#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:45:19 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180802 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/33/2013390.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013390_Fobs loop_ _publ_author_name 'Celestian, Aaron J.' 'Parise, John B.' 'Tripathi, Akhilesh' 'Kvick, \%Ake' 'Vaughan, Gavin M. B.' _publ_section_title ; (K~4~Li~4~)Al~8~Ge~8~O~32~·8H~2~O: an Li^+-exchanged potassium aluminogermanate with the zeolite gismondine (GIS) topology ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first i74 _journal_page_last i76 _journal_volume 59 _journal_year 2003 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 134.119 _cell_angle_gamma 90.000 _cell_length_a 14.8075 _cell_length_b 9.5404 _cell_length_c 10.3937 _exptl_crystal_F_000 762.00 _reflns_d_resolution_high 0.8510 _cod_data_source_file bc1016Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Li K GIS in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 212.08 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 8675.12 8553.96 151.52 o 8 0 0 4026.36 4073.18 157.86 o 10 0 0 140.95 124.14 6.60 o 12 0 0 3080.96 3191.35 137.92 o 7 1 0 13805.51 12609.11 356.62 o 9 1 0 21.97 24.08 3.41 o 11 1 0 295.53 292.85 11.41 o 6 2 0 592.95 638.99 15.96 o 8 2 0 7240.76 7520.88 174.71 o 10 2 0 478.65 452.20 14.31 o 12 2 0 5019.67 5169.89 128.61 o 5 3 0 28666.11 26554.63 850.73 o 7 3 0 6096.78 5743.05 147.91 o 9 3 0 5540.40 5495.65 191.24 o 11 3 0 4022.96 4112.97 101.04 o 4 4 0 8991.66 9483.70 286.17 o 6 4 0 3606.51 3531.99 176.57 o 8 4 0 2596.73 2788.50 49.18 o 10 4 0 15.45 23.79 2.45 o 1 5 0 5.77 13.35 2.96 o 3 5 0 5928.90 7353.43 456.87 o 5 5 0 6200.98 6014.13 223.37 o 7 5 0 446.62 334.22 25.70 o 9 5 0 6002.39 5917.02 249.11 o 11 5 0 2363.69 2414.34 46.46 o 0 6 0 10855.74 11617.19 1161.33 o 2 6 0 3027.34 3283.49 183.83 o 4 6 0 7295.84 7499.68 475.75 o 6 6 0 6732.09 6136.60 348.44 o 8 6 0 9869.87 9748.00 549.13 o 10 6 0 1470.13 1424.07 33.38 o 1 7 0 32.39 26.16 3.34 o 3 7 0 44.90 107.95 20.53 o 5 7 0 6220.45 6022.47 626.16 o 7 7 0 1091.49 1076.73 89.53 o 9 7 0 6379.77 7134.61 188.09 o 0 8 0 5328.19 5769.64 388.24 o 2 8 0 287.19 322.06 12.17 o 4 8 0 1002.71 1366.35 240.16 o 6 8 0 467.34 418.26 48.86 o 8 8 0 180.71 188.45 18.03 o 1 9 0 5547.98 6012.40 429.15 o 3 9 0 2110.10 2148.52 90.76 o 5 9 0 8175.49 8712.24 1181.64 o 7 9 0 2063.38 2314.26 175.67 o 0 10 0 552.94 719.68 188.75 o 2 10 0 0.05 5.44 2.53 o 4 10 0 2855.84 2727.59 76.34 o 1 11 0 708.99 640.86 36.45 o -13 1 1 16.32 13.30 4.38 o -11 1 1 6042.17 6255.64 129.01 o -9 1 1 820.35 789.21 21.20 o -7 1 1 10246.96 9764.69 168.47 o 5 1 1 22011.94 21756.05 277.80 o 7 1 1 4068.29 3907.56 62.22 o 9 1 1 5571.21 5982.53 115.89 o 11 1 1 1769.84 1756.02 62.76 o -12 2 1 2735.00 2517.38 55.35 o -10 2 1 4611.47 4632.07 117.23 o -8 2 1 5219.46 4846.05 140.60 o -6 2 1 15349.21 16322.78 908.00 o 4 2 1 3299.05 3237.93 100.31 o 6 2 1 35792.52 36776.04 785.97 o 8 2 1 3038.38 3000.60 52.28 o 10 2 1 5664.43 5558.11 160.02 o -11 3 1 120.30 136.57 5.05 o -9 3 1 110.01 141.11 4.60 o -7 3 1 1785.24 1801.89 34.06 o -5 3 1 1775.08 2089.28 24.13 o 5 3 1 3382.56 3527.64 69.29 o 7 3 1 53.16 76.91 3.98 o 9 3 1 1403.52 1637.04 38.55 o -12 4 1 10.47 19.00 5.65 o -10 4 1 9864.71 10532.53 108.72 o -8 4 1 7552.68 