#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:48:25 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180804 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/35/2013518.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013518_Fobs loop_ _publ_author_name 'Vasiliev, Alexander D.' 'Astachov, Alexander M.' 'Molokeev, Maxim S.' 'Kruglyakova, Ludmila A.' 'Stepanov, Rudolf S.' _publ_section_title ; 2-Nitrimino-1-nitroimidazolidine ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o499 _journal_page_last o501 _journal_volume 59 _journal_year 2003 _space_group_IT_number 106 _symmetry_space_group_name_Hall 'P 4c -2ab' _symmetry_space_group_name_H-M 'P 42 b c' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 12.8970 _cell_length_b 12.8970 _cell_length_c 8.0078 _exptl_crystal_F_000 720.00 _reflns_d_resolution_high 0.7826 _cod_data_source_file sk1660Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 01-17 P4(2)bc' _shelx_refln_list_code 4 _shelx_f_calc_maximum 139.57 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x, z+1/2' 'x+1/2, -y+1/2, z' 'y+1/2, x+1/2, z+1/2' '-x, -y, z' 'y, -x, z+1/2' '-x+1/2, y+1/2, z' '-y+1/2, -x+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 0 154.66 186.65 3.06 o 0 2 0 84.74 74.41 2.62 o 1 2 0 3415.50 3534.91 49.51 o 2 2 0 14222.83 13033.57 127.00 o 1 3 0 6.95 6.04 2.03 o 2 3 0 3243.76 3327.96 20.67 o 3 3 0 4457.55 4190.14 25.81 o 0 4 0 75.95 55.26 2.12 o 1 4 0 4003.20 3460.65 22.90 o 2 4 0 698.86 715.17 10.28 o 3 4 0 814.49 790.00 11.58 o 4 4 0 298.82 272.66 7.36 o 1 5 0 688.82 658.00 10.66 o 2 5 0 297.39 271.60 7.16 o 3 5 0 49.90 52.73 2.06 o 4 5 0 1312.76 1343.90 17.86 o 5 5 0 1994.29 1901.29 23.05 o 0 6 0 317.63 307.23 15.11 o 1 6 0 0.65 1.40 1.44 o 2 6 0 142.30 130.61 4.07 o 3 6 0 1996.41 2062.63 75.71 o 4 6 0 203.28 193.43 5.17 o 5 6 0 394.30 386.01 11.35 o 6 6 0 244.12 260.65 9.92 o 1 7 0 2009.49 1942.60 42.83 o 2 7 0 273.54 246.75 6.12 o 3 7 0 392.13 461.58 8.45 o 4 7 0 139.28 125.75 5.38 o 5 7 0 101.01 101.78 3.83 o 6 7 0 12.60 16.06 0.86 o 7 7 0 244.65 270.01 10.22 o 0 8 0 1175.32 1178.44 57.21 o 1 8 0 823.31 739.74 31.80 o 2 8 0 63.57 68.53 2.03 o 3 8 0 185.28 169.81 6.14 o 4 8 0 0.11 1.84 2.00 o 5 8 0 2.12 5.25 2.59 o 6 8 0 123.35 130.23 3.62 o 7 8 0 288.19 284.41 7.82 o 8 8 0 833.77 897.36 21.97 o 1 9 0 59.02 69.33 1.84 o 2 9 0 47.50 58.98 4.48 o 3 9 0 9.42 3.23 2.96 o 4 9 0 312.44 340.55 