#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2013593.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013593_Fobs loop_ _publ_author_name 'Hatch, Dana M.' 'Wacholtz, William F.' 'Mague, Joel T.' _publ_section_title ; A dimeric heteroleptic five-coordinate zinc(II) complex containing a non-motionally restricted N,N'-heterocyclic ligand ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m452 _journal_page_last m453 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.179 _cell_angle_gamma 90.000 _cell_length_a 10.8591 _cell_length_b 9.5227 _cell_length_c 13.9104 _exptl_crystal_F_000 736.00 _reflns_d_resolution_high 0.7635 _[local]_cod_data_source_file fr1434Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' wfw120 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 240.88 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2431.37 2601.81 39.22 o 4 0 0 10914.73 11445.53 166.95 o 6 0 0 418.29 425.80 11.30 o 8 0 0 2052.81 2061.65 37.64 o 10 0 0 2984.64 2901.84 65.47 o 12 0 0 2321.30 2286.34 57.56 o 1 1 0 11424.83 12699.33 157.33 o 2 1 0 915.12 993.77 11.64 o 3 1 0 9208.92 9879.82 101.66 o 4 1 0 12.97 17.55 1.54 o 5 1 0 6485.00 6836.15 72.43 o 6 1 0 4500.70 4870.76 53.50 o 7 1 0 641.47 650.82 11.01 o 8 1 0 624.13 567.03 14.75 o 9 1 0 733.62 741.70 17.45 o 10 1 0 3380.08 3490.89 54.83 o 11 1 0 500.38 487.63 14.92 o 12 1 0 77.93 85.78 8.87 o 13 1 0 213.11 217.16 32.26 o 14 1 0 701.00 664.77 38.35 o 0 2 0 8502.05 9150.20 132.53 o 1 2 0 4124.89 4372.69 50.16 o 2 2 0 798.63 873.23 18.54 o 3 2 0 539.69 558.90 9.00 o 4 2 0 509.61 516.03 7.78 o 5 2 0 7719.80 8268.75 86.91 o 6 2 0 2919.49 3130.54 35.91 o 7 2 0 836.41 827.02 14.78 o 8 2 0 640.13 636.42 13.14 o 9 2 0 6110.76 5889.33 73.47 o 10 2 0 188.79 195.06 8.03 o 11 2 0 1237.52 1281.39 23.25 o 12 2 0 513.34 462.02 22.27 o 13 2 0 1158.12 1121.46 38.01 o 14 2 0 0.06 17.78 8.04 o 1 3 0 14.44 17.74 1.45 o 2 3 0 471.86 446.08 6.96 o 3 3 0 106.92 95.58 3.50 o 4 3 0 1214.34 1230.55 17.75 o 5 3 0 2349.05 2450.86 32.11 o 6 3 0 1936.05 1771.08 25.15 o 7 3 0 1936.73 1817.95 26.42 o 8 3 0 444.34 396.97 18.45 o 9 3 0 126.41 127.21 8.64 o 10 3 0 2550.37 2500.73 42.05 o 11 3 0 317.60 310.05 14.03 o 12 3 0 4.72 4.20 5.71 o 13 3 0 139.02 110.35 13.69 o 0 4 0 5564.81 5990.26 89.69 o 1 4 0 1027.39 1106.70 16.43 o 2 4 0 457.79 407.88 6.90 o 3 4 0 964.81 1090.31 14.07 o 4 4 0 8183.71 8450.26 97.98 o 5 4 0 1844.55 1844.87 25.80 o 6 4 0 129.35 152.38 7.08 o 7 4 0 683.42 