#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2013632.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013632_Fobs loop_ _publ_author_name 'Bull, Ivor' 'Parise, John B.' _publ_section_title ; Cs[Si~3~O~6~(OH)] and Rb[Si~2~O~4~(OH)]: two novel phyllosilicates ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first i100 _journal_page_last i102 _journal_volume 59 _journal_year 2003 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2n 2ac' _symmetry_space_group_name_H-M 'P c m n' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 4.8147 _cell_length_b 8.2670 _cell_length_c 12.8140 _exptl_crystal_F_000 424.00 _reflns_d_resolution_high 0.7524 _[local]_cod_data_source_file iz1030IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' orbscsi in P c m n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 178.78 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z+1/2' 'x+1/2, -y, -z+1/2' '-x, y+1/2, -z' '-x, -y, -z' 'x-1/2, y-1/2, -z-1/2' '-x-1/2, y, z-1/2' 'x, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 16836.86 17119.70 605.39 o 4 0 0 6663.49 6557.21 109.72 o 6 0 0 971.80 974.89 56.32 o 1 1 0 783.63 722.21 14.05 o 3 1 0 707.97 689.20 16.60 o 5 1 0 1429.15 1444.06 42.30 o 0 2 0 277.30 476.04 9.64 o 2 2 0 6656.73 7340.94 159.97 o 4 2 0 26.74 22.48 7.32 o 6 2 0 138.71 123.32 32.04 o 1 3 0 822.11 988.12 26.83 o 3 3 0 1166.54 1195.38 42.36 o 5 3 0 214.62 228.62 25.58 o 0 4 0 27608.99 27069.52 1071.99 o 2 4 0 3946.24 4278.07 65.14 o 4 4 0 485.49 492.83 21.46 o 1 5 0 1678.05 1673.76 25.20 o 3 5 0 254.20 266.53 14.10 o 5 5 0 1525.50 1445.98 101.00 o 0 6 0 10902.59 10364.52 136.91 o 2 6 0 8740.03 8608.03 185.26 o 4 6 0 3288.63 3237.15 52.77 o 1 7 0 174.60 175.18 14.23 o 3 7 0 622.60 627.81 22.06 o 0 8 0 436.74 418.50 33.99 o 2 8 0 184.42 188.42 15.86 o 4 8 0 462.96 501.16 37.30 o 1 9 0 180.24 195.09 21.46 o 3 9 0 71.75 70.76 21.25 o 1 0 1 2262.50 1973.89 38.87 o 2 0 1 767.75 863.01 28.63 o 3 0 1 3386.20 3479.56 61.67 o 4 0 1 8.22 3.67 7.70 o 5 0 1 227.72 249.17 20.56 o 6 0 1 309.94 298.81 25.40 o 1 1 1 6569.59 6766.83 131.66 o 2 1 1 1746.37 1695.97 29.69 o 3 1 1 840.69 839.84 22.59 o 4 1 1 1521.89 1505.46 24.44 o 5 1 1 184.76 198.07 13.95 o 6 1 1 510.27 493.36 24.73 o 1 2 1 22507.04 21477.93 241.49 o 2 2 1 1247.66 1453.06 31.08 o 3 2 1 3363.68 3500.91 81.98 o 4 2 1 37.34 37.73 5.98 o 5 2 1 701.75 735.58 19.75 o 6 2 1 1.45 2.50 14.37 o 1 3 1 848.37 772.01 22.88 o 2 3 1 1800.59 1741.33 16.13 o 3 3 1 938.72 990.35 14.85 o 4 3 1 1655.92 1750.90 36.26 o 5 3 1 1254.48 1222.45 35.46 o 1 4 1 4213.59 3977.89 43.51 o 2 4 1 121.90 131.40 4.27 o 3 4 1 3915.39 3593.72 51.53 o 4 4 1 4.72 -1.55 5.58 o 5 4 1 568.18 