#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/34/2013454.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013454_Fobs loop_ _publ_author_name 'Gathergood, Nicholas' 'Scammells, Peter J.' 'Fallon, Gary D.' _publ_section_title ; Inter- and intramolecular C---H···\p interactions in morphine bis(1-naphthoate) ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o485 _journal_page_last o487 _journal_volume 59 _journal_year 2003 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.8435 _cell_length_b 9.7218 _cell_length_c 39.5921 _exptl_crystal_F_000 1248.00 _reflns_d_resolution_high 0.7601 _[local]_cod_data_source_file gd1262Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' import in P 21 21 21' _shelx_refln_list_code 4 _shelx_f_calc_maximum 163.18 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2167.89 2116.67 88.54 o 4 0 0 3770.72 3842.83 112.02 o 6 0 0 240.06 213.80 28.21 o 8 0 0 0.14 16.58 31.88 o 10 0 0 35.66 -7.73 38.26 o 2 1 0 37.87 34.92 6.10 o 3 1 0 1867.24 1777.53 45.26 o 4 1 0 83.78 86.65 12.65 o 5 1 0 98.94 111.96 16.02 o 6 1 0 352.92 379.35 22.80 o 7 1 0 59.30 52.87 27.59 o 8 1 0 119.94 150.30 25.31 o 9 1 0 93.41 104.63 27.99 o 10 1 0 28.94 25.19 24.83 o 0 2 0 16736.76 15668.32 351.57 o 1 2 0 976.99 892.72 15.75 o 2 2 0 2155.20 1945.72 44.74 o 3 2 0 752.28 788.89 24.87 o 4 2 0 765.38 794.68 26.82 o 5 2 0 51.42 55.36 15.31 o 6 2 0 274.76 274.52 43.22 o 7 2 0 25.83 23.79 18.27 o 8 2 0 165.95 182.02 25.72 o 9 2 0 92.56 95.61 32.12 o 10 2 0 3.40 47.53 33.21 o 1 3 0 196.25 219.36 7.73 o 2 3 0 10.27 12.60 4.60 o 3 3 0 23.37 35.39 8.38 o 4 3 0 4524.09 4863.19 140.03 o 5 3 0 39.25 27.55 14.45 o 6 3 0 32.69 48.56 19.48 o 7 3 0 122.77 99.37 19.93 o 8 3 0 17.64 19.94 21.78 o 9 3 0 0.73 -26.67 26.67 o 10 3 0 120.53 89.89 27.53 o 0 4 0 1591.41 1568.18 30.93 o 1 4 0 1166.04 1192.69 26.48 o 2 4 0 84.54 86.81 6.25 o 3 4 0 64.90 81.98 7.50 o 4 4 0 384.43 416.32 15.75 o 5 4 0 0.00 15.15 11.06 o 6 4 0 546.04 508.67 26.71 o 7 4 0 0.48 13.14 19.14 o 8 4 0 228.19 330.18 27.37 o 9 4 0 7.56 35.23 26.85 o 1 5 0 2049.29 2178.46 43.93 o 2 5 0 7.87 6.39 5.47 o 3 5 0 252.52 231.09 10.88 o 4 5 0 661.95 673.92 20.78 o 5 5 0 1162.05 1184.68 30.76 o 6 5 0 108.23 104.60 17.46 o 7 5 0 0.20 6.81 18.22 o 8 5 0 18.29 -1.26 22.46 o 9 5 0 17.02 -13.27 26.30 o 0 6 0 176.98 159.86 14.61 o 1 6 0 1172.49 1279.84 28.89 o 2 6 0 313.51 320.40 