#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/35/2013597.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013597_Fobs loop_ _publ_author_name 'Kennedy, Alan R.' 'Mair, Francis S.' _publ_section_title ; A magnesium--bis(diaryldiketiminate) complex ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m549 _journal_page_last m551 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.484 _cell_angle_gamma 90.000 _cell_length_a 16.6252 _cell_length_b 10.6287 _cell_length_c 23.8314 _exptl_crystal_F_000 1496.00 _reflns_d_resolution_high 0.7694 _[local]_cod_data_source_file fr1440Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' fm1 173K colourless prism 0.28 0.14 0.12' _shelx_refln_list_code 4 _shelx_f_calc_maximum 196.98 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 170.24 158.80 4.84 o 4 0 0 20105.65 19017.34 235.94 o 5 0 0 21.92 19.66 6.20 o 6 0 0 2790.42 2913.68 42.05 o 7 0 0 108.04 156.84 10.74 o 8 0 0 941.23 857.54 20.57 o 9 0 0 2161.52 2424.11 38.26 o 10 0 0 1161.82 1244.12 32.97 o 11 0 0 1167.75 1274.52 30.55 o 12 0 0 6.36 -19.66 15.12 o 13 0 0 1242.41 1214.17 40.68 o 14 0 0 66.31 50.06 21.48 o 15 0 0 339.18 393.38 29.34 o 16 0 0 451.53 452.52 29.79 o 17 0 0 1122.93 1206.00 48.55 o 18 0 0 606.17 648.83 53.54 o 19 0 0 596.84 615.56 48.25 o 20 0 0 88.76 246.83 56.26 o 21 0 0 338.61 503.49 76.83 o 2 1 0 184.05 194.29 3.05 o 3 1 0 3610.94 3344.21 31.32 o 4 1 0 1689.97 1765.69 16.15 o 5 1 0 1191.00 1177.86 13.21 o 6 1 0 1985.60 1967.05 20.63 o 7 1 0 314.16 319.43 8.35 o 8 1 0 31.72 51.27 6.31 o 9 1 0 16.01 29.17 8.36 o 10 1 0 1316.29 1408.51 25.73 o 11 1 0 903.50 837.30 19.48 o 12 1 0 10.78 4.68 11.30 o 13 1 0 541.46 582.04 32.67 o 14 1 0 741.02 693.52 25.48 o 15 1 0 68.66 52.65 17.22 o 16 1 0 171.93 198.81 29.72 o 17 1 0 16.81 8.23 19.71 o 18 1 0 978.02 1019.93 35.98 o 19 1 0 16.37 47.37 27.86 o 20 1 0 2.06 -31.30 30.29 o 21 1 0 5.75 -6.12 34.75 o 0 2 0 16.40 15.47 2.71 o 1 2 0 3989.02 3754.81 35.23 o 2 2 0 349.27 365.27 5.22 o 4 2 0 824.57 762.42 9.09 o 5 2 0 700.03 689.19 8.66 o 6 2 0 5.95 2.16 5.62 o 7 2 0 62.46 67.65 4.72 o 8 2 0 2045.63 2368.85 26.74 o 9 2 0 1407.56 1456.98 18.88 o 10 2 0 27.10 35.44 9.38 o 11 2 0 84.75 69.95 12.10 o 12 2 0 337.83 330.05 24.65 o 13 2 0 1058.73 1009.54 21.01 o 14 2 0 50.64 43.58 12.25 