690.08 17.99 o 8 4 0 3423.63 3327.46 44.63 o 9 4 0 2282.20 2121.52 36.44 o 10 4 0 673.28 642.25 27.39 o 11 4 0 399.24 385.19 19.55 o 12 4 0 550.91 549.57 20.26 o 13 4 0 244.09 295.05 16.47 o 1 5 0 933.98 885.45 12.73 o 2 5 0 863.50 757.44 11.28 o 3 5 0 668.77 611.61 9.68 o 4 5 0 131.61 89.22 4.47 o 5 5 0 8568.84 8343.80 108.91 o 6 5 0 103.35 133.22 7.42 o 7 5 0 1753.03 1719.20 26.19 o 8 5 0 690.28 658.30 16.55 o 9 5 0 336.80 348.06 18.19 o 10 5 0 60.29 51.02 7.36 o 11 5 0 991.37 947.64 33.34 o 12 5 0 19.43 18.98 6.77 o 13 5 0 145.04 141.49 16.34 o 0 6 0 2763.13 2829.00 47.07 o 1 6 0 2734.49 2703.48 32.07 o 2 6 0 2892.99 3093.07 36.11 o 3 6 0 2667.18 2593.57 34.61 o 4 6 0 2939.36 2877.29 45.57 o 5 6 0 2028.24 2026.39 36.51 o 6 6 0 270.62 269.26 9.78 o 7 6 0 992.72 935.81 21.62 o 8 6 0 3797.76 3732.94 67.24 o 9 6 0 82.58 82.13 8.90 o 10 6 0 455.40 431.00 19.80 o 11 6 0 371.18 361.98 16.62 o 12 6 0 155.79 143.13 12.86 o 1 7 0 1296.16 1300.54 18.49 o 2 7 0 8526.59 8532.01 146.48 o 3 7 0 443.52 448.89 10.42 o 4 7 0 3.45 2.77 2.64 o 5 7 0 1051.35 970.85 20.47 o 6 7 0 78.11 90.70 6.71 o 7 7 0 282.42 253.11 17.33 o 8 7 0 861.20 840.71 24.24 o 9 7 0 15.32 8.58 5.20 o 10 7 0 971.20 984.83 34.43 o 11 7 0 2.60 2.95 5.28 o 0 8 0 280.49 279.21 13.32 o 1 8 0 2272.17 2336.67 57.09 o 2 8 0 223.65 228.79 13.27 o 3 8 0 3759.37 3815.11 57.12 o 4 8 0 67.73 70.96 6.21 o 5 8 0 2625.45 2666.82 53.42 o 6 8 0 1375.05 1330.79 31.74 o 7 8 0 2729.09 2803.38 55.05 o 8 8 0 505.14 431.61 21.51 o 9 8 0 47.03 47.73 8.02 o 10 8 0 18.07 11.24 6.16 o 1 9 0 304.79 273.11 8.90 o 2 9 0 909.55 886.22 22.98 o 3 9 0 1839.57 1813.89 32.85 o 4 9 0 57.30 61.69 6.42 o 5 9 0 66.08 66.55 8.53 o 6 9 0 21.88 20.87 6.08 o 7 9 0 625.36 559.06 25.78 o 8 9 0 190.79 204.23 13.78 o 9 9 0 1002.99 1013.37 30.32 o 0 10 0 1705.30 1606.80 44.14 o 1 10 0 0.52 4.54 4.44 o 2 10 0 711.91 665.85 17.56 o 3 10 0 174.71 184.88 9.96 o 4 10 0 997.86 1008.27 27.53 o 5 10 0 53.54 67.99 8.94 o 6 10 0 253.74 264.01 14.75 o 7 10 0 30.30 34.78 7.61 o 8 10 0 423.98 425.05 19.14 o 1 11 0 25.65 35.92 10.96 o 2 11 0 168.49 156.41 11.08 o 3 11 0 237.62 233.23 13.55 o 4 11 0 58.11 54.92 8.31 o 5 11 0 126.27 138.18 11.92 o 6 11 0 599.14 600.11 29.10 o 0 12 0 138.07 127.84 18.26 o 1 12 0 33.70 33.48 11.57 o 2 12 0 120.88 194.20 22.52 o 3 12 0 711.60 835.83 45.66 o -13 0 1 6.60 28.00 10.96 o -11 0 1 4211.01 4271.67 91.54 o -9 0 1 2969.30 2915.26 51.22 o -7 0 1 13.37 26.54 3.74 o -5 0 1 8440.69 