#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2013507.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013507_Fobs loop_ _publ_author_name 'Bowes, Katharine F.' 'Ferguson, George' 'Lough, Alan J.' 'Glidewell, Christopher' _publ_section_title ; 4,4'-Trimethylenedipyridinium bis[carboxymethylphosphonate(1--)]: a three-dimensional framework structure built from O---H···O, N---H···O and C---H···O hydrogen bonds ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o464 _journal_page_last o466 _journal_volume 59 _journal_year 2003 _space_group_IT_number 43 _symmetry_space_group_name_Hall 'F 2 -2d' _symmetry_space_group_name_H-M 'F d d 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 27.3660 _cell_length_b 32.3470 _cell_length_c 4.8818 _exptl_crystal_F_000 2000.00 _reflns_d_resolution_high 0.7703 _[local]_cod_data_source_file sk1644Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' KFB46 k0398a in Fdd2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 449.64 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' 'x+1/4, -y+1/4, z+1/4' '-x+1/4, y+1/4, z+1/4' 'x, y+1/2, z+1/2' '-x, -y+1/2, z+1/2' 'x+1/4, -y+3/4, z+3/4' '-x+1/4, y+3/4, z+3/4' 'x+1/2, y, z+1/2' '-x+1/2, -y, z+1/2' 'x+3/4, -y+1/4, z+3/4' '-x+3/4, y+1/4, z+3/4' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z' 'x+3/4, -y+3/4, z+1/4' '-x+3/4, y+3/4, z+1/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 8 2 -6 40.17 157.32 501.81 o 8 4 -6 943.63 631.04 223.92 o 8 6 -6 211.14 36.27 268.51 o 10 6 -6 873.07 1842.76 548.76 o 8 8 -6 1525.72 1585.74 333.35 o 1 1 -5 5064.42 5047.81 272.96 o 3 1 -5 951.66 1018.05 136.57 o 5 1 -5 380.34 296.91 78.31 o 7 1 -5 2112.02 2298.02 131.46 o 9 1 -5 164.40 85.78 88.49 o 11 1 -5 1692.69 1663.65 109.68 o 13 1 -5 1508.45 1609.46 115.49 o 15 1 -5 63.94 36.94 67.69 o 17 1 -5 1132.73 1566.31 215.20 o 1 3 -5 605.95 503.25 119.70 o 3 3 -5 717.07 666.71 157.80 o 5 3 -5 2816.49 3115.44 163.08 o 7 3 -5 4954.65 5478.30 214.25 o 9 3 -5 770.65 826.26 96.34 o 11 3 -5 131.72 69.72 76.49 o 13 3 -5 460.11 475.21 75.56 o 15 3 -5 741.61 624.26 129.03 o 1 5 -5 1577.98 1460.86 163.18 o 3 5 -5 2266.15 2036.15 182.56 o 5 5 -5 237.91 116.79 80.09 o 7 5 -5 2173.32 2296.40 129.74 o 9 5 -5 2131.25 2394.93 131.01 o 11 5 -5 2553.10 2681.65 147.98 o 13 5 -5 170.33 139.59 100.25 o 15 5 -5 1249.84 1132.29 192.04 o 19 5 -5 2652.93 2871.39 324.17 o 21 5 -5 1275.49 1189.78 546.80 o 1 7 -5 2904.00 3158.53 286.78 o 3 7 -5 1337.40 1427.05 169.45 o 5 7 -5 252.82 129.86 96.30 o 7 7 -5 543.63 425.19 82.40 o 9 7 -5 1099.19 1085.67 93.29 o 11 7 -5 2035.09 