o 15 2 0 91.85 95.11 14.41 o 16 2 0 49.13 63.97 17.52 o 17 2 0 4.63 -6.61 18.81 o 18 2 0 61.04 85.36 23.47 o 19 2 0 3.65 14.92 26.14 o 20 2 0 52.47 29.00 29.82 o 21 2 0 67.90 83.27 37.62 o 1 3 0 575.30 619.44 7.40 o 2 3 0 30269.72 30055.67 350.43 o 3 3 0 473.88 551.39 7.01 o 4 3 0 1530.03 1527.63 15.03 o 5 3 0 8877.42 9261.67 123.57 o 6 3 0 215.75 182.23 12.48 o 7 3 0 1442.89 1477.87 16.95 o 8 3 0 448.84 381.43 15.12 o 9 3 0 13.39 7.25 6.81 o 10 3 0 1243.74 1188.69 20.62 o 11 3 0 4079.01 3920.18 51.31 o 12 3 0 75.76 82.28 10.67 o 13 3 0 154.28 153.86 12.48 o 14 3 0 84.12 71.19 17.54 o 15 3 0 19.07 18.30 14.08 o 16 3 0 11.60 29.37 24.88 o 17 3 0 28.86 11.24 30.25 o 18 3 0 7.91 35.29 28.82 o 19 3 0 51.22 56.00 78.04 o 20 3 0 48.26 27.51 41.72 o 0 4 0 63.77 34.07 10.59 o 1 4 0 1687.37 1622.69 18.83 o 2 4 0 49.84 46.26 2.83 o 3 4 0 14.97 4.92 3.89 o 4 4 0 6468.79 6573.42 59.12 o 5 4 0 2312.16 2248.25 22.03 o 6 4 0 6529.98 6530.37 66.24 o 7 4 0 47.03 28.29 4.62 o 8 4 0 0.24 -2.66 5.22 o 9 4 0 150.35 126.59 7.13 o 10 4 0 231.58 244.08 15.20 o 11 4 0 478.62 414.18 12.89 o 12 4 0 59.81 38.00 15.12 o 13 4 0 523.28 452.17 17.83 o 14 4 0 77.58 58.15 13.48 o 15 4 0 76.47 76.35 15.06 o 16 4 0 149.79 208.23 37.43 o 17 4 0 58.87 50.30 22.76 o 18 4 0 193.06 180.31 29.98 o 19 4 0 1.31 -1.48 34.71 o 20 4 0 140.69 154.60 53.84 o 1 5 0 910.06 1113.49 33.73 o 2 5 0 5852.03 6311.31 67.60 o 3 5 0 110.95 84.20 4.54 o 4 5 0 573.31 583.40 10.64 o 5 5 0 6610.54 7039.87 71.76 o 6 5 0 296.46 286.83 8.78 o 7 5 0 775.84 765.76 12.86 o 8 5 0 5368.56 5575.39 63.53 o 9 5 0 12.79 14.76 6.32 o 10 5 0 7.61 3.08 7.49 o 11 5 0 325.75 362.02 14.21 o 12 5 0 0.64 -8.65 13.61 o 13 5 0 337.30 316.42 32.14 o 14 5 0 19.55 13.52 15.39 o 15 5 0 54.57 65.12 18.98 o 16 5 0 107.14 145.15 44.39 o 17 5 0 146.46 135.66 26.69 o 18 5 0 142.99 181.10 80.01 o 19 5 0 0.19 21.31 35.21 o 20 5 0 3.42 55.67 41.71 o 0 6 0 308.19 336.75 8.90 o 1 6 0 38.17 34.03 3.20 o 2 6 0 26.57 31.40 12.86 o 3 6 0 524.63 657.40 19.06 o 4 6 0 9.02 16.64 5.85 o 5 6 0 197.62 159.57 8.95 o 6 6 0 1407.82 1427.87 22.59 o 7 6 0 639.27 615.83 14.24 o 8 6 0 473.66 460.88 11.99 o 9 6 0 848.04 771.38 19.93 o 10 6 0 66.09 64.82 12.41 o 11 6 0 506.08 447.77 14.16 o 12 6 0 125.40 116.00 12.29 o 13 6 0 9.07 27.62 17.15 o 14 6 0 133.78 