14.03 o 5 9 0 7.81 7.02 2.74 o 6 9 0 228.85 254.82 7.42 o 7 9 0 13.01 11.86 1.34 o 8 9 0 264.53 256.01 7.10 o 9 9 0 113.51 115.34 4.54 o 0 10 0 2.46 2.35 2.29 o 1 10 0 405.48 410.06 9.96 o 2 10 0 0.79 0.00 2.16 o 3 10 0 160.39 158.23 4.30 o 4 10 0 413.66 404.57 10.31 o 5 10 0 14.07 9.43 1.28 o 6 10 0 434.41 430.75 10.97 o 7 10 0 46.01 55.10 1.63 o 8 10 0 93.79 98.73 2.92 o 9 10 0 25.14 26.57 2.89 o 10 10 0 20.99 18.77 1.34 o 1 11 0 33.19 31.97 1.20 o 2 11 0 257.12 256.10 7.56 o 3 11 0 9.10 15.92 3.91 o 4 11 0 0.18 0.00 2.60 o 5 11 0 111.18 100.29 2.81 o 6 11 0 58.39 62.20 1.78 o 7 11 0 0.01 0.00 2.54 o 8 11 0 2.49 8.45 3.93 o 9 11 0 7.56 5.76 0.94 o 10 11 0 36.39 35.34 0.99 o 11 11 0 0.36 0.00 2.75 o 0 12 0 161.33 172.92 5.17 o 1 12 0 31.88 29.57 1.21 o 2 12 0 38.96 36.26 1.26 o 3 12 0 0.33 0.00 2.63 o 4 12 0 11.22 9.92 3.33 o 5 12 0 2.16 5.63 3.17 o 6 12 0 43.97 47.69 1.74 o 7 12 0 201.18 210.84 6.08 o 8 12 0 75.83 72.74 4.37 o 9 12 0 10.34 9.82 0.72 o 10 12 0 0.69 0.92 1.69 o 11 12 0 1.51 1.49 2.85 o 1 13 0 64.74 79.28 6.01 o 2 13 0 133.53 137.34 3.93 o 3 13 0 314.53 330.46 9.06 o 4 13 0 4.85 3.87 2.52 o 5 13 0 278.33 261.97 11.39 o 6 13 0 163.89 174.44 8.11 o 7 13 0 15.89 18.97 1.66 o 8 13 0 16.80 17.08 0.94 o 9 13 0 30.01 30.02 1.93 o 10 13 0 0.09 0.10 5.96 o 0 14 0 4.38 4.56 2.47 o 1 14 0 16.12 20.26 2.02 o 2 14 0 152.68 181.66 5.05 o 3 14 0 149.82 144.26 3.98 o 4 14 0 15.89 16.55 1.50 o 5 14 0 53.24 60.44 3.41 o 6 14 0 0.86 3.00 3.13 o 7 14 0 1.98 1.75 1.66 o 8 14 0 47.24 47.50 2.16 o 1 15 0 2.13 1.10 2.88 o 2 15 0 66.81 72.48 3.14 o 3 15 0 6.02 3.97 2.34 o 4 15 0 74.11 75.11 3.66 o 5 15 0 1.03 1.05 2.36 o 6 15 0 0.10 0.10 5.11 o 0 16 0 1.47 1.52 3.13 o 1 16 0 0.01 0.03 7.86 o 2 16 0 3.38 3.37 3.55 o 3 16 0 0.34 0.33 5.52 o 0 2 1 5046.06 4916.48 62.76 o 1 2 1 3722.80 3807.59 19.50 o 1 3 1 1231.32 1236.89 11.84 o 2 3 1 2458.46 2447.44 18.10 o 0 4 1 1818.51 1786.20 15.69 o 1 4 1 24.67 17.03 0.77 o 2 4 1 471.54 450.21 8.44 o 3 4 1 1247.53 1174.56 14.52 o 1 5 1 1360.87 1326.32 15.55 o 2 5 1 376.54 414.24 8.93 o 3 5 1 641.36 646.62 11.86 o 4 5 1 318.22 337.18 9.15 o 0 6 1 2824.24 2798.08 25.03 o 1 6 1 429.45 365.52 9.09 o 2 6 1 250.97 274.48 8.20 o 3 6 1 401.63 452.00 10.92 o 4 6 1 2597.23 2772.44 28.79 o 5 6 1 198.19 218.81 8.53 o 1 7 1 100.10 107.75 4.00 o 2 7 1 1138.89 1142.24 18.25 o 3 7 1 222.42 241.63 8.83 o 4 7 1 94.94 92.81 3.74 o 5 7 1 56.21 56.93 2.06 