14.82 o 3 6 0 211.38 211.12 11.21 o 4 6 0 185.21 190.51 12.91 o 5 6 0 553.74 623.58 23.24 o 6 6 0 185.74 240.32 23.93 o 7 6 0 51.45 -6.69 21.14 o 8 6 0 120.48 136.76 25.51 o 9 6 0 1.45 -2.48 30.54 o 1 7 0 464.69 479.15 23.61 o 2 7 0 175.23 204.23 29.76 o 3 7 0 3.39 31.13 17.54 o 4 7 0 229.47 222.80 24.83 o 5 7 0 219.19 236.94 29.37 o 6 7 0 353.37 352.17 53.98 o 7 7 0 14.52 -50.31 50.31 o 8 7 0 1.29 32.79 32.00 o 0 8 0 417.53 445.75 46.95 o 1 8 0 39.83 51.71 22.79 o 2 8 0 75.40 76.69 24.37 o 3 8 0 32.60 -10.43 34.25 o 4 8 0 169.92 189.31 31.43 o 5 8 0 11.22 15.24 58.03 o 6 8 0 9.38 32.27 51.53 o 7 8 0 24.53 113.77 63.46 o 1 9 0 157.68 100.43 30.16 o 2 9 0 16.85 43.86 27.94 o 3 9 0 0.04 45.65 28.60 o 4 9 0 260.02 286.06 41.21 o 5 9 0 331.92 357.01 45.14 o 6 9 0 262.06 272.19 67.28 o 7 9 0 0.09 -18.66 46.49 o 0 10 0 668.32 536.28 69.58 o 1 10 0 310.72 409.93 42.45 o 2 10 0 7.04 19.61 39.07 o 3 10 0 6.78 79.82 55.05 o 4 10 0 17.67 25.83 41.03 o 5 10 0 1.61 -3.71 46.09 o 6 10 0 86.26 253.69 78.45 o 1 11 0 0.10 3.41 37.24 o 2 11 0 152.42 119.41 36.13 o 3 11 0 98.81 25.00 40.82 o 4 11 0 527.86 627.66 100.39 o 5 11 0 152.16 274.46 55.51 o 0 12 0 177.35 219.59 71.72 o 1 12 0 121.30 64.23 44.35 o 2 12 0 55.39 62.51 44.73 o 3 12 0 124.03 50.31 68.35 o 2 0 1 1364.54 1264.97 31.59 o 3 0 1 1195.85 1242.88 32.50 o 4 0 1 689.48 633.84 23.36 o 5 0 1 151.09 139.39 22.09 o 6 0 1 131.40 119.71 17.35 o 7 0 1 438.90 446.97 26.43 o 8 0 1 23.54 13.40 22.07 o 9 0 1 4.52 -2.22 26.66 o 10 0 1 57.63 77.73 27.10 o 2 1 1 1052.22 946.56 17.40 o 3 1 1 1236.30 1179.11 28.29 o 4 1 1 3149.76 3217.26 51.63 o 5 1 1 1001.55 1042.10 22.94 o 6 1 1 310.80 335.51 15.37 o 7 1 1 314.16 305.20 25.53 o 8 1 1 99.56 99.29 17.05 o 9 1 1 36.93 45.07 19.64 o 10 1 1 26.29 18.49 19.46 o 0 2 1 42.51 42.05 2.53 o 1 2 1 2824.47 2685.61 37.61 o 2 2 1 635.34 568.27 10.81 o 3 2 1 1576.44 1423.23 26.52 o 4 2 1 203.35 226.80 10.90 o 5 2 1 331.89 337.93 15.10 o 6 2 1 1372.58 1347.37 28.89 o 7 2 1 57.87 55.15 13.45 o 8 2 1 216.21 231.07 17.36 o 9 2 1 20.36 23.18 20.89 o 10 2 1 25.78 -1.16 17.29 o 0 3 1 6191.15 5917.03 140.74 o 1 3 1 2573.03 2493.71 41.54 o 2 3 1 1337.36 1370.32 22.94 o 3 3 1 2047.12 2203.52 37.08 o 4 3 1 159.80 177.20 12.16 o 5 3 1 140.60 140.79 12.09 o 6 3 1 335.54 379.46 18.64 o 7 3 1 130.65 118.85 14.88 o 8 3 1 109.34 123.87 16.65 o 9 3 1 53.23 20.33 18.70 o 10 3 1 20.98 -15.03 18.16 o 0 4 1 1880.51 1948.87 47.45 o 1 4 1 2853.43 2797.47 43.22 o 2 4 1 1042.30 1037.14 14.02 o 3 4 1 1194.25 1193.72 17.25 o 4 4 1 192.23 193.47 8.87 o 5 4 1 301.04 313.64 14.30 o 6 4 1 614.16 633.75 21.08 o 7 4 1 246.02 247.47 17.19 o 8 4 1 229.38 303.69 19.55 o 9 4 1 114.88 127.25 20.68 o 0 5 1 3689.10 3734.29 88.97 o 1 5 1 2721.94 2846.83 46.86 o 2 5 1 173.51 185.44 5.90 o 3 5 1 136.65 141.17 6.55 o 4 5 1 334.92 312.98 10.04 o 5 5 1 93.32 88.27 10.21 o 6 5 1 41.65 45.74 10.77 o 7 5 1 42.78 25.68 13.26 o 8 5 1 136.50 165.44 16.54 o 9 5 1 3.75 0.83 18.23 o 0 6 1 0.52 3.76 7.57 o 1 6 1 505.59 533.21 16.61 o 2 6 1 205.31 195.51 7.40 o 3 6 1 134.27 142.20 8.68 o 4 6 1 547.76 544.45 12.93 o 5 6 1 17.89 12.73 9.50 o 6 6 1 345.19 309.89 14.47 o 7 6 1 5.30 3.31 14.65 o 8 6 1 13.92 -1.79 16.69 o 9 6 1 38.96 7.70 22.69 o 0 7 1 330.71 339.32 31.79 o 1 7 1 237.82 228.33 14.79 o 2 7 1 1201.24 1134.13 30.99 o 3 7 1 273.77 283.60 18.06 o 4 7 1 54.78 44.49 14.15 o 5 7 1 171.01 180.92 24.38 o 6 7 1 5.96 26.32 24.76 o 7 7 1 11.90 -22.30 40.75 o 8 7 1 21.26 43.78 38.31 o 0 8 1 72.88 74.74 23.16 o 1 8 1 56.04 58.86 16.35 o 2 8 1 379.73 316.48 22.00 o 3 8 1 55.38 15.47 17.19 o 4 8 1 6.95 -11.10 17.80 o 5 8 1 1240.97 1329.56 43.92 o 6 8 1 39.30 19.00 34.64 o 7 8 1 49.58 8.72 41.00 o 0 9 1 207.73 214.68 63.38 o 1 9 1 22.07 72.95 19.78 o 2 9 1 23.01 12.59 19.31 o 3 9 1 3.98 -4.85 20.29 o 4 9 1 50.78 63.66 24.66 o 5 9 1 385.26 424.83 33.32 o 6 9 1 74.28 63.98 61.70 o 7 9 1 29.16 41.45 37.97 o 0 10 1 42.95 64.96 37.40 o 1 10 1 154.58 160.73 43.40 o 2 10 1 3.64 -0.56 20.81 o 3 10 1 44.16 27.21 26.53 o 4 10 1 113.86 117.11 32.27 o 5 10 1 163.33 260.41 44.61 o 6 10 1 48.77 -16.75 54.08 o 0 11 1 2.19 28.75 58.11 o 1 11 1 7.19 -10.98 28.52 o 2 11 1 8.60 1.86 30.55 o 3 11 1 89.67 88.86 37.96 o 4 11 1 12.06 134.98 91.76 o 5 11 1 87.31 68.48 34.82 o 0 12 1 244.99 356.08 161.63 o 1 12 1 162.74 176.95 32.26 o 2 12 1 20.62 -14.68 26.05 o 3 12 1 33.48 23.45 48.51 o 2 0 2 1130.53 986.57 24.98 o 3 0 2 24.65 34.55 8.23 o 4 0 2 119.71 125.24 13.25 o 5 0 2 30.93 28.39 13.90 o 6 0 2 180.01 159.07 17.25 o 7 0 2 301.75 310.77 24.18 o 8 0 2 0.15 5.39 21.81 o 9 0 2 49.27 62.75 25.68 o 10 0 2 16.14 10.31 44.35 o 2 1 2 3404.23 3279.81 74.43 o 3 1 2 919.66 880.02 17.35 o 4 1 2 1163.82 1222.02 24.18 o 5 1 2 251.07 240.11 12.18 o 6 1 2 270.65 260.76 15.93 o 7 1 2 26.63 