8989.43 132.90 o -3 0 1 4043.43 4169.73 62.30 o -1 0 1 5020.08 5652.39 82.29 o 1 0 1 17958.22 18786.54 270.49 o 3 0 1 14371.11 15737.53 277.56 o 5 0 1 8263.99 8626.12 128.16 o 7 0 1 309.82 309.49 15.22 o 9 0 1 1160.12 1132.95 29.98 o 11 0 1 345.35 328.27 17.33 o 13 0 1 2344.47 2488.02 93.75 o -14 1 1 801.46 890.62 45.66 o -13 1 1 564.41 621.43 24.75 o -12 1 1 1509.66 1508.14 34.95 o -11 1 1 2064.84 2066.99 37.70 o -10 1 1 440.05 447.48 11.66 o -9 1 1 995.35 990.21 20.53 o -8 1 1 2393.21 2364.05 29.68 o -7 1 1 581.19 534.56 9.66 o -6 1 1 653.52 593.16 9.80 o -5 1 1 1059.25 915.65 12.67 o -4 1 1 1841.13 1760.61 20.65 o -3 1 1 3561.44 3750.41 39.99 o -2 1 1 372.52 381.33 5.39 o -1 1 1 7858.41 8468.78 86.76 o 0 1 1 8729.38 9802.18 100.22 o 1 1 1 10629.94 11639.42 131.10 o 2 1 1 145.31 144.54 6.80 o 3 1 1 449.91 460.95 6.80 o 4 1 1 24042.75 25385.77 257.95 o 5 1 1 925.63 946.89 13.10 o 6 1 1 47.78 38.07 2.74 o 7 1 1 756.33 773.31 12.47 o 8 1 1 273.34 275.51 7.27 o 9 1 1 20.64 16.68 3.60 o 10 1 1 2685.18 2751.87 41.12 o 11 1 1 878.26 849.59 20.22 o 12 1 1 141.40 168.19 15.74 o 13 1 1 24.83 25.36 6.84 o 14 1 1 627.68 600.85 40.79 o -13 2 1 296.36 306.59 19.55 o -12 2 1 11.28 15.59 5.42 o -11 2 1 315.61 308.82 11.58 o -10 2 1 1864.53 1776.84 28.27 o -9 2 1 401.57 350.52 10.36 o -8 2 1 896.84 794.34 15.11 o -7 2 1 3046.15 3176.07 37.21 o -6 2 1 7783.35 7825.21 91.40 o -5 2 1 864.75 963.59 13.15 o -4 2 1 648.07 657.49 9.42 o -3 2 1 251.63 255.80 4.50 o -2 2 1 2636.01 2703.73 29.26 o -1 2 1 3286.66 3594.76 38.00 o 0 2 1 1484.00 1617.36 18.00 o 1 2 1 25918.08 27634.11 300.29 o 2 2 1 6030.18 6429.19 79.08 o 3 2 1 5109.01 5250.25 61.01 o 4 2 1 540.55 552.59 8.30 o 5 2 1 116.54 177.66 5.49 o 6 2 1 4673.83 4909.33 54.13 o 7 2 1 45.64 36.28 3.63 o 8 2 1 7.57 17.35 3.50 o 9 2 1 802.78 817.79 21.75 o 10 2 1 388.80 381.66 17.90 o 11 2 1 1387.77 1383.41 31.11 o 12 2 1 76.20 80.55 10.95 o 13 2 1 504.80 502.39 24.25 o -13 3 1 984.00 983.73 58.75 o -12 3 1 159.04 179.05 12.27 o -11 3 1 2814.30 2782.31 53.84 o -10 3 1 192.56 180.83 9.13 o -9 3 1 6873.40 6661.81 82.15 o -8 3 1 894.21 832.60 15.65 o -7 3 1 505.56 522.91 11.30 o -6 3 1 522.43 417.04 9.23 o -5 3 1 6944.59 6763.61 79.60 o -4 3 1 2231.57 2184.25 28.33 o -3 3 1 1898.81 1999.96 23.09 o -2 3 1 35.59 38.16 1.89 o -1 3 1 6436.77 6642.74 69.34 o 0 3 1 1892.96 2031.43 22.84 o 1 3 1 368.61 380.96 8.11 o 2 3 1 171.89 193.89 4.40 o 3 3 1 4919.43 5321.31 62.42 o 4 3 1 6846.21 