#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2013506.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013506_Fobs loop_ _publ_author_name 'Bowes, Katharine F.' 'Ferguson, George' 'Lough, Alan J.' 'Glidewell, Christopher' _publ_section_title ; 1,4,8,11-Tetraazoniacyclotetradecane tetrakis(phenylphosphonate) dihydrate forms hydrogen-bonded sheets ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o461 _journal_page_last o463 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.513 _cell_angle_gamma 90.000 _cell_length_a 13.0678 _cell_length_b 8.7475 _cell_length_c 17.6106 _exptl_crystal_F_000 920.00 _reflns_d_resolution_high 0.7717 _[local]_cod_data_source_file sk1643Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 209 KFB18 in P21/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 153.15 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 5971.74 5921.09 232.68 o 6 0 0 3829.40 3591.72 146.16 o 8 0 0 597.24 558.18 24.94 o 10 0 0 483.47 496.76 33.19 o 12 0 0 220.83 232.42 11.43 o 14 0 0 1158.55 1124.93 83.84 o 16 0 0 146.08 144.91 25.79 o 1 1 0 25.96 33.51 5.32 o 2 1 0 13745.85 13468.07 1235.32 o 3 1 0 11151.19 10877.98 416.14 o 4 1 0 3315.22 3604.08 113.76 o 5 1 0 178.72 147.81 7.60 o 6 1 0 3720.82 3652.02 115.31 o 7 1 0 290.15 323.34 29.76 o 8 1 0 2114.06 2123.43 90.28 o 9 1 0 1930.93 1895.34 92.16 o 10 1 0 172.42 181.03 9.50 o 11 1 0 34.76 37.24 3.88 o 12 1 0 489.40 557.28 27.99 o 13 1 0 54.33 68.77 4.89 o 14 1 0 0.52 3.90 2.59 o 15 1 0 144.38 139.87 13.20 o 16 1 0 0.11 9.89 7.59 o 0 2 0 8290.84 8288.15 534.02 o 1 2 0 1714.48 1744.73 78.83 o 2 2 0 237.90 228.83 10.93 o 3 2 0 1621.19 1552.45 51.71 o 4 2 0 2174.78 2377.99 106.81 o 5 2 0 64.89 50.79 3.04 o 6 2 0 5045.23 5112.09 273.70 o 7 2 0 1904.39 1667.08 229.53 o 8 2 0 125.34 112.43 7.01 o 9 2 0 99.32 87.23 4.21 o 10 2 0 256.47 223.37 25.49 o 11 2 0 2148.30 2165.75 101.34 o 12 2 0 944.52 949.44 34.24 o 13 2 0 127.42 153.30 23.32 o 14 2 0 1.68 2.48 4.38 o 15 2 0 4.11 3.73 6.15 o 16 2 0 2.06 -6.48 6.48 o 1 3 0 3745.26 3773.61 192.84 o 2 3 0 90.32 146.63 6.07 o 3 3 0 279.19 302.30 10.58 o 4 3 0 22.68 15.84 4.43 o 5 3 0 2657.84 2537.08 93.51 o 6 3 0 758.54 748.54 60.52 o 7 3 0 40.21 44.24 4.52 o 8 3 0 29.21 36.23 2.85 o 9 3 0 2938.89 3073.30 120.35 o 10 3 0 1822.87 1750.95 103.77 o 11 3 0 190.47 212.74 8.05 o 12 3 0 681.98 732.56 42.41 o 13 3 0 162.76 151.70 9.47 o 14 3 0 3.70 1.54 4.61 o 15 3 0 122.61 97.72 11.30 o 16 3 0 481.86 435.60 30.13 o 0 4 0 