2407.70 194.79 o 13 7 -5 1507.61 1633.97 182.78 o 15 7 -5 466.35 505.85 144.94 o 17 7 -5 107.67 -50.77 248.28 o 19 7 -5 544.80 384.21 191.42 o 21 7 -5 765.00 322.76 476.89 o 1 9 -5 655.34 637.57 150.60 o 3 9 -5 61.54 13.79 115.84 o 5 9 -5 4216.97 4834.74 216.69 o 7 9 -5 356.19 379.65 88.92 o 9 9 -5 1057.89 1098.44 79.06 o 11 9 -5 17.19 69.39 158.43 o 13 9 -5 25.92 -26.42 161.51 o 15 9 -5 869.78 749.43 184.30 o 17 9 -5 202.85 382.80 203.40 o 19 9 -5 2298.76 2711.07 364.38 o 1 11 -5 1313.77 1472.86 149.62 o 3 11 -5 1382.98 1368.30 127.40 o 5 11 -5 513.76 704.42 107.21 o 7 11 -5 74.31 61.06 63.18 o 9 11 -5 1744.45 1780.88 243.98 o 11 11 -5 945.30 724.39 180.78 o 13 11 -5 89.73 55.21 146.95 o 15 11 -5 593.51 560.59 193.79 o 17 11 -5 470.99 699.43 231.11 o 19 11 -5 1303.20 1553.37 297.84 o 1 13 -5 1570.64 1560.43 169.19 o 3 13 -5 548.19 427.41 108.66 o 5 13 -5 1408.87 1260.13 127.90 o 7 13 -5 488.56 426.23 91.98 o 9 13 -5 1919.19 1725.30 224.85 o 11 13 -5 214.93 460.76 165.65 o 13 13 -5 311.89 284.05 187.14 o 15 13 -5 146.87 114.61 205.47 o 17 13 -5 1913.57 2258.05 390.08 o 1 15 -5 2197.86 2411.79 170.94 o 3 15 -5 1328.07 1213.73 142.13 o 5 15 -5 652.99 682.88 112.53 o 7 15 -5 697.01 452.56 164.08 o 9 15 -5 283.68 246.72 238.98 o 11 15 -5 85.65 256.18 220.91 o 13 15 -5 429.01 338.53 270.04 o 15 15 -5 228.55 129.83 246.59 o 17 15 -5 1211.64 1515.61 370.89 o 1 17 -5 1033.26 638.79 165.42 o 3 17 -5 1387.34 1170.60 204.41 o 5 17 -5 210.73 -200.52 200.52 o 7 17 -5 1551.44 1122.60 421.67 o 9 17 -5 123.47 47.60 143.73 o 11 17 -5 492.90 340.36 187.58 o 13 17 -5 2046.95 2181.41 339.82 o 15 17 -5 187.61 210.82 232.99 o 1 19 -5 1197.42 1156.94 276.04 o 3 19 -5 664.34 897.57 261.68 o 5 19 -5 333.03 86.12 206.35 o 7 19 -5 789.62 585.16 182.16 o 9 19 -5 425.36 74.22 185.53 o 11 19 -5 244.35 163.98 216.27 o 13 19 -5 752.57 985.10 303.13 o 1 21 -5 927.32 841.82 355.06 o 3 21 -5 1712.62 1630.91 349.82 o 5 21 -5 291.55 -2.08 277.27 o 7 21 -5 518.37 -329.32 329.32 o 9 21 -5 42.12 170.78 223.32 o 11 21 -5 871.91 438.19 301.12 o 1 23 -5 728.46 888.33 376.11 o 3 23 -5 907.63 889.62 286.29 o 5 23 -5 187.30 291.68 305.22 o 7 23 -5 2115.35 2554.13 603.61 o 9 23 -5 592.82 739.18 257.30 o 1 25 -5 633.70 334.62 233.24 o 3 25 -5 519.17 631.65 244.33 o 5 25 -5 1184.19 1281.97 495.40 o 4 0 -4 24364.22 26267.20 1092.28 o 8 0 -4 21275.62 23241.45 653.11 o 12 0 -4 1407.07 877.55 229.82 o 16 0 -4 6388.61 7333.16 470.10 o 20 0 -4 1941.90 1918.12 274.73 o 24 0 -4 673.47 871.42 161.75 o 2 2 -4 520.26 633.45 76.20 o 4 2 -4 265.10 229.99 78.99 o 6 2 -4 4439.82 4924.73 152.16 o 