#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/35/2013562.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013562_Fobs loop_ _publ_author_name 'Zhang, You-Ming' 'Xian, Liang' 'Wei, Tai-Bao' _publ_section_title ; Chlorobis[N'-ethoxycarbonyl-N-(4-methylphenyl)thiourea-\kS]copper(I) ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m473 _journal_page_last m474 _journal_volume 59 _journal_year 2003 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 22.8265 _cell_length_b 6.9706 _cell_length_c 16.5925 _exptl_crystal_F_000 1192.00 _reflns_d_resolution_high 0.7988 _[local]_cod_data_source_file de1224Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 030717H in Pnma' _shelx_refln_list_code 4 _shelx_f_calc_maximum 636.08 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 5647.56 5955.09 145.57 o 6 0 0 7.97 8.32 13.84 o 8 0 0 2232.51 2314.52 74.86 o 10 0 0 270.42 240.38 25.98 o 12 0 0 3543.45 3761.99 96.53 o 14 0 0 208.54 213.63 29.95 o 16 0 0 132.28 135.92 35.35 o 18 0 0 52.12 40.79 36.89 o 20 0 0 161.35 102.54 42.57 o 22 0 0 624.76 506.17 70.70 o 24 0 0 166.61 183.00 83.18 o 26 0 0 168.96 253.70 91.50 o 28 0 0 44.92 -87.34 95.66 o 2 1 0 2005.68 1984.01 32.76 o 4 1 0 17154.84 17854.07 250.33 o 6 1 0 5310.21 5632.29 74.58 o 8 1 0 6510.11 6577.71 88.69 o 10 1 0 6123.05 6785.65 94.95 o 12 1 0 11800.11 12520.46 174.09 o 14 1 0 1581.71 1568.60 34.03 o 16 1 0 393.62 403.74 26.28 o 18 1 0 3166.36 3025.39 84.64 o 20 1 0 1462.76 1432.38 66.07 o 22 1 0 998.19 888.83 53.59 o 24 1 0 504.57 459.59 51.99 o 26 1 0 40.78 -48.43 74.85 o 28 1 0 473.94 433.40 76.46 o 0 2 0 404600.38 400260.34 16417.84 o 2 2 0 93203.01 95699.33 1249.41 o 4 2 0 283.65 259.22 37.43 o 6 2 0 231.64 198.43 31.19 o 8 2 0 807.66 835.76 25.44 o 10 2 0 454.99 484.74 38.48 o 12 2 0 670.39 711.84 53.76 o 14 2 0 65.42 64.18 18.11 o 16 2 0 1067.98 1059.40 47.69 o 18 2 0 91.83 65.67 35.16 o 20 2 0 434.10 445.15 54.93 o 22 2 0 269.09 193.37 48.52 o 24 2 0 137.38 101.02 48.79 o 26 2 0 125.26 123.72 84.06 o 2 3 0 432.51 360.73 31.63 o 4 3 0 8372.04 8108.13 123.26 o 6 3 0 1030.07 1052.69 95.66 o 8 3 0 2674.43 2900.68 143.49 o 10 3 0 3421.67 3439.95 92.32 o 12 3 0 2778.27 2746.18 85.13 o 14 3 0 1423.91 1308.94 62.77 o 16 3 0 236.94 250.38 42.95 o 18 3 0 1513.90 1529.76 77.56 o 20 3 0 341.54 269.57 54.07 o 22 3 0 260.87 308.95 60.23 o 24 3 0 217.02 