153.96 21.20 o 15 6 0 62.14 43.14 17.99 o 16 6 0 18.13 -3.95 27.31 o 17 6 0 84.57 81.48 28.66 o 18 6 0 35.33 93.42 39.90 o 19 6 0 55.81 174.16 43.53 o 1 7 0 89.81 80.29 9.83 o 2 7 0 1008.36 1079.67 17.00 o 3 7 0 663.92 680.39 15.12 o 4 7 0 611.57 632.02 18.78 o 5 7 0 233.44 264.09 11.52 o 6 7 0 152.79 156.58 10.93 o 7 7 0 2.47 19.45 8.64 o 8 7 0 276.80 230.00 26.09 o 9 7 0 114.25 109.26 8.01 o 10 7 0 221.30 178.49 18.16 o 11 7 0 359.16 289.01 21.87 o 12 7 0 535.17 531.68 26.54 o 13 7 0 683.37 701.23 33.98 o 14 7 0 7.21 2.86 24.00 o 15 7 0 321.95 263.48 38.49 o 16 7 0 0.37 -4.80 34.63 o 17 7 0 0.59 42.47 45.46 o 18 7 0 0.17 16.46 53.61 o 0 8 0 118.87 121.63 6.20 o 1 8 0 208.99 198.71 6.26 o 2 8 0 373.56 416.20 9.91 o 3 8 0 1332.44 1455.54 25.26 o 4 8 0 4.14 22.86 13.54 o 5 8 0 867.68 824.63 22.49 o 6 8 0 3.87 8.53 19.51 o 7 8 0 549.93 589.95 19.91 o 8 8 0 149.09 124.55 15.99 o 9 8 0 9.82 8.17 14.21 o 10 8 0 64.04 30.60 16.49 o 11 8 0 195.85 159.35 25.11 o 12 8 0 5.21 -16.59 19.20 o 13 8 0 36.66 35.79 28.22 o 14 8 0 60.72 102.12 38.39 o 15 8 0 82.98 76.81 57.55 o 16 8 0 13.81 16.77 39.06 o 17 8 0 4.94 -89.72 59.81 o 1 9 0 147.86 139.80 9.27 o 2 9 0 98.06 103.35 9.14 o 3 9 0 130.22 134.09 8.20 o 4 9 0 8.10 -7.36 14.57 o 5 9 0 2.24 -15.83 18.13 o 6 9 0 425.58 377.69 21.24 o 7 9 0 127.61 137.49 21.12 o 8 9 0 907.83 971.66 57.40 o 9 9 0 587.29 590.89 32.81 o 10 9 0 85.56 72.03 25.75 o 11 9 0 34.79 -1.47 25.71 o 12 9 0 77.00 86.78 30.55 o 13 9 0 5.33 33.12 34.03 o 14 9 0 127.36 138.37 40.10 o 15 9 0 12.20 9.40 57.08 o 16 9 0 32.24 -18.30 89.54 o 0 10 0 376.96 376.60 36.98 o 1 10 0 5.66 15.12 11.19 o 2 10 0 17.15 47.26 31.69 o 3 10 0 15.30 9.05 27.15 o 4 10 0 6.03 12.55 23.28 o 5 10 0 47.86 8.04 42.95 o 6 10 0 14.53 35.00 35.39 o 7 10 0 193.98 175.12 25.92 o 8 10 0 691.68 698.28 68.59 o 9 10 0 0.19 21.24 30.92 o 10 10 0 0.07 72.21 54.45 o 11 10 0 18.92 -24.65 33.68 o 12 10 0 98.37 52.93 68.21 o 13 10 0 0.00 -15.50 33.66 o 14 10 0 8.84 -9.75 87.72 o 1 11 0 181.86 167.73 23.14 o 2 11 0 58.42 97.62 49.23 o 3 11 0 698.69 711.98 81.29 o 4 11 0 70.03 86.82 28.87 o 5 11 0 24.57 66.14 29.50 o 6 11 0 289.08 378.81 39.70 o 7 11 0 4.42 -5.21 34.59 o 8 11 0 24.88 21.03 32.54 o 9 11 0 83.47 80.76 44.39 o 10 11 0 272.75 352.83 42.14 o 11 11 0 8.15 58.19 44.09 o 12 