#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:45:19 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180802 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/33/2013362.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013362_Fobs loop_ _publ_author_name 'Arranz Mascar\'os, Paloma' 'Guti\'errez Valero, M. Dolores' 'Low, John N.' 'Glidewell, Christopher' _publ_section_title ; N-(6-Amino-3,4-dihydro-3-methyl-5-nitroso-4-oxopyrimidin-2-yl)-(S)-glutamic acid: a three-dimensional framework structure built from O---H···O, N---H···O and O---H···N hydrogen bonds ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o210 _journal_page_last o212 _journal_volume 59 _journal_year 2003 _space_group_IT_number 18 _symmetry_space_group_name_Hall 'P 2 2ab' _symmetry_space_group_name_H-M 'P 21 21 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 19.4182 _cell_length_b 6.9420 _cell_length_c 9.0534 _exptl_crystal_F_000 624.00 _reflns_d_resolution_high 0.7713 _cod_data_source_file sk1626VIIsup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 058 - SHELXL' _shelx_refln_list_code 4 _shelx_f_calc_maximum 121.08 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' 'x+1/2, -y+1/2, -z' '-x+1/2, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 263.02 287.00 11.52 o 8 0 0 164.25 175.43 11.70 o 10 0 0 1622.69 1828.50 72.51 o 12 0 0 716.02 662.71 32.54 o 14 0 0 94.59 99.24 14.82 o 16 0 0 148.02 115.33 19.00 o 18 0 0 672.48 666.50 39.33 o 20 0 0 11.78 -13.41 37.93 o 22 0 0 0.15 26.76 37.85 o 24 0 0 138.62 159.94 106.55 o 1 1 0 635.86 607.98 29.36 o 2 1 0 526.67 541.97 16.78 o 3 1 0 1028.43 972.00 23.27 o 4 1 0 6971.21 6319.95 85.02 o 5 1 0 2088.22 1950.16 39.42 o 6 1 0 2462.27 2395.28 37.82 o 7 1 0 30.54 14.86 9.81 o 8 1 0 316.54 278.86 10.47 o 9 1 0 219.81 284.45 14.00 o 10 1 0 1454.98 1620.27 41.41 o 11 1 0 33.14 20.03 8.57 o 12 1 0 118.42 142.77 10.85 o 13 1 0 323.79 350.62 20.68 o 14 1 0 0.02 17.65 9.33 o 15 1 0 0.74 12.85 9.33 o 16 1 0 1.20 4.26 11.92 o 17 1 0 4.51 -2.18 11.65 o 18 1 0 299.10 349.81 19.70 o 19 1 0 23.06 22.28 17.44 o 20 1 0 17.76 36.69 23.47 o 21 1 0 0.50 17.79 30.88 o 22 1 0 28.93 26.70 37.85 o 23 1 0 0.13 -26.70 80.22 o 24 1 0 8.59 -44.47 44.47 o 25 1 0 1.12 -26.70 80.22 o 0 2 0 10591.30 9651.26 177.34 o 1 2 0 8917.97 7466.02 91.45 