7863.12 91.04 o 5 3 1 196.88 152.49 5.11 o 6 3 1 7.97 5.14 3.98 o 7 3 1 2885.22 2846.18 38.13 o 8 3 1 692.74 650.41 13.59 o 9 3 1 668.54 644.03 16.41 o 10 3 1 680.36 628.27 16.89 o 11 3 1 1400.60 1379.79 28.57 o 12 3 1 286.54 273.03 14.35 o 13 3 1 398.53 417.75 22.19 o -13 4 1 348.52 328.72 20.65 o -12 4 1 0.03 7.68 6.66 o -11 4 1 666.73 664.59 21.43 o -10 4 1 2970.51 2847.30 54.45 o -9 4 1 23.88 24.19 4.33 o -8 4 1 1184.11 1093.97 21.81 o -7 4 1 8178.07 8377.26 99.51 o -6 4 1 3088.02 2918.29 86.82 o -5 4 1 1159.73 1117.54 19.41 o -4 4 1 2965.14 3043.52 38.55 o -3 4 1 5995.42 6114.68 65.14 o -2 4 1 855.07 896.15 13.23 o -1 4 1 4195.06 4271.74 46.29 o 0 4 1 812.72 811.44 11.21 o 1 4 1 1021.20 944.97 13.67 o 2 4 1 765.39 816.06 19.88 o 3 4 1 156.82 174.46 5.07 o 4 4 1 705.18 730.84 12.44 o 5 4 1 2539.85 2434.74 32.50 o 6 4 1 421.69 416.14 17.31 o 7 4 1 1189.38 1184.53 21.82 o 8 4 1 2.56 4.05 3.33 o 9 4 1 2408.03 2274.93 46.78 o 10 4 1 1656.52 1534.06 39.81 o 11 4 1 1912.44 1945.98 42.60 o 12 4 1 312.25 287.21 15.18 o 13 4 1 126.90 168.06 16.47 o -13 5 1 30.86 37.26 10.74 o -12 5 1 341.21 333.73 16.03 o -11 5 1 46.64 56.21 8.20 o -10 5 1 238.24 230.55 12.87 o -9 5 1 419.01 379.53 24.76 o -8 5 1 3269.72 3097.44 47.88 o -7 5 1 101.73 94.75 5.50 o -6 5 1 1329.12 1258.14 20.18 o -5 5 1 2465.93 2448.52 42.09 o -4 5 1 12748.79 12978.22 148.64 o -3 5 1 1493.50 1456.04 18.75 o -2 5 1 811.68 872.85 13.63 o -1 5 1 4567.76 5378.37 58.25 o 0 5 1 5463.12 5858.66 63.04 o 1 5 1 1793.27 1913.55 23.28 o 2 5 1 832.55 898.95 12.77 o 3 5 1 139.66 113.23 4.40 o 4 5 1 3855.12 3897.88 56.56 o 5 5 1 63.39 72.95 5.79 o 6 5 1 2279.59 2341.35 37.66 o 7 5 1 127.29 116.18 7.22 o 8 5 1 6327.55 6260.01 88.63 o 9 5 1 417.79 359.96 14.33 o 10 5 1 128.35 129.15 10.65 o 11 5 1 564.63 562.56 20.36 o 12 5 1 836.05 885.98 27.29 o -12 6 1 193.14 208.31 14.51 o -11 6 1 6.86 9.91 5.36 o -10 6 1 25.10 28.26 6.35 o -9 6 1 63.07 63.22 7.83 o -8 6 1 421.02 403.02 17.79 o -7 6 1 297.70 272.99 15.56 o -6 6 1 3307.89 3410.07 45.21 o -5 6 1 603.38 574.99 12.06 o -4 6 1 0.92 7.68 2.78 o -3 6 1 1820.49 1796.39 26.49 o -2 6 1 1735.85 1661.15 25.31 o -1 6 1 3730.96 3831.72 43.55 o 0 6 1 110.96 114.69 4.31 o 1 6 1 564.43 623.13 10.47 o 2 6 1 7614.87 7497.74 98.50 o 3 6 1 611.99 589.47 11.56 o 4 6 1 1146.17 1101.51 18.09 o 5 6 1 2010.87 1989.20 33.17 o 6 6 1 3625.05 3676.76 55.46 o 7 6 1 2.86 4.62 3.29 o 8 6 1 696.94 730.86 21.01 o 9 6 1 1246.80 1263.74 31.51 o 10 6 