99.33 41.77 5.57 o 1 4 0 1341.16 1285.93 59.30 o 2 4 0 346.55 329.38 10.75 o 3 4 0 16.85 15.86 2.36 o 4 4 0 376.59 407.49 17.29 o 5 4 0 117.98 136.59 7.86 o 6 4 0 6118.29 5793.34 440.05 o 7 4 0 1.24 5.95 4.96 o 8 4 0 3419.48 3475.81 98.94 o 9 4 0 940.80 927.42 27.98 o 10 4 0 77.60 72.55 4.19 o 11 4 0 27.73 17.17 6.00 o 12 4 0 384.98 350.07 23.44 o 13 4 0 302.97 277.32 17.11 o 14 4 0 1507.89 1558.04 138.50 o 15 4 0 32.74 19.72 9.31 o 1 5 0 2149.29 2301.40 96.45 o 2 5 0 217.47 168.95 10.37 o 3 5 0 109.95 116.68 4.77 o 4 5 0 765.36 795.45 31.89 o 5 5 0 10.24 3.46 2.24 o 6 5 0 213.83 214.88 9.13 o 7 5 0 1568.24 1423.57 47.44 o 8 5 0 179.84 192.97 9.34 o 9 5 0 0.62 2.72 2.49 o 10 5 0 256.53 266.23 9.33 o 11 5 0 6.00 7.56 2.17 o 12 5 0 167.15 154.79 12.36 o 13 5 0 12.00 13.59 8.88 o 14 5 0 0.04 7.50 11.39 o 15 5 0 730.15 675.92 36.77 o 0 6 0 2221.46 2242.04 126.87 o 1 6 0 357.26 334.37 14.32 o 2 6 0 1180.14 1185.57 61.83 o 3 6 0 838.85 839.65 32.75 o 4 6 0 47.19 42.04 3.30 o 5 6 0 1419.22 1495.02 49.09 o 6 6 0 136.06 119.36 7.51 o 7 6 0 73.37 67.54 4.63 o 8 6 0 171.01 172.20 11.16 o 9 6 0 89.35 89.99 5.51 o 10 6 0 235.01 222.13 15.28 o 11 6 0 548.79 581.46 21.96 o 12 6 0 1.34 9.29 5.78 o 13 6 0 90.63 66.91 12.15 o 14 6 0 685.31 677.81 45.37 o 1 7 0 11.75 3.74 6.10 o 2 7 0 377.95 399.74 23.02 o 3 7 0 434.11 442.50 17.40 o 4 7 0 791.82 787.43 38.38 o 5 7 0 249.74 250.69 10.36 o 6 7 0 390.87 363.64 17.61 o 7 7 0 241.92 219.64 9.99 o 8 7 0 18.04 24.97 3.78 o 9 7 0 1003.16 1040.30 49.91 o 10 7 0 0.81 3.50 3.43 o 11 7 0 7.92 16.98 4.24 o 12 7 0 68.70 80.31 14.72 o 13 7 0 1.34 -2.16 7.89 o 0 8 0 10148.06 10484.85 701.97 o 1 8 0 500.09 448.94 21.08 o 2 8 0 10.03 20.69 6.90 o 3 8 0 231.47 222.03 8.10 o 4 8 0 35.89 26.31 4.15 o 5 8 0 545.30 610.51 28.15 o 6 8 0 931.91 934.77 45.31 o 7 8 0 40.80 38.70 8.88 o 8 8 0 449.32 446.74 22.81 o 9 8 0 116.45 117.76 7.19 o 10 8 0 90.65 101.26 9.33 o 11 8 0 356.91 394.17 29.35 o 1 9 0 305.26 319.43 21.94 o 2 9 0 778.88 796.42 44.16 o 3 9 0 130.44 134.51 12.15 o 4 9 0 192.63 187.71 8.56 o 5 9 0 0.00 -2.79 4.63 o 6 9 0 168.71 188.53 14.68 o 7 9 0 1404.25 1465.36 102.07 o 8 9 0 296.45 305.09 17.25 o 9 9 0 28.40 28.83 4.64 o 10 9 0 2.48 5.80 9.18 o 0 10 0 833.68 815.58 72.11 o 1 10 0 409.90 427.50 30.48 o 2 10 0 55.28 39.53 13.96 o 3 10 0 1023.84 1125.68 76.86 o 4 10 0 933.91 965.06 68.31 o 5 10 0 32.36 22.03 4.50 o 6 10 0 412.51 396.00 44.92 o 1 11 0 213.75 199.39 27.51 o 2 11 0 122.79 79.64 22.22 o 4 