#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2013503.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013503_Fobs loop_ _publ_author_name 'Zakaria, Choudhury M.' 'Ferguson, George' 'Lough, Alan J.' 'Glidewell, Christopher' _publ_section_title ; Adducts of hexamethylenetetramine with ferrocenecarboxylic acid and ferrocene-1,1'-dicarboxylic acid: multiple disorder in space groups Fmm2 and Cmcm ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m271 _journal_page_last m274 _journal_volume 59 _journal_year 2003 _space_group_IT_number 63 _symmetry_space_group_name_Hall '-C 2c 2' _symmetry_space_group_name_H-M 'C m c m' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 10.0096 _cell_length_b 7.1396 _cell_length_c 24.2841 _exptl_crystal_F_000 864.00 _reflns_d_resolution_high 0.8405 _[local]_cod_data_source_file sk1641IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' 57 CMZ31 in Cmcm' _shelx_refln_list_code 4 _shelx_f_calc_maximum 210.25 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' 'x, -y, -z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z+1/2' 'x+1/2, -y+1/2, -z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, y, -z-1/2' '-x, y, z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, y+1/2, -z-1/2' '-x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 760.19 944.52 54.38 o 6 0 0 1973.47 2080.80 110.19 o 8 0 0 6366.73 6540.08 359.20 o 10 0 0 791.31 704.10 55.81 o 1 1 0 14538.43 13862.96 543.81 o 3 1 0 4425.41 3905.44 108.76 o 5 1 0 2105.45 2105.13 57.24 o 7 1 0 1872.02 2000.66 68.69 o 9 1 0 821.62 848.64 44.36 o 11 1 0 38.30 8.59 21.47 o 0 2 0 2452.89 2491.53 83.00 o 2 2 0 5143.97 5461.04 130.23 o 4 2 0 30057.44 31559.81 857.22 o 6 2 0 6262.01 6940.78 216.09 o 8 2 0 151.55 170.30 18.60 o 10 2 0 16.59 58.67 17.17 o 1 3 0 10082.49 9257.71 234.70 o 3 3 0 774.97 664.03 22.90 o 5 3 0 425.49 389.26 15.74 o 7 3 0 384.41 310.55 17.17 o 9 3 0 57.98 31.48 12.88 o 11 3 0 51.76 75.85 30.05 o 0 4 0 21000.57 21360.43 797.12 o 2 4 0 8985.49 9020.15 220.39 o 4 4 0 1526.51 1611.41 52.95 o 6 4 0 1319.46 1250.77 50.09 o 8 4 0 966.53 917.33 42.93 o 10 4 0 11.86 47.23 45.79 o 1 5 0 2940.53 2945.18 75.85 o 3 5 0 3689.27 3669.31 100.18 o 5 5 0 3356.68 3325.85 161.71 o 7 5 0 1165.31 1210.70 52.95 o 9 5 0 156.02 171.73 