31.56 12.84 o 8 1 2 10.45 -10.47 14.73 o 9 1 2 44.29 87.45 16.91 o 10 1 2 218.97 316.61 29.35 o 0 2 2 8809.58 8662.56 118.90 o 1 2 2 28.50 32.98 2.39 o 2 2 2 148.99 128.52 4.63 o 3 2 2 2993.62 3165.74 50.56 o 4 2 2 52.69 37.97 8.01 o 5 2 2 60.97 65.79 10.43 o 6 2 2 836.46 880.16 22.91 o 7 2 2 405.37 369.02 20.71 o 8 2 2 125.02 119.17 17.88 o 9 2 2 54.87 20.89 19.02 o 10 2 2 22.08 34.49 16.01 o 0 3 2 9523.58 9124.87 215.29 o 1 3 2 1984.03 1811.61 26.01 o 2 3 2 341.24 332.11 6.95 o 3 3 2 871.49 928.85 15.99 o 4 3 2 355.38 355.14 12.57 o 5 3 2 241.66 248.49 12.65 o 6 3 2 1368.60 1371.91 29.96 o 7 3 2 879.64 824.29 24.02 o 8 3 2 191.46 220.35 17.57 o 9 3 2 16.35 -1.35 18.15 o 10 3 2 5.22 -2.53 17.98 o 0 4 2 35.47 29.71 8.65 o 1 4 2 997.73 1019.08 20.97 o 2 4 2 3573.24 3489.83 40.37 o 3 4 2 327.46 323.10 8.41 o 4 4 2 433.84 449.11 12.05 o 5 4 2 394.24 426.11 15.11 o 6 4 2 180.90 180.74 13.72 o 7 4 2 229.54 237.52 15.71 o 8 4 2 14.74 7.90 15.25 o 9 4 2 110.35 101.84 18.55 o 0 5 2 112.02 105.12 8.34 o 1 5 2 1546.69 1636.60 19.37 o 2 5 2 1248.41 1306.73 17.13 o 3 5 2 774.47 778.06 16.93 o 4 5 2 413.36 444.22 11.78 o 5 5 2 535.11 565.16 15.78 o 6 5 2 35.00 28.56 10.18 o 7 5 2 35.35 34.78 12.78 o 8 5 2 97.71 93.90 16.04 o 9 5 2 63.83 25.78 19.45 o 0 6 2 38.14 24.28 9.61 o 1 6 2 92.51 94.15 6.61 o 2 6 2 164.99 182.61 8.69 o 3 6 2 388.42 371.84 10.41 o 4 6 2 880.91 893.93 16.36 o 5 6 2 917.94 940.98 20.72 o 6 6 2 148.94 149.19 13.05 o 7 6 2 31.91 27.84 14.51 o 8 6 2 36.70 69.25 22.29 o 9 6 2 21.62 -20.55 20.55 o 0 7 2 23.81 21.00 12.48 o 1 7 2 201.78 236.26 14.96 o 2 7 2 1208.45 1184.39 36.15 o 3 7 2 271.32 258.93 17.83 o 4 7 2 217.45 225.70 24.70 o 5 7 2 499.64 433.58 33.33 o 6 7 2 545.97 599.00 37.07 o 7 7 2 12.10 -14.02 28.82 o 8 7 2 40.81 83.06 144.81 o 0 8 2 28.09 57.56 22.75 o 1 8 2 1832.60 1703.03 45.45 o 2 8 2 82.94 80.09 18.20 o 3 8 2 95.13 82.70 18.16 o 4 8 2 46.82 53.04 19.86 o 5 8 2 337.54 353.76 39.51 o 6 8 2 166.63 149.65 43.06 o 7 8 2 1.25 -34.55 41.97 o 0 9 2 111.78 82.51 36.09 o 1 9 2 542.35 529.63 28.59 o 2 9 2 45.20 12.16 18.94 o 3 9 2 130.68 134.25 27.73 o 4 9 2 47.14 31.03 37.54 o 5 9 2 19.96 13.11 26.12 o 6 9 2 82.82 62.22 41.68 o 7 9 2 72.70 28.29 33.85 o 0 10 2 31.99 6.56 32.62 o 1 10 2 530.68 547.18 32.60 o 2 10 2 32.86 24.84 22.05 o 3 10 2 7.25 0.53 25.27 o 4 10 2 227.49 294.25 63.81 o 5 10 2 68.58 65.58 33.60 o 6 