#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/35/2013526.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013526_Fobs loop_ _publ_author_name 'Lima, Ricardo J. C.' 'Sasaki, Jose M.' 'Ayala, Alejandro P.' 'Freire, Paulo T. C.' 'Mendes-Filho, Josue' 'Melo, Francisco E. A.' 'Ellena, Javier' 'Santos Jr, Sauli' _publ_section_title ; New crystals in the lithium sulfate family ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first i67 _journal_page_last i70 _journal_volume 59 _journal_year 2003 _space_group_IT_number 7 _symmetry_space_group_name_Hall 'P -2yc' _symmetry_space_group_name_H-M 'P 1 c 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.297 _cell_angle_gamma 90.000 _cell_length_a 5.0530 _cell_length_b 5.1990 _cell_length_c 15.9840 _exptl_crystal_F_000 324.56 _reflns_d_resolution_high 0.7705 _[local]_cod_data_source_file ta1399IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' Ricardo' _shelx_refln_list_code 4 _shelx_f_calc_maximum 153.40 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status -1 0 -20 256.66 255.56 23.61 o 0 0 -20 912.45 1055.14 56.79 o -1 1 -20 19.65 9.27 4.94 o 0 1 -20 15.72 13.21 4.69 o 1 1 -20 27.80 16.07 4.26 o -2 1 -19 237.44 175.26 17.04 o -1 1 -19 144.63 135.11 10.11 o 0 1 -19 342.02 330.31 15.16 o 1 1 -19 611.93 678.00 42.50 o 2 1 -19 450.42 412.35 32.36 o -1 2 -19 46.34 33.72 5.26 o 0 2 -19 37.50 36.19 4.55 o 1 2 -19 52.13 52.23 9.31 o -3 0 -18 624.31 665.15 58.74 o -2 0 -18 356.10 385.54 16.38 o -1 0 -18 1290.43 1433.30 47.59 o 0 0 -18 236.74 278.49 10.12 o -3 1 -18 28.65 25.34 4.58 o -2 1 -18 10.14 9.27 3.90 o -1 1 -18 29.65 27.45 2.79 o 0 1 -18 28.06 26.09 2.51 o 1 1 -18 33.91 29.67 3.29 o 2 1 -18 6.68 9.27 2.18 o 3 1 -18 45.66 34.40 5.76 o -2 2 -18 114.54 104.07 8.10 o -1 2 -18 1101.00 1149.80 51.63 o 0 2 -18 113.03 109.56 6.34 o 1 2 -18 528.28 561.40 32.35 o 2 2 -18 97.92 99.47 9.06 o -1 3 -18 131.62 121.36 10.00 o 0 3 -18 53.42 42.60 4.94 o 1 3 -18 76.72 64.06 15.76 o -3 1 -17 328.67 349.09 29.73 o -2 1 -17 869.82 951.74 44.55 o -1 1 -17 506.22 556.10 16.99 o 0 1 -17 1830.84 2008.36 47.99 o 1 1 -17 701.13 705.06 27.24 o 2 1 -17 1080.83 1166.92 45.52 o 3 1 -17 420.10 487.81 31.81 o -3 2 -17 19.47 10.34 4.62 o -2 2 -17 136.86 127.72 7.27 o -1 2 -17 30.63 30.71 3.97 o 0 2 -17 165.48 157.59 8.07 o 1 2 -17 88.96 100.22 4.94 o 2 2 -17 226.08 235.34 12.20 o 3 2 -17 75.32 69.01 6.91 o -2 3 -17 442.89 406.96 