89 59.26 o 0 20 0 50.44 51.81 76.40 o 1 20 0 62.35 78.84 54.89 o 2 20 0 3.51 11.07 39.06 o 3 20 0 62.68 73.13 50.60 o 4 20 0 19.59 29.10 45.32 o 5 20 0 12.74 34.25 84.30 o 6 20 0 18.49 36.00 67.62 o 7 20 0 1.66 77.28 79.03 o 8 20 0 0.10 29.86 70.25 o 1 21 0 22.20 24.93 43.35 o 2 21 0 86.59 162.03 120.74 o 3 21 0 4.97 45.15 42.62 o 4 21 0 70.09 -60.59 67.62 o 5 21 0 8.29 54.44 72.88 o 6 21 0 5.86 67.62 76.40 o -22 1 1 24.12 31.25 36.07 o -21 1 1 9.43 65.18 45.63 o -20 1 1 76.82 18.90 43.15 o -19 1 1 261.14 270.49 81.35 o -18 1 1 32.72 26.97 44.94 o -17 1 1 63.68 50.07 46.80 o -16 1 1 21.05 51.32 41.58 o -15 1 1 1.47 15.05 35.22 o -14 1 1 5.05 -2.30 36.32 o -13 1 1 60.50 72.02 38.67 o -12 1 1 23.09 13.88 24.35 o -11 1 1 1627.40 1749.84 73.27 o -10 1 1 333.62 362.39 38.72 o -9 1 1 138.98 143.79 28.93 o -8 1 1 503.06 522.01 33.66 o -7 1 1 508.46 474.11 29.99 o -6 1 1 11596.59 11992.88 124.28 o -5 1 1 37592.96 36052.91 195.88 o -4 1 1 15275.40 14801.40 275.27 o -3 1 1 765.76 727.87 25.57 o -2 1 1 680.95 673.33 24.77 o -1 1 1 15565.76 15375.86 124.97 o 0 1 1 2264.30 2012.68 40.94 o 1 1 1 21062.40 19353.62 235.01 o 2 1 1 21.46 25.56 12.32 o 3 1 1 4402.49 4537.87 91.32 o 4 1 1 2205.58 2356.41 75.00 o 5 1 1 317.10 353.08 36.52 o 6 1 1 216.04 216.69 34.73 o 7 1 1 4.95 5.20 19.44 o 8 1 1 508.06 571.44 44.27 o 9 1 1 205.27 268.34 41.36 o 10 1 1 900.91 940.43 60.60 o 11 1 1 0.62 6.30 24.07 o 12 1 1 74.13 55.28 31.25 o 13 1 1 599.26 612.56 56.98 o 14 1 1 60.48 91.27 35.39 o 15 1 1 212.46 238.37 61.85 o 16 1 1 248.58 343.11 85.72 o 17 1 1 47.76 68.08 52.87 o 18 1 1 14.49 -9.66 31.67 o 19 1 1 260.40 267.38 83.18 o 20 1 1 21.71 35.89 38.82 o 21 1 1 4.99 55.71 45.56 o -21 2 1 17.09 7.69 38.20 o -20 2 1 8.58 -11.03 37.55 o -19 2 1 47.18 100.72 51.06 o -18 2 1 389.97 462.09 92.72 o -17 2 1 678.15 658.88 100.27 o -16 2 1 23.06 49.02 44.38 o -15 2 1 138.33 178.66 70.78 o -14 2 1 78.55 88.38 42.58 o -13 2 1 259.23 297.09 61.76 o -12 2 1 15.41 20.36 33.24 o -11 2 1 113.47 87.13 29.27 o -10 2 1 123.56 201.24 32.26 o -9 2 1 3290.52 3421.39 81.46 o -8 2 1 2186.10 2294.15 61.53 o -7 2 1 737.94 772.85 34.87 o -6 2 1 7234.63 7468.47 90.64 o -5 2 1 16566.12 16328.40 170.06 o -4 2 1 4430.54 4482.93 83.91 o -3 2 1 29470.97 28492.74 189.96 o -2 2 1 2258.73 2076.33 37.10 o -1 2 1 10.73 13.32 7.55 o 0 2 1 498.48 450.49 22.48 o 1 2 1 67.89 85.26 16.89 o 2 2 1 3483.60 3427.35 68.72 o 3 2 1 2568.98 2505.77 120.98 o 4 2 1 23935.50 23464.50 356.20 o 5 2 1 619.72 606.79 45.38 o 6 2 1 455.52 452.27 43.57 o 7 2 1 23.45 28.29 23.13 o 8 2 1 57.36 51.80 28.40 o 9 2 1 1033.14 1104.56 75.20 o 10 2 1 441.27 435.51 45.14 o 11 2 1 157.45 278.98 44.47 o 12 2 1 41.84 37.08 27.74 o 13 2 1 208.96 274.35 45.33 o 14 2 1 55.58 59.04 39.71 o 15 2 1 0.00 51.37 39.59 o 16 2 1 0.18 10.90 32.18 o 17 2 1 233.60 189.58 65.83 o 18 2 1 18.16 27.21 40.35 o 19 2 1 45.73 18.54 74.20 o 20 2 1 19.44 46.65 40.76 o 21 2 1 2.19 33.06 39.43 o -21 3 1 145.16 125.34 62.38 o -20 3 1 176.85 143.04 65.14 o -19 3 1 6.00 9.96 39.52 o -18 3 1 299.14 251.09 80.37 o -17 3 1 49.05 45.76 51.82 o -16 3 1 253.75 280.89 83.80 o -15 3 1 854.23 794.19 103.07 o -14 3 1 248.30 326.81 67.90 o -13 3 1 0.01 60.88 39.78 o -12 3 1 514.44 557.69 64.97 o -11 3 1 1.31 5.11 16.83 o -10 3 1 178.23 238.12 31.31 o -9 3 1 1133.92 1192.25 55.86 o -8 3 1 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