o 2 2 0 9691.74 8575.35 349.04 o 3 2 0 14659.85 13423.04 212.68 o 4 2 0 11102.27 11013.71 151.42 o 5 2 0 114.35 109.26 11.75 o 6 2 0 24.75 52.20 11.65 o 7 2 0 516.19 512.75 12.81 o 8 2 0 392.74 370.33 12.24 o 9 2 0 35.38 26.08 9.86 o 10 2 0 10.11 -7.56 9.99 o 11 2 0 327.96 311.22 11.37 o 12 2 0 421.56 424.43 27.75 o 13 2 0 38.28 40.29 8.62 o 14 2 0 8.46 16.59 10.49 o 15 2 0 176.69 175.15 17.24 o 16 2 0 83.99 45.08 13.53 o 17 2 0 127.28 137.00 15.53 o 18 2 0 17.35 34.81 14.55 o 19 2 0 78.94 56.59 23.00 o 20 2 0 285.00 289.22 33.84 o 21 2 0 1.55 17.36 30.12 o 22 2 0 6.04 58.65 48.88 o 23 2 0 42.07 135.74 48.97 o 24 2 0 0.04 -26.95 80.60 o 1 3 0 92.66 90.26 13.66 o 2 3 0 110.91 117.27 11.00 o 3 3 0 312.34 272.24 13.25 o 4 3 0 5.32 5.33 11.91 o 5 3 0 1819.17 1635.62 37.27 o 6 3 0 40.13 46.27 13.22 o 7 3 0 2.37 13.06 14.95 o 8 3 0 89.26 85.66 11.66 o 9 3 0 1.12 5.18 11.59 o 10 3 0 0.89 15.86 11.81 o 11 3 0 329.93 338.37 14.32 o 12 3 0 103.87 91.21 10.89 o 13 3 0 98.50 84.91 10.18 o 14 3 0 55.48 86.44 9.97 o 15 3 0 6.97 -7.41 10.60 o 16 3 0 1.43 16.63 12.73 o 17 3 0 12.26 20.48 22.83 o 18 3 0 29.69 22.27 17.50 o 19 3 0 7.93 -22.26 22.26 o 20 3 0 27.60 46.43 26.28 o 21 3 0 46.30 61.30 30.31 o 22 3 0 62.55 76.73 68.37 o 23 3 0 0.39 -38.87 40.42 o 0 4 0 28.11 -13.66 19.32 o 1 4 0 156.58 157.24 11.27 o 2 4 0 124.00 98.34 12.00 o 3 4 0 858.12 910.81 30.97 o 4 4 0 3760.54 4006.65 79.25 o 5 4 0 2475.39 2593.30 51.57 o 6 4 0 1093.69 1078.26 27.82 o 7 4 0 1566.10 1460.18 44.11 o 8 4 0 35.25 15.77 11.75 o 9 4 0 3.71 -5.24 11.71 o 10 4 0 54.27 57.45 16.33 o 11 4 0 33.04 26.03 15.64 o 12 4 0 67.45 69.63 11.12 o 13 4 0 268.31 273.18 16.69 o 14 4 0 53.20 46.97 13.70 o 15 4 0 1.10 -9.85 13.96 o 16 4 0 86.86 92.74 16.92 o 17 4 0 0.02 0.00 15.81 o 18 4 0 83.79 77.19 24.34 o 19 4 0 80.38 116.79 37.09 o 20 4 0 25.35 93.46 47.41 o 21 4 0 0.13 40.11 61.12 o 22 4 0 5.19 38.74 66.00 o 1 5 0 748.28 788.91 20.37 o 2 5 0 134.81 132.42 10.98 o 3 5 0 3.61 5.37 12.00 o 4 5 0 112.45 123.48 14.63 o 5 5 0 43.93 69.87 12.02 o 6 5 0 102.92 98.67 11.74 o 7 5 0 658.77 671.41 23.60 o 8 5 0 281.36 325.66 26.35 o 9 5 0 105.16 137.45 18.82 o 10 5 0 1.46 15.97 12.54 o 11 5 0 56.28 46.25 16.41 o 12 5 0 25.55 26.83 14.88 o 13 5 0 55.04 8.74 30.27 o 14 5 0 214.29 188.62 37.65 o 15 5 0 1.37 -39.81 39.81 