28.29 o -1 3 -17 169.30 170.16 8.39 o 0 3 -17 716.84 661.08 40.03 o 1 3 -17 227.25 184.91 18.04 o 2 3 -17 546.82 501.93 50.99 o -4 0 -16 69.11 61.98 8.63 o -3 0 -16 814.25 795.17 42.86 o -2 0 -16 464.28 443.30 15.18 o -1 0 -16 1130.04 1196.58 32.94 o 0 0 -16 312.40 299.46 9.84 o -4 1 -16 23.15 11.85 6.12 o -3 1 -16 27.77 26.88 3.15 o -2 1 -16 16.72 16.07 2.43 o -1 1 -16 3.88 -0.72 1.79 o 0 1 -16 71.33 70.91 2.87 o 1 1 -16 17.94 18.93 1.47 o 2 1 -16 60.86 63.16 3.01 o 3 1 -16 29.86 24.38 2.43 o 4 1 -16 10.10 6.44 3.26 o -3 2 -16 777.63 682.12 76.38 o -2 2 -16 505.45 480.89 19.14 o -1 2 -16 856.14 816.44 23.89 o 0 2 -16 426.42 435.96 15.03 o 1 2 -16 950.88 992.22 40.74 o 2 2 -16 381.64 409.90 17.64 o 3 2 -16 603.74 607.70 49.59 o -2 3 -16 13.28 9.63 2.83 o -1 3 -16 47.98 37.13 3.90 o 0 3 -16 33.26 30.53 2.51 o 1 3 -16 170.94 192.62 11.04 o 2 3 -16 29.62 27.27 4.94 o 3 3 -16 94.49 87.39 14.86 o -1 4 -16 463.18 415.49 37.10 o 0 4 -16 310.06 297.27 21.57 o 1 4 -16 656.91 624.87 111.97 o -4 1 -15 466.69 445.46 52.03 o -3 1 -15 248.97 264.18 11.70 o -2 1 -15 947.21 977.09 30.91 o -1 1 -15 905.24 902.50 27.44 o 0 1 -15 666.98 608.13 15.92 o 1 1 -15 458.57 435.52 18.21 o 2 1 -15 624.35 659.08 15.61 o 3 1 -15 448.04 439.14 19.06 o 4 1 -15 533.09 528.58 27.02 o -4 2 -15 10.99 6.80 7.91 o -3 2 -15 30.44 28.67 3.65 o -2 2 -15 6.42 3.58 1.79 o -1 2 -15 9.62 12.53 2.15 o 0 2 -15 20.74 16.86 2.18 o 1 2 -15 14.32 12.53 2.15 o 2 2 -15 2.88 2.11 2.15 o 3 2 -15 33.66 33.97 3.54 o 4 2 -15 34.49 29.67 4.72 o -3 3 -15 235.48 203.92 17.86 o -2 3 -15 606.31 594.81 33.32 o -1 3 -15 561.13 557.30 20.60 o 0 3 -15 723.60 758.66 23.02 o 1 3 -15 282.42 281.16 10.16 o 2 3 -15 902.59 1028.57 49.98 o 3 3 -15 383.93 352.84 43.44 o -2 4 -15 31.94 23.62 4.98 o -1 4 -15 17.38 13.21 3.58 o 0 4 -15 13.39 10.70 3.22 o 1 4 -15 11.75 4.33 3.61 o 2 4 -15 13.60 9.27 3.90 o -4 0 -14 878.51 948.14 49.17 o -3 0 -14 1160.26 1295.97 45.24 o -2 0 -14 1494.76 1624.01 47.71 o -1 0 -14 1528.93 1635.94 43.30 o 0 0 -14 4796.67 5069.08 108.47 o -4 1 -14 81.41 64.07 5.16 o -3 1 -14 74.52 77.11 4.66 o -2 1 -14 84.77 84.25 3.47 o -1 1 -14 235.32 237.85 6.43 o 0 1 -14 28.00 30.53 1.90 o 1 1 -14 170.23 175.24 5.02 o 2 1 -14 102.43 122.21 3.76 o 3 1 -14 61.35 60.19 3.51 o 4 1 -14 98.53 86.00 5.62 o -4 2 -14 666.37 594.10 58.30 o -3 2 -14 444.12 426.50 20.36 o -2 2 -14 1052.79 1088.49 31.39 o -1 2 -14 604.66 640.77 19.22 