203.67 147.65 o 26 3 0 15.54 -61.03 70.93 o 0 4 0 57185.09 51867.47 1193.65 o 2 4 0 18795.24 17388.88 302.74 o 4 4 0 390.61 279.98 83.01 o 6 4 0 58.65 14.46 41.59 o 8 4 0 86.56 125.05 30.77 o 10 4 0 169.15 178.64 83.18 o 12 4 0 111.22 159.47 62.39 o 14 4 0 1.35 -47.83 47.83 o 16 4 0 368.73 367.81 51.40 o 18 4 0 8.12 -2.85 50.90 o 20 4 0 132.44 157.35 72.78 o 22 4 0 98.46 158.04 228.75 o 24 4 0 49.08 -83.18 83.18 o 2 5 0 413.25 366.17 54.08 o 4 5 0 809.15 732.88 56.15 o 6 5 0 581.57 515.07 47.05 o 8 5 0 341.24 381.34 46.78 o 10 5 0 470.20 446.22 50.90 o 12 5 0 648.32 613.21 54.35 o 14 5 0 193.82 134.48 51.96 o 16 5 0 22.95 -52.93 52.93 o 18 5 0 243.87 280.85 114.37 o 20 5 0 101.99 31.89 64.95 o 22 5 0 80.89 11.31 128.93 o 0 6 0 7265.97 6196.98 220.43 o 2 6 0 1782.36 1612.41 106.54 o 4 6 0 164.67 149.05 39.97 o 6 6 0 2.60 -33.27 44.11 o 8 6 0 10.86 10.76 91.50 o 10 6 0 47.22 46.21 51.96 o 12 6 0 32.76 56.04 53.82 o 14 6 0 33.23 98.95 60.75 o 16 6 0 10.12 -28.28 63.80 o 18 6 0 12.86 26.84 89.42 o 20 6 0 6.41 -76.82 76.82 o 2 7 0 60.24 103.30 54.35 o 4 7 0 100.40 223.64 58.82 o 6 7 0 54.98 45.29 55.01 o 8 7 0 41.57 -19.71 76.94 o 10 7 0 23.20 73.20 62.29 o 12 7 0 67.67 41.94 67.69 o 14 7 0 17.73 -85.26 85.26 o 16 7 0 0.74 66.47 81.10 o 0 8 0 478.86 636.33 103.98 o 2 8 0 219.62 397.72 70.58 o 4 8 0 10.12 155.69 67.45 o 6 8 0 0.24 -21.72 66.12 o 8 8 0 3.61 12.22 70.40 o 10 8 0 7.16 -64.14 64.14 o 1 0 1 4249.26 18.02 10.40 o 2 0 1 2127.12 2191.82 58.23 o 3 0 1 1131.54 1274.78 26.47 o 4 0 1 4450.55 4795.80 102.05 o 5 0 1 21.40 35.21 13.21 o 6 0 1 7164.58 7780.19 163.88 o 7 0 1 5093.83 5869.30 78.45 o 8 0 1 2372.36 2331.68 34.60 o 9 0 1 449.32 527.51 16.52 o 10 0 1 8969.43 9173.05 105.30 o 11 0 1 15855.21 17744.37 191.89 o 12 0 1 5663.67 6075.66 76.72 o 13 0 1 494.21 669.41 21.99 o 14 0 1 1766.24 1827.85 35.43 o 15 0 1 109.48 105.14 22.59 o 16 0 1 100.00 67.06 24.70 o 17 0 1 654.99 592.75 31.78 o 18 0 1 491.36 467.51 33.00 o 19 0 1 745.91 773.75 38.47 o 20 0 1 961.06 904.51 42.52 o 21 0 1 13.33 35.96 32.41 o 22 0 1 0.91 -34.26 34.26 o 23 0 1 329.13 251.48 58.82 o 24 0 1 79.29 29.97 57.29 o 25 0 1 96.45 70.70 61.76 o 26 0 1 1.12 63.99 74.86 o 27 0 1 1.80 15.48 63.18 o 28 0 1 82.77 141.41 70.58 o 0 1 1 15437.75 16973.27 330.64 o 1 1 1 7103.47 7162.99 77.36 o 2 1 1 19826.46 20801.10 403.93 o 3 1 1 1718.19 1816.66 25.46 o 4 1 