8 2 -4 1327.25 1513.55 82.55 o 10 2 -4 5122.60 5770.77 176.96 o 12 2 -4 329.26 341.67 121.28 o 14 2 -4 4314.89 4613.90 164.48 o 16 2 -4 1773.06 1915.30 120.95 o 18 2 -4 584.70 671.15 87.87 o 20 2 -4 742.18 582.95 121.17 o 22 2 -4 132.85 88.17 74.58 o 24 2 -4 36.09 -147.25 147.25 o 26 2 -4 471.31 -207.37 207.44 o 0 4 -4 5322.79 5992.32 366.99 o 2 4 -4 14400.27 15406.74 390.82 o 4 4 -4 18652.21 19803.22 510.82 o 6 4 -4 2733.45 2451.46 169.76 o 8 4 -4 2111.02 2093.24 100.47 o 10 4 -4 3109.66 3155.86 142.70 o 12 4 -4 626.51 605.45 60.76 o 14 4 -4 117.45 162.56 59.63 o 16 4 -4 784.13 926.28 93.35 o 18 4 -4 2751.60 2632.12 116.37 o 20 4 -4 780.26 905.45 94.52 o 22 4 -4 3420.11 3502.75 690.92 o 24 4 -4 2968.72 2847.79 334.85 o 26 4 -4 991.31 689.04 364.94 o 2 6 -4 340.70 308.13 80.10 o 4 6 -4 1305.84 1541.74 128.35 o 6 6 -4 1401.47 1471.77 102.29 o 8 6 -4 346.96 424.52 90.60 o 10 6 -4 1480.05 1546.20 86.85 o 12 6 -4 740.52 823.66 59.51 o 14 6 -4 828.09 593.55 117.04 o 16 6 -4 1968.80 1680.24 153.93 o 18 6 -4 1716.05 1626.84 163.98 o 20 6 -4 3995.21 3881.46 237.14 o 22 6 -4 15.10 226.56 330.59 o 24 6 -4 295.64 304.30 197.40 o 26 6 -4 54.18 112.40 336.52 o 0 8 -4 4661.16 4695.78 326.75 o 2 8 -4 10857.96 11598.07 331.27 o 4 8 -4 1264.70 1128.33 94.12 o 6 8 -4 14434.51 15542.06 411.09 o 8 8 -4 950.17 887.98 102.19 o 10 8 -4 2724.63 2683.24 121.08 o 12 8 -4 330.16 485.91 112.36 o 14 8 -4 605.36 584.46 121.44 o 16 8 -4 88.88 135.04 140.74 o 18 8 -4 1859.09 1812.52 167.75 o 20 8 -4 427.68 455.06 168.28 o 22 8 -4 2461.28 2633.39 330.87 o 24 8 -4 1000.27 552.27 205.21 o 26 8 -4 650.98 247.45 748.91 o 2 10 -4 4509.00 4917.02 231.22 o 4 10 -4 1244.17 1317.87 104.32 o 6 10 -4 434.27 275.58 98.13 o 8 10 -4 262.27 265.86 39.42 o 10 10 -4 701.87 761.29 144.77 o 12 10 -4 6847.11 7156.54 298.46 o 14 10 -4 639.36 622.74 122.09 o 16 10 -4 594.47 410.87 120.68 o 18 10 -4 1171.80 1030.16 151.64 o 20 10 -4 2613.71 2224.07 209.57 o 22 10 -4 12.06 95.56 277.90 o 24 10 -4 118.81 234.11 202.57 o 26 10 -4 260.72 -230.51 461.01 o 0 12 -4 9595.04 9665.00 777.43 o 2 12 -4 7957.32 8402.83 309.72 o 4 12 -4 4567.47 4413.33 246.36 o 6 12 -4 2977.73 3088.80 206.69 o 8 12 -4 13053.63 13654.81 457.21 o 10 12 -4 2294.47 2477.38 174.76 o 12 12 -4 145.31 117.25 108.76 o 14 12 -4 537.52 618.56 125.99 o 16 12 -4 51.53 -99.52 104.50 o 18 12 -4 935.15 680.11 160.96 o 20 12 -4 99.14 111.25 133.31 o 22 12 -4 1438.13 1421.14 276.70 o 24 12 -4 320.94 -216.02 216.02 o 2 14 -4 551.33 396.26 93.34 o 4 14 -4 1706.20 1662.87 107.51 o 6 14 -4 6909.09 7396.61 250.94 o 8 14 -4 1519.86 1714.65 