603.33 19.89 o 1 5 1 6708.99 6672.43 110.20 o 2 5 1 617.10 587.77 10.11 o 3 5 1 1730.43 1733.68 23.96 o 4 5 1 782.59 758.99 17.99 o 5 5 1 902.85 899.37 21.33 o 1 6 1 3403.62 3531.60 48.99 o 2 6 1 45.68 41.54 4.72 o 3 6 1 464.58 459.08 12.84 o 4 6 1 83.70 93.39 8.50 o 5 6 1 43.13 47.03 9.33 o 1 7 1 3.60 4.92 5.38 o 2 7 1 637.55 641.26 14.23 o 3 7 1 6.09 -0.77 5.45 o 4 7 1 674.09 646.31 17.26 o 1 8 1 3036.52 3055.81 65.26 o 2 8 1 3.53 1.73 6.30 o 3 8 1 2297.27 2292.43 35.54 o 4 8 1 8.55 -12.22 12.22 o 1 9 1 16.07 10.35 8.22 o 2 9 1 207.54 211.25 12.91 o 3 9 1 70.95 66.45 13.82 o 1 10 1 735.56 715.02 25.84 o 2 10 1 0.34 -4.16 11.88 o 0 0 2 114.05 148.09 8.93 o 1 0 2 30.11 33.58 3.41 o 2 0 2 3458.15 3580.23 87.57 o 3 0 2 6.02 3.08 5.55 o 4 0 2 399.43 370.50 17.62 o 5 0 2 516.43 525.92 28.49 o 6 0 2 2.37 3.72 12.30 o 0 1 2 229.30 225.08 5.07 o 1 1 2 332.95 312.50 7.90 o 2 1 2 105.64 87.63 4.33 o 3 1 2 2476.85 2431.36 24.80 o 4 1 2 72.09 67.84 7.27 o 5 1 2 559.34 535.60 18.98 o 6 1 2 10.59 3.22 8.93 o 0 2 2 21687.49 19951.24 130.78 o 1 2 2 1140.11 1166.44 18.01 o 2 2 2 6760.16 6127.70 82.52 o 3 2 2 2480.56 2547.87 31.63 o 4 2 2 6717.17 6714.06 94.32 o 5 2 2 65.20 66.60 8.75 o 6 2 2 345.39 365.66 60.20 o 0 3 2 5063.65 4900.02 79.75 o 1 3 2 2684.04 2770.41 32.76 o 2 3 2 5880.57 5768.76 69.93 o 3 3 2 948.43 919.23 14.22 o 4 3 2 1535.90 1609.77 39.64 o 5 3 2 1648.18 1721.80 50.51 o 0 4 2 5567.54 5277.80 101.12 o 1 4 2 2.90 2.26 2.97 o 2 4 2 4712.01 4682.01 73.13 o 3 4 2 118.96 110.63 6.84 o 4 4 2 467.65 470.06 13.16 o 5 4 2 484.59 457.47 17.23 o 0 5 2 63.77 90.32 7.86 o 1 5 2 18.15 20.79 3.77 o 2 5 2 365.09 375.66 8.63 o 3 5 2 1888.23 1890.66 32.03 o 4 5 2 18.96 17.10 6.50 o 5 5 2 91.26 87.39 10.70 o 0 6 2 365.57 360.36 16.44 o 1 6 2 403.17 374.87 20.06 o 2 6 2 686.17 682.20 13.50 o 3 6 2 375.01 356.62 10.47 o 4 6 2 176.97 188.44 11.72 o 5 6 2 11.31 7.00 10.34 o 0 7 2 861.79 831.43 30.50 o 1 7 2 691.45 665.51 17.95 o 2 7 2 1169.65 1171.70 25.55 o 3 7 2 283.11 298.86 13.73 o 4 7 2 210.08 207.07 12.39 o 0 8 2 6803.34 6358.34 91.64 o 1 8 2 0.65 -1.29 6.53 o 2 8 2 2990.44 3008.95 63.04 o 3 8 2 247.60 283.35 17.48 o 4 8 2 1748.58 1941.05 159.75 o 0 9 2 548.81 496.95 28.81 o 1 9 2 28.28 24.54 9.45 o 2 9 2 349.09 382.89 17.02 o 3 9 2 606.48 576.84 23.59 o 0 10 2 36.20 31.19 14.75 o 1 10 2 114.40 107.52 13.69 o 2 10 2 320.32 279.65 42.72 o 1 0 3 31961.81 29867.84 281.13 o 2 0 3 3484.72 3922.11 134.73 o 3 0 3 11104.30 10964.54 225.65 o 4 0 3 609.42 563.94 28.20 o 5 0 3 1877.69 1912.98 49.78 o 6 0 3 11.29 15.05 15.11 o 1 1 3 2294.91 2151.74 44.16 o 2 1 3 182.54 162.91 5.14 o 3 1 3 795.95 808.03 13.94 o 4 1 3 753.65 734.46 19.67 o 5 