o 6 7 1 440.44 499.33 14.45 o 0 8 1 31.96 33.64 1.49 o 1 8 1 529.36 467.36 12.62 o 2 8 1 1047.33 1118.43 19.77 o 3 8 1 33.57 37.06 1.54 o 4 8 1 137.56 141.96 5.78 o 5 8 1 192.35 200.72 8.19 o 6 8 1 489.88 494.80 15.24 o 7 8 1 122.47 132.18 5.13 o 1 9 1 474.26 448.86 13.45 o 2 9 1 44.21 45.85 1.80 o 3 9 1 96.93 102.63 4.10 o 4 9 1 33.06 31.30 1.59 o 5 9 1 287.21 301.45 11.16 o 6 9 1 253.82 260.33 10.51 o 7 9 1 83.72 88.95 3.79 o 8 9 1 217.51 219.53 9.00 o 0 10 1 128.47 125.20 5.16 o 1 10 1 93.61 101.74 4.07 o 2 10 1 41.26 41.13 1.72 o 3 10 1 74.93 66.35 2.52 o 4 10 1 140.70 134.44 4.98 o 5 10 1 110.31 122.88 5.18 o 6 10 1 53.50 62.14 2.68 o 8 10 1 16.04 11.03 4.24 o 9 10 1 63.02 69.96 2.83 o 1 11 1 56.34 67.96 2.73 o 2 11 1 243.33 258.87 10.17 o 3 11 1 449.25 418.04 15.14 o 4 11 1 589.64 613.18 18.20 o 5 11 1 132.71 124.01 4.82 o 8 11 1 48.71 50.48 2.98 o 9 11 1 139.80 135.58 5.55 o 10 11 1 9.47 9.56 3.21 o 1 12 1 120.99 116.34 4.77 o 2 12 1 55.59 64.36 2.55 o 3 12 1 163.64 182.17 7.30 o 4 12 1 75.17 74.41 3.78 o 5 12 1 128.52 121.77 4.98 o 8 12 1 29.48 39.68 2.37 o 9 12 1 6.11 8.43 1.54 o 10 12 1 12.18 11.70 0.87 o 11 12 1 14.73 14.81 3.11 o 1 13 1 97.09 91.34 3.92 o 2 13 1 62.92 57.89 3.37 o 3 13 1 47.89 51.36 3.32 o 4 13 1 99.16 99.85 4.43 o 5 13 1 7.67 8.87 2.03 o 8 13 1 11.35 14.91 1.54 o 9 13 1 6.58 6.66 2.67 o 10 13 1 32.16 32.20 2.40 o 1 14 1 12.89 17.79 2.13 o 2 14 1 11.00 12.18 1.98 o 3 14 1 28.99 30.32 2.34 o 4 14 1 32.47 37.86 2.39 o 5 14 1 11.09 14.73 1.80 o 7 14 1 14.10 14.11 3.39 o 8 14 1 7.72 7.71 3.06 o 1 15 1 18.34 14.04 1.72 o 2 15 1 29.44 26.06 1.93 o 3 15 1 15.83 12.11 1.67 o 4 15 1 6.51 5.27 1.29 o 5 15 1 3.62 3.60 2.44 o 6 15 1 2.85 2.83 1.88 o 0 16 1 4.68 4.75 4.57 o 1 16 1 1.31 1.31 4.55 o 2 16 1 1.67 1.62 2.70 o 3 16 1 3.92 3.86 2.29 o 0 0 2 10409.13 10087.83 110.11 o 1 1 2 11598.58 11952.66 126.44 o 0 2 2 2490.50 2596.02 18.12 o 1 2 2 8669.77 8541.61 107.77 o 2 2 2 19481.16 20514.54 196.32 o 1 3 2 4528.61 4683.26 27.79 o 2 3 2 1742.82 1772.68 16.90 o 3 3 2 6544.75 7053.05 38.68 o 0 4 2 3458.84 3436.19 25.18 o 1 4 2 445.62 418.29 8.55 o 2 4 2 962.44 962.22 13.41 o 3 4 2 1470.04 1512.57 17.77 o 4 4 2 2268.63 2491.13 24.50 o 1 5 2 575.45 610.32 11.23 o 2 5 2 694.60 702.30 12.48 o 3 5 2 149.95 151.55 5.35 o 4 5 2 168.47 170.78 6.54 o 5 5 2 1117.77 1158.33 18.89 o 0 6 2 1024.51 1065.32 16.31 o 1 6 2 944.66 957.10 15.54 o 2 6 2 545.15 550.21 