6740.56 237.47 o -6 4 1 27367.22 27544.27 473.11 o -4 4 1 14672.46 15907.69 441.01 o 2 4 1 3528.01 2700.67 648.60 o 4 4 1 206.63 210.12 16.70 o 6 4 1 14171.98 14284.11 620.52 o 8 4 1 78.99 40.74 3.73 o 10 4 1 5253.34 5534.45 144.86 o -11 5 1 7142.32 7449.94 174.37 o -9 5 1 1201.85 1202.96 52.52 o -7 5 1 13092.06 13913.91 189.22 o -5 5 1 4883.80 5083.83 227.00 o -3 5 1 20878.55 25130.41 1940.09 o -1 5 1 6653.14 8300.69 389.62 o 1 5 1 18346.79 18784.34 1549.14 o 3 5 1 5344.50 4730.12 743.22 o 5 5 1 6789.38 6173.17 465.61 o 7 5 1 5321.12 5786.29 357.65 o 9 5 1 3435.86 3208.51 81.73 o -10 6 1 123.30 76.58 3.29 o -8 6 1 0.46 8.54 2.40 o -6 6 1 470.35 507.33 13.64 o -4 6 1 8.90 4.33 2.43 o -2 6 1 10.66 7.34 2.09 o 0 6 1 18.33 11.99 3.05 o 2 6 1 1520.74 1574.67 64.48 o 4 6 1 448.62 448.94 49.74 o 6 6 1 328.92 224.68 19.38 o 8 6 1 108.68 115.30 6.66 o -9 7 1 1195.62 1071.62 58.50 o -7 7 1 9397.89 10387.52 211.57 o -5 7 1 5859.48 6014.09 263.10 o -3 7 1 20673.22 21777.39 1025.08 o -1 7 1 2905.45 3431.20 236.54 o 1 7 1 13165.28 14539.02 1480.91 o 3 7 1 21.27 20.59 3.67 o 5 7 1 3302.12 2799.03 372.33 o 7 7 1 1829.33 1966.26 61.13 o -8 8 1 652.44 598.53 28.09 o -6 8 1 14122.22 14409.79 270.71 o -4 8 1 5237.17 5835.11 199.67 o -2 8 1 9552.28 11049.85 815.62 o 0 8 1 3957.24 4217.67 189.73 o 2 8 1 7440.91 7551.81 482.76 o 4 8 1 115.98 110.77 4.48 o 6 8 1 3829.71 3423.79 268.56 o -7 9 1 742.77 743.39 20.21 o -5 9 1 29.35 10.37 2.51 o -3 9 1 1128.20 1231.62 62.94 o -1 9 1 666.23 822.55 91.11 o 1 9 1 185.35 210.63 7.71 o 3 9 1 8.20 12.29 6.44 o 5 9 1 100.88 81.82 4.44 o -6 10 1 3149.76 3239.48 251.21 o -4 10 1 613.67 605.99 27.02 o -2 10 1 3790.61 4353.98 163.91 o 0 10 1 102.64 101.91 8.35 o 2 10 1 5291.85 5584.11 421.45 o 4 10 1 299.03 324.36 16.04 o -3 11 1 6635.39 6045.72 777.00 o -1 11 1 874.35 899.25 85.97 o 1 11 1 7601.04 7130.30 286.24 o -14 0 2 7097.40 7842.63 306.52 o -12 0 2 12045.24 12906.98 398.33 o -10 0 2 16437.53 17139.86 456.31 o -8 0 2 23322.58 25708.27 372.36 o 4 0 2 27104.84 26467.83 578.13 o 6 0 2 175.56 140.23 5.78 o 8 0 2 15945.33 16191.37 429.42 o 10 0 2 1049.98 1130.83 63.37 o -13 1 2 4713.23 4688.78 68.27 o -11 1 2 101.35 96.81 5.32 o -9 1 2 17759.38 18519.56 306.46 o -7 1 2 5849.63 6431.86 118.90 o 3 1 2 921.93 849.33 11.15 o 5 1 2 4610.43 4284.45 78.46 o 7 1 2 2652.31 2415.97 38.81 o 9 1 2 591.27 581.99 8.06 o -14 2 2 992.74 975.18 43.26 o -12 2 2 48.67 62.42 3.18 o -10 2 2 823.71 810.47 23.47 o -8 2 2 4853.44 4945.69 80.77 o 4 2 2 4251.99 4124.78 113.25 o 6 2 2 38.56 42.78 2.76 o 8 2 2 381.95 349.67 5.64 o 10 2 2 310.80 343.04 19.41 o -13 3 2 10634.74 11061.74 334.74 o -11 3 2 360.70 299.05 4.94 o -9 3 2 33688.57 31949.16 1884.47 o -7 3 2 692.81 602.58 17.12 o 3 3 2 34578.58 30642.08 1448.45 o 5 3 2 4168.72 3740.02 92.54 o 7 3 2 11520.61 10867.10 270.38 o 9 3 2 588.94 518.55 15.72 o -12 4 2 2579.23 2544.25 113.61 o -10 4 2 6499.70 6102.31 126.06 o -8 4 2 1567.09 1618.59 31.73 o -6 4 2 21909.22 22362.07 867.15 o 2 4 2 35.86 26.31 4.57 o 4 4 2 1381.69 1241.52 57.60 o 6 4 2 9.42 11.85 2.82 o 8 4 2 3550.55 3478.15 92.79 o -11 5 2 27.46 45.65 2.75 o -9 5 2 819.43 828.26 14.02 o -7 5 2 1778.22 1692.48 45.26 o -5 5 2 3605.70 3930.98 114.06 o -3 5 2 2531.14 2509.92 158.53 o -1 5 2 15393.13 17854.74 2149.75 o 1 5 2 3060.48 2357.11 659.68 o 3 5 