o 16 5 0 0.50 6.34 20.59 o 17 5 0 49.09 31.55 31.43 o 18 5 0 0.06 25.62 42.20 o 19 5 0 4.07 51.46 36.36 o 20 5 0 0.31 30.62 42.17 o 0 6 0 449.54 507.88 164.76 o 1 6 0 66.94 60.44 13.47 o 2 6 0 0.09 -5.98 13.05 o 3 6 0 130.35 142.07 14.68 o 4 6 0 153.75 130.31 16.84 o 5 6 0 0.20 -2.93 13.00 o 6 6 0 492.30 445.81 27.00 o 7 6 0 1085.38 1312.83 41.92 o 8 6 0 427.06 556.75 44.60 o 9 6 0 239.16 289.82 33.61 o 10 6 0 38.93 65.42 37.04 o 11 6 0 90.65 67.11 26.86 o 12 6 0 0.17 -6.71 27.05 o 13 6 0 10.11 35.00 21.78 o 14 6 0 71.00 80.97 34.65 o 15 6 0 14.01 -15.44 39.77 o 16 6 0 21.37 -29.77 42.89 o 17 6 0 1.02 17.83 30.83 o 18 6 0 52.20 106.77 34.14 o 1 7 0 21.25 13.62 17.28 o 2 7 0 46.86 46.32 15.06 o 3 7 0 66.36 108.74 135.86 o 4 7 0 60.96 52.95 21.54 o 5 7 0 36.33 4.43 16.81 o 6 7 0 37.18 5.33 20.04 o 7 7 0 10.04 -13.45 46.58 o 8 7 0 18.38 30.22 34.45 o 9 7 0 52.64 54.60 38.60 o 10 7 0 5.77 -21.86 21.86 o 11 7 0 51.26 44.81 52.79 o 12 7 0 72.94 39.25 38.43 o 13 7 0 0.08 17.85 33.14 o 14 7 0 0.82 22.86 38.42 o 15 7 0 1.63 33.62 34.31 o 0 8 0 10.69 26.70 53.40 o 1 8 0 11.40 -26.70 37.76 o 2 8 0 2.67 0.00 22.07 o 3 8 0 9.14 26.69 37.75 o 4 8 0 0.01 46.42 21.54 o 5 8 0 10.51 13.19 21.41 o 6 8 0 2.22 -21.41 21.41 o 7 8 0 5.02 11.99 22.50 o 8 8 0 90.84 113.65 44.14 o 9 8 0 101.04 110.04 34.22 o 10 8 0 187.00 122.10 50.44 o 11 8 0 52.74 43.55 34.43 o 2 0 1 2008.86 1868.86 33.15 o 3 0 1 335.39 269.71 8.59 o 4 0 1 2773.70 2694.10 59.24 o 5 0 1 2.72 6.71 13.41 o 6 0 1 27.38 24.39 17.19 o 7 0 1 185.16 133.72 7.94 o 8 0 1 161.50 200.66 8.06 o 9 0 1 2300.48 2179.93 41.61 o 10 0 1 219.90 205.30 8.14 o 11 0 1 220.41 230.07 9.29 o 12 0 1 14.85 12.87 8.39 o 13 0 1 16.55 23.34 8.17 o 14 0 1 4.04 1.39 8.48 o 15 0 1 105.70 105.95 15.91 o 16 0 1 11.03 31.22 13.83 o 17 0 1 1032.69 1071.41 30.67 o 18 0 1 607.21 615.85 36.26 o 19 0 1 367.65 392.23 51.03 o 20 0 1 67.34 35.73 35.22 o 21 0 1 253.54 268.89 43.30 o 22 0 1 5.77 33.38 26.73 o 23 0 1 42.45 66.59 39.80 o 24 0 1 51.85 0.00 79.85 o 25 0 1 10.11 -26.70 47.74 o 0 1 1 3068.24 2716.96 41.93 o 1 1 1 296.87 265.16 7.65 o 2 1 1 5872.43 5255.04 52.87 o 3 1 1 585.01 540.81 7.07 o 4 1 1 363.68 333.28 6.76 o 5 1 1 1932.15 1797.15 21.84 o 6 1 1 3776.97 3765.80 38.75 o 7 1 1 2125.78 2239.16 29.71 o 8 1 1 374.27 360.09 9.98 o 9 1 1 2794.47 