12.07 o 3 6 2 294.14 270.57 8.93 o 4 6 2 149.57 154.13 6.77 o 5 6 2 194.92 204.57 8.27 o 6 6 2 260.00 280.52 10.51 o 1 7 2 52.35 43.47 1.78 o 2 7 2 457.42 452.75 11.97 o 3 7 2 83.69 92.10 3.43 o 4 7 2 31.01 31.38 3.03 o 5 7 2 106.99 103.00 4.05 o 6 7 2 95.96 93.99 3.94 o 7 7 2 732.05 754.98 19.14 o 0 8 2 581.68 611.33 14.88 o 1 8 2 72.36 63.01 2.86 o 2 8 2 99.32 107.91 4.18 o 3 8 2 226.10 233.77 8.72 o 4 8 2 40.76 41.47 1.93 o 5 8 2 542.73 543.74 15.79 o 6 8 2 114.89 108.60 4.18 o 7 8 2 183.85 185.22 7.18 o 8 8 2 213.71 208.72 8.40 o 1 9 2 216.18 200.65 7.81 o 2 9 2 87.35 85.26 3.19 o 3 9 2 33.48 28.37 1.49 o 4 9 2 164.57 166.78 6.20 o 5 9 2 16.69 14.19 1.36 o 6 9 2 185.95 172.90 7.00 o 7 9 2 52.80 51.08 2.14 o 8 9 2 5.22 4.60 3.96 o 9 9 2 32.41 33.41 1.67 o 0 10 2 617.99 565.42 16.44 o 1 10 2 54.88 54.14 2.24 o 2 10 2 112.78 116.32 4.79 o 3 10 2 266.87 264.64 9.94 o 4 10 2 4.07 9.66 3.80 o 5 10 2 60.18 54.97 2.21 o 6 10 2 460.89 445.86 15.69 o 7 10 2 235.00 226.34 8.66 o 8 10 2 86.54 81.14 2.91 o 9 10 2 31.94 34.03 1.54 o 10 10 2 34.18 32.38 1.39 o 1 11 2 181.84 206.63 7.90 o 2 11 2 134.94 143.98 5.57 o 3 11 2 71.56 73.71 2.91 o 4 11 2 407.62 387.64 14.32 o 5 11 2 3.10 6.30 3.57 o 6 11 2 74.09 70.37 2.78 o 7 11 2 104.24 88.01 4.17 o 8 11 2 61.71 62.11 2.47 o 9 11 2 5.11 3.57 3.03 o 10 11 2 2.80 3.39 0.82 o 11 11 2 8.82 8.92 4.70 o 0 12 2 332.04 317.82 12.91 o 1 12 2 20.24 23.73 1.59 o 2 12 2 53.89 50.77 1.90 o 4 12 2 135.44 121.89 4.87 o 5 12 2 71.04 67.20 3.40 o 6 12 2 65.97 62.82 3.22 o 7 12 2 21.11 19.64 1.26 o 8 12 2 28.11 27.06 1.23 o 9 12 2 10.11 8.69 0.90 o 10 12 2 1.21 1.21 6.58 o 1 13 2 79.57 66.37 2.81 o 2 13 2 113.39 113.99 4.20 o 3 13 2 56.48 58.94 3.24 o 4 13 2 64.89 58.72 3.17 o 5 13 2 11.25 13.49 1.98 o 6 13 2 4.29 7.07 1.64 o 7 13 2 21.16 19.70 1.75 o 8 13 2 1.06 3.62 1.95 o 9 13 2 0.47 0.46 7.17 o 0 14 2 97.31 115.61 4.02 o 1 14 2 13.24 15.06 1.18 o 3 14 2 1.20 0.00 2.72 o 5 14 2 46.97 49.37 2.29 o 6 14 2 13.82 15.68 1.54 o 7 14 2 46.78 46.66 3.79 o 8 14 2 2.91 2.93 3.11 o 1 15 2 19.14 21.03 1.03 o 3 15 2 39.32 30.96 1.85 o 4 15 2 1.70 1.75 5.16 o 5 15 2 11.24 11.16 4.16 o 6 15 2 0.65 0.64 3.31 o 0 16 2 22.30 22.54 2.42 o 1 16 2 15.68 15.74 4.27 o 2 16 2 13.92 14.04 2.01 o 0 2 3 1085.02 1060.86 13.45 o 1 2 3 1217.29 1238.58 14.84 o 1 3 3 1200.88 1264.93 15.73 o 2 3 3 139.03 119.10 4.83 o 0 4 3 476.00 507.53 10.52 o 1 4 3 360.35 389.08 9.38 