o 0 2 -14 2749.51 2972.16 69.26 o 1 2 -14 1007.18 1096.13 32.77 o 2 2 -14 1785.14 1910.70 55.17 o 3 2 -14 800.06 865.31 33.55 o 4 2 -14 429.30 434.94 25.31 o -3 3 -14 136.86 121.37 10.00 o -2 3 -14 352.32 353.56 17.82 o -1 3 -14 275.27 273.59 9.41 o 0 3 -14 294.51 310.59 8.69 o 1 3 -14 167.90 185.87 6.70 o 2 3 -14 246.86 261.09 11.02 o 3 3 -14 185.50 165.79 16.56 o -2 4 -14 218.13 177.25 13.13 o -1 4 -14 191.68 169.25 8.86 o 0 4 -14 475.04 457.70 22.73 o 1 4 -14 369.82 344.33 19.01 o 2 4 -14 376.56 324.23 24.57 o -4 1 -13 310.57 310.56 19.35 o -3 1 -13 1634.21 1617.35 49.17 o -2 1 -13 1366.24 1339.12 36.33 o -1 1 -13 4031.17 4056.16 91.67 o 0 1 -13 1982.89 2021.44 37.96 o 1 1 -13 3440.06 3604.25 83.73 o 2 1 -13 667.29 741.43 18.63 o 3 1 -13 1465.75 1562.48 45.28 o 4 1 -13 778.32 869.44 34.72 o 5 1 -13 553.43 499.38 38.15 o -4 2 -13 39.20 31.14 4.65 o -3 2 -13 204.84 211.02 7.71 o -2 2 -13 20.52 20.11 2.22 o -1 2 -13 46.16 47.98 2.61 o 0 2 -13 165.06 159.56 3.84 o 1 2 -13 164.33 175.72 5.52 o 2 2 -13 160.19 180.75 6.10 o 3 2 -13 162.08 180.72 9.18 o 4 2 -13 90.94 79.44 6.09 o -4 3 -13 78.68 54.47 6.16 o -3 3 -13 950.30 1015.77 42.42 o -2 3 -13 596.23 569.37 22.63 o -1 3 -13 1395.51 1353.13 43.50 o 0 3 -13 959.98 959.89 22.42 o 1 3 -13 1220.98 1279.79 34.11 o 2 3 -13 191.43 180.29 6.60 o 3 3 -13 726.23 776.33 33.87 o 4 3 -13 165.87 149.58 12.51 o -3 4 -13 150.78 111.17 10.79 o -2 4 -13 126.36 99.50 9.07 o -1 4 -13 64.21 65.89 4.01 o 0 4 -13 188.06 186.40 7.24 o 1 4 -13 166.31 174.66 9.00 o 2 4 -13 211.03 217.63 9.50 o 3 4 -13 100.88 92.45 8.74 o -1 5 -13 537.40 492.56 51.35 o 0 5 -13 66.40 61.98 7.45 o 1 5 -13 379.58 368.65 23.28 o -5 0 -12 194.70 175.69 9.04 o -4 0 -12 581.80 509.30 16.28 o -3 0 -12 577.13 601.83 15.83 o -2 0 -12 1317.06 1335.89 33.51 o -1 0 -12 93.44 76.83 3.33 o 0 0 -12 1313.82 1277.96 21.85 o -5 1 -12 23.25 15.78 3.15 o -4 1 -12 18.44 19.25 2.15 o -3 1 -12 26.91 23.27 2.54 o -2 1 -12 59.00 54.76 2.51 o -1 1 -12 18.61 20.12 1.86 o 0 1 -12 108.63 110.00 3.19 o 1 1 -12 91.58 92.48 3.65 o 2 1 -12 41.77 38.74 2.11 o 3 1 -12 53.68 53.64 2.51 o 4 1 -12 3.88 2.11 1.75 o 5 1 -12 17.39 14.32 2.43 o -4 2 -12 879.87 787.22 47.99 o -3 2 -12 391.67 396.40 11.33 o -2 2 -12 1518.58 1520.80 43.22 o -1 2 -12 251.08 245.59 7.72 o 0 2 -12 1590.54 1576.38 30.39 o 1 2 -12 411.63 424.51 10.15 o 2 2 -12 1461.96 1459.32 37.94 o 3 2 -12 234.24 251.99 9.62 o 4 2 -12 654.40 