1 9905.84 9942.57 90.91 o 5 1 1 251.55 301.87 8.69 o 6 1 1 3110.55 3490.51 35.65 o 7 1 1 578.51 609.80 12.53 o 8 1 1 1580.42 1730.19 23.33 o 9 1 1 1370.21 1424.95 20.23 o 10 1 1 1801.95 2043.20 26.42 o 11 1 1 1802.83 1595.54 23.99 o 12 1 1 470.01 471.78 15.26 o 13 1 1 2723.96 2650.96 33.97 o 14 1 1 183.60 176.21 13.84 o 15 1 1 1048.00 1165.90 24.01 o 16 1 1 486.04 452.40 19.95 o 17 1 1 102.47 116.73 18.43 o 18 1 1 323.03 282.88 22.10 o 19 1 1 1.83 -33.66 33.66 o 20 1 1 581.18 597.40 32.99 o 21 1 1 326.81 242.96 29.40 o 22 1 1 299.25 346.00 33.66 o 23 1 1 166.47 168.54 32.43 o 24 1 1 191.77 207.36 34.05 o 25 1 1 74.37 79.61 33.57 o 26 1 1 159.72 126.54 44.74 o 27 1 1 7.32 50.13 42.89 o 28 1 1 76.88 115.33 49.84 o 1 2 1 1333.94 1423.52 25.38 o 2 2 1 132.34 163.43 33.66 o 3 2 1 3685.15 3464.01 44.33 o 4 2 1 1255.58 1195.76 26.00 o 5 2 1 1142.91 1170.10 23.15 o 6 2 1 6216.27 6537.63 78.84 o 7 2 1 1467.89 1524.14 27.33 o 8 2 1 1788.86 1648.33 29.62 o 9 2 1 1.08 20.80 9.95 o 10 2 1 4088.82 4003.35 47.44 o 11 2 1 4898.92 5044.29 54.72 o 12 2 1 4721.87 4622.78 53.05 o 13 2 1 1152.95 1245.05 26.53 o 14 2 1 746.37 757.49 21.77 o 15 2 1 261.85 256.66 18.36 o 16 2 1 14.37 -0.32 16.40 o 17 2 1 532.31 519.90 24.61 o 18 2 1 268.22 283.69 26.51 o 19 2 1 292.79 261.27 25.27 o 20 2 1 762.45 600.43 36.50 o 21 2 1 82.76 79.35 29.19 o 22 2 1 0.44 2.74 30.87 o 23 2 1 122.21 89.38 33.20 o 24 2 1 38.07 17.43 34.63 o 25 2 1 77.32 57.87 36.87 o 26 2 1 0.56 -2.99 36.57 o 27 2 1 7.94 -3.19 40.33 o 0 3 1 12621.92 12081.35 152.66 o 1 3 1 15.17 -1.31 10.72 o 2 3 1 4668.17 4239.11 51.45 o 3 3 1 373.71 316.82 15.08 o 4 3 1 3115.75 2955.05 38.75 o 5 3 1 270.87 258.31 15.45 o 6 3 1 206.53 193.92 14.10 o 7 3 1 27.38 22.07 17.04 o 8 3 1 313.47 272.66 28.81 o 9 3 1 328.09 303.92 23.35 o 10 3 1 467.51 504.80 53.43 o 11 3 1 913.76 804.47 33.17 o 12 3 1 66.53 53.82 23.73 o 13 3 1 557.84 577.03 32.09 o 14 3 1 316.97 321.95 29.39 o 15 3 1 1225.77 1054.88 42.52 o 16 3 1 63.30 73.38 40.22 o 17 3 1 275.65 340.34 30.69 o 18 3 1 361.50 421.91 33.28 o 19 3 1 90.07 101.53 39.02 o 20 3 1 80.28 65.78 36.79 o 21 3 1 71.07 42.26 38.09 o 22 3 1 149.03 147.82 41.20 o 23 3 1 107.25 116.85 43.67 o 24 3 1 80.66 72.85 46.20 o 25 3 1 35.80 45.56 50.41 o 26 3 1 89.25 69.39 51.18 o 1 4 1 620.47 727.74 57.73 o 2 4 1 4.89 -33.15 33.15 o 3 4 1 402.44 266.38 32.52 o 4 4 1 686.60 