11 0 0.99 43.43 47.63 o 0 12 0 200.10 186.33 88.17 o 1 12 0 0.41 42.20 67.76 o 2 12 0 271.35 385.67 74.86 o 3 12 0 196.11 207.05 31.31 o 4 12 0 310.06 358.75 41.29 o 5 12 0 364.70 499.10 48.72 o 6 12 0 247.70 201.47 35.75 o 7 12 0 81.00 108.37 35.49 o 8 12 0 3.95 12.43 37.75 o 9 12 0 0.25 4.08 46.19 o 10 12 0 1.39 92.19 42.17 o 1 13 0 357.54 348.46 89.99 o 2 13 0 98.48 33.12 78.34 o 3 13 0 357.42 415.31 80.76 o 4 13 0 1.00 111.92 143.98 o 5 13 0 0.03 80.01 101.63 o 6 13 0 7.87 73.81 54.14 o 7 13 0 3.09 -66.70 60.35 o -21 1 1 235.10 310.88 42.79 o -20 1 1 145.49 170.61 49.76 o -19 1 1 77.56 108.14 28.51 o -18 1 1 184.52 228.80 46.51 o -17 1 1 104.68 114.07 27.37 o -16 1 1 163.31 186.82 28.06 o -15 1 1 1588.48 1584.81 36.05 o -14 1 1 920.70 857.86 22.37 o -13 1 1 1.21 -14.32 10.18 o -12 1 1 142.43 137.47 12.93 o -11 1 1 454.79 431.88 16.86 o -10 1 1 9.53 1.81 10.59 o -9 1 1 0.18 12.13 7.43 o -8 1 1 557.83 563.75 10.17 o -7 1 1 206.02 187.97 11.65 o -6 1 1 61.78 88.09 14.44 o -5 1 1 535.79 594.56 8.02 o -4 1 1 2714.79 2701.61 22.89 o -3 1 1 4174.47 4144.30 37.08 o -2 1 1 8.36 8.17 2.19 o 2 1 1 4112.59 3774.43 42.13 o 3 1 1 8082.97 7773.71 96.04 o 4 1 1 7852.28 7563.39 74.01 o 5 1 1 19298.20 18962.55 181.34 o 6 1 1 46.99 40.17 5.40 o 7 1 1 1328.31 1361.66 17.16 o 8 1 1 732.29 786.24 13.90 o 9 1 1 1008.66 990.67 17.17 o 10 1 1 1097.88 1063.20 20.53 o 11 1 1 535.32 494.02 14.48 o 12 1 1 2284.90 2360.32 45.37 o 13 1 1 146.15 129.28 19.29 o 14 1 1 94.57 78.88 18.04 o 15 1 1 398.79 424.70 28.13 o 16 1 1 45.42 55.16 29.57 o 17 1 1 146.15 162.80 23.52 o 18 1 1 547.83 566.92 30.55 o 19 1 1 30.41 45.43 25.18 o 20 1 1 267.90 291.97 35.47 o 21 1 1 3.95 -4.35 14.44 o -21 2 1 0.89 -11.45 36.41 o -20 2 1 13.40 -17.03 33.12 o -19 2 1 341.56 371.16 52.18 o -18 2 1 61.52 84.04 24.85 o -17 2 1 23.04 -5.43 21.34 o -16 2 1 775.48 832.34 34.86 o -15 2 1 1703.04 1703.35 39.33 o -14 2 1 471.38 470.88 15.51 o -13 2 1 907.98 878.36 24.27 o -12 2 1 605.10 670.92 15.67 o -11 2 1 1362.29 1415.10 21.65 o -10 2 1 240.43 228.83 9.59 o -9 2 1 357.11 322.10 9.30 o -8 2 1 374.32 298.28 7.41 o -7 2 1 304.58 250.77 6.83 o -6 2 1 1265.94 1183.29 17.39 o -5 2 1 5374.66 5348.29 44.22 o -4 2 1 5816.30 5537.92 46.94 o -3 2 1 5762.56 5633.69 49.51 o -2 2 1 25661.83 24924.10 234.47 o -1 2 