630.90 30.53 o 5 2 -12 336.36 329.54 23.37 o -4 3 -12 4.66 2.54 3.26 o -3 3 -12 136.22 142.71 6.34 o -2 3 -12 27.78 25.70 3.26 o -1 3 -12 76.35 67.77 3.12 o 0 3 -12 20.24 15.32 1.47 o 1 3 -12 16.16 10.70 1.72 o 2 3 -12 16.52 14.32 2.15 o 3 3 -12 29.97 34.40 3.33 o 4 3 -12 20.25 16.86 2.79 o -3 4 -12 419.31 413.05 33.89 o -2 4 -12 1102.98 1163.35 54.52 o -1 4 -12 529.27 566.17 18.07 o 0 4 -12 1370.73 1467.67 54.07 o 1 4 -12 555.35 607.72 26.18 o 2 4 -12 1537.01 1653.07 72.91 o 3 4 -12 247.32 235.96 16.29 o -2 5 -12 144.28 137.75 19.57 o -1 5 -12 9.06 1.43 5.01 o 0 5 -12 74.01 77.42 5.34 o 1 5 -12 25.43 20.11 4.22 o 2 5 -12 110.47 98.37 13.51 o -5 1 -11 624.35 673.14 34.47 o -4 1 -11 470.29 433.02 18.17 o -3 1 -11 1952.59 1927.02 63.92 o -2 1 -11 453.62 483.95 11.71 o -1 1 -11 4128.26 4035.02 74.44 o 0 1 -11 1183.77 1185.32 25.00 o 1 1 -11 3222.81 3232.31 79.44 o 2 1 -11 1227.12 1223.14 30.72 o 3 1 -11 2786.52 2972.19 71.40 o 4 1 -11 241.91 238.96 7.61 o 5 1 -11 598.58 590.97 27.69 o -5 2 -11 76.61 71.87 7.38 o -4 2 -11 93.81 79.81 6.41 o -3 2 -11 54.75 40.18 3.12 o -2 2 -11 148.88 159.06 5.27 o -1 2 -11 277.68 294.29 8.44 o 0 2 -11 184.02 191.23 4.70 o 1 2 -11 118.91 108.83 3.55 o 2 2 -11 40.41 41.64 2.18 o 3 2 -11 102.16 92.08 4.73 o 4 2 -11 69.34 67.75 5.30 o 5 2 -11 78.58 73.16 6.80 o -4 3 -11 244.43 205.58 17.36 o -3 3 -11 866.01 846.22 45.37 o -2 3 -11 418.70 425.07 14.07 o -1 3 -11 2570.66 2483.15 78.62 o 0 3 -11 378.83 404.16 9.14 o 1 3 -11 2950.03 3158.63 71.53 o 2 3 -11 564.09 598.83 15.79 o 3 3 -11 1988.60 2121.80 75.81 o 4 3 -11 181.38 164.82 10.22 o -3 4 -11 191.10 178.21 10.11 o -2 4 -11 150.12 144.09 7.74 o -1 4 -11 434.31 430.49 15.76 o 0 4 -11 342.15 381.21 11.10 o 1 4 -11 248.28 234.32 9.30 o 2 4 -11 48.42 46.15 3.33 o 3 4 -11 249.84 234.26 11.59 o -2 5 -11 122.49 111.57 21.60 o -1 5 -11 852.26 866.52 53.70 o 0 5 -11 271.13 279.83 13.96 o 1 5 -11 862.36 815.91 49.95 o 2 5 -11 319.38 314.55 34.29 o -5 0 -10 744.97 772.20 32.72 o -4 0 -10 2622.36 2994.47 71.52 o -3 0 -10 1770.00 1748.22 43.25 o -2 0 -10 4756.29 4970.69 96.84 o -1 0 -10 3117.77 3059.50 62.37 o 0 0 -10 11192.54 12140.77 214.49 o -5 1 -10 25.55 22.55 1.79 o -4 1 -10 45.12 42.60 2.97 o -3 1 -10 192.54 192.78 6.31 o -2 1 -10 253.24 271.32 9.99 o -1 1 -10 217.97 197.78 4.27 o 0 1 -10 508.75 479.35 9.14 o 1 1 -10 22.04 34.40 2.43 o 2 1 -10 193.37 190.74 5.74 o 3 1 -10 45.57 42.36 2.47 