2827.73 41.81 o 10 1 1 816.94 890.87 15.12 o 11 1 1 704.52 660.57 11.55 o 12 1 1 89.94 93.20 6.95 o 13 1 1 469.65 530.88 14.51 o 14 1 1 32.05 25.87 5.89 o 15 1 1 93.21 83.17 7.17 o 16 1 1 410.82 420.04 12.50 o 17 1 1 577.56 596.87 17.38 o 18 1 1 402.72 409.17 17.20 o 19 1 1 179.09 171.34 17.17 o 20 1 1 44.89 56.38 15.24 o 21 1 1 30.84 34.05 15.95 o 22 1 1 53.36 26.70 31.45 o 23 1 1 8.90 80.15 31.45 o 24 1 1 25.36 22.93 45.40 o 0 2 1 38.16 54.89 27.45 o 1 2 1 1903.37 1889.23 19.66 o 2 2 1 3062.87 2927.94 87.06 o 3 2 1 1276.32 1291.85 33.52 o 4 2 1 1475.45 1331.89 18.99 o 5 2 1 1309.22 1186.79 19.63 o 6 2 1 54.76 42.12 8.33 o 7 2 1 63.68 62.00 6.76 o 8 2 1 658.26 701.16 12.42 o 9 2 1 1146.74 1159.89 18.91 o 10 2 1 264.87 283.47 6.71 o 11 2 1 249.23 234.40 6.86 o 12 2 1 71.21 76.16 5.79 o 13 2 1 98.92 98.89 6.60 o 14 2 1 468.11 536.66 19.06 o 15 2 1 211.64 190.44 10.06 o 16 2 1 333.25 313.32 12.37 o 17 2 1 281.89 307.79 13.27 o 18 2 1 1.47 13.67 10.66 o 19 2 1 117.64 123.41 18.20 o 20 2 1 99.68 128.45 17.26 o 21 2 1 233.12 262.21 25.62 o 22 2 1 115.53 172.93 25.38 o 23 2 1 7.16 50.93 26.80 o 24 2 1 5.44 0.05 42.00 o 0 3 1 128.06 127.46 9.03 o 1 3 1 115.08 104.27 8.55 o 2 3 1 1347.59 1372.32 37.68 o 3 3 1 898.46 926.50 14.69 o 4 3 1 463.70 466.93 8.87 o 5 3 1 2725.04 2713.15 29.26 o 6 3 1 1744.70 1841.31 25.66 o 7 3 1 106.49 101.63 7.57 o 8 3 1 435.06 418.98 10.25 o 9 3 1 7.68 14.09 7.25 o 10 3 1 483.60 465.06 9.40 o 11 3 1 438.85 428.25 9.54 o 12 3 1 155.93 184.40 9.55 o 13 3 1 100.69 102.52 7.98 o 14 3 1 846.19 881.34 24.48 o 15 3 1 2.95 -0.01 8.79 o 16 3 1 37.33 42.31 8.93 o 17 3 1 3.82 1.64 10.10 o 18 3 1 23.84 31.11 10.88 o 19 3 1 59.14 75.69 14.70 o 20 3 1 50.96 36.25 17.87 o 21 3 1 113.79 143.82 28.05 o 22 3 1 73.07 60.64 29.64 o 23 3 1 69.43 38.23 32.68 o 0 4 1 90.78 90.50 9.52 o 1 4 1 176.68 177.23 6.52 o 2 4 1 107.50 102.61 7.75 o 3 4 1 147.49 136.89 8.07 o 4 4 1 257.13 273.73 7.11 o 5 4 1 1552.78 1604.35 28.28 o 6 4 1 367.23 380.32 12.37 o 7 4 1 247.00 249.38 11.39 o 8 4 1 476.83 456.86 13.80 o 9 4 1 18.54 33.13 9.69 o 10 4 1 24.37 41.47 9.94 o 11 4 1 15.11 27.88 9.85 o 12 4 1 194.04 185.24 11.64 o 13 4 1 215.69 197.79 14.26 o 14 4 1 269.25 258.36 18.93 o 15 4 1 73.10 95.97 10.12 o 16 4 1 35.72 47.74 10.63 o 17 4 1 1.46 -10.00 10.00 o 18 4 1 6.01 -2.06 11.61 o 19 4 1 0.69 10.48 21.66 o 20 4 1 12.81 22.75 33.24 o 21 4 1 61.94 43.69 30.20 o 22 4 1 43.63 63.63 36.15 o 0 5 1 55.31 53.75 10.16 o 1 5 1 395.72 379.35 13.36 o 2 5 1 373.30 385.50 9.11 o 3 5 1 56.25 76.03 8.01 o 4 5 1 105.44 112.72 9.39 o 5 5 1 264.72 257.90 12.28 o 6 5 1 103.41 122.47 10.73 o 7 5 1 247.41 254.19 11.83 o 8 5 1 136.45 118.72 10.36 o 9 5 1 44.72 42.90 11.64 o 10 5 1 193.63 213.72 16.92 o 11 5 1 143.37 164.01 13.87 o 12 5 1 5.69 21.24 13.27 o 13 5 1 168.12 205.83 20.85 o 14 5 1 135.57 133.94 14.25 o 15 5 1 0.67 -0.94 14.49 o 16 5 1 21.73 33.00 17.36 o 17 5 1 98.62 125.02 36.38 o 18 5 1 53.76 69.35 37.35 o 19 5 1 21.17 12.85 41.24 o 20 5 1 8.10 20.11 44.87 o 0 6 1 19.04 13.44 13.44 o 1 6 1 29.89 44.04 8.89 o 2 6 1 38.28 29.71 8.85 o 3 6 1 14.89 9.79 8.31 o 4 6 1 147.26 146.36 16.09 o 5 6 1 38.91 38.32 8.38 o 6 6 1 60.62 74.87 11.49 o 7 6 1 231.38 206.71 18.89 o 8 6 1 180.55 169.58 15.48 o 9 6 1 130.46 112.20 20.18 o 10 6 1 296.79 340.73 19.57 o 11 6 1 90.20 108.60 17.10 o 12 6 1 84.08 83.15 17.24 o 13 6 1 54.50 53.43 23.18 o 14 6 1 15.74 -1.17 20.46 o 15 6 1 9.88 41.21 25.93 o 16 6 1 48.77 62.70 19.61 o 17 6 1 0.84 -7.82 17.37 o 18 6 1 33.17 23.33 21.94 o 0 7 1 91.38 97.45 12.85 o 1 7 1 118.58 95.29 9.99 o 2 7 1 321.59 381.21 20.37 o 3 7 1 121.29 123.78 31.44 o 4 7 1 2.15 -7.65 10.94 o 5 7 1 64.11 52.41 12.41 o 6 7 1 89.91 73.56 22.75 o 7 7 1 18.70 26.75 23.93 o 8 7 1 162.00 187.73 25.67 o 9 7 1 2.18 11.40 17.83 o 10 7 1 163.75 181.23 22.83 o 11 7 1 36.58 26.84 21.90 o 12 7 1 10.32 34.78 22.99 o 13 7 1 62.14 64.31 21.40 o 14 7 1 22.98 50.93 29.13 o 15 7 1 9.91 -13.53 18.86 o 0 8 1 14.12 -26.69 37.75 o 1 8 1 3.22 4.49 19.15 o 2 8 1 2.89 5.40 13.53 o 3 8 1 32.80 26.89 20.39 o 4 8 1 22.00 36.94 19.84 o 5 8 1 8.49 0.00 15.82 o 6 8 1 2.19 0.02 17.47 o 7 8 1 42.50 26.44 17.55 o 8 8 1 67.70 45.51 24.63 o 9 8 1 12.09 12.31 16.30 o 10 8 1 107.88 134.25 27.63 o 11 8 1 14.84 16.63 19.45 o 0 0 2 2548.99 2060.96 64.75 o 2 0 2 265.48 199.19 13.54 o 3 0 2 1837.83 1549.90 35.95 o 4 0 2 10824.85 10817.84 270.62 o 5 0 2 1154.68 1070.08 38.15 o 6 0 2 3438.90 3735.51 75.16 o 7 0 2 25.94 30.35 10.60 o 8 0 2 3749.94 3902.36 56.41 o 9 0 2 37.47 50.37 10.27 o 10 0 2 1.57 -2.89 8.56 o 11 0 2 116.36 128.08 8.56 o 12 0 2 8.63 20.73 8.16 o 13 0 2 70.62 