10 2 19.37 33.99 50.49 o 0 11 2 149.08 125.14 44.92 o 1 11 2 113.41 71.12 27.59 o 2 11 2 127.90 85.06 33.22 o 3 11 2 24.78 77.34 73.45 o 4 11 2 13.24 15.74 29.47 o 5 11 2 134.40 88.28 40.27 o 0 12 2 0.12 -28.35 43.01 o 1 12 2 81.01 51.25 31.88 o 2 12 2 10.10 1.00 26.55 o 3 12 2 10.91 50.74 84.49 o 2 0 3 127.47 114.84 7.41 o 3 0 3 163.28 155.80 16.33 o 4 0 3 229.45 234.88 15.46 o 5 0 3 403.30 441.63 32.44 o 6 0 3 207.93 188.48 19.52 o 7 0 3 136.88 111.32 18.38 o 8 0 3 219.69 208.56 23.86 o 9 0 3 15.29 43.38 28.13 o 10 0 3 135.54 239.91 38.95 o 2 1 3 325.93 291.49 8.06 o 3 1 3 297.93 262.54 9.25 o 4 1 3 1148.70 1187.01 22.42 o 5 1 3 38.89 40.41 9.11 o 6 1 3 748.34 751.27 21.77 o 7 1 3 105.58 93.68 13.80 o 8 1 3 189.70 178.97 16.86 o 9 1 3 60.16 66.46 19.37 o 10 1 3 1.28 28.11 22.82 o 0 2 3 91.65 101.59 2.82 o 1 2 3 8537.89 8202.46 96.65 o 2 2 3 2558.94 2391.83 31.67 o 3 2 3 144.92 126.76 7.04 o 4 2 3 310.39 359.28 12.80 o 5 2 3 218.42 217.58 12.40 o 6 2 3 288.36 280.79 14.17 o 7 2 3 43.20 33.99 12.30 o 8 2 3 27.67 23.27 15.83 o 9 2 3 12.05 -17.72 17.72 o 10 2 3 1.29 -4.73 16.49 o 0 3 3 6573.21 6365.43 124.32 o 1 3 3 1161.79 1160.59 16.15 o 2 3 3 34.34 25.54 3.47 o 3 3 3 462.37 501.62 11.13 o 4 3 3 129.34 134.39 8.37 o 5 3 3 135.50 134.64 12.61 o 6 3 3 173.43 165.27 13.35 o 7 3 3 15.12 23.98 13.30 o 8 3 3 42.89 21.36 16.35 o 9 3 3 104.44 95.54 18.34 o 10 3 3 5.01 9.36 15.70 o 0 4 3 1919.37 1948.90 53.81 o 1 4 3 903.58 923.08 15.49 o 2 4 3 367.01 398.29 8.26 o 3 4 3 35.31 37.53 5.05 o 4 4 3 165.87 157.47 9.04 o 5 4 3 325.15 342.72 13.14 o 6 4 3 380.43 368.89 25.47 o 7 4 3 11.21 0.46 12.62 o 8 4 3 87.15 120.51 18.21 o 9 4 3 10.97 1.48 17.73 o 0 5 3 1259.56 1423.48 38.62 o 1 5 3 2366.37 2387.13 25.77 o 2 5 3 1295.19 1347.73 17.23 o 3 5 3 67.31 60.23 5.61 o 4 5 3 186.37 195.36 9.64 o 5 5 3 248.53 241.43 17.50 o 6 5 3 103.81 118.63 13.51 o 7 5 3 38.14 45.88 12.61 o 8 5 3 32.25 15.92 14.43 o 9 5 3 321.25 453.43 29.17 o 0 6 3 66.89 85.63 15.58 o 1 6 3 235.65 259.95 8.86 o 2 6 3 648.87 644.96 14.61 o 3 6 3 26.73 30.70 6.39 o 4 6 3 178.45 200.72 10.01 o 5 6 3 2369.12 2487.52 38.44 o 6 6 3 70.13 66.69 12.00 o 7 6 3 9.45 52.05 15.06 o 8 6 3 13.16 2.68 17.44 o 9 6 3 5.23 7.95 20.92 o 0 7 3 4.06 -3.94 13.61 o 1 7 3 93.16 100.66 13.19 o 2 7 3 162.74 150.69 19.81 o 3 7 3 65.72 61.57 13.62 o 4 7 3 114.88 100.86 15.10 o 5 7 3 558.72 559.76 30.28 o 6 