2 11561.00 10471.53 735.93 o 5 5 2 6.15 37.60 3.08 o 7 5 2 733.57 667.05 31.41 o -12 6 2 779.60 658.75 58.54 o -10 6 2 1270.61 1335.03 44.66 o -8 6 2 8469.48 8782.15 196.07 o -6 6 2 87.64 120.57 17.35 o -4 6 2 22914.63 22766.23 837.99 o -2 6 2 14794.70 14502.21 1236.22 o 0 6 2 20542.09 17945.93 3750.88 o 2 6 2 21939.44 16557.60 5493.82 o 4 6 2 7999.44 7604.52 553.87 o 6 6 2 4197.39 4166.09 304.83 o 8 6 2 2629.16 2431.43 91.47 o -11 7 2 10.06 28.77 2.27 o -9 7 2 1795.16 1663.00 38.23 o -7 7 2 56.45 60.18 3.22 o -5 7 2 12133.17 12724.86 277.72 o -3 7 2 2897.21 3046.15 119.66 o -1 7 2 11618.83 12767.11 928.36 o 1 7 2 1147.80 1301.59 107.56 o 3 7 2 5323.50 3513.88 1241.14 o 5 7 2 59.97 64.21 5.39 o 7 7 2 2721.44 2824.73 262.65 o -10 8 2 960.14 845.12 35.46 o -8 8 2 340.56 295.94 5.52 o -6 8 2 364.82 365.69 8.37 o -4 8 2 1155.48 1316.39 47.48 o -2 8 2 2113.51 2211.18 320.30 o 0 8 2 1783.80 1873.88 150.51 o 2 8 2 541.18 555.05 49.88 o 4 8 2 530.74 365.32 113.65 o 6 8 2 2.67 1.42 1.38 o -9 9 2 5207.68 5341.10 219.21 o -7 9 2 233.35 293.31 15.96 o -5 9 2 7624.86 7897.06 340.21 o -3 9 2 676.92 607.51 64.18 o -1 9 2 10047.45 11075.48 1131.21 o 1 9 2 695.71 746.75 74.36 o 3 9 2 12230.18 12251.15 471.46 o 5 9 2 92.51 140.87 16.07 o -6 10 2 335.22 363.01 21.76 o -4 10 2 8188.05 7559.16 961.62 o -2 10 2 541.81 509.54 49.06 o 0 10 2 7157.00 7407.32 843.25 o 2 10 2 1796.53 1831.44 172.73 o -3 11 2 999.28 1104.53 200.22 o -1 11 2 25.34 25.52 5.62 o -15 1 3 5376.13 7001.52 178.51 o -13 1 3 278.69 282.39 9.28 o -11 1 3 9367.69 9314.17 229.60 o -9 1 3 801.34 889.38 18.42 o 3 1 3 1705.30 1719.25 17.08 o 5 1 3 5427.91 5062.97 119.43 o 7 1 3 46.69 45.73 2.56 o 9 1 3 4999.15 5232.74 272.81 o -14 2 3 3688.17 4259.45 354.37 o -12 2 3 5685.91 5469.21 332.59 o -10 2 3 8444.00 8267.41 261.55 o -8 2 3 30863.11 30414.08 526.44 o 2 2 3 6069.50 5386.43 137.56 o 4 2 3 6237.04 6078.34 94.64 o 6 2 3 2544.35 2706.81 35.78 o 8 2 3 1529.30 1496.20 21.71 o -13 3 3 437.60 510.42 14.35 o -11 3 3 822.65 927.30 34.28 o -9 3 3 288.25 319.91 9.51 o -7 3 3 722.67 676.79 17.57 o 1 3 3 280.16 268.26 19.40 o 3 3 3 114.22 176.49 4.63 o 5 3 3 289.26 301.72 8.32 o 7 3 3 343.58 378.64 9.01 o -14 4 3 1695.84 1713.50 44.11 o -12 4 3 5410.94 4827.13 129.62 o -10 4 3 1883.73 1798.49 31.62 o -8 4 3 10882.23 10176.42 269.20 o -6 4 3 2345.87 2387.47 39.09 o -4 4 3 16931.09 17645.25 644.18 o -2 4 3 21152.03 20993.12 2054.08 o 0 4 3 6122.51 5491.50 721.63 o 2 4 3 10182.45 9584.53 776.11 o 4 4 3 9880.20 8894.25 181.60 o 6 4 3 2618.16 2671.99 64.65 o 8 4 3 4364.81 4425.46 81.03 o -13 5 3 639.29 638.61 24.06 o -11 5 3 5996.53 6674.55 100.92 o -9 5 3 9.33 10.81 3.08 o -7 5 3 19582.29 19546.90 434.95 o -5 5 3 184.85 229.72 17.21 o -3 5 3 35712.98 38370.54 1028.36 o -1 5 3 744.49 773.22 72.57 o 1 5 3 16857.52 15401.57 1622.35 o 3 5 3 337.20 339.73 24.58 o 5 5 3 7006.82 7005.94 389.33 o 7 5 3 28.53 42.64 4.27 o -12 6 3 0.34 5.76 2.43 o -10 6 3 1213.59 1147.96 35.62 o -8 6 3 123.01 170.35 8.33 o -6 6 3 3016.27 3252.32 108.94 o -4 6 3 873.30 845.07 32.35 o -2 6 3 115.42 105.97 10.64 o 0 6 3 3557.16 3555.10 485.18 o 2 6 3 142.81 121.96 14.91 o 4 6 3 27.05 19.44 2.61 o 6 6 3 19.38 31.64 2.90 o -11 7 3 1553.66 1395.29 43.94 o -9 7 3 1015.21 1041.41 14.55 o -7 7 3 2075.15 2204.40 51.69 o -5 7 3 29.79 37.69 4.00 o -3 7 3 