30.05 o 0 6 0 203.80 227.54 22.90 o 2 6 0 867.90 890.14 31.48 o 4 6 0 1681.24 1718.74 74.42 o 6 6 0 573.02 586.75 35.78 o 8 6 0 1.37 51.52 27.19 o 1 7 0 443.90 480.85 31.48 o 3 7 0 2958.30 3084.00 145.97 o 5 7 0 1911.42 1851.83 161.71 o 0 8 0 403.04 319.13 37.21 o 2 8 0 609.39 569.57 37.21 o 1 1 1 1982.80 1879.02 48.66 o 3 1 1 1637.21 1587.08 32.92 o 5 1 1 200.49 208.94 8.59 o 7 1 1 39.10 30.05 8.59 o 9 1 1 0.05 2.86 10.02 o 11 1 1 24.61 -7.16 15.74 o 0 2 1 27.96 52.95 7.16 o 2 2 1 108.22 110.19 5.72 o 4 2 1 91.54 223.25 14.31 o 6 2 1 133.88 148.83 10.02 o 8 2 1 64.54 32.92 11.45 o 10 2 1 112.08 133.09 24.33 o 1 3 1 1838.94 1847.54 34.35 o 3 3 1 2.83 1.43 4.29 o 5 3 1 1.11 5.72 5.72 o 7 3 1 1.00 4.29 7.16 o 9 3 1 0.20 0.00 8.59 o 11 3 1 0.25 18.60 15.74 o 0 4 1 16.11 25.76 8.59 o 2 4 1 5.15 -2.86 4.29 o 4 4 1 0.13 15.74 5.72 o 6 4 1 165.46 210.37 10.02 o 8 4 1 23.03 52.95 11.45 o 10 4 1 0.20 -10.02 15.74 o 1 5 1 4.03 11.45 5.72 o 3 5 1 227.18 241.85 10.02 o 5 5 1 110.09 90.16 10.02 o 7 5 1 9.41 -8.59 8.59 o 9 5 1 25.88 22.90 14.31 o 0 6 1 5.99 0.00 10.02 o 2 6 1 315.13 310.55 12.88 o 4 6 1 1095.10 1099.08 34.35 o 6 6 1 238.85 196.06 15.74 o 8 6 1 5.06 -7.16 17.17 o 1 7 1 35.07 24.33 10.02 o 3 7 1 202.50 196.06 15.74 o 5 7 1 132.38 125.94 21.47 o 0 8 1 1454.77 1569.90 70.12 o 2 8 1 258.65 240.42 17.17 o 2 0 2 5068.33 4754.08 151.70 o 4 0 2 3583.02 3739.44 128.80 o 6 0 2 288.25 286.22 15.74 o 8 0 2 35.19 27.19 12.88 o 10 0 2 51.67 83.00 18.60 o 1 1 2 44204.21 42381.70 1003.19 o 3 1 2 6054.85 6066.39 123.07 o 5 1 2 2768.44 2867.90 57.24 o 7 1 2 1562.57 1647.18 44.36 o 9 1 2 339.34 356.34 18.60 o 11 1 2 8.07 -2.86 15.74 o 0 2 2 7268.68 6804.83 173.16 o 2 2 2 479.73 450.79 10.02 o 4 2 2 106.73 200.35 8.59 o 6 2 2 640.44 646.85 17.17 o 8 2 2 896.23 993.18 30.05 o 10 2 2 56.23 38.64 17.17 o 1 3 2 7199.67 7105.36 124.50 o 3 3 2 7421.22 7506.06 148.83 o 5 3 2 4064.73 4253.20 94.45 o 7 3 2 1152.18 1212.13 35.78 o 9 3 2 295.43 320.56 17.17 o 11 3 2 0.21 10.02 18.60 o 0 4 2 8812.34 8586.53 240.42 o 2 4 2 6137.26 5883.21 104.47 o 4 4 2 3780.03 3845.34 77.28 o 6 4 2 1346.65 1360.97 30.05 o 8 4 2 214.57 246.15 12.88 o 10 4 2 25.54 45.79 18.60 o 1 5 2 2954.36 2900.82 55.81 o 3 5 2 3469.90 3636.40 72.99 o 5 5 2 1953.58 2003.52 44.36 o 7 5 2 432.57 419.31 