o 2 4 3 1485.26 1528.48 19.09 o 3 4 3 1025.56 999.34 16.06 o 1 5 3 69.30 83.92 3.35 o 2 5 3 139.63 148.21 5.73 o 3 5 3 551.92 598.10 13.19 o 4 5 3 634.73 628.09 14.21 o 0 6 3 118.58 117.50 4.57 o 1 6 3 65.00 64.22 2.52 o 2 6 3 25.31 28.47 1.31 o 3 6 3 63.28 72.91 2.91 o 4 6 3 925.07 938.02 18.44 o 5 6 3 331.64 352.28 11.94 o 1 7 3 86.51 81.85 3.22 o 2 7 3 107.37 111.13 4.46 o 3 7 3 50.66 47.94 2.06 o 4 7 3 158.08 152.77 6.48 o 5 7 3 113.37 120.49 4.56 o 6 7 3 113.13 109.60 4.30 o 0 8 3 957.10 979.94 19.76 o 1 8 3 176.54 173.02 6.97 o 2 8 3 493.10 485.67 14.28 o 3 8 3 150.62 138.35 5.11 o 4 8 3 1.48 4.45 3.42 o 5 8 3 41.47 40.85 1.72 o 6 8 3 798.05 805.38 20.19 o 7 8 3 123.40 118.36 4.85 o 1 9 3 28.02 25.53 1.47 o 2 9 3 209.94 200.64 8.27 o 3 9 3 258.73 261.05 10.82 o 4 9 3 180.74 185.05 7.64 o 5 9 3 24.02 24.97 1.57 o 6 9 3 10.05 12.72 4.55 o 7 9 3 178.34 178.55 7.80 o 8 9 3 123.16 126.72 4.69 o 0 10 3 851.67 845.60 20.38 o 1 10 3 479.06 459.62 15.65 o 2 10 3 156.74 149.77 5.86 o 3 10 3 87.60 90.74 3.76 o 4 10 3 44.46 44.07 1.85 o 5 10 3 44.85 42.81 1.85 o 6 10 3 9.03 7.76 1.23 o 7 10 3 58.88 58.06 2.47 o 8 10 3 65.42 54.73 2.47 o 9 10 3 8.13 6.17 3.29 o 1 11 3 7.68 12.36 4.29 o 2 11 3 132.37 123.16 5.47 o 3 11 3 5.13 8.04 3.78 o 4 11 3 58.95 60.02 2.24 o 5 11 3 8.11 5.40 3.96 o 6 11 3 123.33 110.10 4.67 o 7 11 3 14.93 17.02 1.23 o 8 11 3 9.46 7.66 3.50 o 9 11 3 70.17 64.49 2.58 o 10 11 3 21.16 24.58 1.00 o 1 12 3 44.73 48.01 1.96 o 2 12 3 50.28 46.13 1.85 o 3 12 3 21.76 23.50 1.44 o 4 12 3 41.95 42.83 1.88 o 5 12 3 65.32 65.75 2.75 o 6 12 3 55.52 54.18 1.90 o 7 12 3 22.18 19.57 1.21 o 8 12 3 16.96 19.21 1.03 o 9 12 3 10.85 10.85 3.93 o 10 12 3 15.28 15.33 2.60 o 1 13 3 8.78 3.75 3.26 o 2 13 3 68.66 65.78 2.29 o 3 13 3 6.35 0.00 3.16 o 4 13 3 85.33 96.35 4.04 o 5 13 3 33.39 34.55 1.36 o 6 13 3 3.89 4.50 3.03 o 7 13 3 19.84 23.40 1.00 o 8 13 3 9.51 9.56 1.39 o 1 14 3 51.70 60.54 2.34 o 2 14 3 7.72 8.40 3.03 o 3 14 3 1.55 1.00 2.49 o 4 14 3 1.19 0.00 2.65 o 5 14 3 57.79 55.99 2.47 o 6 14 3 27.08 27.19 2.08 o 7 14 3 21.74 21.74 3.94 o 1 15 3 13.65 13.68 2.75 o 2 15 3 6.56 6.58 5.94 o 3 15 3 0.19 0.18 8.94 o 4 15 3 20.12 20.19 4.45 o 0 0 4 6191.28 6165.60 40.33 o 1 1 4 557.40 485.89 10.73 o 0 2 4 860.94 833.27 14.23 o 1 2 4 530.40 510.91 11.29 o 2 2 4 177.19 166.86 6.65 o 1 3 4 154.50 163.72 6.64 o 2 3 4 501.61 491.52 11.71 o 3 3 4 4041.04 4339.45 37.47 o 0 4 4 