9455.46 8670.39 922.55 o -1 7 3 1013.01 838.00 165.59 o 1 7 3 7426.63 4946.69 1738.93 o 3 7 3 407.75 404.15 46.82 o 5 7 3 6518.95 5860.30 344.57 o -10 8 3 278.60 284.71 13.59 o -8 8 3 5560.74 5471.05 183.63 o -6 8 3 1167.00 1206.77 85.04 o -4 8 3 1494.65 1412.59 113.70 o -2 8 3 5278.52 6481.90 332.76 o 0 8 3 3247.35 2533.68 687.50 o 2 8 3 9799.39 9955.83 655.60 o 4 8 3 5406.97 4288.25 661.91 o -9 9 3 59.56 73.65 4.91 o -7 9 3 25.45 32.55 3.82 o -5 9 3 190.89 266.92 9.59 o -3 9 3 1.63 11.56 2.17 o -1 9 3 63.98 58.54 5.27 o 1 9 3 1553.42 1915.58 211.50 o 3 9 3 22.99 31.80 3.89 o -6 10 3 139.06 146.31 14.86 o -4 10 3 2423.25 2069.18 400.09 o -2 10 3 827.98 855.50 81.04 o 0 10 3 892.88 915.77 74.25 o -14 0 4 6567.24 6793.00 122.88 o -12 0 4 4202.31 3929.28 58.62 o -10 0 4 12885.89 12145.19 619.50 o -8 0 4 5296.62 5798.02 101.31 o 0 0 4 8036.26 8460.94 508.83 o 2 0 4 21119.33 20379.46 666.69 o 4 0 4 3959.44 4073.14 106.55 o 6 0 4 9293.83 8978.71 131.72 o -15 1 4 1840.12 1830.32 194.61 o -13 1 4 969.53 984.07 30.71 o -11 1 4 1595.67 1656.70 35.59 o -9 1 4 33.47 46.97 3.26 o 1 1 4 800.54 737.52 16.48 o 3 1 4 16220.21 16419.35 178.84 o 5 1 4 1453.97 1509.95 26.38 o 7 1 4 1520.76 1521.89 32.61 o -14 2 4 1031.52 1000.07 26.64 o -12 2 4 468.04 548.25 17.80 o -10 2 4 2584.03 2635.86 41.09 o -8 2 4 3699.53 3900.50 48.44 o 0 2 4 2088.13 1959.83 53.34 o 2 2 4 3368.16 3347.95 100.55 o 4 2 4 1281.76 1414.30 29.76 o 6 2 4 217.63 282.37 4.60 o -15 3 4 1633.62 1672.74 65.03 o -13 3 4 5480.79 5442.56 172.06 o -11 3 4 10915.43 10821.44 214.97 o -9 3 4 25287.44 25863.79 284.90 o -7 3 4 7507.55 7223.86 161.02 o -5 3 4 31869.70 29075.04 752.89 o -3 3 4 120.17 83.21 3.15 o -1 3 4 22015.46 20756.80 491.73 o 1 3 4 4344.67 4292.26 138.35 o 3 3 4 17066.64 16601.94 587.12 o 5 3 4 2165.06 2064.57 103.39 o 7 3 4 3970.39 3642.55 54.99 o -14 4 4 2308.75 2394.40 48.24 o -12 4 4 138.09 107.17 4.33 o -10 4 4 713.62 703.82 17.55 o -8 4 4 1583.81 1639.81 34.43 o -6 4 4 4376.21 4722.42 81.03 o -4 4 4 1807.08 1919.31 67.80 o -2 4 4 21283.67 20611.35 1427.64 o 0 4 4 2737.55 2496.62 234.96 o 2 4 4 12090.01 11763.67 386.22 o 4 4 4 378.15 318.67 16.93 o 6 4 4 3187.92 3136.75 125.41 o -13 5 4 3685.01 3790.21 77.70 o -11 5 4 2140.51 2194.19 60.57 o -9 5 4 7155.10 7500.40 156.99 o -7 5 4 5429.33 5611.36 187.29 o -5 5 4 144.14 146.14 8.78 o -3 5 4 5198.95 4722.79 439.70 o -1 5 4 19.89 19.55 7.37 o 1 5 4 1206.23 1071.37 132.53 o 3 5 4 1500.77 1391.77 85.79 o 5 5 4 443.89 337.13 13.25 o -12 6 4 653.60 595.59 20.82 o -10 6 4 22180.47 22137.77 709.66 o -8 6 4 3733.45 3653.14 71.57 o -6 6 4 42715.14 43215.89 1324.45 o -4 6 4 1008.05 1217.13 53.32 o -2 6 4 21345.21 19658.57 2622.53 o 0 6 4 139.59 150.56 25.60 o 2 6 4 3878.72 3831.47 193.16 o 4 6 4 1485.19 1517.94 122.57 o -11 7 4 30.60 20.78 4.07 o -9 7 4 5222.19 5196.50 114.35 o -7 7 4 2455.57 2567.03 135.83 o -5 7 4 5291.31 5379.03 240.34 o -3 7 4 6193.53 6809.88 378.77 o -1 7 4 4306.48 4119.43 628.76 o 1 7 4 921.37 747.37 125.37 o 3 7 4 1178.61 1133.25 78.75 o -10 8 4 1159.69 1190.83 34.46 o -8 8 4 0.16 5.62 2.42 o -6 8 4 647.70 631.00 24.88 o -4 8 4 10.09 4.14 1.97 o -2 8 4 676.96 671.96 61.72 o 0 8 4 6.86 23.59 2.77 o 2 8 4 988.92 799.85 130.11 o -9 9 4 5964.98 5817.02 269.46 o -7 9 4 5819.54 6230.62 246.40 o -5 9 4 3269.46 3480.69 85.17 o -3 9 4 