192.68 o 10 14 -4 294.13 180.37 108.93 o 12 14 -4 2397.89 2535.64 192.32 o 14 14 -4 1430.99 1266.29 184.87 o 16 14 -4 2595.27 2725.84 211.29 o 18 14 -4 545.14 496.32 164.30 o 20 14 -4 681.81 843.91 181.58 o 22 14 -4 144.37 -61.46 218.49 o 24 14 -4 55.79 231.75 218.28 o 0 16 -4 14243.04 15707.85 1304.35 o 2 16 -4 249.90 230.76 93.16 o 4 16 -4 7878.94 9472.46 338.09 o 6 16 -4 54.00 170.99 93.23 o 8 16 -4 3123.33 3209.12 195.51 o 10 16 -4 379.88 381.01 119.32 o 12 16 -4 214.77 240.46 141.54 o 14 16 -4 969.09 1242.17 168.04 o 16 16 -4 913.76 703.41 181.17 o 18 16 -4 497.90 197.30 150.50 o 20 16 -4 1265.34 1210.83 215.30 o 22 16 -4 864.39 693.93 390.62 o 24 16 -4 2067.85 2227.58 415.14 o 2 18 -4 50.19 -66.08 106.12 o 4 18 -4 1498.92 1204.49 105.14 o 6 18 -4 6130.63 6490.14 305.06 o 8 18 -4 1727.65 1612.21 187.23 o 10 18 -4 1085.82 996.35 153.21 o 12 18 -4 194.05 256.98 129.90 o 14 18 -4 2976.31 3223.65 358.51 o 16 18 -4 994.33 841.80 202.80 o 18 18 -4 911.47 825.91 205.16 o 20 18 -4 596.89 592.93 213.59 o 22 18 -4 1108.72 1117.53 252.79 o 0 20 -4 5892.14 5832.48 686.33 o 2 20 -4 2174.07 1859.03 169.13 o 4 20 -4 7825.25 8583.05 357.84 o 6 20 -4 1764.46 1528.44 171.96 o 8 20 -4 337.54 416.21 140.32 o 10 20 -4 1172.90 1050.23 142.56 o 12 20 -4 32.97 46.46 204.32 o 14 20 -4 1220.56 1313.19 232.60 o 16 20 -4 1341.89 1695.09 224.73 o 18 20 -4 274.68 261.36 199.61 o 20 20 -4 3305.18 2946.61 435.07 o 2 22 -4 1054.84 951.22 117.73 o 4 22 -4 55.29 32.88 75.46 o 6 22 -4 488.47 736.29 248.67 o 8 22 -4 329.51 174.95 105.74 o 10 22 -4 2683.58 2309.70 195.46 o 12 22 -4 471.05 356.45 157.20 o 14 22 -4 4865.86 5244.27 401.74 o 16 22 -4 171.23 9.81 147.33 o 18 22 -4 696.02 775.97 536.17 o 20 22 -4 298.62 503.11 263.15 o 0 24 -4 582.09 665.26 360.95 o 2 24 -4 4034.20 4252.60 257.94 o 4 24 -4 167.45 118.69 92.12 o 6 24 -4 1058.75 1027.32 164.21 o 8 24 -4 2148.14 2154.07 363.68 o 10 24 -4 1733.05 1791.34 247.39 o 12 24 -4 419.28 260.93 214.51 o 14 24 -4 19.09 -158.12 197.75 o 16 24 -4 632.14 815.72 229.17 o 18 24 -4 276.43 52.80 227.87 o 2 26 -4 279.91 491.86 134.23 o 4 26 -4 1174.06 896.40 301.43 o 6 26 -4 1584.79 692.85 358.43 o 8 26 -4 120.20 235.89 317.93 o 10 26 -4 345.36 89.51 190.02 o 12 26 -4 872.77 1058.22 256.24 o 14 26 -4 285.49 50.08 169.63 o 16 26 -4 441.96 437.82 282.00 o 0 28 -4 2826.24 3025.41 622.22 o 2 28 -4 1977.24 2504.81 398.67 o 4 28 -4 1609.85 1670.63 313.67 o 6 28 -4 1101.73 605.93 236.77 o 8 28 -4 182.36 99.47 291.77 o 10 28 -4 71.98 -180.81 204.50 o 12 28 -4 388.61 488.38 259.11 o 14 28 -4 162.16 630.28 287.25 o 2 30 -4 158.86 -79.36 213.48 o 4 30 -4 295.11 321.74 253.75 o 6 30 -4 74.69 15.30 318.37 o 8 30 -4 925.00 1040.50 736.45 o 10 30 -4 587.82 612.83 223.61 o 2 32 -4 131.78 439.92 480.75 o 1 1 -3 13127.47 12596.13 358.13 o 3 1 -3 8460.62 8415.98 248.04 o 5 1 -3 2558.39 2321.02 129.02 o 7 1 -3 7088.28 6933.43 194.43 o 9 1 -3 2258.90 2645.76 110.61 o 11 1 -3 7823.19 8290.15 304.29 o 13 1 -3 1587.25 1646.58 87.39 o 15 1 -3 7239.38 7604.75 262.54 o 17 1 -3 958.51 897.45 90.44 o 19 1 -3 393.84 532.24 88.71 o 21 1 -3 2434.03 2699.24 178.10 o 23 1 -3 354.27 222.18 191.46 o 25 1 -3 1215.04 1244.01 144.22 o 27 1 -3 2092.28 2279.39 251.99 o 29 1 -3 2978.57 2611.55 377.03 o 1 3 -3 2681.44 2773.06 114.76 o 3 3 -3 12235.06 12467.68 337.16 o 5 3 -3 2701.92 2631.34 118.83 o 7 3 -3 22878.79 23993.84 623.78 o 9 3 -3 3132.07 3479.52 115.87 o 11 3 -3 900.05 790.85 67.99 o 13 3 -3 8193.59 7812.28 284.67 o 15 3 -3 99.00 317.14 61.81 o 17 3 -3 8588.73 9039.54 431.83 o 19 3 -3 1059.73 1112.26 100.99 o 21 3 -3 1555.34 1674.92 145.31 o 23 3 -3 232.77 135.08 91.62 o 25 3 -3 213.03 259.90 100.66 o 27 3 -3 1216.44 1185.97 380.13 o 29 3 -3 149.60 -113.27 197.57 o 1 5 -3 8313.84 7918.82 269.72 o 3 5 -3 137.58 127.37 62.47 o 5 5 -3 3280.74 3153.04 126.27 o 7 5 -3 5257.37 5181.84 195.69 o 9 5 -3 9898.88 10360.63 338.94 o 11 5 -3 3164.75 3160.35 188.08 o 13 5 -3 4568.23 4600.55 175.56 o 15 5 -3 5226.75 5101.28 185.27 o 17 5 -3 1343.46 1198.49 206.15 o 19 5 -3 2998.06 3019.88 293.48 o 21 5 -3 339.01 391.19 77.99 o 23 5 -3 609.98 637.43 138.62 o 25 5 -3 412.98 213.20 100.47 o 27 5 -3 6.49 79.09 331.25 o 29 5 -3 727.41 454.49 270.06 o 1 7 -3 3461.65 3457.33 145.66 o 3 7 -3 2359.76 2314.99 183.87 o 5 7 -3 5937.77 6231.98 180.45 o 7 7 -3 3303.94 3642.54 111.94 o 9 7 -3 2820.18 3029.93 128.17 o 11 7 -3 2734.61 2541.25 144.55 o 13 7 -3 4480.51 4011.38 264.02 o 15 7 -3 5486.92 5732.69 244.16 o 17 7 -3 7429.92 7634.63 351.13 o 19 7 -3 1115.41 1427.47 190.12 o 21 7 -3 3830.16 3375.53 280.98 o 23 7 -3 2540.38 2654.97 172.96 o 25 7 -3 1034.93 979.39 195.87 o 27 7 -3 760.87 1154.04 313.54 o 1 9 -3 12161.02 12405.55 363.60 o 3 9 -3 6135.70 5921.32 193.23 o 5 9 -3 425.27 357.52 90.14 o 7 9 -3 2121.54 2177.50 106.62 o 9 9 -3 5392.56 5515.25 197.63 o 11 9 -3 1492.45 1553.36 114.84 o 13 9 -3 2835.16 2471.00 146.42 o 15 9 -3 6015.77 5924.36 360.32 o 17 9 -3 14717.71 14992.90 627.80 o 19 9 -3 4324.84 4295.89 397.72 o 21 9 -3 1964.60 2019.58 349.27 o 23 9 -3 2418.78 2791.38 298.57 o 25 9 -3 214.30 -48.05 194.59 o 27 9 -3 620.02 358.32 271.37 o 29 9 -3 684.61 976.16 316.17 o 1 11 -3 4284.38 4130.48 192.54 