1 42.68 53.08 7.93 o 11 6 1 842.05 790.79 25.40 o 12 6 1 651.38 694.32 24.54 o -11 7 1 134.47 134.96 11.91 o -10 7 1 19.59 20.91 6.26 o -9 7 1 537.14 536.04 19.43 o -8 7 1 15.10 15.76 5.55 o -7 7 1 1854.38 1820.39 38.90 o -6 7 1 0.07 4.80 3.78 o -5 7 1 28.03 25.62 3.60 o -4 7 1 2596.74 2610.65 36.13 o -3 7 1 2121.44 2084.43 29.79 o -2 7 1 949.57 941.33 16.40 o -1 7 1 2829.62 2773.48 33.80 o 0 7 1 218.47 205.72 6.10 o 1 7 1 2037.67 1990.85 25.64 o 2 7 1 85.32 89.53 4.97 o 3 7 1 2957.43 2931.64 60.16 o 4 7 1 1040.02 999.75 20.60 o 5 7 1 162.59 152.49 11.98 o 6 7 1 3179.59 3116.44 56.80 o 7 7 1 1998.32 1958.70 39.19 o 8 7 1 675.50 665.10 21.31 o 9 7 1 91.61 85.05 11.87 o 10 7 1 28.21 22.37 6.35 o 11 7 1 1102.17 1149.17 32.53 o -10 8 1 805.92 759.08 26.70 o -9 8 1 526.28 507.71 19.68 o -8 8 1 6.08 4.63 4.68 o -7 8 1 1.92 11.82 5.03 o -6 8 1 643.79 631.66 20.03 o -5 8 1 336.99 316.99 13.47 o -4 8 1 12.52 12.62 3.12 o -3 8 1 776.56 687.53 19.64 o -2 8 1 1787.11 1719.82 26.26 o -1 8 1 632.11 575.88 19.60 o 0 8 1 34.02 29.80 4.08 o 1 8 1 217.24 196.46 7.17 o 2 8 1 5733.56 5859.80 82.32 o 3 8 1 1662.29 1682.57 42.88 o 4 8 1 1.85 4.19 3.28 o 5 8 1 629.43 663.01 17.17 o 6 8 1 4582.06 4525.96 68.38 o 7 8 1 143.27 145.87 13.26 o 8 8 1 593.89 600.01 20.97 o 9 8 1 263.36 249.83 20.18 o 10 8 1 79.04 74.67 9.55 o -9 9 1 293.14 290.43 20.01 o -8 9 1 2129.76 2125.16 47.09 o -7 9 1 10.74 11.16 5.48 o -6 9 1 3.71 4.90 4.63 o -5 9 1 9.14 5.67 4.65 o -4 9 1 900.25 870.50 23.89 o -3 9 1 1.99 5.73 3.59 o -2 9 1 1364.56 1370.49 23.12 o -1 9 1 2118.19 2052.43 39.35 o 0 9 1 362.59 378.73 11.62 o 1 9 1 1782.75 1623.91 29.60 o 2 9 1 158.46 171.88 8.89 o 3 9 1 1504.30 1486.27 28.68 o 4 9 1 918.48 913.80 21.29 o 5 9 1 793.59 777.83 19.60 o 6 9 1 292.44 301.74 23.72 o 7 9 1 942.39 916.87 27.04 o 8 9 1 159.36 148.35 12.27 o 9 9 1 5.56 0.61 5.71 o -8 10 1 29.50 37.86 8.38 o -7 10 1 951.60 1030.03 36.16 o -6 10 1 572.86 591.17 25.82 o -5 10 1 28.41 30.94 8.52 o -4 10 1 1.48 1.89 6.39 o -3 10 1 2450.76 2574.12 51.05 o -2 10 1 682.04 619.44 16.69 o -1 10 1 105.82 137.59 11.83 o 0 10 1 41.31 37.92 6.20 o 1 10 1 3276.92 3354.10 61.24 o 2 10 1 64.10 84.33 7.45 o 3 10 1 30.56 38.11 5.86 o 4 10 1 39.92 45.99 6.31 o 5 10 1 14.68 16.62 5.54 o 6 10 1 14.38 10.51 5.73 o 7 10 1 681.80 665.04 23.31 o 8 10 1 10.00 16.61 6.71 o -6 11 1 41.32 50.91 8.49 o -5 11 1 141.69 142.44 12.18 o -4 11 1 443.82 430.24 17.92 o -3 11 1 943.95 1020.35 44.44 o -2 11 1 2248.74 