842.17 1026.24 54.58 o -1 9 4 3927.30 3442.07 611.83 o 1 9 4 10.09 9.71 1.96 o -6 10 4 3495.77 3540.20 153.11 o -4 10 4 321.82 266.14 132.33 o -2 10 4 1541.12 1506.49 40.77 o -15 1 5 2424.95 2391.20 50.07 o -13 1 5 11131.22 11365.85 265.07 o -11 1 5 5964.43 5800.51 114.27 o -9 1 5 6114.83 6228.07 108.97 o -7 1 5 7498.22 7320.69 107.47 o -3 1 5 16106.27 16185.54 324.05 o -1 1 5 5101.29 5389.33 74.40 o 1 1 5 15016.94 14326.33 289.39 o 3 1 5 938.51 1078.63 19.84 o 5 1 5 5932.16 5691.90 70.05 o -16 2 5 11541.45 11387.99 461.10 o -14 2 5 1085.51 1101.79 32.54 o -12 2 5 21172.00 21482.81 368.61 o -10 2 5 4674.49 4917.99 105.11 o -8 2 5 4567.31 4595.70 54.00 o -6 2 5 1773.69 1763.92 30.23 o -4 2 5 5047.14 4430.90 69.60 o -2 2 5 7516.40 7595.08 154.76 o 0 2 5 15093.46 14772.36 461.13 o 2 2 5 4616.28 4606.20 76.98 o 4 2 5 12035.18 12350.56 191.67 o 6 2 5 85.87 83.61 5.52 o -15 3 5 181.98 174.71 7.29 o -13 3 5 2075.45 1990.33 56.79 o -11 3 5 2461.22 2335.16 50.62 o -9 3 5 1263.59 1181.73 13.34 o -7 3 5 5322.62 5884.29 78.85 o -5 3 5 5979.98 5405.70 116.80 o -3 3 5 1145.32 1130.35 74.47 o -1 3 5 4830.69 4926.32 237.57 o 1 3 5 1351.84 1393.66 33.91 o 3 3 5 2.01 4.45 1.82 o 5 3 5 1532.68 1692.37 69.72 o -14 4 5 127.61 103.45 10.22 o -12 4 5 11191.63 11580.07 433.86 o -10 4 5 1223.83 1209.32 15.11 o -8 4 5 16951.56 17433.36 279.12 o -6 4 5 131.34 132.03 3.62 o -4 4 5 30213.96 30755.72 1449.51 o -2 4 5 149.64 123.43 10.80 o 0 4 5 17035.76 16062.42 521.92 o 2 4 5 154.44 168.47 6.35 o 4 4 5 2029.37 2021.92 78.39 o -13 5 5 2686.64 2523.33 61.78 o -11 5 5 4744.38 4886.70 165.54 o -9 5 5 4812.25 4924.82 79.49 o -7 5 5 11962.06 11571.59 145.64 o -5 5 5 13060.03 13011.46 570.40 o -3 5 5 7247.36 6255.93 348.70 o -1 5 5 8410.23 7736.33 536.51 o 1 5 5 2595.08 2601.44 120.67 o 3 5 5 1842.24 1756.30 47.47 o -14 6 5 77.31 65.31 7.50 o -12 6 5 47.39 55.42 2.81 o -10 6 5 266.81 294.77 5.18 o -8 6 5 491.24 398.61 16.25 o -6 6 5 213.02 170.37 8.14 o -4 6 5 5.00 4.01 1.78 o -2 6 5 25.35 41.35 3.13 o 0 6 5 22.52 23.98 4.93 o 2 6 5 3.97 2.20 2.07 o 4 6 5 501.96 577.38 27.03 o -13 7 5 933.23 862.46 27.99 o -11 7 5 4415.42 4320.64 117.02 o -9 7 5 1624.29 1768.82 40.86 o -7 7 5 7778.63 7608.29 463.64 o -5 7 5 11663.36 12546.95 683.36 o -3 7 5 3906.77 3851.10 300.31 o -1 7 5 7194.43 6106.23 909.20 o 1 7 5 668.53 599.96 60.83 o 3 7 5 637.84 747.05 51.82 o -12 8 5 5364.10 5273.46 519.08 o -10 8 5 136.03 146.79 5.31 o -8 8 5 15579.74 15128.15 549.12 o -6 8 5 32.98 8.43 2.04 o -4 8 5 15087.16 14981.56 924.57 o -2 8 5 312.38 258.84 21.11 o 0 8 5 7146.28 6219.36 1108.57 o 2 8 5 439.61 358.88 42.58 o -9 9 5 326.02 348.37 20.02 o -7 9 5 2621.46 2682.35 259.08 o -5 9 5 677.43 548.75 36.78 o -3 9 5 289.69 237.97 21.83 o -1 9 5 1170.80 925.55 107.08 o -6 10 5 71.21 61.69 5.51 o -4 10 5 1464.17 1144.38 31.87 o -16 0 6 9.44 15.28 4.51 o -14 0 6 11270.40 11491.55 451.36 o -12 0 6 762.85 722.41 22.02 o -10 0 6 29375.82 30949.47 1253.25 o -8 0 6 21683.17 21986.91 390.44 o -6 0 6 44976.26 47677.96 3143.01 o -4 0 6 18131.14 18866.53 335.18 o -2 0 6 5468.21 5242.68 192.59 o 0 0 6 2046.41 2023.10 66.64 o 2 0 6 3057.31 3166.99 65.44 o 4 0 6 277.81 340.15 10.86 o -15 1 6 2393.61 2502.35 72.44 o -13 1 6 3905.90 3882.43 84.58 o -11 1 6 16719.42 16607.85 390.94 o -9 1 6 4073.72 4253.58 54.50 o -7 1 6 15073.60 14792.57 