67.60 8.49 o 14 0 2 112.44 99.36 8.83 o 15 0 2 15.02 11.87 11.75 o 16 0 2 499.30 505.90 18.71 o 17 0 2 634.62 583.57 23.58 o 18 0 2 0.88 -8.83 21.61 o 19 0 2 101.58 148.36 27.10 o 20 0 2 28.49 13.31 25.18 o 21 0 2 59.73 48.67 26.71 o 22 0 2 1.83 26.57 56.28 o 23 0 2 6.53 39.80 37.58 o 24 0 2 0.46 -26.57 79.72 o 0 1 2 2065.63 1886.40 32.90 o 1 1 2 2189.40 1909.13 22.56 o 2 1 2 3467.55 3133.15 86.20 o 3 1 2 2448.70 2378.06 35.37 o 4 1 2 70.79 60.87 9.06 o 5 1 2 810.08 798.06 13.43 o 6 1 2 3093.44 3160.18 34.48 o 7 1 2 192.32 221.88 6.45 o 8 1 2 257.59 269.43 6.82 o 9 1 2 68.71 67.76 6.22 o 10 1 2 1287.59 1389.12 27.03 o 11 1 2 221.94 217.09 8.31 o 12 1 2 366.56 388.70 12.00 o 13 1 2 129.46 133.54 7.04 o 14 1 2 1.78 7.50 5.99 o 15 1 2 236.68 262.16 11.58 o 16 1 2 259.20 252.43 11.98 o 17 1 2 99.84 75.35 9.74 o 18 1 2 268.69 254.44 14.60 o 19 1 2 50.88 69.50 13.80 o 20 1 2 14.07 1.56 16.63 o 21 1 2 33.62 15.11 22.81 o 22 1 2 46.45 10.19 26.83 o 23 1 2 23.02 -13.33 26.67 o 24 1 2 3.05 -23.42 36.55 o 0 2 2 2982.84 3122.22 55.07 o 1 2 2 52.03 37.10 11.84 o 2 2 2 26.10 35.31 10.80 o 3 2 2 530.53 496.24 8.45 o 4 2 2 1402.27 1282.02 20.82 o 5 2 2 217.71 222.23 6.83 o 6 2 2 590.27 647.28 12.49 o 7 2 2 1611.32 1647.28 21.49 o 8 2 2 349.35 397.84 8.27 o 9 2 2 466.81 514.20 11.92 o 10 2 2 127.99 118.89 7.42 o 11 2 2 248.91 233.47 7.21 o 12 2 2 701.50 711.79 12.99 o 13 2 2 21.04 13.79 6.51 o 14 2 2 293.39 292.78 10.05 o 15 2 2 267.90 283.40 11.88 o 16 2 2 189.29 187.03 11.38 o 17 2 2 222.51 166.58 12.93 o 18 2 2 7.70 -4.58 14.52 o 19 2 2 148.85 151.45 18.84 o 20 2 2 43.09 44.21 19.47 o 21 2 2 15.13 1.55 27.09 o 22 2 2 75.46 119.45 29.68 o 23 2 2 23.37 36.85 30.88 o 24 2 2 16.89 33.47 37.60 o 0 3 2 536.41 573.17 13.45 o 1 3 2 128.92 132.46 6.92 o 2 3 2 1569.54 1534.40 22.31 o 3 3 2 73.61 77.80 8.03 o 4 3 2 241.59 247.94 6.89 o 5 3 2 350.23 338.78 9.22 o 6 3 2 17.36 18.33 8.29 o 7 3 2 217.54 223.62 7.65 o 8 3 2 68.16 77.16 6.59 o 9 3 2 30.66 33.89 7.57 o 10 3 2 271.49 245.10 7.59 o 11 3 2 18.92 22.19 6.59 o 12 3 2 263.96 274.64 10.44 o 13 3 2 143.82 130.90 7.80 o 14 3 2 402.77 399.17 11.57 o 15 3 2 33.79 15.49 7.83 o 16 3 2 32.45 39.48 8.62 o 17 3 2 22.41 30.11 12.81 o 18 3 2 14.36 21.43 16.83 o 19 3 2 36.09 74.08 19.55 o 20 3 2 30.43 37.12 19.61 o 21 3 2 38.19 33.45 30.63 