1 30.29 32.90 1.24 o 0 2 1 10494.62 10045.45 99.25 o 1 2 1 13644.67 13028.56 127.69 o 2 2 1 48.79 52.08 6.13 o 3 2 1 19070.29 18018.65 172.46 o 4 2 1 4084.91 4003.61 38.29 o 5 2 1 125.34 106.57 4.78 o 6 2 1 1603.88 1713.81 18.23 o 7 2 1 2009.74 1861.81 21.34 o 8 2 1 636.08 570.70 24.20 o 9 2 1 1325.50 1260.70 19.36 o 10 2 1 1612.99 1759.26 28.77 o 11 2 1 3.78 1.81 10.10 o 12 2 1 10.55 11.88 11.19 o 13 2 1 1161.23 1152.21 25.12 o 14 2 1 649.73 639.11 19.66 o 15 2 1 796.91 773.50 36.52 o 16 2 1 200.55 211.94 20.75 o 17 2 1 331.42 376.06 26.12 o 18 2 1 36.44 49.85 25.18 o 19 2 1 271.04 303.81 40.38 o 20 2 1 10.16 7.10 31.71 o 21 2 1 9.67 -26.12 43.59 o -21 3 1 98.59 115.31 40.33 o -20 3 1 8.49 -19.31 43.86 o -19 3 1 44.81 36.94 62.77 o -18 3 1 346.85 363.57 27.95 o -17 3 1 15.04 4.23 23.69 o -16 3 1 2.94 11.83 34.71 o -15 3 1 126.56 99.21 18.00 o -14 3 1 20.55 8.04 10.84 o -13 3 1 595.76 596.10 16.43 o -12 3 1 1395.58 1369.28 30.17 o -11 3 1 2.31 4.09 9.00 o -10 3 1 1378.47 1465.78 29.87 o -9 3 1 429.65 485.51 10.27 o -8 3 1 900.32 984.15 15.88 o -7 3 1 176.81 179.84 10.89 o -6 3 1 3276.55 3584.52 32.94 o -5 3 1 5110.44 5306.73 47.56 o -4 3 1 3916.40 3912.53 33.89 o -3 3 1 23.16 27.40 2.13 o -2 3 1 1485.67 1519.26 16.00 o -1 3 1 27201.68 27061.01 278.74 o 0 3 1 623.05 535.52 8.23 o 1 3 1 14339.93 13715.74 142.26 o 2 3 1 3435.68 3283.07 37.89 o 3 3 1 5117.62 5015.32 46.73 o 4 3 1 8847.90 8708.58 84.53 o 5 3 1 10351.81 10800.73 105.66 o 6 3 1 902.16 1049.45 12.46 o 7 3 1 3.90 8.67 4.72 o 8 3 1 26.03 22.77 8.24 o 9 3 1 195.72 237.03 13.08 o 10 3 1 191.23 202.25 9.79 o 11 3 1 37.92 48.88 9.34 o 12 3 1 346.70 335.41 13.37 o 13 3 1 36.75 63.62 11.07 o 14 3 1 556.79 557.18 17.64 o 15 3 1 0.03 -18.30 13.50 o 16 3 1 1.77 -19.23 17.73 o 17 3 1 2.69 11.29 21.10 o 18 3 1 2.58 5.09 24.57 o 19 3 1 70.76 61.41 27.29 o 20 3 1 2.28 13.58 34.84 o -20 4 1 29.81 -22.46 39.19 o -19 4 1 10.53 41.01 31.33 o -18 4 1 77.67 57.44 29.16 o -17 4 1 11.14 -3.71 21.67 o -16 4 1 58.93 51.01 21.61 o -15 4 1 7.64 -18.18 20.78 o -14 4 1 102.00 85.66 13.83 o -13 4 1 3573.72 3674.21 106.10 o -12 4 1 600.26 567.91 16.31 o -11 4 1 147.81 127.76 11.49 o -10 4 1 19.00 27.89 11.19 o -9 4 1 171.95 151.27 18.22 o -8 4 1 13.28 10.42 5.29 o -7 4 1 146.71 176.55 6.91 o -6 4 1 43.48 26.85 4.65 