345.78 o -5 1 6 473.33 436.08 106.64 o -3 1 6 2745.65 2900.31 75.61 o -1 1 6 111.31 124.08 3.22 o 1 1 6 655.65 621.84 15.50 o 3 1 6 304.27 286.43 5.79 o -16 2 6 1813.45 1766.79 100.42 o -14 2 6 324.27 278.69 9.97 o -12 2 6 2067.94 2119.18 28.20 o -10 2 6 2164.05 2040.55 34.99 o -8 2 6 139.04 149.29 4.34 o -6 2 6 5687.22 6168.65 95.22 o -4 2 6 273.24 231.43 7.49 o -2 2 6 1166.93 893.11 162.06 o 0 2 6 407.35 318.02 8.12 o 2 2 6 2137.20 1978.43 53.35 o 4 2 6 292.03 266.95 8.99 o -15 3 6 6970.02 7069.98 212.40 o -13 3 6 1740.24 1666.68 24.03 o -11 3 6 17298.98 17374.56 292.82 o -9 3 6 142.27 127.89 3.57 o -7 3 6 22548.17 22846.85 637.25 o -5 3 6 5296.71 4872.43 395.54 o -3 3 6 12015.22 12546.96 316.98 o -1 3 6 5439.15 5087.91 107.38 o 1 3 6 8266.92 8234.97 226.04 o 3 3 6 2367.67 2658.06 55.06 o -14 4 6 5895.04 6260.41 194.30 o -12 4 6 158.28 173.56 3.99 o -10 4 6 16144.48 15235.71 285.51 o -8 4 6 380.94 308.31 8.29 o -6 4 6 9561.30 9395.99 226.55 o -4 4 6 1257.44 1237.12 80.75 o -2 4 6 1760.56 1798.29 57.46 o 0 4 6 173.89 177.99 7.39 o 2 4 6 971.43 931.09 25.77 o -15 5 6 1786.17 1712.16 96.32 o -13 5 6 773.77 650.49 18.31 o -11 5 6 1287.84 1348.40 35.65 o -9 5 6 3.74 0.60 2.44 o -7 5 6 91.17 92.57 6.66 o -5 5 6 6573.18 5685.54 408.59 o -3 5 6 31.35 30.39 3.23 o -1 5 6 2443.07 2497.77 81.39 o 1 5 6 3881.90 3731.51 48.05 o 3 5 6 191.31 178.33 13.98 o -14 6 6 1775.57 1706.40 141.69 o -12 6 6 1130.18 1324.47 73.86 o -10 6 6 3826.33 3710.14 96.74 o -8 6 6 103.35 97.27 8.09 o -6 6 6 15462.52 14381.00 939.20 o -4 6 6 12.89 7.79 2.64 o -2 6 6 16663.36 14117.20 766.32 o 0 6 6 123.30 135.99 7.37 o 2 6 6 9252.27 8386.88 657.91 o -13 7 6 27.47 16.39 2.32 o -11 7 6 2182.80 1883.34 100.37 o -9 7 6 1017.14 1022.28 37.02 o -7 7 6 309.83 262.22 15.12 o -5 7 6 1894.93 1958.70 191.72 o -3 7 6 1794.66 1817.36 151.06 o -1 7 6 2490.43 1907.11 293.48 o 1 7 6 2434.77 2226.14 169.71 o -12 8 6 56.03 63.11 3.89 o -10 8 6 1887.27 1712.17 73.44 o -8 8 6 20.75 24.82 2.34 o -6 8 6 3293.27 2816.45 178.96 o -4 8 6 21.95 10.74 1.07 o -2 8 6 361.84 283.38 60.86 o 0 8 6 121.36 101.73 10.71 o -9 9 6 522.64 504.39 23.51 o -7 9 6 3204.77 2926.41 162.00 o -5 9 6 2492.58 2936.87 195.35 o -3 9 6 4656.14 4529.29 544.35 o -17 1 7 1673.59 1985.21 202.07 o -15 1 7 8.56 16.61 3.33 o -13 1 7 7022.36 7283.65 190.13 o -11 1 7 8217.76 8320.06 268.18 o -9 1 7 19511.72 19063.93 698.83 o -7 1 7 3743.91 3463.47 43.85 o -5 1 7 23680.17 23715.42 357.31 o -3 1 7 39.23 30.62 2.74 o -1 1 7 11616.27 12008.13 126.44 o 1 1 7 213.55 229.75 4.91 o 3 1 7 2015.44 2095.66 61.10 o -16 2 7 1711.95 1633.76 32.96 o -14 2 7 942.93 975.26 22.43 o -12 2 7 14490.94 13837.40 225.54 o -10 2 7 1688.81 1591.79 49.35 o -8 2 7 25870.56 27085.33 518.86 o -6 2 7 7893.02 7796.85 162.53 o -4 2 7 16122.21 15521.36 327.70 o -2 2 7 12897.11 12558.69 399.18 o 0 2 7 4667.54 4969.66 102.83 o 2 2 7 2564.48 2738.49 73.49 o -15 3 7 893.96 799.12 26.28 o -13 3 7 527.98 560.35 13.84 o -11 3 7 3163.17 3269.20 78.29 o -9 3 7 3422.37 3320.94 78.47 o -7 3 7 523.17 540.70 14.60 o -5 3 7 8770.43 9140.54 293.44 o -3 3 7 1016.06 1004.51 33.21 o -1 3 7 804.90 639.21 28.87 o 1 3 7 2444.48 2474.15 57.20 o -16 4 7 4016.79 4181.45 494.65 o -14 4 7 13519.53 12958.17 493.33 o -12 4 7 2311.31 2375.41 25.65 o -10 4 7 7101.94 6546.03 68.77 o -8 4 7 42.79 42.40 