7 3 100.00 93.93 25.42 o 7 7 3 32.77 46.16 24.83 o 8 7 3 5.64 -37.86 42.59 o 0 8 3 9.00 29.05 22.49 o 1 8 3 903.70 831.09 30.60 o 2 8 3 511.44 470.17 24.06 o 3 8 3 236.02 229.38 21.44 o 4 8 3 482.56 458.78 27.62 o 5 8 3 1054.84 1128.88 48.78 o 6 8 3 103.98 154.70 39.03 o 7 8 3 146.25 199.22 50.92 o 0 9 3 7.00 -5.97 26.09 o 1 9 3 301.00 288.57 24.27 o 2 9 3 105.77 68.12 20.41 o 3 9 3 151.54 179.36 27.47 o 4 9 3 0.14 37.05 23.74 o 5 9 3 33.04 -4.68 26.13 o 6 9 3 4.33 -34.85 40.93 o 7 9 3 25.87 10.00 68.12 o 0 10 3 0.10 -32.32 32.32 o 1 10 3 14.61 13.21 22.27 o 2 10 3 62.21 81.33 23.74 o 3 10 3 5.43 17.56 27.45 o 4 10 3 64.51 38.16 26.52 o 5 10 3 283.31 263.43 35.68 o 6 10 3 2.40 -15.23 52.37 o 0 11 3 32.32 105.65 42.80 o 1 11 3 375.82 439.09 35.07 o 2 11 3 53.42 22.01 43.58 o 3 11 3 52.81 38.63 24.37 o 4 11 3 55.33 22.61 27.21 o 5 11 3 12.53 60.23 34.77 o 0 12 3 10.00 64.94 46.44 o 1 12 3 14.50 -11.39 32.69 o 2 12 3 51.32 -20.39 38.87 o 3 12 3 48.52 85.83 47.00 o 2 0 4 4643.69 4277.02 78.49 o 3 0 4 8.61 19.48 7.95 o 4 0 4 2227.70 2393.29 55.01 o 5 0 4 379.04 380.35 22.47 o 6 0 4 336.51 339.79 21.06 o 7 0 4 1547.29 1452.16 71.56 o 8 0 4 11.45 0.49 16.64 o 9 0 4 29.90 59.17 23.61 o 10 0 4 18.34 19.35 27.59 o 1 1 4 742.41 705.77 9.91 o 2 1 4 694.38 634.09 12.78 o 3 1 4 1331.77 1339.90 22.74 o 4 1 4 126.10 119.09 9.14 o 5 1 4 424.93 455.48 15.47 o 6 1 4 220.58 242.57 15.51 o 7 1 4 819.33 790.32 25.29 o 8 1 4 47.72 32.68 15.77 o 9 1 4 36.85 32.23 18.09 o 10 1 4 30.85 22.99 18.55 o 0 2 4 24284.46 24262.04 450.40 o 1 2 4 378.75 349.67 5.97 o 2 2 4 139.02 127.00 4.93 o 3 2 4 2797.67 2769.48 40.20 o 4 2 4 1808.79 1921.35 29.81 o 5 2 4 56.16 45.56 9.11 o 6 2 4 148.83 143.68 12.73 o 7 2 4 472.54 485.87 25.28 o 8 2 4 142.13 148.24 16.62 o 9 2 4 33.59 16.61 17.96 o 10 2 4 0.77 13.55 17.36 o 0 3 4 108.47 117.33 11.32 o 1 3 4 686.53 672.08 14.58 o 2 3 4 1454.25 1448.98 19.87 o 3 3 4 880.31 896.20 15.62 o 4 3 4 734.67 768.14 16.55 o 5 3 4 70.99 66.74 12.85 o 6 3 4 366.94 364.07 15.49 o 7 3 4 138.25 163.86 15.43 o 8 3 4 62.16 51.25 16.61 o 9 3 4 62.17 95.97 20.35 o 0 4 4 831.02 797.43 19.90 o 1 4 4 12853.27 12906.03 213.73 o 2 4 4 660.95 752.76 12.00 o 3 4 4 1014.46 983.48 16.01 o 4 4 4 71.43 71.21 7.86 o 5 4 4 54.60 49.83 9.47 o 6 4 4 257.74 267.42 13.57 o 7 4 4 109.62 115.67 14.35 o 8 4 4 92.11 83.70 18.12 o 9 4 4 2.10 -9.22 18.69 o 0 5 4 169.00 