1 3 35.42 42.60 8.77 o 6 1 3 450.52 423.93 20.99 o 1 2 3 2931.11 3209.87 51.77 o 2 2 3 26.23 21.55 3.17 o 3 2 3 41.83 64.94 4.77 o 4 2 3 793.97 744.32 18.72 o 5 2 3 71.00 64.14 8.88 o 6 2 3 751.24 832.15 52.43 o 1 3 3 5893.12 5514.62 64.78 o 2 3 3 96.78 90.88 4.63 o 3 3 3 2609.40 2517.23 44.70 o 4 3 3 126.00 129.22 7.09 o 5 3 3 821.56 827.53 32.15 o 1 4 3 5786.80 5768.08 106.84 o 2 4 3 1909.19 1887.26 17.64 o 3 4 3 1732.05 1709.15 30.65 o 4 4 3 488.16 468.72 14.56 o 5 4 3 98.69 112.67 12.20 o 1 5 3 438.14 426.54 9.31 o 2 5 3 141.95 164.05 7.75 o 3 5 3 134.92 152.81 8.39 o 4 5 3 781.11 802.98 18.82 o 5 5 3 34.73 21.33 9.24 o 1 6 3 8284.11 8205.37 93.57 o 2 6 3 18.22 14.22 4.50 o 3 6 3 3125.32 3166.50 37.08 o 4 6 3 351.25 339.12 15.08 o 5 6 3 694.99 768.61 35.42 o 1 7 3 1381.87 1370.43 28.44 o 2 7 3 86.65 83.72 8.01 o 3 7 3 687.97 703.03 16.45 o 4 7 3 83.48 75.94 9.50 o 1 8 3 71.19 66.77 9.31 o 2 8 3 563.74 563.60 18.05 o 3 8 3 59.13 40.00 9.90 o 4 8 3 192.22 230.13 44.67 o 1 9 3 804.51 755.66 22.27 o 2 9 3 16.78 2.95 7.46 o 3 9 3 377.61 386.44 28.21 o 1 10 3 2306.28 2454.28 53.25 o 2 10 3 10.73 14.01 13.23 o 0 0 4 8084.68 8707.94 385.49 o 1 0 4 2879.54 3516.26 55.47 o 2 0 4 1303.98 1277.56 13.78 o 3 0 4 1225.36 1166.21 26.58 o 4 0 4 1864.63 1898.37 38.66 o 5 0 4 1224.27 1084.97 46.12 o 6 0 4 7.03 -12.62 12.62 o 0 1 4 16915.16 16951.70 142.26 o 1 1 4 322.75 325.16 11.17 o 2 1 4 9926.05 10423.63 128.04 o 3 1 4 289.37 293.41 11.06 o 4 1 4 1255.90 1204.40 18.74 o 5 1 4 422.99 422.64 15.51 o 6 1 4 182.91 190.68 18.94 o 0 2 4 3695.86 3512.30 102.72 o 1 2 4 2968.88 3227.93 55.28 o 2 2 4 3944.12 4055.79 58.65 o 3 2 4 148.65 152.22 7.04 o 4 2 4 69.81 84.56 7.51 o 5 2 4 194.30 192.01 11.25 o 6 2 4 157.65 134.43 17.54 o 0 3 4 2898.67 3108.68 71.58 o 1 3 4 44.10 54.92 4.74 o 2 3 4 142.24 160.62 7.16 o 3 3 4 842.01 876.12 17.21 o 4 3 4 218.71 228.29 10.08 o 5 3 4 130.85 146.34 11.42 o 0 4 4 2726.44 2834.78 24.89 o 1 4 4 464.04 521.46 10.34 o 2 4 4 1367.45 1314.59 19.46 o 3 4 4 266.44 255.66 9.13 o 4 4 4 835.03 821.53 30.46 o 5 4 4 628.83 579.36 23.25 o 0 5 4 10017.68 10054.60 172.67 o 1 5 4 448.61 456.69 15.46 o 2 5 4 11878.66 11588.15 118.81 o 3 5 4 39.85 49.13 6.13 o 4 5 4 1946.16 1731.77 39.91 o 5 5 4 426.81 442.56 18.32 o 0 6 4 2692.36 2702.91 94.66 o 1 6 4 270.59 299.53 11.05 o 2 6 4 1036.88 1029.75 18.16 o 3 6 4 637.56 651.60 15.38 o 4 6 4 232.85 236.66 14.66 o 5 6 4 237.19 243.72 40.78 o 0 7 4 2366.88 2182.31 57.55 o 1 7 4 8.83 12.68 6.13 o 2 7 4 138.90 165.03 10.90 o 3 7 4 380.33 386.49 14.40 o 4 7 4 28.14 35.51 9.62 o 0 8 4 417.52 421.52 34.96 o 1 8 4 3.42 -1.89 6.84 o 2 8 4 808.55 817.73 22.77 o 3 8 4 9.03 10.96 9.24 