359.22 404.36 10.84 o 1 4 4 1246.54 1249.12 19.27 o 2 4 4 6.18 5.11 0.87 o 3 4 4 1136.25 1237.46 20.13 o 4 4 4 900.43 877.57 17.69 o 1 5 4 806.77 813.17 16.34 o 2 5 4 214.22 219.18 8.77 o 3 5 4 851.88 876.90 17.93 o 4 5 4 372.80 355.07 11.87 o 5 5 4 609.75 620.34 16.03 o 0 6 4 113.98 109.25 4.38 o 1 6 4 65.92 65.39 2.65 o 2 6 4 265.50 245.87 9.51 o 3 6 4 82.35 79.72 3.71 o 4 6 4 121.56 107.68 3.97 o 5 6 4 172.60 198.12 7.62 o 6 6 4 11.98 8.07 3.34 o 1 7 4 109.39 112.02 4.36 o 2 7 4 63.58 72.15 3.09 o 3 7 4 217.21 228.73 8.84 o 4 7 4 183.89 177.95 7.26 o 5 7 4 65.17 61.26 2.06 o 6 7 4 58.52 54.61 1.96 o 7 7 4 104.65 103.28 4.10 o 0 8 4 307.64 302.12 12.05 o 1 8 4 153.54 154.65 5.68 o 2 8 4 50.74 48.17 2.44 o 3 8 4 433.21 411.93 14.30 o 4 8 4 148.92 143.81 5.68 o 5 8 4 133.16 118.21 4.26 o 6 8 4 13.27 11.70 1.29 o 7 8 4 0.68 1.88 3.62 o 8 8 4 189.91 188.03 7.44 o 1 9 4 136.31 137.41 5.55 o 2 9 4 165.04 172.11 7.02 o 3 9 4 168.23 151.70 5.70 o 4 9 4 55.77 53.27 2.11 o 5 9 4 326.89 327.74 13.04 o 6 9 4 2.25 10.46 3.93 o 7 9 4 11.39 4.52 4.16 o 8 9 4 124.22 133.53 5.57 o 9 9 4 32.79 29.99 1.39 o 0 10 4 47.57 56.14 2.52 o 1 10 4 92.36 89.23 3.74 o 2 10 4 444.91 436.09 14.95 o 3 10 4 89.07 87.14 3.76 o 4 10 4 21.20 21.08 1.52 o 5 10 4 286.81 281.40 11.45 o 6 10 4 175.65 167.38 6.77 o 7 10 4 38.40 35.81 1.54 o 8 10 4 31.87 27.57 1.36 o 9 10 4 4.85 6.71 2.62 o 10 10 4 15.12 13.96 0.87 o 1 11 4 113.55 109.70 4.61 o 2 11 4 11.92 13.55 4.63 o 3 11 4 23.55 25.71 1.52 o 4 11 4 76.83 73.57 2.81 o 5 11 4 14.18 13.03 1.23 o 6 11 4 96.57 80.84 3.43 o 7 11 4 7.92 6.45 0.98 o 8 11 4 1.77 1.98 2.49 o 9 11 4 2.06 5.42 2.13 o 10 11 4 2.41 2.42 2.42 o 0 12 4 239.93 244.09 9.44 o 1 12 4 11.17 10.36 3.80 o 2 12 4 41.50 42.63 1.90 o 3 12 4 5.65 3.65 1.08 o 4 12 4 6.93 7.74 3.19 o 5 12 4 16.21 15.06 1.16 o 6 12 4 30.68 31.77 1.36 o 7 12 4 9.73 10.41 0.90 o 8 12 4 13.30 13.32 3.03 o 9 12 4 7.15 7.12 2.80 o 1 13 4 1.01 3.13 3.03 o 2 13 4 9.27 9.25 1.00 o 3 13 4 36.18 39.75 1.41 o 4 13 4 9.06 10.31 0.95 o 5 13 4 88.92 82.52 3.15 o 6 13 4 4.39 4.63 2.39 o 7 13 4 22.74 22.84 2.50 o 0 14 4 22.80 24.12 1.03 o 1 14 4 29.90 30.46 1.11 o 2 14 4 13.73 10.41 0.82 o 3 14 4 52.97 50.63 2.21 o 4 14 4 8.72 8.71 1.67 o 5 14 4 2.63 2.67 1.52 o 1 15 4 4.16 4.16 3.16 o 2 15 4 1.68 1.67 7.14 o 0 2 5 928.02 946.22 17.77 o 1 2 5 372.02 383.43 11.59 o 1 3 5 191.35 194.37 7.93 o 2 3 5 90.14 88.30 3.79 o 0 4 5 117.06 