11 0 63.28 61.74 18.83 o -15 0 1 301.45 231.27 27.98 o -13 0 1 102.48 101.42 23.80 o -11 0 1 1147.49 1083.08 112.56 o -9 0 1 156.85 149.20 11.09 o -7 0 1 509.53 494.18 20.08 o -5 0 1 894.06 835.41 35.43 o 3 0 1 105.07 93.59 4.76 o 5 0 1 393.32 291.73 17.13 o 7 0 1 51.75 55.36 4.10 o 9 0 1 847.95 887.78 48.00 o 11 0 1 1442.73 1467.28 83.10 o 13 0 1 137.61 125.29 8.90 o -16 1 1 0.07 -3.76 3.76 o -15 1 1 13.18 11.70 3.91 o -14 1 1 79.64 68.90 6.00 o -13 1 1 25.03 30.14 4.13 o -12 1 1 1000.65 948.50 58.77 o -11 1 1 475.57 478.70 22.02 o -10 1 1 408.92 384.31 22.49 o -9 1 1 1108.13 1115.58 38.04 o -8 1 1 262.17 276.90 9.14 o -7 1 1 231.63 211.60 8.32 o -6 1 1 176.45 262.38 11.18 o -5 1 1 2772.31 2928.97 97.16 o -4 1 1 1667.12 1467.19 51.23 o -3 1 1 1231.91 1192.43 68.20 o -2 1 1 2646.03 2611.45 106.68 o -1 1 1 667.59 486.87 22.65 o 0 1 1 421.28 152.72 26.74 o 1 1 1 18.82 21.23 2.10 o 2 1 1 740.86 632.42 22.93 o 3 1 1 382.82 462.71 25.53 o 4 1 1 84.87 96.97 4.60 o 5 1 1 4054.82 3827.20 223.55 o 6 1 1 34.83 37.41 3.84 o 7 1 1 168.94 213.08 15.67 o 8 1 1 842.45 744.87 49.34 o 9 1 1 3080.43 3112.15 95.63 o 10 1 1 1185.03 1190.74 55.60 o 11 1 1 450.80 447.53 26.49 o 12 1 1 25.75 36.70 3.33 o 13 1 1 393.84 381.46 21.81 o 14 1 1 65.21 56.13 12.85 o 15 1 1 0.54 -2.57 4.45 o 16 1 1 17.70 23.20 7.51 o -16 2 1 0.20 -1.62 8.03 o -15 2 1 40.96 46.05 5.71 o -14 2 1 346.46 364.18 20.64 o -13 2 1 172.08 162.16 12.66 o -12 2 1 1544.09 1554.23 90.89 o -11 2 1 155.10 122.63 6.32 o -10 2 1 818.46 845.37 30.36 o -9 2 1 265.89 241.78 13.58 o -8 2 1 743.92 625.27 29.92 o -7 2 1 1193.66 1298.69 45.32 o -6 2 1 86.57 87.63 4.50 o -5 2 1 153.75 151.45 8.84 o -4 2 1 1263.82 1225.93 50.93 o -3 2 1 905.86 899.24 35.14 o -2 2 1 4594.50 4371.42 170.62 o -1 2 1 111.19 118.75 8.40 o 0 2 1 3088.34 2844.47 110.59 o 1 2 1 13.81 11.89 2.80 o 2 2 1 3997.22 3602.73 187.79 o 3 2 1 2754.78 2777.45 165.46 o 4 2 1 2905.64 2930.20 95.36 o 5 2 1 156.37 139.20 5.27 o 6 2 1 640.88 621.84 25.11 o 7 2 1 311.36 285.39 9.99 o 8 2 1 102.42 89.39 3.98 o 9 2 1 289.88 262.25 13.88 o 10 2 1 3881.36 3801.08 145.97 o 11 2 1 0.04 -1.63 2.39 o 12 2 1 91.83 87.18 10.96 o 13 2 1 17.51 17.37 6.04 o 14 2 1 852.09 888.37 65.93 o 15 2 1 58.88 46.49 8.17 o 16 2 1 204.49 187.26 17.87 o -16 3 1 2.38 7.18 10.63 o -15 3 1 0.84 1.65 2.65 o -14 3 1 303.47 284.99 15.27 o -13 3 1 166.49 174.70 10.04 o -12 3 1 37.33 29.33 5.90 o -11 3 1 509.04 482.37 14.19 o -10 3 1 64.58 64.10 4.67 o -9 3 1 28.08 24.46 