20.04 o 9 5 2 7.54 22.90 18.60 o 0 6 2 480.17 443.64 21.47 o 2 6 2 1600.89 1604.25 40.07 o 4 6 2 3476.05 3543.38 84.43 o 6 6 2 1442.46 1365.26 50.09 o 8 6 2 242.75 274.77 28.62 o 1 7 2 994.07 986.02 37.21 o 3 7 2 509.91 490.86 24.33 o 5 7 2 345.71 313.41 32.92 o 0 8 2 2444.71 2457.18 123.07 o 2 8 2 1843.57 1899.06 84.43 o 1 1 3 7804.80 7966.87 133.09 o 3 1 3 930.78 987.45 21.47 o 5 1 3 276.88 320.56 10.02 o 7 1 3 613.25 652.58 20.04 o 9 1 3 150.12 105.90 11.45 o 11 1 3 2.04 14.31 18.60 o 0 2 3 2677.94 2640.36 61.54 o 2 2 3 1005.11 983.16 18.60 o 4 2 3 4214.46 4588.07 78.71 o 6 2 3 790.72 858.65 21.47 o 8 2 3 32.14 55.81 8.59 o 10 2 3 49.47 27.19 11.45 o 1 3 3 1578.94 1569.90 32.92 o 3 3 3 3883.11 4170.19 83.00 o 5 3 3 2419.39 2603.15 51.52 o 7 3 3 128.55 138.82 10.02 o 9 3 3 252.33 178.89 14.31 o 11 3 3 0.47 8.59 21.47 o 0 4 3 202.40 197.49 10.02 o 2 4 3 33.44 25.76 4.29 o 4 4 3 93.23 88.73 7.16 o 6 4 3 6.18 0.00 10.02 o 8 4 3 6.06 24.33 8.59 o 10 4 3 26.78 15.74 17.17 o 1 5 3 17.73 7.16 5.72 o 3 5 3 92.92 93.02 8.59 o 5 5 3 53.47 40.07 10.02 o 7 5 3 4.12 21.47 11.45 o 9 5 3 22.05 1.43 17.17 o 0 6 3 0.78 -8.59 10.02 o 2 6 3 32.15 20.04 12.88 o 4 6 3 91.53 83.00 11.45 o 6 6 3 53.97 38.64 14.31 o 8 6 3 30.71 80.14 22.90 o 1 7 3 711.36 691.22 25.76 o 3 7 3 223.03 204.65 17.17 o 5 7 3 0.00 -15.74 15.74 o 0 8 3 48.04 25.76 17.17 o 2 8 3 1.50 -12.88 12.88 o 0 0 4 12922.37 11264.10 845.77 o 2 0 4 8349.54 7850.95 276.20 o 4 0 4 6448.72 6155.11 181.75 o 6 0 4 2768.86 2810.66 88.73 o 8 0 4 450.70 553.83 27.19 o 10 0 4 1.21 18.60 17.17 o 1 1 4 2771.17 2753.42 47.23 o 3 1 4 2420.27 2332.68 40.07 o 5 1 4 354.11 306.25 10.02 o 7 1 4 140.83 115.92 10.02 o 9 1 4 85.24 48.66 12.88 o 11 1 4 5.37 1.43 15.74 o 0 2 4 14267.64 14143.45 306.25 o 2 2 4 10262.20 10009.04 173.16 o 4 2 4 3750.91 3677.90 68.69 o 6 2 4 1113.04 1177.79 30.05 o 8 2 4 341.03 366.36 14.31 o 10 2 4 133.87 84.43 12.88 o 1 3 4 1979.39 1873.30 35.78 o 3 3 4 3210.26 3225.67 58.67 o 5 3 4 3503.26 3550.53 68.69 o 7 3 4 715.75 891.57 27.19 o 9 3 4 5.03 1.43 11.45 o 11 3 4 1.31 21.47 18.60 o 0 4 4 885.94 818.58 24.33 o 2 4 4 2613.40 2462.90 45.79 o 4 4 4 2392.00 2501.54 51.52 o 6 4 4 374.14 339.17 12.88 o 8 4 4 17.38 31.48 10.02 o 10 4 4 0.82 -5.72 17.17 o 1 5 4 3133.48 3215.66 62.97 o 3 5 