173.56 9.66 o 1 5 4 1342.38 1493.45 29.97 o 2 5 4 1116.75 1238.23 17.41 o 3 5 4 165.29 164.53 7.23 o 4 5 4 468.70 479.79 12.77 o 5 5 4 432.96 454.50 14.80 o 6 5 4 69.87 77.29 11.90 o 7 5 4 148.04 157.81 18.29 o 8 5 4 5.98 -12.70 14.94 o 9 5 4 49.41 69.29 18.28 o 0 6 4 195.43 186.84 13.63 o 1 6 4 313.82 325.42 15.43 o 2 6 4 93.40 100.92 7.04 o 3 6 4 415.28 424.43 10.18 o 4 6 4 138.63 144.69 9.22 o 5 6 4 224.73 229.22 12.66 o 6 6 4 132.57 130.04 12.77 o 7 6 4 54.42 38.41 16.39 o 8 6 4 46.51 53.64 19.14 o 9 6 4 37.39 32.35 18.53 o 0 7 4 16.06 23.54 13.13 o 1 7 4 32.17 43.28 17.46 o 2 7 4 353.35 367.99 18.55 o 3 7 4 902.97 886.90 27.22 o 4 7 4 934.62 917.76 25.89 o 5 7 4 74.14 82.29 16.48 o 6 7 4 364.61 435.28 44.25 o 7 7 4 43.72 78.70 37.50 o 8 7 4 16.62 5.73 27.70 o 0 8 4 45.74 42.52 22.64 o 1 8 4 405.32 351.32 22.32 o 2 8 4 202.85 197.09 19.55 o 3 8 4 505.43 486.80 28.65 o 4 8 4 95.76 124.89 20.87 o 5 8 4 62.40 86.66 27.91 o 6 8 4 0.36 36.38 34.54 o 7 8 4 12.18 -20.52 41.49 o 0 9 4 265.00 307.94 36.00 o 1 9 4 407.26 368.26 26.19 o 2 9 4 406.93 373.77 26.58 o 3 9 4 94.76 117.44 26.39 o 4 9 4 24.58 32.44 23.82 o 5 9 4 65.19 124.23 27.81 o 6 9 4 0.41 8.71 41.44 o 7 9 4 14.43 32.57 67.13 o 0 10 4 0.10 47.12 33.23 o 1 10 4 84.79 69.56 23.94 o 2 10 4 1.17 2.72 24.04 o 3 10 4 29.88 18.91 22.74 o 4 10 4 121.40 117.14 31.34 o 5 10 4 188.57 207.83 37.65 o 6 10 4 27.99 -11.30 103.30 o 0 11 4 177.29 116.40 41.98 o 1 11 4 85.87 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41 16.36 74.24 77.22 o 0 7 41 8.85 45.62 45.48 o 1 7 41 36.75 62.42 27.55 o 2 7 41 4.51 25.07 41.32 o 0 0 42 55.52 14.68 52.91 o 1 0 42 10.02 58.57 50.77 o 2 0 42 144.38 149.75 40.02 o 3 0 42 47.26 61.08 35.92 o 4 0 42 446.24 549.05 42.59 o 5 0 42 0.11 67.11 67.36 o 6 0 42 4.52 2.32 40.40 o 0 1 42 4.02 -41.33 48.32 o 1 1 42 35.84 21.14 22.78 o 2 1 42 129.19 118.23 18.62 o 3 1 42 123.24 126.45 26.27 o 4 1 42 3.79 22.21 26.03 o 5 1 42 47.09 16.93 27.84 o 6 1 42 12.53 7.32 31.64 o 0 2 42 168.33 230.37 39.91 o 1 2 42 101.88 130.95 30.62 o 2 2 42 225.81 222.78 28.88 o 3 2 42 30.78 36.00 24.90 o 4 2 42 1.31 30.98 26.05 o 5 2 42 80.25 58.44 31.83 o 0 3 42 15.29 58.81 58.57 o 1 3 42 92.08 113.61 35.47 o 2 3 42 54.16 37.91 24.55 o 3 3 42 44.02 49.77 23.56 o 4 3 42 71.11 124.68 36.88 o 5 3 42 82.64 129.02 42.71 o 0 4 42 199.87 158.12 63.46 o 1 4 42 130.65 131.58 37.11 o 2 4 