3.40 o -8 3 1 188.64 178.38 10.90 o -7 3 1 944.22 838.06 69.44 o -6 3 1 3360.60 3060.41 184.26 o -5 3 1 3.16 4.81 2.40 o -4 3 1 36.40 51.53 3.65 o -3 3 1 915.17 959.57 41.15 o -2 3 1 7.68 0.91 1.28 o -1 3 1 31.84 17.10 3.62 o 0 3 1 568.81 518.82 19.59 o 1 3 1 78.19 74.95 3.99 o 2 3 1 940.31 1016.55 29.43 o 3 3 1 987.06 942.96 124.66 o 4 3 1 3138.40 3168.16 186.90 o 5 3 1 251.71 297.88 10.90 o 6 3 1 104.86 119.78 6.07 o 7 3 1 604.02 643.99 42.82 o 8 3 1 3473.52 3317.95 289.04 o 9 3 1 1.99 0.43 3.31 o 10 3 1 367.97 370.37 12.71 o 11 3 1 430.14 485.48 19.99 o 12 3 1 63.84 66.66 7.58 o 13 3 1 494.67 443.76 29.18 o 14 3 1 88.17 98.95 11.23 o 15 3 1 17.69 27.87 11.15 o 16 3 1 914.44 870.56 57.61 o -15 4 1 194.09 178.90 19.46 o -14 4 1 4.72 -1.22 5.65 o -13 4 1 18.80 21.04 4.12 o -12 4 1 138.06 114.92 7.40 o -11 4 1 5434.20 5641.07 276.38 o -10 4 1 1292.65 1320.45 57.41 o -9 4 1 94.22 95.30 7.50 o -8 4 1 21.33 21.82 6.89 o -7 4 1 9.62 13.73 5.44 o -6 4 1 229.08 224.01 9.70 o -5 4 1 694.49 634.31 23.38 o -4 4 1 30.50 27.84 2.74 o -3 4 1 133.65 115.31 12.70 o -2 4 1 61.19 44.53 2.77 o -1 4 1 1070.86 1262.11 50.39 o 0 4 1 2704.52 2732.83 93.08 o 1 4 1 459.13 469.39 18.41 o 2 4 1 187.87 179.61 10.62 o 3 4 1 1788.91 1564.64 194.41 o 4 4 1 112.74 148.75 6.33 o 5 4 1 529.78 536.61 21.45 o 6 4 1 31.66 34.27 5.39 o 7 4 1 517.46 462.93 48.96 o 8 4 1 57.24 47.80 5.11 o 9 4 1 182.99 181.68 5.51 o 10 4 1 299.01 310.28 16.79 o 11 4 1 1.82 1.07 4.79 o 12 4 1 6.28 2.61 5.26 o 13 4 1 1463.06 1476.69 83.54 o 14 4 1 403.26 396.21 38.10 o 15 4 1 5.16 4.76 7.20 o -15 5 1 27.14 28.97 9.40 o -14 5 1 468.85 463.44 36.93 o -13 5 1 507.01 476.94 33.22 o -12 5 1 0.58 1.15 2.69 o -11 5 1 133.57 129.69 7.99 o -10 5 1 3.86 7.06 2.70 o -9 5 1 124.52 128.07 6.89 o -8 5 1 38.90 30.43 9.60 o -7 5 1 486.17 460.15 17.23 o -6 5 1 2394.45 2397.10 82.63 o -5 5 1 394.78 358.26 15.61 o -4 5 1 1006.29 1054.40 46.80 o -3 5 1 975.71 949.61 29.48 o -2 5 1 39.49 32.38 3.87 o -1 5 1 1093.10 1155.72 37.93 o 0 5 1 524.98 486.21 15.09 o 1 5 1 94.31 106.27 3.29 o 2 5 1 4125.24 4332.64 161.04 o 3 5 1 445.01 487.42 23.59 o 4 5 1 893.95 783.21 38.48 o 5 5 1 561.08 501.42 20.92 o 6 5 1 80.04 61.64 3.96 o 7 5 1 810.54 768.28 31.88 o 8 5 1 0.53 2.02 1.71 o 9 5 1 75.63 61.50 5.68 o 10 5 1 330.36 323.27 14.50 o 11 5 1 352.23 356.98 17.62 o 12 5 1 78.41 71.02 8.55 o 13 5 1 20.42 23.83 8.10 o 14 5 1 125.80 112.62 13.30 o 15 5 1 23.45 42.55 8.75 o -14 6 1 490.32 421.82 27.46 o -13 6 1 1.87 