4 350.58 326.29 12.88 o 5 5 4 17.24 15.74 10.02 o 7 5 4 36.69 21.47 14.31 o 9 5 4 167.02 153.13 22.90 o 0 6 4 1098.66 1079.04 37.21 o 2 6 4 243.44 238.99 11.45 o 4 6 4 4.80 7.16 10.02 o 6 6 4 127.73 145.97 15.74 o 8 6 4 65.01 37.21 17.17 o 1 7 4 558.25 605.35 24.33 o 3 7 4 2114.26 2219.62 70.12 o 5 7 4 1729.45 1692.98 88.73 o 0 8 4 778.53 838.62 50.09 o 2 8 4 965.70 1016.07 48.66 o 1 1 5 31595.20 30764.12 560.99 o 3 1 5 2266.91 2442.87 51.52 o 5 1 5 3220.08 3519.05 78.71 o 7 1 5 298.27 256.16 12.88 o 9 1 5 385.82 320.56 17.17 o 11 1 5 33.33 17.17 17.17 o 0 2 5 6383.42 6873.52 138.82 o 2 2 5 1191.80 1150.60 22.90 o 4 2 5 159.73 251.87 8.59 o 6 2 5 0.59 12.88 7.16 o 8 2 5 267.21 306.25 12.88 o 10 2 5 150.61 121.64 18.60 o 1 3 5 3531.23 3600.62 62.97 o 3 3 5 8.37 2.86 5.72 o 5 3 5 153.02 198.92 8.59 o 7 3 5 83.48 83.00 10.02 o 9 3 5 76.77 52.95 11.45 o 0 4 5 332.72 279.06 14.31 o 2 4 5 10.17 -4.29 5.72 o 4 4 5 10.38 18.60 7.16 o 6 4 5 23.52 32.92 7.16 o 8 4 5 8.49 1.43 8.59 o 10 4 5 0.63 28.62 34.35 o 1 5 5 1152.31 1184.94 25.76 o 3 5 5 361.88 352.05 14.31 o 5 5 5 780.54 741.30 21.47 o 7 5 5 0.51 -5.72 7.16 o 9 5 5 21.84 21.47 20.04 o 0 6 5 222.58 203.21 14.31 o 2 6 5 21.04 17.17 5.72 o 4 6 5 220.50 191.77 14.31 o 6 6 5 11.52 18.60 15.74 o 8 6 5 69.18 60.11 20.04 o 1 7 5 498.74 512.33 24.33 o 3 7 5 76.12 65.83 20.04 o 5 7 5 22.00 30.05 17.17 o 0 8 5 721.28 666.89 38.64 o 2 8 5 118.48 84.43 18.60 o 0 0 6 1863.89 1941.99 68.69 o 2 0 6 1012.43 1100.51 34.35 o 4 0 6 2752.38 2618.89 74.42 o 6 0 6 31.41 4.29 7.16 o 8 0 6 540.61 465.10 27.19 o 10 0 6 36.29 18.60 18.60 o 1 1 6 209.58 276.20 5.72 o 3 1 6 3779.16 3510.46 65.83 o 5 1 6 2175.32 2022.13 48.66 o 7 1 6 137.55 164.58 10.02 o 9 1 6 8.43 -2.86 10.02 o 11 1 6 0.47 12.88 17.17 o 0 2 6 524.91 495.16 15.74 o 2 2 6 1870.53 1828.93 34.35 o 4 2 6 1213.57 1136.28 22.90 o 6 2 6 626.21 623.95 17.17 o 8 2 6 116.62 95.88 10.02 o 10 2 6 3.34 2.86 11.45 o 1 3 6 5029.15 4765.53 91.59 o 3 3 6 2237.77 2158.08 40.07 o 5 3 6 257.82 297.67 10.02 o 7 3 6 89.93 91.59 8.59 o 9 3 6 162.67 115.92 14.31 o 0 4 6 3326.58 3278.63 72.99 o 2 4 6 3225.51 3156.98 54.38 o 4 4 6 1678.12 1707.29 35.78 o 6 4 6 380.77 410.72 15.74 o 8 4 6 43.75 47.23 10.02 o 10 4 6 24.39 -2.86 25.76 o 1 5 6 1205.57 1227.87 28.62 o 3 5 6 912.37 