528.77 20.27 o 5 4 1 144.52 139.94 14.96 o 6 4 1 1531.62 1411.39 29.53 o 7 4 1 206.27 195.24 21.07 o 8 4 1 553.02 555.90 26.59 o 9 4 1 3.85 28.36 29.45 o 10 4 1 1018.23 987.21 35.92 o 11 4 1 850.45 919.23 61.15 o 12 4 1 1278.40 1298.58 46.20 o 13 4 1 346.82 352.28 43.22 o 14 4 1 217.01 180.06 32.62 o 15 4 1 118.71 151.54 31.64 o 16 4 1 1.82 -13.74 31.06 o 17 4 1 169.33 145.25 36.62 o 18 4 1 88.32 79.65 32.10 o 19 4 1 111.64 84.51 46.30 o 20 4 1 192.14 197.96 42.71 o 21 4 1 19.41 70.61 44.38 o 22 4 1 4.60 47.06 44.01 o 23 4 1 49.81 -36.00 51.21 o 24 4 1 16.08 12.05 49.07 o 25 4 1 14.80 10.25 53.22 o 0 5 1 1557.35 1450.39 78.32 o 1 5 1 113.24 85.12 18.43 o 2 5 1 1508.32 1270.33 28.69 o 3 5 1 4.41 10.49 18.85 o 4 5 1 364.76 334.24 30.10 o 5 5 1 4.17 -20.18 24.43 o 6 5 1 3.44 -25.58 39.02 o 7 5 1 0.55 -15.79 25.68 o 8 5 1 20.52 -19.30 25.44 o 9 5 1 16.05 74.19 28.89 o 10 5 1 35.70 -2.24 30.01 o 11 5 1 100.08 78.75 31.38 o 12 5 1 20.90 61.06 48.02 o 13 5 1 214.70 188.05 36.36 o 14 5 1 24.62 60.23 32.82 o 15 5 1 96.38 73.08 36.03 o 16 5 1 79.87 93.25 38.64 o 17 5 1 2.44 10.05 40.58 o 18 5 1 30.64 36.80 41.40 o 19 5 1 0.87 -35.14 38.46 o 20 5 1 24.08 22.79 46.59 o 21 5 1 52.80 40.89 48.71 o 22 5 1 12.53 -27.80 49.21 o 23 5 1 24.91 -11.38 53.33 o 1 6 1 153.63 349.49 40.61 o 2 6 1 9.49 115.83 29.76 o 3 6 1 3.92 55.11 27.59 o 4 6 1 181.19 123.13 26.08 o 5 6 1 1.72 -25.34 25.34 o 6 6 1 147.46 135.36 73.84 o 7 6 1 36.19 -19.32 32.18 o 8 6 1 76.58 22.94 33.08 o 9 6 1 0.16 -19.77 36.62 o 10 6 1 151.14 131.10 36.36 o 11 6 1 161.85 211.03 39.02 o 12 6 1 139.65 186.92 40.58 o 13 6 1 14.38 66.47 53.43 o 14 6 1 60.71 31.22 45.02 o 15 6 1 5.71 15.46 43.44 o 16 6 1 0.47 -31.42 43.51 o 17 6 1 32.41 31.98 51.03 o 18 6 1 13.24 92.51 82.84 o 19 6 1 23.83 -7.83 51.06 o 20 6 1 24.47 -5.91 46.00 o 0 7 1 140.39 253.80 55.88 o 1 7 1 12.49 27.54 36.79 o 2 7 1 157.88 196.74 39.51 o 3 7 1 4.13 8.58 37.83 o 4 7 1 50.27 104.75 37.92 o 5 7 1 3.51 1.44 30.51 o 6 7 1 2.70 -7.16 32.03 o 7 7 1 0.24 -22.46 34.47 o 8 7 1 0.65 -32.23 40.93 o 9 7 1 0.13 -41.23 41.39 o 10 7 1 0.94 -33.07 41.69 o 11 7 1 2.93 14.18 63.03 o 12 7 1 1.45 74.55 46.58 o 13 7 1 22.59 59.74 52.83 o 14 7 1 1.97 -12.04 72.04 o 15 7 1 12.47 29.96 51.51 o 16 7 1 11.09 -56.43 56.43 o 17 7 1 2.47 21.13 72.01 o 1 8 1 14.24 246.73 49.30 o 2 8 1 3.66 191.80 58.97 o 3 8 1 2.24 86.79 46.75 