114.80 4.46 o 1 4 5 69.80 60.71 2.42 o 2 4 5 306.61 286.57 10.86 o 3 4 5 38.90 38.84 1.54 o 1 5 5 170.61 171.72 7.15 o 2 5 5 4.30 6.66 3.67 o 3 5 5 36.84 38.99 1.59 o 4 5 5 243.49 221.64 9.00 o 0 6 5 677.83 693.23 17.52 o 1 6 5 95.92 97.44 3.58 o 2 6 5 36.74 39.28 1.65 o 3 6 5 90.11 98.22 3.86 o 4 6 5 96.34 89.40 3.61 o 5 6 5 16.13 9.97 4.27 o 1 7 5 47.00 45.38 1.75 o 2 7 5 244.70 241.46 9.75 o 3 7 5 227.83 221.38 9.23 o 4 7 5 79.18 75.16 2.99 o 5 7 5 189.28 192.83 7.80 o 6 7 5 48.60 51.41 1.88 o 0 8 5 73.88 75.44 2.63 o 1 8 5 54.51 54.12 2.29 o 2 8 5 162.59 171.35 6.43 o 3 8 5 93.68 82.00 3.27 o 4 8 5 18.43 18.87 1.47 o 5 8 5 187.08 199.98 7.57 o 6 8 5 445.23 454.54 15.01 o 7 8 5 5.47 5.88 3.26 o 1 9 5 148.89 141.43 5.01 o 2 9 5 107.09 97.44 4.20 o 3 9 5 210.61 195.48 7.91 o 4 9 5 39.03 35.14 1.72 o 5 9 5 68.43 62.09 2.78 o 6 9 5 45.82 49.01 2.11 o 7 9 5 12.97 4.06 3.24 o 8 9 5 7.94 9.30 3.47 o 0 10 5 113.57 102.90 4.00 o 1 10 5 45.83 45.33 1.78 o 2 10 5 37.88 44.94 1.77 o 3 10 5 57.45 57.70 2.52 o 4 10 5 59.30 51.27 2.21 o 5 10 5 8.07 11.64 1.13 o 6 10 5 2.48 0.00 2.93 o 7 10 5 3.04 1.31 3.08 o 8 10 5 7.60 5.04 2.60 o 9 10 5 3.35 4.37 2.18 o 1 11 5 12.35 10.72 3.80 o 2 11 5 78.17 82.13 3.32 o 3 11 5 1.83 3.96 3.67 o 4 11 5 39.97 38.00 1.49 o 5 11 5 10.50 13.47 1.08 o 6 11 5 33.60 33.18 1.26 o 7 11 5 13.96 15.60 0.95 o 8 11 5 2.31 2.31 2.70 o 9 11 5 6.87 6.73 3.11 o 1 12 5 9.58 9.25 1.03 o 2 12 5 7.38 4.42 3.29 o 3 12 5 41.10 41.84 1.93 o 4 12 5 12.88 15.32 1.00 o 5 12 5 7.74 6.17 0.80 o 6 12 5 1.73 0.95 2.26 o 7 12 5 2.25 2.26 4.03 o 1 13 5 15.11 17.28 0.95 o 2 13 5 14.07 17.15 0.98 o 3 13 5 15.67 17.82 0.90 o 4 13 5 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151.30 5.83 o 0 8 6 224.44 243.31 9.41 o 1 8 6 13.63 15.58 1.31 o 2 8 6 9.72 10.67 3.75 o 3 8 6 82.41 89.11 3.68 o 4 8 6 58.87 67.74 2.86 o 5 8 6 18.00 17.66 1.36 o 6 8 6 34.51 35.06 1.49 o 7 8 6 55.02 55.59 1.83 o 8 8 6 6.93 4.24 2.96 o 1 9 6 77.33 79.62 2.88 o 2 9 6 124.58 112.14 4.80 o 3 9 6 186.37 171.76 6.79 o 4 9 6 3.30 3.60 3.47 o 5 9 6 23.96 23.12 1.29 o 6 9 6 16.88 17.33 1.13 o 7 9 6 10.41 8.74 0.95 o 8 9 6 10.43 9.10 3.06 o 9 9 6 1.35 1.34 6.48 o 0 10 6 5.87 3.60 3.08 o 1 10 6 3.01 1.36 2.72 o 2 10 6 4.59 3.37 3.06 o 3 10 6 14.72 17.27 1.16 o 4 10 6 20.67 20.98 1.23 o 5 10 6 25.29 27.13 1.21 o 6 10 6 5.82 3.55 2.85 o 7 10 6 11.35 12.18 0.87 o 8 10 6 10.66 10.64 3.68 o 1 11 6 2.13 