o 3 11 -3 589.74 548.36 92.65 o 5 11 -3 2350.23 2424.02 100.27 o 7 11 -3 14950.13 14861.84 414.42 o 9 11 -3 5269.86 5318.14 204.19 o 11 11 -3 252.76 170.18 78.46 o 13 11 -3 2489.09 2126.07 148.58 o 15 11 -3 7349.42 7452.43 322.03 o 17 11 -3 2380.35 2088.69 175.53 o 19 11 -3 2826.54 3165.50 209.71 o 21 11 -3 134.53 283.61 152.92 o 23 11 -3 3977.46 3631.52 380.97 o 25 11 -3 883.26 844.49 329.36 o 27 11 -3 81.77 -172.54 187.03 o 29 11 -3 2931.71 2859.28 578.71 o 1 13 -3 5654.92 5735.90 253.07 o 3 13 -3 1832.37 1770.42 100.54 o 5 13 -3 6437.66 6661.75 194.51 o 7 13 -3 1465.26 1327.43 110.89 o 9 13 -3 5419.24 5237.25 229.65 o 11 13 -3 6515.50 6133.24 251.73 o 13 13 -3 3882.37 3804.11 185.08 o 15 13 -3 2099.93 1646.26 136.89 o 17 13 -3 1754.75 1521.96 140.43 o 19 13 -3 3371.48 2970.23 225.28 o 21 13 -3 2371.28 2072.03 194.76 o 23 13 -3 458.96 201.73 142.98 o 25 13 -3 729.57 1433.32 387.31 o 27 13 -3 558.05 403.10 331.96 o 1 15 -3 2206.14 2308.81 142.90 o 3 15 -3 9231.84 9310.38 298.82 o 5 15 -3 11529.51 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11 39 1 3.52 -61.68 404.34 o 1 41 1 555.39 54.40 231.38 o 3 41 1 1100.89 1310.79 295.78 o 5 41 1 277.78 489.04 278.50 o 2 0 2 2342.83 2233.87 186.73 o 10 0 2 52918.16 51651.87 2437.19 o 14 0 2 16898.84 16527.70 614.32 o 18 0 2 8218.19 8447.46 958.49 o 22 0 2 5557.07 5910.09 346.98 o 26 0 2 642.65 508.30 180.31 o 30 0 2 847.59 883.00 231.01 o 0 2 2 11943.65 11704.13 563.34 o 2 2 2 114.88 89.52 53.42 o 4 2 2 14286.17 13348.78 394.84 o 6 2 2 611.51 701.29 111.06 o 8 2 2 9200.25 7961.00 585.82 o 10 2 2 13909.96 14869.68 634.85 o 12 2 2 7364.20 8451.69 257.36 o 14 2 2 1812.96 2215.38 124.83 o 16 2 2 1419.12 1630.78 103.50 o 18 2 2 1488.55 1795.14 130.33 o 20 2 2 6236.30 6734.36 230.15 o 22 2 2 1069.93 1119.54 112.66 o 24 2 2 5087.29 5204.77 277.00 o 26 2 2 1611.44 1556.58 161.11 o 28 2 2 2438.79 2564.14 219.42 o 30 2 2 579.03 577.89 146.85 o 32 2 2 1919.42 2001.85 264.21 o 2 4 2 18302.05 16660.07 462.62 o 4 4 2 24522.18 24013.78 781.15 o 6 4 2 12579.14 12768.01 701.73 o 8 4 2 12839.22 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12096.89 12087.61 732.50 o 10 8 2 2650.07 3177.39 182.14 o 12 8 2 14315.49 14599.06 577.73 o 14 8 2 2633.00 2378.99 197.17 o 16 8 2 25252.27 26500.51 708.91 o 18 8 2 2599.82 3095.05 168.82 o 20 8 2 5848.26 6639.73 425.49 o 22 8 2 338.03 330.92 86.03 o 24 8 2 1944.36 1804.00 220.68 o 26 8 2 161.68 -38.54 105.51 o 28 8 2 390.01 314.18 135.51 o 30 8 2 513.91 500.10 156.88 o 32 8 2 1786.25 2091.49 358.39 o 0 10 2 5955.64 5968.42 235.74 o 2 10 2 14224.91 14225.25 