o -5 4 1 7151.58 7395.82 60.94 o -4 4 1 47.75 39.10 2.87 o -3 4 1 172.73 183.78 4.82 o -2 4 1 2685.50 2656.17 36.15 o -1 4 1 3006.94 3174.65 35.52 o 0 4 1 205.81 184.21 5.58 o 1 4 1 58.40 58.68 3.42 o 2 4 1 1957.38 2145.79 21.55 o 3 4 1 162.56 156.21 3.74 o 4 4 1 30.65 32.65 6.13 o 5 4 1 1389.88 1381.72 17.29 o 6 4 1 5670.54 5953.27 59.41 o 7 4 1 578.76 568.34 10.21 o 8 4 1 135.81 145.69 7.49 o 9 4 1 261.72 251.97 8.57 o 10 4 1 288.64 303.08 18.07 o 11 4 1 332.96 371.05 22.01 o 12 4 1 894.70 898.70 20.59 o 13 4 1 431.83 399.76 14.91 o 14 4 1 252.74 210.55 16.38 o 15 4 1 23.91 38.79 12.75 o 16 4 1 0.49 -21.48 20.84 o 17 4 1 5.72 36.91 21.08 o 18 4 1 66.51 97.98 30.52 o 19 4 1 23.72 20.36 37.38 o 20 4 1 29.74 -39.52 53.01 o -20 5 1 0.45 40.56 73.88 o -19 5 1 54.69 71.61 86.28 o -18 5 1 227.06 250.95 50.67 o -17 5 1 11.30 46.19 26.16 o -16 5 1 95.15 117.98 25.33 o -15 5 1 15.89 14.61 30.10 o -14 5 1 0.31 8.84 12.40 o -13 5 1 239.20 241.65 14.52 o -12 5 1 27.80 56.61 20.49 o -11 5 1 111.53 118.89 11.13 o -10 5 1 49.56 45.72 9.32 o -9 5 1 540.26 487.68 20.72 o -8 5 1 488.16 458.04 12.40 o -7 5 1 381.88 403.48 8.82 o -6 5 1 566.88 601.59 10.03 o -5 5 1 1540.43 1488.65 18.71 o -4 5 1 9679.65 9850.04 98.28 o -3 5 1 48.82 63.77 4.05 o -2 5 1 232.84 270.60 5.47 o -1 5 1 292.76 235.84 4.58 o 0 5 1 1567.29 1470.51 18.64 o 1 5 1 24.02 37.81 2.99 o 2 5 1 959.94 976.20 12.10 o 3 5 1 512.14 482.85 10.68 o 4 5 1 8.51 4.73 7.78 o 5 5 1 27.21 36.91 3.47 o 6 5 1 1078.89 1006.27 14.73 o 7 5 1 66.65 58.92 7.29 o 8 5 1 481.36 503.65 17.47 o 9 5 1 1545.98 1497.91 51.04 o 10 5 1 1017.61 1022.31 20.70 o 11 5 1 1.87 -8.77 10.07 o 12 5 1 15.60 12.79 12.02 o 13 5 1 41.01 45.31 18.07 o 14 5 1 6.76 1.07 19.59 o 15 5 1 476.40 468.75 24.26 o 16 5 1 42.80 44.03 25.40 o 17 5 1 332.84 384.89 78.42 o 18 5 1 28.73 83.50 36.37 o 19 5 1 43.97 40.42 30.41 o -19 6 1 78.05 105.19 34.23 o -18 6 1 241.73 301.81 38.85 o -17 6 1 25.86 35.63 29.40 o -16 6 1 0.06 24.98 48.47 o -15 6 1 195.58 199.72 23.41 o -14 6 1 23.27 28.74 18.69 o -13 6 1 648.45 674.74 25.72 o -12 6 1 982.41 977.86 25.41 o -11 6 1 75.72 96.50 13.38 o -10 6 1 917.33 838.79 19.40 o -9 6 1 64.43 70.76 5.12 o -8 6 1 0.90 6.93 6.53 o -7 6 1 284.99 282.69 7.47 o -6 6 1 529.59 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