o 22 3 2 15.22 16.60 34.86 o 23 3 2 7.13 9.43 28.55 o 0 4 2 271.65 331.20 11.87 o 1 4 2 87.28 83.78 6.72 o 2 4 2 87.45 88.79 6.71 o 3 4 2 480.06 486.05 9.36 o 4 4 2 58.39 58.35 8.06 o 5 4 2 173.76 165.94 7.31 o 6 4 2 205.83 212.07 7.54 o 7 4 2 219.35 251.03 8.31 o 8 4 2 93.73 99.82 8.42 o 9 4 2 85.26 81.15 6.89 o 10 4 2 66.44 63.74 8.15 o 11 4 2 294.63 311.47 14.59 o 12 4 2 914.83 930.86 33.63 o 13 4 2 193.62 171.48 11.11 o 14 4 2 3.75 -2.49 8.59 o 15 4 2 215.65 236.58 11.63 o 16 4 2 117.71 96.79 19.60 o 17 4 2 5.49 8.13 10.96 o 18 4 2 1.18 24.40 13.77 o 19 4 2 45.24 40.06 30.64 o 20 4 2 95.18 76.45 28.12 o 21 4 2 41.74 88.87 40.59 o 22 4 2 7.78 -14.91 31.34 o 0 5 2 4.87 19.29 10.22 o 1 5 2 19.12 21.15 8.05 o 2 5 2 130.16 126.07 7.08 o 3 5 2 214.06 183.97 7.69 o 4 5 2 136.92 131.81 7.83 o 5 5 2 51.85 37.34 8.01 o 6 5 2 71.87 77.56 8.21 o 7 5 2 53.21 65.72 8.49 o 8 5 2 276.13 240.35 15.31 o 9 5 2 25.05 7.99 9.15 o 10 5 2 216.91 177.06 12.20 o 11 5 2 527.55 563.34 17.19 o 12 5 2 20.31 -10.63 13.36 o 13 5 2 61.52 114.61 62.55 o 14 5 2 0.68 0.01 11.66 o 15 5 2 96.14 100.18 13.87 o 16 5 2 42.74 20.26 13.82 o 17 5 2 29.18 13.07 15.15 o 18 5 2 57.83 103.59 25.08 o 19 5 2 5.97 16.09 21.88 o 20 5 2 3.65 -17.98 34.48 o 0 6 2 293.50 289.46 11.33 o 1 6 2 57.38 43.40 7.65 o 2 6 2 20.58 18.94 8.57 o 3 6 2 139.89 148.46 8.72 o 4 6 2 39.34 48.91 10.88 o 5 6 2 6.40 -0.02 10.28 o 6 6 2 66.48 73.11 13.84 o 7 6 2 79.80 87.80 12.28 o 8 6 2 214.16 238.07 22.25 o 9 6 2 46.97 32.73 16.18 o 10 6 2 38.20 24.14 13.52 o 11 6 2 185.06 248.93 30.16 o 12 6 2 43.96 37.11 21.65 o 13 6 2 3.71 -21.31 21.31 o 14 6 2 3.37 10.18 21.28 o 15 6 2 84.95 64.80 26.53 o 16 6 2 113.60 144.91 30.68 o 17 6 2 5.27 -6.55 28.88 o 18 6 2 8.82 -27.52 27.52 o 0 7 2 0.07 13.55 15.23 o 1 7 2 7.37 -3.39 9.92 o 2 7 2 27.35 40.03 9.80 o 3 7 2 52.75 46.58 12.37 o 4 7 2 20.65 18.94 15.98 o 5 7 2 16.65 -34.53 34.53 o 6 7 2 10.13 29.48 19.39 o 7 7 2 51.88 39.52 18.65 o 8 7 2 89.38 81.78 20.58 o 9 7 2 12.89 30.04 15.43 o 10 7 2 71.89 32.87 19.46 o 11 7 2 3.21 5.30 18.57 o 12 7 2 12.67 38.50 18.12 o 13 7 2 35.26 46.59 21.75 o 14 7 2 0.17 10.77 18.71 o 15 7 2 15.79 34.65 32.46 o 0 8 2 40.75 13.28 37.73 o 1 8 2 0.84 -13.76 13.76 o 2 8 2 26.83 5.26 19.81 o 3 8 2 1.39 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