42 14.96 -21.42 27.80 o 3 4 42 26.48 22.28 35.01 o 4 4 42 57.91 60.39 30.17 o 5 4 42 10.12 -1.30 24.08 o 0 5 42 478.09 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0 4 44 443.55 702.35 80.59 o 1 4 44 67.76 37.22 33.95 o 2 4 44 34.63 53.37 85.63 o 3 4 44 3.39 -25.25 27.67 o 4 4 44 3.14 -36.40 36.40 o 0 5 44 10.64 12.72 106.28 o 1 5 44 46.84 72.47 38.67 o 2 5 44 25.10 54.07 61.63 o 3 5 44 34.90 29.47 20.39 o 0 6 44 275.04 424.01 57.82 o 1 6 44 12.46 -0.01 29.41 o 2 6 44 20.81 83.49 57.50 o 1 0 45 161.94 104.75 56.43 o 2 0 45 0.12 -32.56 32.56 o 3 0 45 0.00 -28.63 35.44 o 4 0 45 15.64 -8.33 36.31 o 5 0 45 119.58 141.81 50.41 o 0 1 45 24.11 -17.34 31.81 o 1 1 45 119.60 137.76 35.39 o 2 1 45 230.40 284.07 31.24 o 3 1 45 89.49 71.22 39.40 o 4 1 45 0.81 28.18 27.54 o 5 1 45 21.79 -20.09 29.04 o 0 2 45 64.55 58.05 43.94 o 1 2 45 142.50 62.17 28.65 o 2 2 45 58.78 44.32 30.60 o 3 2 45 60.70 89.71 28.15 o 4 2 45 43.68 -25.01 25.01 o 0 3 45 0.21 45.78 32.54 o 1 3 45 9.11 24.41 28.47 o 2 3 45 8.40 24.19 24.43 o 3 3 45 10.25 -0.49 22.90 o 4 3 45 172.43 252.42 50.31 o 0 4 45 74.25 -0.59 45.73 o 1 4 45 55.94 96.40 30.08 o 2 4 45 9.49 -27.55 41.67 o 3 4 45 17.05 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97.70 53.34 31.96 o 3 0 47 53.51 10.87 54.97 o 4 0 47 208.97 268.90 50.47 o 0 1 47 0.62 -32.93 32.93 o 1 1 47 193.57 214.44 29.86 o 2 1 47 16.96 5.13 24.91 o 3 1 47 2.56 -14.83 27.22 o 4 1 47 34.99 1.80 31.21 o 0 2 47 33.67 105.21 53.83 o 1 2 47 16.70 6.28 27.84 o 2 2 47 83.95 77.48 33.10 o 3 2 47 65.51 65.13 25.79 o 4 2 47 20.12 22.08 23.24 o 0 3 47 14.62 -12.11 26.95 o 1 3 47 0.83 39.59 27.03 o 2 3 47 115.10 43.45 68.20 o 3 3 47 33.47 7.34 20.12 o 0 4 47 20.36 75.80 45.78 o 1 4 47 41.43 27.40 52.99 o 2 4 47 32.37 18.75 40.95 o 3 4 47 33.07 -2.29 24.77 o 0 5 47 261.53 151.62 119.12 o 1 5 47 231.19 395.18 69.39 o 0 0 48 400.92 382.44 69.73 o 1 0 48 0.71 -19.33 42.53 o 2 0 48 7.71 16.72 36.34 o 3 0 48 11.66 -7.61 62.47 o 4 0 48 30.35 -19.01 44.61 o 0 1 48 169.20 187.02 56.91 o 1 1 48 22.08 11.77 27.05 o 2 1 48 46.00 26.19 32.64 o 3 1 48 46.51 -12.64 27.98 o 0 2 48 7.20 -17.30 59.33 o 1 2 48 57.01 28.60 30.19 o 2 2 48 18.80 31.97 43.65 o 3 2 48 14.87 10.45 22.06 o 0 3 48 52.89 -27.37 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38.19 28.09 o 0 2 51 77.02 100.42 39.01 o 1 2 51 46.43 171.59 120.27 o 0 0 52 57.87 64.99 70.80 o