978.86 25.76 o 5 5 6 407.77 417.88 18.60 o 7 5 6 100.02 138.82 14.31 o 9 5 6 3.84 45.79 22.90 o 0 6 6 2597.64 2701.90 77.28 o 2 6 6 1546.87 1564.18 38.64 o 4 6 6 392.73 369.22 17.17 o 6 6 6 209.14 198.92 18.60 o 8 6 6 229.38 240.42 24.33 o 1 7 6 1475.84 1448.26 52.95 o 3 7 6 203.66 208.94 17.17 o 5 7 6 66.93 52.95 18.60 o 0 8 6 1404.08 1315.17 72.99 o 2 8 6 754.21 672.61 34.35 o 1 1 7 21606.73 21390.49 384.96 o 3 1 7 294.19 277.63 8.59 o 5 1 7 393.28 366.36 11.45 o 7 1 7 23.46 12.88 7.16 o 9 1 7 41.34 4.29 12.88 o 11 1 7 53.07 2.86 21.47 o 0 2 7 3110.33 3086.86 71.55 o 2 2 7 648.16 615.37 12.88 o 4 2 7 57.69 60.11 5.72 o 6 2 7 37.51 40.07 7.16 o 8 2 7 7.50 -4.29 7.16 o 10 2 7 45.45 27.19 25.76 o 1 3 7 1125.81 1219.29 24.33 o 3 3 7 6.08 7.16 5.72 o 5 3 7 67.15 58.67 5.72 o 7 3 7 25.76 14.31 8.59 o 9 3 7 4.93 25.76 11.45 o 0 4 7 50.47 55.81 8.59 o 2 4 7 365.30 393.55 11.45 o 4 4 7 2067.20 1963.45 40.07 o 6 4 7 867.36 918.76 28.62 o 8 4 7 7.32 28.62 10.02 o 10 4 7 22.75 -7.16 24.33 o 1 5 7 1089.20 1137.72 25.76 o 3 5 7 253.24 254.73 11.45 o 5 5 7 149.87 155.99 11.45 o 7 5 7 130.48 113.06 14.31 o 9 5 7 12.79 -1.43 25.76 o 0 6 7 36.33 20.04 11.45 o 2 6 7 14.12 5.72 10.02 o 4 6 7 199.26 168.87 15.74 o 6 6 7 74.35 85.87 17.17 o 1 7 7 30.04 31.48 10.02 o 3 7 7 155.01 141.68 17.17 o 5 7 7 156.59 84.43 18.60 o 0 8 7 0.13 -8.59 27.19 o 2 8 7 0.26 10.02 17.17 o 0 0 8 8895.62 8142.90 340.60 o 2 0 8 7946.79 7503.20 211.80 o 4 0 8 2251.31 2166.67 61.54 o 6 0 8 1571.25 1548.44 57.24 o 8 0 8 992.40 1047.56 60.11 o 10 0 8 149.60 77.28 18.60 o 1 1 8 4337.34 4268.94 65.83 o 3 1 8 8606.56 8590.83 184.61 o 5 1 8 3981.29 3905.44 84.43 o 7 1 8 447.79 522.35 17.17 o 9 1 8 1.90 -2.86 8.59 o 11 1 8 0.29 27.19 18.60 o 0 2 8 3401.76 3805.27 81.57 o 2 2 8 1236.66 1110.53 20.04 o 4 2 8 7829.09 8137.17 180.32 o 6 2 8 814.68 825.74 20.04 o 8 2 8 75.12 35.78 7.16 o 10 2 8 14.28 22.90 14.31 o 1 3 8 1865.98 1801.74 28.62 o 3 3 8 3046.56 2919.42 52.95 o 5 3 8 877.01 824.31 20.04 o 7 3 8 25.76 15.74 8.59 o 9 3 8 0.68 -10.02 10.02 o 0 4 8 7669.45 7646.31 218.96 o 2 4 8 1698.49 1671.51 35.78 o 4 4 8 138.00 121.64 8.59 o 6 4 8 13.02 25.76 7.16 o 8 4 8 365.54 383.53 22.90 o 1 5 8 3774.21 3758.04 83.00 o 3 5 8 1138.55 1160.61 30.05 o 5 5 8 365.38 389.26 15.74 o 7 5 8 425.42 