#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2013363.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013363_Fobs loop_ _publ_author_name 'Anderson, James N.' 'Brookes, Neil J.' 'Coe, Benjamin J.' 'Coles, Simon J.' 'Light, Mark E.' 'Hursthouse, Michael B.' _publ_section_title ; trans-Bis[1,2-bis(diphenylphosphino)ethane-\k^2^P,P']bis[4-(trimethylsilyl)buta-1,3-diynyl]ruthenium(II) and trans-bis[1,2-bis(diphenylphosphino)ethane-\k^2^P,P']bis(buta-1,3-diynyl)ruthenium(II) ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m215 _journal_page_last m217 _journal_volume 59 _journal_year 2003 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 110.325 _cell_angle_beta 93.158 _cell_angle_gamma 96.365 _cell_length_a 12.6771 _cell_length_b 16.0582 _cell_length_c 16.0851 _exptl_crystal_F_000 1188.00 _reflns_d_resolution_high 0.7707 _[local]_cod_data_source_file sk1628Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' SHELXL INS file, from DIRDIF output for S92' _shelx_refln_list_code 4 _shelx_f_calc_maximum 275.62 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4580.79 3895.49 92.80 o 3 0 0 1452.31 1358.91 39.43 o 4 0 0 246.82 141.53 8.90 o 5 0 0 2282.76 2321.58 56.01 o 6 0 0 2.34 -4.52 9.64 o 7 0 0 1421.56 1169.57 37.28 o 8 0 0 934.06 946.71 34.10 o 9 0 0 84.14 55.09 18.17 o 10 0 0 7.05 -12.12 19.32 o 11 0 0 327.54 397.45 37.74 o 12 0 0 134.61 74.09 30.81 o 13 0 0 2699.03 2497.82 174.52 o 14 0 0 801.66 795.62 65.19 o 15 0 0 1989.02 2099.07 133.54 o 16 0 0 443.71 553.44 72.86 o -16 1 0 174.22 121.78 59.51 o -15 1 0 403.90 313.10 50.11 o -14 1 0 1546.74 1629.13 108.34 o -13 1 0 392.40 482.36 46.50 o -12 1 0 3750.82 3972.49 176.43 o -11 1 0 187.56 124.64 23.28 o -10 1 0 1502.14 1570.53 66.94 o -9 1 0 321.84 325.68 26.87 o -8 1 0 5520.83 5128.73 142.59 o -7 1 0 294.23 230.19 20.36 o -6 1 0 234.68 239.93 16.21 o 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7541.00 6627.48 145.91 o -1 2 0 283.07 237.27 9.30 o 1 2 0 0.44 4.91 2.65 o 2 2 0 4049.64 3522.12 183.65 o 3 2 0 6757.35 7013.95 195.84 o 4 2 0 558.50 366.96 17.26 o 5 2 0 6314.42 6235.64 233.82 o 6 2 0 683.03 696.79 25.88 o 7 2 0 3162.83 2974.98 105.20 o 8 2 0 321.00 296.95 22.52 o 9 2 0 742.83 628.02 33.17 o 10 2 0 156.54 135.78 27.59 o 11 2 0 1493.80 1657.67 70.04 o 12 2 0 288.52 203.93 32.98 o 13 2 0 190.82 194.19 39.78 o 14 2 0 451.39 599.76 76.77 o 15 2 0 3.14 -27.21 71.57 o -16 3 0 44.82 79.87 85.77 o -15 3 0 401.44 411.91 60.32 o -14 3 0 77.73 140.58 43.64 o -13 3 0 67.61 82.50 34.57 o -12 3 0 4.45 -26.48 23.56 o -11 3 0 987.25 943.01 43.35 o -10 3 0 4593.46 4558.11 121.18 o -9 3 0 2507.55 2632.73 71.22 o -8 3 0 5877.52 5685.41 125.63 o -7 3 0 1587.10 1451.15 47.09 o -6 3 0 498.87 470.35 21.15 o -5 3 0 905.16 825.43 25.51 o -4 3 0 447.94 544.62 17.96 o -3 3 0 464.89 589.78 17.76 o -2 3 0 3896.33 3759.29 89.00 o -1 3 0 2564.29 2739.65 101.91 o 0 3 0 5341.23 5099.58 284.08 o 1 3 0 4093.06 3813.96 247.28 o 2 3 0 2482.67 2463.36 179.09 o 3 3 0 2762.01 2765.88 77.79 o 4 3 0 12004.07 12309.12 