o 4 1 -10 45.32 42.60 2.97 o 5 1 -10 15.82 16.07 2.11 o -5 2 -10 431.43 379.88 32.53 o -4 2 -10 1331.18 1350.97 68.65 o -3 2 -10 1209.48 1214.81 42.53 o -2 2 -10 2209.84 2219.15 59.77 o -1 2 -10 1787.46 1737.84 41.59 o 0 2 -10 5454.24 5449.23 104.84 o 1 2 -10 1807.19 1842.40 36.23 o 2 2 -10 2320.90 2392.82 48.92 o 3 2 -10 1252.44 1295.29 42.56 o 4 2 -10 1668.82 1774.03 74.03 o 5 2 -10 400.44 399.20 20.45 o -4 3 -10 248.00 276.61 17.01 o -3 3 -10 380.34 370.34 18.23 o -2 3 -10 534.09 525.89 19.17 o -1 3 -10 491.89 514.54 13.76 o 0 3 -10 475.55 460.07 10.59 o 1 3 -10 417.79 445.91 10.40 o 2 3 -10 201.58 203.97 7.03 o 3 3 -10 259.85 264.27 8.00 o 4 3 -10 178.82 185.86 9.29 o -4 4 -10 212.54 156.21 17.03 o -3 4 -10 302.81 334.33 17.31 o -2 4 -10 583.91 577.52 20.07 o -1 4 -10 252.15 230.88 10.95 o 0 4 -10 1398.46 1432.02 43.34 o 1 4 -10 310.32 304.68 9.91 o 2 4 -10 592.36 589.48 20.29 o 3 4 -10 304.87 277.40 12.64 o 4 4 -10 397.89 347.20 25.44 o -3 5 -10 97.86 71.24 18.84 o -2 5 -10 257.40 258.02 21.92 o -1 5 -10 101.81 98.73 6.77 o 0 5 -10 180.90 164.83 8.75 o 1 5 -10 99.60 88.12 6.41 o 2 5 -10 181.48 163.34 10.15 o 3 5 -10 31.23 16.86 3.58 o -5 1 -9 371.42 356.44 15.74 o -4 1 -9 440.17 433.81 15.80 o -3 1 -9 1539.29 1476.68 39.70 o -2 1 -9 1615.18 1546.34 31.65 o -1 1 -9 1674.92 1600.67 29.21 o 0 1 -9 1469.92 1328.55 23.80 o 1 1 -9 6108.55 6455.91 121.86 o 2 1 -9 1985.41 1941.25 40.68 o 3 1 -9 2345.98 2381.92 58.21 o 4 1 -9 577.30 571.37 16.33 o 5 1 -9 624.92 643.16 22.16 o -5 2 -9 34.63 34.40 3.54 o -4 2 -9 11.69 8.59 2.11 o -3 2 -9 129.05 112.41 4.80 o -2 2 -9 24.71 19.76 2.51 o -1 2 -9 312.07 292.68 7.12 o 0 2 -9 32.13 27.46 1.79 o 1 2 -9 393.64 393.39 8.29 o 2 2 -9 109.75 104.91 3.12 o 3 2 -9 59.74 61.67 3.26 o 4 2 -9 148.36 145.90 5.95 o 5 2 -9 98.91 92.06 5.80 o -5 3 -9 255.22 255.55 24.22 o -4 3 -9 479.30 475.81 25.65 o -3 3 -9 1003.43 947.41 31.63 o -2 3 -9 663.34 675.78 19.75 o -1 3 -9 1492.68 1507.12 43.05 o 0 3 -9 737.85 766.05 17.91 o 1 3 -9 2528.39 2641.80 53.48 o 2 3 -9 1523.94 1573.09 43.95 o 3 3 -9 958.96 990.75 22.78 o 4 3 -9 492.15 492.58 17.67 o 5 3 -9 405.50 347.94 35.36 o -4 4 -9 1.40 5.33 3.58 o -3 4 -9 297.23 261.85 16.55 o -2 4 -9 27.90 30.10 2.90 o -1 4 -9 294.94 270.61 8.73 o 0 4 -9 15.60 11.09 2.15 o 1 4 -9 234.35 227.98 9.15 o 2 4 -9 27.82 29.06 2.43 o 3 4 -9 143.56 152.83 7.02 o 4 4 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