7.91 12.44 o -12 6 1 222.51 248.44 12.72 o -11 6 1 1526.67 1553.59 64.34 o -10 6 1 0.20 -2.09 2.09 o -9 6 1 48.70 40.04 5.64 o -8 6 1 713.05 746.04 32.46 o -7 6 1 1978.76 1934.26 80.32 o -6 6 1 245.45 262.47 9.64 o -5 6 1 4.02 5.61 3.30 o -4 6 1 1619.19 1631.77 68.34 o -3 6 1 98.56 95.61 8.94 o -2 6 1 20.46 19.95 5.48 o -1 6 1 2157.27 2238.57 85.60 o 0 6 1 183.56 141.06 6.38 o 1 6 1 658.81 619.22 26.89 o 2 6 1 205.16 181.50 8.32 o 3 6 1 190.84 177.12 8.80 o 4 6 1 744.74 729.00 25.19 o 5 6 1 71.22 71.75 5.50 o 6 6 1 606.13 597.62 18.48 o 7 6 1 44.59 43.22 3.89 o 8 6 1 436.21 431.12 15.11 o 9 6 1 894.12 828.38 28.77 o 10 6 1 1414.28 1498.26 65.98 o 11 6 1 170.02 160.36 11.91 o 12 6 1 2.28 -4.83 6.01 o 13 6 1 118.92 118.74 15.46 o 14 6 1 168.31 167.29 16.43 o -13 7 1 160.40 143.26 18.28 o -12 7 1 351.20 353.71 25.58 o -11 7 1 6.17 4.58 4.13 o -10 7 1 132.06 110.68 8.62 o -9 7 1 7.33 16.48 3.26 o -8 7 1 14.27 17.11 4.07 o -7 7 1 0.14 -3.39 4.36 o -6 7 1 402.06 451.95 15.06 o -5 7 1 2745.26 2888.15 99.72 o -4 7 1 482.24 495.59 27.50 o -3 7 1 14.63 18.04 4.91 o -2 7 1 1160.78 1188.31 33.88 o -1 7 1 802.78 836.88 26.37 o 0 7 1 535.93 483.01 19.24 o 1 7 1 0.55 -4.63 6.56 o 2 7 1 290.64 262.87 8.40 o 3 7 1 10.45 18.11 3.39 o 4 7 1 331.19 313.78 17.39 o 5 7 1 870.61 868.31 28.67 o 6 7 1 280.01 295.26 11.20 o 7 7 1 694.61 698.37 28.73 o 8 7 1 422.33 437.39 17.38 o 9 7 1 0.20 -1.30 2.94 o 10 7 1 227.96 224.92 12.71 o 11 7 1 28.45 34.50 7.81 o 12 7 1 32.50 27.73 7.14 o 13 7 1 279.08 276.48 28.51 o -11 8 1 188.89 203.24 18.57 o -10 8 1 111.06 127.81 11.74 o -9 8 1 3.02 2.55 3.88 o -8 8 1 473.22 430.84 31.14 o -7 8 1 193.31 158.98 13.70 o -6 8 1 814.84 764.90 47.26 o -5 8 1 404.23 372.20 31.57 o -4 8 1 31.48 25.66 4.31 o -3 8 1 628.62 669.26 24.47 o -2 8 1 438.76 418.41 15.21 o -1 8 1 1470.73 1543.93 86.49 o 0 8 1 1020.04 1072.66 53.40 o 1 8 1 523.00 527.97 27.07 o 2 8 1 104.83 95.41 9.68 o 3 8 1 512.78 525.42 29.21 o 4 8 1 1165.64 1238.65 57.89 o 5 8 1 1.87 -0.57 5.80 o 6 8 1 40.33 49.32 3.63 o 7 8 1 273.86 254.47 13.97 o 8 8 1 121.49 116.43 7.84 o 9 8 1 195.04 210.99 12.30 o 10 8 1 397.19 391.22 24.10 o 11 8 1 138.51 147.95 16.24 o -10 9 1 98.22 58.49 13.03 o -9 9 1 195.16 235.97 15.93 o -8 9 1 179.14 162.66 15.19 o -7 9 1 27.93 20.84 6.08 o -6 9 1 532.72 517.75 27.03 o -5 9 1 9.25 -0.83 11.44 o -4 9 1 6.00 7.24 2.28 o -3 9 1 627.38 618.77 27.61 o -2 9 1 251.18 260.84 23.66 o -1 9 1 363.92 351.58 20.93 o 0 9 1 206.91 213.40 16.33 o 1 9 