2.86 o -6 4 7 24.97 20.04 3.35 o -4 4 7 2876.89 3007.93 114.35 o -2 4 7 39.56 34.19 4.12 o 0 4 7 9727.49 9526.42 413.88 o 2 4 7 193.55 159.29 62.38 o -15 5 7 185.01 217.59 9.29 o -13 5 7 8755.77 8690.45 230.11 o -11 5 7 42.73 41.13 2.84 o -9 5 7 8771.13 9823.13 271.77 o -7 5 7 15.57 26.82 3.19 o -5 5 7 7315.23 7439.94 265.12 o -3 5 7 742.58 729.43 31.68 o -1 5 7 5268.75 5395.19 135.78 o 1 5 7 1233.15 1181.05 67.00 o -14 6 7 195.53 216.91 7.97 o -12 6 7 2.62 3.36 2.22 o -10 6 7 1.69 -1.74 2.80 o -8 6 7 707.43 602.40 27.73 o -6 6 7 33.41 82.87 6.79 o -4 6 7 876.83 739.94 75.74 o -2 6 7 3.18 2.56 1.73 o 0 6 7 15.57 15.57 1.61 o -13 7 7 7274.75 7216.36 468.46 o -11 7 7 179.99 167.55 8.86 o -9 7 7 6176.95 6335.24 211.97 o -7 7 7 275.69 234.41 8.85 o -5 7 7 2599.43 2905.91 138.79 o -3 7 7 9.62 18.59 3.03 o -1 7 7 1757.49 1651.08 80.30 o -10 8 7 5893.33 6107.91 252.30 o -8 8 7 730.62 803.73 14.07 o -6 8 7 944.79 1187.28 42.97 o -4 8 7 2709.36 2563.87 159.64 o -2 8 7 8.01 12.31 2.37 o -9 9 7 2.39 16.62 7.26 o -7 9 7 60.46 86.35 7.06 o -5 9 7 277.39 290.28 16.90 o -16 0 8 8878.54 8585.81 154.93 o -14 0 8 3082.60 2982.86 55.56 o -12 0 8 4963.17 4953.38 90.08 o -10 0 8 8257.26 7951.04 202.10 o -8 0 8 13209.68 13377.22 238.74 o -6 0 8 9191.81 9726.95 174.22 o -4 0 8 10306.07 10177.66 297.11 o -2 0 8 5697.19 5807.86 117.56 o 0 0 8 4264.93 4063.19 100.82 o -17 1 8 446.04 436.01 25.43 o -15 1 8 1168.85 1158.56 35.17 o -13 1 8 399.53 447.65 11.22 o -11 1 8 1410.15 1471.02 34.66 o -9 1 8 123.03 146.07 4.56 o -7 1 8 7298.38 2242.65 2433.09 o -5 1 8 233.78 230.19 4.85 o -3 1 8 6247.05 7029.24 120.46 o -1 1 8 8.03 10.88 2.22 o 1 1 8 2146.51 2067.95 143.50 o -16 2 8 1207.63 1126.56 27.68 o -14 2 8 670.22 596.78 9.81 o -12 2 8 2667.59 2767.87 36.37 o -10 2 8 124.87 167.36 4.47 o -8 2 8 8247.41 8403.46 121.37 o -6 2 8 1206.27 1295.52 25.65 o -4 2 8 1995.18 1869.57 181.80 o -2 2 8 1079.13 1098.10 16.57 o 0 2 8 143.80 152.17 3.57 o -15 3 8 12767.99 12626.86 888.42 o -13 3 8 926.04 914.90 11.98 o -11 3 8 7828.10 7815.28 193.85 o -9 3 8 288.71 358.39 5.91 o -7 3 8 9839.07 9983.34 250.07 o -5 3 8 283.30 320.26 6.20 o -3 3 8 11162.88 11473.08 268.54 o -1 3 8 36.96 41.26 4.83 o -16 4 8 1422.89 1264.69 27.97 o -14 4 8 8.22 3.83 2.79 o -12 4 8 1167.33 1234.31 16.31 o -10 4 8 730.93 590.48 13.00 o -8 4 8 787.14 786.70 34.69 o -6 4 8 2911.53 2665.97 122.94 o -4 4 8 776.02 807.83 70.66 o -2 4 8 2805.72 3056.93 94.19 o 0 4 8 973.55 996.06 92.13 o -15 5 8 2552.08 2293.80 133.53 o -13 5 8 39.13 40.73 3.02 o -11 5 8 2616.04 2954.55 61.95 o -9 5 8 2015.61 1994.73 55.12 o -7 5 8 3697.73 3851.94 339.52 o -5 5 8 282.66 391.29 13.61 o -3 5 8 1149.13 1240.74 64.99 o -1 5 8 0.34 1.60 2.81 o -14 6 8 4404.15 4423.42 218.44 o -12 6 8 5945.58 5595.17 130.13 o -10 6 8 4404.92 3884.45 160.97 o -8 6 8 8388.48 8041.98 604.31 o -6 6 8 1739.58 1677.37 60.79 o -4 6 8 3594.01 3410.89 213.12 o -2 6 8 1083.95 982.51 88.18 o -13 7 8 556.25 578.08 20.17 o -11 7 8 3263.49 3309.04 122.07 o -9 7 8 206.18 177.87 9.02 o -7 7 8 1984.47 1619.64 114.60 o -5 7 8 4.10 7.13 2.33 o -3 7 8 1536.49 1505.18 114.76 o -10 8 8 439.43 427.08 58.40 o -8 8 8 2529.36 2690.10 163.77 o -6 8 8 369.07 310.01 27.17 o -17 1 9 3591.19 3638.99 94.24 o -15 1 9 2866.56 2775.24 33.02 o -13 1 9 6979.12 6892.62 228.06 o -11 1 9 5132.42 5276.77 