449.36 24.33 o 9 5 8 194.23 249.01 32.92 o 0 6 8 755.54 801.41 31.48 o 2 6 8 950.76 937.36 25.76 o 4 6 8 712.35 705.53 25.76 o 6 6 8 136.31 87.30 18.60 o 1 7 8 1446.67 1469.73 47.23 o 3 7 8 304.45 306.25 21.47 o 5 7 8 24.97 44.36 14.31 o 0 8 8 832.81 867.24 74.42 o 2 8 8 297.37 270.48 24.33 o 1 1 9 882.36 884.41 14.31 o 3 1 9 776.61 812.86 20.04 o 5 1 9 575.59 656.87 20.04 o 7 1 9 7.98 14.31 5.72 o 9 1 9 3.70 0.00 8.59 o 11 1 9 33.45 38.64 21.47 o 0 2 9 5398.56 5665.68 121.64 o 2 2 9 2185.32 2241.09 41.50 o 4 2 9 62.35 67.26 7.16 o 6 2 9 10.55 10.02 4.29 o 8 2 9 86.09 48.66 10.02 o 10 2 9 86.66 104.47 21.47 o 1 3 9 1168.54 1266.51 22.90 o 3 3 9 85.14 65.83 5.72 o 5 3 9 0.27 -7.16 7.16 o 7 3 9 2.39 -7.16 7.16 o 9 3 9 0.17 -8.59 11.45 o 0 4 9 389.77 356.34 15.74 o 2 4 9 491.85 536.66 12.88 o 4 4 9 3927.28 3999.89 77.28 o 6 4 9 1303.04 1362.40 37.21 o 8 4 9 1.15 17.17 10.02 o 1 5 9 4.90 11.45 5.72 o 3 5 9 20.21 8.59 8.59 o 5 5 9 27.73 24.33 8.59 o 7 5 9 65.72 51.52 17.17 o 0 6 9 972.61 967.42 34.35 o 2 6 9 442.69 397.84 17.17 o 4 6 9 0.10 -1.43 12.88 o 6 6 9 5.77 -21.47 21.47 o 1 7 9 339.19 304.82 24.33 o 3 7 9 65.42 -5.72 17.17 o 5 7 9 0.55 -15.74 15.74 o 0 8 9 0.62 24.33 25.76 o 0 0 10 2934.56 2887.94 114.49 o 2 0 10 6092.95 6054.94 158.85 o 4 0 10 9157.92 9505.29 231.84 o 6 0 10 2776.11 3055.38 98.75 o 8 0 10 36.49 11.45 11.45 o 10 0 10 7.23 -1.43 17.17 o 1 1 10 715.78 619.66 11.45 o 3 1 10 6058.41 6286.77 128.80 o 5 1 10 3729.73 3904.01 85.87 o 7 1 10 537.53 525.21 17.17 o 9 1 10 96.22 85.87 8.59 o 11 1 10 60.37 47.23 24.33 o 0 2 10 13359.17 13908.75 274.77 o 2 2 10 8498.81 8605.14 133.09 o 4 2 10 2497.02 2465.77 57.24 o 6 2 10 696.69 655.44 22.90 o 8 2 10 317.05 350.62 15.74 o 10 2 10 20.59 40.07 25.76 o 1 3 10 7024.42 7400.16 130.23 o 3 3 10 550.49 528.07 15.74 o 5 3 10 86.85 75.85 5.72 o 7 3 10 565.82 526.64 15.74 o 9 3 10 396.59 376.38 32.92 o 0 4 10 1822.69 1947.71 50.09 o 2 4 10 3674.13 3666.45 70.12 o 4 4 10 4547.25 4671.07 90.16 o 6 4 10 1526.68 1564.18 42.93 o 8 4 10 254.74 207.51 17.17 o 1 5 10 1958.19 1891.90 38.64 o 3 5 10 3412.86 3398.84 72.99 o 5 5 10 1953.02 1947.71 60.11 o 7 5 10 241.38 253.30 21.47 o 0 6 10 7839.06 8175.81 294.80 o 2 6 10 3481.69 3494.72 93.02 o 4 6 10 412.49 447.93 21.47 o 6 6 10 346.59 334.87 25.76 o 