1 29.47 27.15 7.31 o 2 9 1 178.78 178.81 15.30 o 3 9 1 3.49 -3.56 6.65 o 4 9 1 443.45 446.56 23.61 o 5 9 1 114.12 110.79 9.02 o 6 9 1 414.86 460.90 21.62 o 7 9 1 51.54 53.20 6.69 o 8 9 1 85.61 91.73 8.29 o 9 9 1 319.57 300.34 26.78 o 10 9 1 301.09 314.84 33.31 o -6 10 1 376.55 362.99 28.98 o -5 10 1 10.57 12.37 5.07 o -4 10 1 0.52 -0.08 8.76 o -3 10 1 43.31 32.87 9.51 o -2 10 1 1207.27 1333.17 67.80 o -1 10 1 144.34 166.81 23.05 o 0 10 1 21.66 19.76 9.27 o 1 10 1 600.70 586.85 39.94 o 2 10 1 126.23 131.93 14.51 o 3 10 1 455.91 499.61 35.03 o 4 10 1 1126.92 1186.82 86.75 o 5 10 1 5.75 -2.39 10.37 o 6 10 1 26.97 28.43 14.47 o 7 10 1 23.40 17.35 9.65 o -3 11 1 216.27 170.39 23.15 o -2 11 1 7.24 -0.97 10.62 o -1 11 1 512.05 531.67 52.49 o 0 11 1 361.31 371.09 25.13 o 1 11 1 86.24 88.36 22.22 o 2 11 1 0.61 -4.36 13.03 o 3 11 1 67.20 75.28 19.30 o -16 0 2 77.09 89.75 17.16 o -14 0 2 5.78 5.72 5.08 o -12 0 2 1604.67 1786.50 114.38 o -10 0 2 22.11 43.07 4.17 o -8 0 2 2791.85 3006.00 125.75 o -6 0 2 142.65 89.25 7.73 o -4 0 2 3181.96 3101.79 144.30 o -2 0 2 18.99 16.50 7.24 o 2 0 2 23455.12 23879.07 1116.02 o 4 0 2 12.45 31.26 4.94 o 6 0 2 1628.71 1759.29 74.69 o 8 0 2 483.37 462.61 23.43 o 10 0 2 3295.41 3443.75 203.36 o 12 0 2 1115.38 1128.93 102.68 o 14 0 2 36.16 16.56 11.22 o 16 0 2 247.17 264.12 35.54 o -16 1 2 15.65 4.46 4.67 o -15 1 2 6.41 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17.01 5.55 o -13 2 2 8.20 5.79 6.17 o -12 2 2 9.93 16.11 4.80 o -11 2 2 1083.06 1140.43 38.72 o -10 2 2 2954.13 2836.36 98.48 o -9 2 2 455.48 424.68 13.84 o -8 2 2 0.10 2.26 3.26 o -7 2 2 780.12 739.27 24.65 o -6 2 2 161.02 224.93 8.23 o -5 2 2 135.55 156.82 21.02 o -4 2 2 3493.23 3612.02 146.63 o -3 2 2 3304.27 3524.34 154.92 o -2 2 2 95.43 124.12 6.33 o 0 2 2 1614.62 1728.49 52.06 o 1 2 2 375.90 373.15 8.10 o 2 2 2 9827.11 10185.00 235.15 o 3 2 2 6794.63 6335.92 187.00 o 4 2 2 9.94 28.02 2.21 o 5 2 2 5105.80 4607.70 185.79 o 6 2 2 1559.87 1468.46 60.28 o 7 2 2 448.75 403.18 14.67 o 8 2 2 191.35 194.65 22.66 o 9 2 2 62.71 57.55 4.99 o 10 2 2 179.84 158.73 8.48 o 11 2 2 180.05 156.45 9.08 o 12 2 2 1120.20 1006.80 75.14 o 13 2 2 1301.78 1294.00 69.14 o 14 2 2 475.65 484.35 38.19 o 15 2 2 80.37 78.24 11.45 o 16 2 2 89.04 87.30 9.45 o -16 3 2 275.86 257.84 31.54 o -15 3 2 162.08 185.99 17.75 o -14 3 2 953.96 1045.90 53.07 o -13 3 2 870.61 908.82 34.76 o -12 3 2 62.50 57.71 7.48 o -11 3 2 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