0.69 2.85 o 2 11 6 10.04 8.04 3.16 o 3 11 6 19.00 20.16 1.11 o 4 11 6 33.93 34.42 1.36 o 5 11 6 20.79 15.71 0.90 o 6 11 6 21.61 21.68 3.01 o 7 11 6 9.87 9.95 2.80 o 0 12 6 21.65 19.67 0.98 o 1 12 6 5.72 0.57 2.39 o 2 12 6 37.01 40.45 1.78 o 3 12 6 43.73 44.07 1.60 o 4 12 6 12.09 12.01 4.70 o 5 12 6 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35.76 1.47 o 6 9 7 3.82 4.03 0.72 o 7 9 7 1.07 1.05 7.14 o 0 10 7 56.62 57.95 2.32 o 1 10 7 6.32 7.50 2.67 o 2 10 7 2.31 1.10 2.49 o 3 10 7 10.93 5.40 2.60 o 4 10 7 13.12 12.24 0.82 o 5 10 7 1.78 1.75 9.38 o 6 10 7 4.25 4.24 2.80 o 1 11 7 7.10 7.09 3.37 o 2 11 7 52.41 52.49 2.42 o 3 11 7 41.04 41.12 3.14 o 4 11 7 9.07 9.05 2.83 o 0 12 7 10.64 10.65 3.16 o 0 0 8 385.60 396.41 14.28 o 1 1 8 17.48 21.82 1.47 o 0 2 8 0.90 0.59 2.95 o 1 2 8 30.07 35.51 1.59 o 2 2 8 32.62 35.59 1.59 o 1 3 8 75.25 74.44 3.42 o 2 3 8 32.91 38.11 1.59 o 3 3 8 55.45 54.10 2.11 o 0 4 8 70.47 73.51 3.45 o 1 4 8 177.48 181.12 7.28 o 2 4 8 4.82 5.29 3.44 o 3 4 8 43.99 52.28 2.34 o 4 4 8 9.11 6.55 3.21 o 1 5 8 48.51 51.31 1.93 o 2 5 8 11.34 12.26 1.13 o 3 5 8 24.52 26.41 1.34 o 4 5 8 6.46 9.59 3.29 o 5 5 8 78.23 75.97 2.91 o 0 6 8 95.88 88.52 3.84 o 1 6 8 46.26 53.44 2.01 o 2 6 8 35.62 35.86 1.62 o 3 6 8 0.67 2.80 2.70 o 4 6 8 1.52 0.00 2.62 o 5 6 8 69.45 66.04 2.88 o 6 6 8 45.27 46.48 1.85 o 1 7 8 5.08 3.93 2.85 o 2 7 8 16.78 15.53 1.03 o 3 7 8 11.93 6.45 3.26 o 4 7 8 2.90 3.60 2.60 o 5 7 8 24.50 22.27 0.98 o 6 7 8 12.50 12.55 4.40 o 7 7 8 60.03 60.36 2.53 o 0 8 8 4.57 4.06 2.80 o 1 8 8 3.52 0.72 2.36 o 2 8 8 23.80 20.78 1.03 o 3 8 8 6.06 5.73 0.75 o 4 8 8 15.90 16.17 0.87 o 5 8 8 4.08 4.11 5.24 o 6 8 8 1.10 1.10 5.91 o 1 9 8 4.07 4.03 4.14 o 2 9 8 21.50 21.48 3.03 o 3 9 8 5.80 5.83 2.24 o 4 9 8 35.01 35.22 3.66 o 0 10 8 53.49 53.60 1.96 o 1 10 8 4.90 4.88 1.34 o 2 10 8 1.57 1.59 7.73 o 0 2 9 13.22 14.78 1.08 o 1 2 9 11.03 12.18 1.00 o 1 3 9 79.72 78.78 2.76 o 2 3 9 40.10 44.28 1.83 o 0 4 9 4.09 3.91 2.39 o 1 4 9 44.45 40.17 1.52 o 2 4 9 3.47 6.89 2.54 o 3 4 9 9.19 6.58 2.65 o 1 5 9 24.99 23.48 1.13 o 2 5 9 2.61 1.67 2.21 o 3 5 9 15.30 15.55 0.85 o 4 5 9 2.40 2.42 2.39 o 0 6 9 23.79 22.38 1.11 o 1 6 9 3.05 1.03 2.06 o 2 6 9 8.19 8.23 4.65 o 3 6 9 6.92 6.94 3.50 o 4 6 9 20.18 20.19 2.24 o 5 6 9 2.61 2.62 2.75 o 1 7 9 3.38 3.42 5.35 o 2 7 9 3.77 3.78 4.50 o 3 7 9 10.71 10.75 2.24 o 0 0 10 64.41 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