o 4 8 1 10.13 46.16 46.24 o 5 8 1 3.37 30.55 46.11 o 6 8 1 13.02 17.25 47.22 o 7 8 1 1.36 -47.76 47.76 o 8 8 1 4.31 -57.35 58.23 o 9 8 1 0.04 -17.57 50.12 o 10 8 1 9.66 -8.16 63.23 o 11 8 1 8.75 -26.03 49.32 o 0 0 2 2146.25 2191.82 58.23 o 1 0 2 2122.44 2240.20 44.11 o 2 0 2 58.53 84.01 8.82 o 3 0 2 24991.20 27005.68 436.71 o 4 0 2 4337.88 4840.92 54.99 o 5 0 2 64.57 89.56 8.04 o 6 0 2 900.77 1056.52 19.16 o 7 0 2 314.36 290.96 12.43 o 8 0 2 1231.46 1300.48 38.39 o 9 0 2 6788.23 6596.74 79.32 o 10 0 2 8872.15 9820.82 112.77 o 11 0 2 19599.74 21783.00 232.89 o 12 0 2 1703.46 2043.08 62.48 o 13 0 2 7338.13 7138.84 89.85 o 14 0 2 144.31 240.44 27.84 o 15 0 2 2555.99 2561.70 54.50 o 16 0 2 200.69 220.85 25.83 o 17 0 2 83.41 80.14 26.79 o 18 0 2 44.42 34.68 29.42 o 19 0 2 356.37 312.94 36.31 o 20 0 2 140.14 145.41 32.88 o 21 0 2 168.70 123.11 33.48 o 22 0 2 373.75 367.79 43.73 o 23 0 2 16.56 77.76 43.98 o 24 0 2 82.93 118.53 58.82 o 25 0 2 34.73 -17.57 60.31 o 26 0 2 1.84 -33.48 60.23 o 27 0 2 11.95 -41.01 63.18 o 28 0 2 10.40 -31.59 69.06 o 1 1 2 17.84 34.68 5.90 o 2 1 2 2034.55 2167.93 23.69 o 3 1 2 2965.78 3119.13 36.38 o 4 1 2 247.27 242.59 7.27 o 5 1 2 1242.20 1320.95 17.44 o 6 1 2 5307.68 5618.65 49.95 o 7 1 2 766.93 730.04 14.29 o 8 1 2 6970.20 7275.23 64.10 o 9 1 2 25.77 54.44 9.63 o 10 1 2 7108.37 7565.73 68.69 o 11 1 2 474.20 584.98 15.96 o 12 1 2 69.30 70.02 11.58 o 13 1 2 13.57 17.23 12.32 o 14 1 2 25.69 23.28 13.38 o 15 1 2 1103.32 1092.90 23.86 o 16 1 2 38.37 54.69 15.31 o 17 1 2 3585.30 3328.10 48.00 o 18 1 2 151.07 212.99 23.58 o 19 1 2 1350.55 1280.14 35.77 o 20 1 2 51.72 51.75 24.28 o 21 1 2 283.63 268.84 30.74 o 22 1 2 18.06 21.78 28.87 o 23 1 2 670.73 578.84 35.95 o 24 1 2 16.14 87.84 33.78 o 25 1 2 417.50 371.06 37.58 o 26 1 2 8.21 61.60 41.45 o 27 1 2 33.64 74.81 45.69 o 28 1 2 21.68 115.88 62.87 o 0 2 2 131.07 200.52 44.32 o 1 2 2 12832.51 13130.37 129.26 o 2 2 2 471.41 465.32 19.53 o 3 2 2 3955.19 4184.24 47.19 o 4 2 2 3944.40 3993.81 45.75 o 5 2 2 454.84 463.64 17.27 o 6 2 2 781.32 771.25 19.11 o 7 2 2 159.86 189.04 13.49 o 8 2 2 1125.76 1108.53 24.11 o 9 2 2 4314.26 4493.29 48.69 o 10 2 2 4596.65 4678.04 50.15 o 11 2 2 9155.14 9267.01 103.13 o 12 2 2 880.12 914.89 22.22 o 13 2 2 7442.81 7298.29 86.26 o 14 2 2 437.50 457.80 21.19 o 15 2 2 601.67 555.32 21.18 o 16 2 2 3.78 -3.31 16.64 o 17 