141.50 o -9 1 9 6919.85 7215.32 106.21 o -7 1 9 1638.47 1673.92 38.66 o -5 1 9 1479.81 1566.23 36.42 o -3 1 9 287.27 289.08 4.60 o -1 1 9 2409.93 2480.05 95.61 o -16 2 9 408.09 385.14 7.99 o -14 2 9 16469.30 15828.88 292.70 o -12 2 9 44.89 60.56 4.09 o -10 2 9 11259.01 10542.36 347.26 o -8 2 9 32.32 44.68 3.67 o -6 2 9 3059.98 2264.19 501.31 o -4 2 9 474.15 495.56 12.78 o -2 2 9 1841.08 1866.39 38.77 o -15 3 9 378.46 381.97 7.93 o -13 3 9 622.91 595.91 18.82 o -11 3 9 1290.27 1134.57 14.34 o -9 3 9 180.38 162.41 4.48 o -7 3 9 504.79 505.02 15.52 o -5 3 9 230.69 225.42 6.54 o -3 3 9 228.94 189.27 39.17 o -16 4 9 1.15 3.22 2.47 o -14 4 9 4106.75 4122.89 115.50 o -12 4 9 429.20 369.51 9.46 o -10 4 9 5236.06 4772.67 130.09 o -8 4 9 3641.25 3571.13 145.12 o -6 4 9 5320.26 5115.34 243.09 o -4 4 9 1184.27 1271.04 67.16 o -2 4 9 5813.78 5261.31 302.35 o -15 5 9 1203.36 1108.86 55.42 o -13 5 9 6434.68 6004.11 122.32 o -11 5 9 1370.11 1313.17 40.96 o -9 5 9 8428.88 8119.41 427.07 o -7 5 9 1364.31 1325.56 37.17 o -5 5 9 5524.74 5870.39 418.67 o -3 5 9 654.58 663.29 30.19 o -14 6 9 356.09 388.12 7.52 o -12 6 9 14.55 28.58 2.76 o -10 6 9 50.00 66.33 3.53 o -8 6 9 208.46 125.77 9.77 o -6 6 9 38.25 81.91 5.28 o -4 6 9 44.87 56.00 4.26 o -11 7 9 55.66 40.79 3.12 o -9 7 9 7649.84 7907.60 189.09 o -7 7 9 497.17 448.81 20.03 o -16 0 10 7592.04 7896.21 929.23 o -14 0 10 791.51 741.96 17.57 o -12 0 10 16081.83 16827.04 1437.52 o -10 0 10 54.01 42.92 5.27 o -8 0 10 15215.74 15156.93 490.45 o -6 0 10 106.18 115.66 10.10 o -4 0 10 6560.09 7116.02 278.11 o -15 1 10 2417.74 2435.01 130.06 o -13 1 10 615.36 540.05 19.02 o -11 1 10 2005.14 2283.57 27.65 o -9 1 10 1345.45 1367.48 40.20 o -7 1 10 1092.35 1161.20 23.64 o -5 1 10 1767.30 1743.84 21.73 o -3 1 10 512.83 494.86 7.12 o -16 2 10 2675.36 2712.19 88.38 o -14 2 10 228.05 201.37 9.81 o -12 2 10 1941.34 1870.29 46.36 o -10 2 10 9.61 14.95 3.27 o -8 2 10 1583.83 1541.35 25.47 o -6 2 10 12.67 18.59 3.73 o -4 2 10 1679.32 1759.84 34.73 o -15 3 10 4185.55 3956.67 125.88 o -13 3 10 5224.13 4682.21 71.72 o -11 3 10 4815.18 5350.18 227.36 o -9 3 10 4378.75 4813.40 55.15 o -7 3 10 4842.01 5193.42 112.36 o -5 3 10 3395.94 3567.86 100.90 o -14 4 10 358.36 373.20 15.36 o -12 4 10 4000.36 4152.54 63.57 o -10 4 10 10.75 17.39 1.93 o -8 4 10 3612.91 3710.49 123.87 o -6 4 10 231.84 228.77 8.82 o -13 5 10 258.90 213.71 4.72 o -11 5 10 14.21 6.52 3.13 o -9 5 10 7.46 5.57 2.50 o -7 5 10 353.54 454.80 31.33 o -12 6 10 4988.78 5492.99 221.96 o -10 6 10 20.15 37.05 3.12 o -8 6 10 4301.01 4578.93 238.48 o -15 1 11 1980.46 1947.82 26.74 o -13 1 11 554.87 585.96 14.61 o -11 1 11 3663.01 2573.77 819.77 o -9 1 11 2462.18 2544.38 49.04 o -7 1 11 2935.55 3006.60 35.94 o -14 2 11 887.24 934.75 32.18 o -12 2 11 6.14 9.18 3.39 o -10 2 11 4792.01 4949.12 151.27 o -8 2 11 474.28 449.88 47.90 o -6 2 11 7689.68 8091.99 652.12 o -15 3 11 557.55 533.68 20.03 o -13 3 11 23.34 21.14 5.24 o -11 3 11 1818.52 1919.43 49.65 o -9 3 11 1239.32 1200.08 36.61 o -7 3 11 19.80 22.10 2.81 o -12 4 11 2542.03 2936.00 39.18 o -10 4 11 5501.35 5146.67 352.13 o -8 4 11 1339.93 1676.88 64.65 o -14 0 12 2804.25 2941.61 235.21 o -12 0 12 1097.90 1095.10 23.66 o -10 0 12 114.89 87.06 4.88 o -13 1 12 388.51 373.76 8.10 o -11 1 12 30.14 49.53 3.69 o -12 2 12 2647.54 2662.72 50.63 o