2272.52 83.40 o -1 11 1 263.90 289.18 16.36 o 0 11 1 622.39 703.73 37.13 o 1 11 1 2.26 1.54 4.63 o 2 11 1 758.10 781.43 23.31 o 3 11 1 59.35 54.19 6.93 o 4 11 1 132.33 138.25 14.22 o 5 11 1 2.49 8.99 5.36 o 6 11 1 20.75 20.05 8.19 o -3 12 1 151.35 163.76 22.52 o -2 12 1 1072.84 1084.21 52.96 o -1 12 1 299.08 329.95 26.79 o 0 12 1 6.22 7.91 7.91 o 1 12 1 182.77 197.85 21.92 o 2 12 1 988.68 1018.38 34.86 o 3 12 1 8.83 11.04 7.52 o -14 0 2 801.13 801.13 43.22 o -12 0 2 2759.57 2883.72 94.36 o -10 0 2 2524.11 2578.99 79.75 o -8 0 2 3018.30 2928.35 50.70 o -6 0 2 344.61 327.11 9.45 o -4 0 2 602.12 486.82 10.53 o -2 0 2 37278.81 37392.50 534.90 o 0 0 2 15841.56 16793.22 241.52 o 2 0 2 5608.96 6058.22 94.61 o 4 0 2 21549.47 22779.34 338.93 o 6 0 2 402.59 380.77 10.85 o 8 0 2 8632.88 8852.46 135.25 o 10 0 2 7009.45 7043.07 138.46 o 12 0 2 435.52 465.10 33.48 o 14 0 2 3491.53 3989.24 136.97 o -14 1 2 325.30 358.56 28.61 o -13 1 2 141.73 148.58 14.19 o -12 1 2 104.06 92.92 9.34 o -11 1 2 780.13 790.37 22.46 o -10 1 2 795.11 778.76 16.19 o -9 1 2 740.19 694.41 15.93 o -8 1 2 122.26 110.55 4.86 o -7 1 2 2457.73 2493.42 30.25 o -6 1 2 3989.28 3903.39 43.81 o -5 1 2 876.14 736.94 10.79 o -4 1 2 151.24 122.44 3.45 o -3 1 2 3979.01 4501.54 47.75 o -2 1 2 1073.58 1098.23 14.26 o -1 1 2 62.06 84.73 3.76 o 0 1 2 325.99 289.09 4.15 o 1 1 2 21.04 27.41 1.52 o 2 1 2 308.44 291.80 4.71 o 3 1 2 4041.69 4229.77 45.28 o 4 1 2 6109.54 6721.33 70.99 o 5 1 2 14170.46 14884.61 153.70 o 6 1 2 823.93 801.27 12.36 o 7 1 2 2936.83 2923.35 34.98 o 8 1 2 1322.77 1290.25 21.06 o 9 1 2 366.13 366.58 10.22 o 10 1 2 718.45 729.33 15.79 o 11 1 2 690.55 705.92 21.92 o 12 1 2 172.03 176.17 12.35 o 13 1 2 1801.32 1868.40 91.31 o -14 2 2 690.39 729.91 42.00 o -13 2 2 503.38 529.63 34.09 o -12 2 2 61.41 54.33 7.72 o -11 2 2 723.20 750.36 18.70 o -10 2 2 727.37 726.49 30.75 o -9 2 2 2528.99 2424.61 34.83 o -8 2 2 1997.35 1807.65 40.95 o -7 2 2 394.99 321.01 7.15 o -6 2 2 1886.90 1967.38 30.13 o -5 2 2 7115.17 7083.74 75.10 o -4 2 2 31.93 36.63 2.05 o -3 2 2 40.21 49.28 2.11 o -2 2 2 515.91 573.53 12.27 o -1 2 2 9981.59 11087.82 113.52 o 0 2 2 796.96 814.51 10.12 o 1 2 2 1.70 11.53 1.53 o 2 2 2 467.26 470.98 6.70 o 3 2 2 8844.25 9493.38 98.31 o 4 2 2 5718.65 5934.82 63.20 o 5 2 2 24.21 36.44 2.36 o 6 2 2 43.42 43.87 2.91 o 7 2 2 4948.97 4832.56 66.40 o 8 2 2 2309.47 2231.37 35.77 o 9 2 2 34.15 34.49 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