2 2 641.64 649.91 26.73 o 18 2 2 9.71 46.77 24.18 o 19 2 2 10.12 2.54 25.67 o 20 2 2 45.48 32.25 27.54 o 21 2 2 8.51 -6.61 28.51 o 22 2 2 276.73 247.91 33.20 o 23 2 2 1.05 22.41 32.71 o 24 2 2 62.96 64.69 35.50 o 25 2 2 20.39 24.90 36.99 o 26 2 2 0.83 1.34 39.88 o 27 2 2 15.10 -25.73 40.88 o 1 3 2 323.85 311.50 16.76 o 2 3 2 124.40 107.81 12.03 o 3 3 2 276.40 261.42 21.08 o 4 3 2 40.98 19.04 16.40 o 5 3 2 48.15 71.15 14.10 o 6 3 2 2447.64 2396.84 39.58 o 7 3 2 554.40 555.32 20.08 o 8 3 2 2292.94 2010.21 37.08 o 9 3 2 48.88 76.05 15.64 o 10 3 2 2081.17 1986.09 52.18 o 11 3 2 17.38 46.96 26.74 o 12 3 2 264.29 265.15 25.43 o 13 3 2 166.79 182.22 31.22 o 14 3 2 50.51 98.36 23.27 o 15 3 2 375.82 422.55 31.36 o 16 3 2 33.60 52.61 25.32 o 17 3 2 1611.19 1505.68 44.24 o 18 3 2 71.18 147.50 33.05 o 19 3 2 641.02 678.27 43.46 o 20 3 2 47.18 20.69 36.17 o 21 3 2 33.78 25.08 37.40 o 22 3 2 3.08 -53.66 53.66 o 23 3 2 283.06 279.00 45.82 o 24 3 2 9.11 -15.95 44.78 o 25 3 2 232.01 125.00 48.29 o 26 3 2 0.42 -27.53 50.63 o 0 4 2 3.52 198.16 46.71 o 1 4 2 1546.85 1461.68 73.87 o 2 4 2 4.28 -6.40 49.78 o 3 4 2 1712.52 1517.54 31.04 o 4 4 2 654.13 573.73 20.48 o 5 4 2 202.41 207.72 15.58 o 6 4 2 247.48 176.46 18.45 o 7 4 2 51.60 87.24 17.37 o 8 4 2 218.74 209.41 40.64 o 9 4 2 916.23 1056.06 37.54 o 10 4 2 930.53 852.90 55.23 o 11 4 2 2256.88 2097.99 80.97 o 12 4 2 402.32 372.11 31.57 o 13 4 2 2264.93 2099.16 57.33 o 14 4 2 159.08 178.46 31.83 o 15 4 2 287.65 233.68 32.65 o 16 4 2 2.72 -27.93 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7 54.71 83.97 34.50 o 12 6 7 62.70 51.32 35.03 o 13 6 7 10.52 29.13 34.74 o 14 6 7 0.98 -7.47 35.18 o 15 6 7 86.18 29.28 38.04 o 16 6 7 0.19 31.76 39.01 o 17 6 7 59.39 -28.33 42.70 o 18 6 7 0.34 15.25 43.64 o 0 7 7 93.50 78.80 53.82 o 1 7 7 9.84 65.26 37.38 o 2 7 7 54.49 54.98 38.65 o 3 7 7 2.45 -0.86 35.19 o 4 7 7 76.96 102.73 35.60 o 5 7 7 12.84 130.14 36.56 o 6 7 7 25.91 72.42 38.03 o 7 7 7 21.85 22.29 39.78 o 8 7 7 0.54 65.88 45.11 o 9 7 7 7.13 6.03 50.71 o 10 7 7 22.81 91.49 46.19 o 11 7 7 5.71 22.22 45.45 o 12 7 7 12.29 59.14 47.47 o 13 7 7 15.96 93.81 50.11 o 14 7 7 7.40 -56.53 58.15 o 1 8 7 2.44 -40.13 47.26 o 2 8 7 0.42 -10.29 48.39 o 3 8 7 0.40 39.10 48.39 o 4 8 7 1.51 -0.87 50.41 o 5 8 7 6.98 16.95 49.68 o 6 8 7 4.30 -10.44 74.02 o 0 0 8 12731.22 12801.77 229.39 o 1 0 8 1090.84 