503.59 o 5 3 0 2081.17 2200.14 62.92 o 6 3 0 10397.45 10757.83 380.46 o 7 3 0 196.97 134.81 17.33 o 8 3 0 4401.95 4442.46 154.00 o 9 3 0 253.23 217.25 22.95 o 10 3 0 23.06 39.13 16.45 o 11 3 0 1186.49 1187.23 59.30 o 12 3 0 1608.62 1733.27 101.04 o 13 3 0 163.57 123.96 73.09 o 14 3 0 110.97 137.39 49.89 o 15 3 0 5.80 -23.97 61.98 o -16 4 0 283.58 338.63 79.78 o -15 4 0 263.01 293.81 60.29 o -14 4 0 33.57 7.13 29.92 o -13 4 0 203.02 287.90 34.89 o -12 4 0 0.88 27.99 22.25 o -11 4 0 1906.31 2033.55 73.48 o -10 4 0 54.60 57.55 14.28 o -9 4 0 2080.10 2493.50 75.72 o -8 4 0 901.34 999.00 33.61 o -7 4 0 3810.24 3931.00 105.04 o -6 4 0 3452.25 3436.19 81.86 o -5 4 0 0.58 3.06 13.11 o -3 4 0 2762.54 2598.22 61.36 o -2 4 0 4606.44 4782.56 118.55 o -1 4 0 673.59 507.73 16.54 o 0 4 0 11868.54 11984.92 675.81 o 1 4 0 1710.14 1644.08 106.55 o 2 4 0 6254.13 6624.60 499.26 o 3 4 0 629.26 706.11 46.29 o 4 4 0 6060.56 6399.15 325.39 o 5 4 0 6984.14 6976.68 399.36 o 6 4 0 219.73 238.02 20.89 o 7 4 0 980.95 978.02 38.50 o 8 4 0 672.72 732.22 33.74 o 9 4 0 5811.97 6143.41 212.45 o 10 4 0 2142.09 2217.71 99.21 o 11 4 0 2787.96 2855.75 135.50 o 12 4 0 368.94 325.76 36.25 o 13 4 0 0.44 -3.44 31.47 o 14 4 0 7.14 65.75 41.12 o 15 4 0 3.66 10.23 82.45 o -16 5 0 733.93 754.11 123.96 o -15 5 0 324.22 424.31 81.06 o -14 5 0 18.13 8.01 26.89 o -13 5 0 46.68 101.49 30.95 o -12 5 0 1002.88 1052.06 53.43 o -11 5 0 167.90 132.24 19.77 o -10 5 0 1289.57 1356.09 74.92 o -9 5 0 315.48 308.49 34.49 o -8 5 0 959.05 1011.45 39.43 o -7 5 0 1316.23 1457.50 62.50 o -6 5 0 478.88 365.39 24.07 o -5 5 0 2617.65 2454.53 65.51 o -4 5 0 6998.42 6973.07 189.63 o -3 5 0 23299.87 21976.38 540.35 o -2 5 0 3993.74 3855.41 92.96 o -1 5 0 44285.53 44730.75 1801.66 o 0 5 0 2368.17 2448.27 150.44 o 1 5 0 489.16 520.94 17.15 o 2 5 0 8924.57 9001.75 661.33 o 3 5 0 4211.94 3974.42 248.72 o 4 5 0 3197.44 3263.21 248.38 o 5 5 0 964.58 948.67 39.20 o 6 5 0 2.84 36.15 14.29 o 7 5 0 37.83 45.86 15.50 o 8 5 0 449.90 529.09 30.68 o 9 5 0 1004.87 983.38 56.13 o 10 5 0 2134.37 2117.63 105.92 o 11 5 0 8.28 5.38 27.33 o 12 5 0 3127.82 3312.88 287.33 o 13 5 0 474.64 418.90 58.62 o 14 5 0 23.04 106.71 82.45 o 15 5 0 0.77 -17.25 71.92 o -16 6 0 86.74 93.48 88.88 o -15 6 0 701.28 769.37 102.89 o -14 6 0 7.72 -31.38 50.34 o -13 6 0 351.17 359.43 61.25 o -12 6 0 0.00 45.02 30.81 o -11 6 0 2893.63 2880.91 104.16 o -10 6 0 314.19 254.44 32.84 o -9 6 0 132.09 96.11 30.47 o -8 6 0 298.67 268.21 32.45 o -7 6 0 2087.79 2122.24 58.95 o -6 6 0 3565.30 3387.22 91.28 o -5 6 0 794.54 723.53 27.27 o -4 6 0 23520.72 22438.42 669.75 o -3 6 0 169.03 211.25 23.30 o -2 6 0 4342.74 4652.83 165.84 o -1 6 0 2059.30 1900.57 53.53 o 0 6 0 7707.33 7959.34 489.46 o 1 6 0 217.71 215.81 14.02 o 2 6 0 5776.31 6508.37 562.04 o 3 6 0 1178.81 1137.53 82.41 o 4 6 0 1074.91 1132.17 65.20 o 5 6 0 428.80 393.41 36.98 o 6 6 0 1838.76 2070.93 104.69 o 7 6 0 702.01 707.71 29.95 o 8 6 0 38.91 49.18 20.85 o 9 6 0 3515.18 3831.41 206.60 o 10 6 0 137.47 137.53 25.38 o 11 6 0 1028.04 