1 7 10 1568.54 1751.65 77.28 o 3 7 10 299.89 337.74 24.33 o 5 7 10 87.96 81.57 18.60 o 1 1 11 830.95 882.98 14.31 o 3 1 11 199.36 200.35 7.16 o 5 1 11 346.45 307.68 14.31 o 7 1 11 62.25 64.40 11.45 o 9 1 11 205.36 113.06 8.59 o 0 2 11 9279.85 9981.85 257.60 o 2 2 11 1242.67 1362.40 27.19 o 4 2 11 42.78 41.50 7.16 o 6 2 11 145.74 155.99 11.45 o 8 2 11 325.93 332.01 25.76 o 10 2 11 27.00 14.31 21.47 o 1 3 11 313.14 380.67 10.02 o 3 3 11 220.80 287.65 10.02 o 5 3 11 213.54 204.65 7.16 o 7 3 11 113.32 98.75 12.88 o 9 3 11 12.08 -15.74 15.74 o 0 4 11 480.57 499.45 18.60 o 2 4 11 139.70 141.68 8.59 o 4 4 11 0.14 -7.16 7.16 o 6 4 11 12.98 15.74 7.16 o 8 4 11 9.23 18.60 20.04 o 1 5 11 24.32 24.33 7.16 o 3 5 11 2099.68 2082.23 45.79 o 5 5 11 785.64 772.79 30.05 o 7 5 11 25.10 45.79 14.31 o 0 6 11 182.02 161.71 21.47 o 2 6 11 63.69 41.50 11.45 o 4 6 11 56.66 34.35 12.88 o 6 6 11 171.59 151.70 21.47 o 1 7 11 135.38 134.52 15.74 o 3 7 11 0.14 27.19 17.17 o 0 0 12 345.45 370.65 17.17 o 2 0 12 1729.37 1753.08 44.36 o 4 0 12 7948.37 8354.70 207.51 o 6 0 12 2421.07 2664.69 90.16 o 8 0 12 408.42 482.28 28.62 o 10 0 12 243.17 342.03 34.35 o 1 1 12 14949.49 14655.78 231.84 o 3 1 12 4590.67 4437.81 91.59 o 5 1 12 2262.54 2322.66 54.38 o 7 1 12 1273.19 1196.39 44.36 o 9 1 12 234.65 243.29 25.76 o 0 2 12 27871.07 28133.78 668.32 o 2 2 12 9205.12 9234.82 153.13 o 4 2 12 744.84 738.44 18.60 o 6 2 12 1066.36 1110.53 31.48 o 8 2 12 1195.81 1111.96 60.11 o 10 2 12 207.47 168.87 25.76 o 1 3 12 4270.21 4290.40 71.55 o 3 3 12 6830.16 6989.44 133.09 o 5 3 12 3860.01 4074.31 110.19 o 7 3 12 640.43 681.20 30.05 o 9 3 12 123.19 95.88 22.90 o 0 4 12 266.05 213.23 12.88 o 2 4 12 676.28 613.94 17.17 o 4 4 12 1782.08 1757.38 38.64 o 6 4 12 1015.97 1027.52 32.92 o 8 4 12 130.93 137.38 24.33 o 1 5 12 3264.57 3285.78 74.42 o 3 5 12 978.70 920.19 24.33 o 5 5 12 333.28 329.15 17.17 o 7 5 12 374.85 231.84 30.05 o 0 6 12 1832.28 1914.80 61.54 o 2 6 12 1562.58 1562.75 48.66 o 4 6 12 712.73 741.30 28.62 o 6 6 12 93.88 71.55 24.33 o 1 7 12 1168.16 1189.23 47.23 o 3 7 12 1132.50 1117.68 51.52 o 1 1 13 590.50 509.47 11.45 o 3 1 13 98.34 80.14 5.72 o 5 1 13 396.68 433.62 14.31 o 7 1 13 42.24 25.76 10.02 o 9 1 13 24.13 28.62 17.17 o 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