1161.32 53.10 o 2 0 8 4392.93 4104.88 64.97 o 3 0 8 1962.09 1892.00 36.28 o 4 0 8 387.04 328.04 20.41 o 5 0 8 57.90 76.13 16.44 o 6 0 8 2729.92 2739.26 49.00 o 7 0 8 1406.05 1287.40 29.14 o 8 0 8 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3 9 249.85 325.18 19.28 o 4 3 9 275.04 353.64 20.07 o 5 3 9 342.98 364.57 19.83 o 6 3 9 73.42 76.84 15.53 o 7 3 9 1127.96 1085.31 25.57 o 8 3 9 39.80 46.68 17.52 o 9 3 9 1559.87 1474.51 32.01 o 10 3 9 2.15 8.66 18.58 o 11 3 9 734.66 681.07 27.69 o 12 3 9 165.27 213.38 24.06 o 13 3 9 918.44 941.72 36.58 o 14 3 9 1341.18 1381.43 45.04 o 15 3 9 242.88 297.51 31.78 o 16 3 9 62.28 58.82 30.28 o 17 3 9 54.20 48.39 31.78 o 18 3 9 5.92 22.52 32.51 o 19 3 9 0.08 -7.98 33.03 o 20 3 9 346.75 273.07 39.36 o 21 3 9 1.26 -11.21 44.09 o 22 3 9 91.87 80.47 45.40 o 23 3 9 23.91 54.17 47.02 o 1 4 9 231.97 255.70 19.88 o 2 4 9 1236.99 1131.25 28.11 o 3 4 9 298.14 373.17 25.94 o 4 4 9 2998.56 2892.44 51.34 o 5 4 9 158.88 238.87 22.26 o 6 4 9 1234.59 1202.17 34.69 o 7 4 9 130.55 167.80 23.32 o 8 4 9 1.41 11.90 21.32 o 9 4 9 91.99 108.01 22.93 o 10 4 9 111.20 155.56 26.67 o 11 4 9 1.36 13.42 30.01 o 12 4 9 204.65 181.26 28.60 o 13 4 9 131.37 131.40 29.98 o 14 4 9 45.16 146.06 30.27 o 15 4 9 357.26 364.03 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681.67 40.00 o 18 0 10 294.29 299.19 39.97 o 19 0 10 87.54 52.70 38.27 o 20 0 10 345.09 287.94 52.94 o 21 0 10 6.99 18.72 50.00 o 22 0 10 75.92 71.66 68.62 o 23 0 10 65.09 91.50 58.82 o 24 0 10 0.73 74.96 85.26 o 1 1 10 566.07 522.79 18.21 o 2 1 10 4235.97 4061.32 51.64 o 3 1 10 4658.76 4808.05 58.58 o 4 1 10 5419.40 5490.59 64.67 o 5 1 10 1967.42 1855.24 32.97 o 6 1 10 968.51 968.90 22.05 o 7 1 10 1822.12 1903.28 31.14 o 8 1 10 0.89 18.29 16.05 o 9 1 10 2881.43 3079.25 45.34 o 10 1 10 7.71 -10.82 21.20 o 11 1 10 370.25 369.20 21.59 o 12 1 10 1.54 -4.98 18.56 o 13 1 10 681.68 689.05 26.21 o 14 1 10 6.20 64.89 20.59 o 15 1 10 519.70 556.23 27.10 o 16 1 10 27.51 75.49 25.36 o 17 1 10 644.33 670.22 32.75 o 18 1 10 25.56 73.67 27.43 o 19 1 10 474.65 471.75 37.53 o 20 1 10 16.26 -17.31 34.00 o 21 1 10 45.54 52.26 36.47 o 22 1 10 29.97 2.88 46.71 o 23 1 10 2.43 39.48 53.49 o 24 1 10 10.13 41.59 70.58 o 0 2 10 191.59 179.98 34.22 o 1 2 10 721.96 725.31 21.36 o 2 2 10 309.67 305.79 23.66 o 3 2 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