953.00 55.17 o 12 6 0 894.38 1086.27 131.38 o 13 6 0 0.14 5.21 35.19 o 14 6 0 367.28 435.03 99.40 o -15 7 0 496.05 539.96 105.59 o -14 7 0 858.74 892.34 100.54 o -13 7 0 61.07 65.61 57.64 o -12 7 0 2328.76 2362.66 192.49 o -11 7 0 19.40 -0.11 25.97 o -10 7 0 372.92 342.42 42.93 o -9 7 0 127.68 127.65 26.93 o -8 7 0 37.54 66.90 21.41 o -7 7 0 491.22 448.50 28.91 o -6 7 0 66.34 88.11 33.84 o -5 7 0 5833.29 5912.32 145.47 o -4 7 0 39.76 18.36 13.67 o -3 7 0 854.87 529.71 43.92 o -2 7 0 1032.80 967.16 60.37 o -1 7 0 3048.64 3063.97 110.10 o 0 7 0 420.73 392.32 19.74 o 1 7 0 10871.13 11598.33 657.74 o 2 7 0 6039.59 5588.54 345.40 o 3 7 0 124.16 153.24 17.84 o 4 7 0 365.13 387.99 32.49 o 5 7 0 68.14 47.04 13.10 o 6 7 0 343.62 381.09 47.90 o 7 7 0 567.23 491.91 42.66 o 8 7 0 1676.96 1775.34 85.91 o 9 7 0 849.14 742.98 45.55 o 10 7 0 947.34 915.56 54.82 o 11 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0 2144.50 2169.83 183.19 o -13 9 0 506.87 447.60 90.56 o -12 9 0 1943.97 2031.56 128.85 o -11 9 0 63.16 61.03 43.80 o -10 9 0 261.85 254.37 41.35 o -9 9 0 627.48 525.74 60.47 o -8 9 0 284.27 359.58 41.35 o -7 9 0 1703.15 1820.41 71.44 o -6 9 0 84.60 64.10 11.22 o -5 9 0 152.90 149.79 47.52 o -4 9 0 2323.44 2385.57 69.96 o -3 9 0 3.25 0.84 16.08 o -2 9 0 1654.36 1640.58 80.18 o -1 9 0 1147.56 1064.53 57.77 o 0 9 0 1201.13 1192.07 61.23 o 1 9 0 10788.27 11015.46 682.85 o 2 9 0 15967.99 16682.21 1083.57 o 3 9 0 570.82 655.64 36.59 o 4 9 0 1142.35 1113.72 82.84 o 5 9 0 1.50 5.36 12.90 o 6 9 0 3640.56 3765.13 200.15 o 7 9 0 1158.01 1244.31 58.70 o 8 9 0 1053.89 1123.02 91.84 o 9 9 0 22.64 57.71 23.65 o 10 9 0 73.24 37.78 31.08 o 11 9 0 8.63 24.69 30.40 o 12 9 0 6.50 -46.48 43.27 o 13 9 0 361.94 416.90 66.37 o -15 10 0 181.21 39.47 132.44 o -14 10 0 65.98 90.77 74.60 o -13 10 0 1579.94 1642.23 146.78 o -12 10 0 42.72 55.63 51.73 o -11 10 0 1412.59 1520.81 89.02 o -10 10 0 1299.75 1402.00 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93.94 100.51 20.33 o 4 12 0 3.44 30.41 20.11 o 5 12 0 2157.10 2203.14 170.65 o 6 12 0 120.79 110.22 30.82 o 7 12 0 1532.19 1492.89 83.38 o 8 12 0 779.52 636.57 65.58 o 9 12 0 335.21 371.41 67.68 o 10 12 0 377.17 340.01 80.11 o 11 12 0 96.57 16.08 44.73 o -13 13 0 7.12 -8.23 130.68 o -12 13 0 77.16 170.01 92.71 o -11 13 0 2.83 -47.29 63.00 o -10 13 0 130.80 119.46 51.43 o -9 13 0 2414.34 2565.52 173.03 o -8 13 0 19.29 26.24 34.65 o -7 13 0 852.81 977.86 43.99 o -6 13 0 112.55 107.61 31.92 o -5 13 0 1409.39 1447.14 74.23 o -4 13 0 536.41 543.53 64.14 o -3 13 0 2411.74 2517.92 110.85 o -2 13 0 2872.01 3128.13 178.92 o -1 13 0 300.65 357.72 36.42 o 0 13 0 177.65 207.75 30.32 o 1 13 0 162.19 122.53 24.78 o 2 13 0 30.38 35.91 19.65 o 3 13 0 41.88 13.74 36.38 o 4 13 0 2588.21 2599.16 154.81 o 5 13 0 30.39 25.81 20.09 o 6 13 0 1477.14 1509.34 78.74 o 7 13 0 155.44 80.28 37.40 o 8 13 0 15.69 6.62 52.06 o 9 13 0 682.62 623.02 106.13 o 10 13 0 340.32 296.45 83.03 o -12 14 0 24.75 84.89 89.58 o 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