417.05 o 4 10 2 20460.25 21096.05 498.34 o 6 10 2 10048.96 10526.86 500.46 o 8 10 2 2258.86 2075.86 234.75 o 10 10 2 1223.81 1423.24 203.63 o 12 10 2 966.27 1102.95 193.71 o 14 10 2 525.64 542.03 121.79 o 16 10 2 224.37 336.49 126.18 o 18 10 2 4629.59 5540.51 208.46 o 20 10 2 276.49 555.90 82.83 o 22 10 2 4372.03 4669.18 232.76 o 24 10 2 1254.41 1207.77 144.86 o 26 10 2 4178.23 4678.74 302.54 o 28 10 2 181.01 247.61 180.68 o 30 10 2 3478.30 2790.19 395.34 o 32 10 2 126.52 280.55 476.80 o 2 12 2 6727.11 6839.53 196.82 o 4 12 2 1830.12 1860.44 84.42 o 6 12 2 29777.03 29694.69 993.65 o 8 12 2 12918.25 12959.83 858.33 o 10 12 2 4522.77 4414.82 341.95 o 12 12 2 19995.42 21804.03 858.08 o 14 12 2 6834.53 6892.86 370.57 o 16 12 2 5100.38 5748.42 354.64 o 18 12 2 1840.26 1511.53 206.62 o 20 12 2 5712.02 6385.05 236.35 o 22 12 2 1338.32 1520.87 162.39 o 24 12 2 493.63 503.82 104.88 o 26 12 2 88.56 122.32 118.44 o 28 12 2 51.35 78.60 121.80 o 30 12 2 1211.97 1463.83 446.66 o 32 12 2 1178.97 391.31 405.80 o 0 14 2 10815.14 10360.79 470.74 o 2 14 2 5031.01 4674.87 161.70 o 4 14 2 20910.15 20698.38 602.61 o 6 14 2 15015.28 14096.31 387.39 o 8 14 2 1077.21 1117.52 177.91 o 10 14 2 4205.88 4430.46 267.60 o 12 14 2 8401.11 9057.48 553.42 o 14 14 2 1192.49 1338.23 188.55 o 16 14 2 2783.87 3089.44 255.67 o 18 14 2 3522.74 3499.59 282.07 o 20 14 2 2503.42 2697.83 269.65 o 22 14 2 25.34 42.46 62.85 o 24 14 2 2729.98 3060.03 177.66 o 26 14 2 2671.43 2819.83 199.86 o 28 14 2 1081.34 1132.06 303.71 o 30 14 2 1175.49 1752.35 570.50 o 2 16 2 12812.37 13335.22 570.53 o 4 16 2 4473.81 5015.90 249.92 o 6 16 2 7854.72 7996.00 220.85 o 8 16 2 22.95 -79.01 79.01 o 10 16 2 30414.67 30934.69 1006.18 o 12 16 2 8705.32 9416.35 455.61 o 14 16 2 15690.77 17641.42 1103.30 o 16 16 2 2927.60 3218.48 272.23 o 18 16 2 8973.88 10386.16 550.62 o 20 16 2 109.37 -10.24 153.54 o 22 16 2 1228.09 1078.21 279.34 o 24 16 2 720.62 797.56 87.05 o 26 16 2 269.18 169.76 134.08 o 28 16 2 128.37 276.60 372.75 o 30 16 2 964.04 569.14 486.14 o 0 18 2 11992.65 12147.19 407.87 o 2 18 2 8240.38 8292.07 412.16 o 4 18 2 6765.25 6818.92 259.61 o 6 18 2 2820.20 3037.56 135.36 o 8 18 2 2009.20 2167.37 180.22 o 10 18 2 5841.75 6363.94 463.53 o 12 18 2 260.70 153.08 256.20 o 14 18 2 1213.70 1038.38 170.95 o 16 18 2 7451.00 7483.94 469.46 o 18 18 2 2501.63 2729.19 288.95 o 20 18 2 3883.87 4120.92 396.48 o 22 18 2 2342.11 2064.54 458.72 o 24 18 2 540.57 333.51 203.19 o 26 18 2 730.46 27.67 275.33 o 28 18 2 1975.80 2181.10 539.01 o 30 18 2 720.38 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