o 4 8 4 118.25 136.91 39.81 o 0 9 4 301.40 331.04 27.11 o 1 9 4 52.05 35.08 10.16 o 2 9 4 414.07 477.10 19.84 o 3 9 4 34.50 8.29 14.92 o 0 10 4 899.72 912.44 40.85 o 1 10 4 3.10 3.80 9.69 o 2 10 4 169.34 167.35 24.26 o 1 0 5 183.86 183.00 10.34 o 2 0 5 2831.33 2794.43 29.95 o 3 0 5 1943.52 2159.88 79.56 o 4 0 5 724.13 697.97 22.28 o 5 0 5 211.50 211.19 18.71 o 6 0 5 246.37 261.20 37.87 o 1 1 5 5275.71 4799.40 111.52 o 2 1 5 549.67 596.49 15.11 o 3 1 5 1469.80 1493.30 18.13 o 4 1 5 151.36 171.41 9.44 o 5 1 5 164.48 148.95 10.67 o 6 1 5 29.47 28.16 20.39 o 1 2 5 2663.52 2491.64 32.66 o 2 2 5 248.36 253.35 6.45 o 3 2 5 6634.18 6980.94 132.72 o 4 2 5 1618.65 1609.91 27.43 o 5 2 5 1371.09 1374.76 24.73 o 6 2 5 570.84 569.98 51.46 o 1 3 5 7557.92 7740.74 115.03 o 2 3 5 374.98 357.62 11.56 o 3 3 5 3666.22 3698.92 69.72 o 4 3 5 731.93 708.90 18.35 o 5 3 5 579.67 574.66 22.30 o 1 4 5 1455.48 1475.27 29.64 o 2 4 5 1574.82 1536.15 31.33 o 3 4 5 105.23 120.12 7.86 o 4 4 5 713.57 690.89 18.95 o 5 4 5 196.28 202.06 14.67 o 1 5 5 1863.88 1925.23 33.17 o 2 5 5 299.96 309.49 10.49 o 3 5 5 348.28 332.16 11.49 o 4 5 5 5.40 2.30 6.79 o 5 5 5 37.96 27.47 9.97 o 1 6 5 392.79 349.28 13.62 o 2 6 5 173.16 204.73 10.10 o 3 6 5 9.36 3.08 6.08 o 4 6 5 571.54 570.23 21.23 o 1 7 5 2172.77 2224.28 50.33 o 2 7 5 70.69 75.34 8.43 o 3 7 5 1246.93 1223.35 41.05 o 4 7 5 296.49 292.25 17.93 o 1 8 5 2874.17 2853.28 45.89 o 2 8 5 442.69 443.06 16.08 o 3 8 5 1537.88 1938.16 64.88 o 1 9 5 1345.70 1420.47 35.12 o 2 9 5 162.21 170.62 12.94 o 3 9 5 446.77 481.02 39.12 o 1 10 5 107.39 103.90 26.22 o 0 0 6 994.47 858.77 37.38 o 1 0 6 2768.95 2868.17 65.36 o 2 0 6 5627.39 6117.86 101.62 o 3 0 6 239.31 246.87 11.87 o 4 0 6 2234.91 2216.27 57.60 o 5 0 6 985.59 979.36 30.38 o 0 1 6 4712.14 4584.55 54.36 o 1 1 6 44.60 56.88 5.47 o 2 1 6 1711.94 1591.58 29.36 o 3 1 6 1.99 -0.26 4.67 o 4 1 6 674.01 711.83 16.27 o 5 1 6 20.79 14.43 8.42 o 0 2 6 1820.42 2005.40 53.34 o 1 2 6 8.10 2.98 3.49 o 2 2 6 241.19 261.81 8.93 o 3 2 6 3573.20 3548.90 40.26 o 4 2 6 393.87 377.64 14.48 o 5 2 6 559.99 586.83 18.06 o 0 3 6 8617.34 9044.57 157.41 o 1 3 6 20.19 20.26 3.59 o 2 3 6 12274.75 13001.84 149.28 o 3 3 6 82.98 92.03 7.68 o 4 3 6 2434.69 2371.39 57.51 o 5 3 6 2.33 -4.86 8.80 o 0 4 6 5.40 5.68 5.88 o 1 4 6 757.63 768.31 12.78 o 2 4 6 557.70 564.81 14.55 o 3 4 6 693.79 676.21 16.77 o 4 4 6 301.53 339.34 15.46 o 5 4 6 762.52 775.02 27.02 o 0 5 6 1574.15 1624.61 70.81 o 1 5 6 83.42 88.84 7.35 o 2 5 6 49.04 53.03 6.89 o 3 5 6 31.93 32.23 6.71 o 4 5 6 176.47 180.62 14.88 o 5 5 6 33.46 10.75 14.65 o 0 6 6 2948.97 3126.07 100.98 o 1 6 6 238.52 250.35 13.67 o 2 6 6 1088.51 1015.21 20.36 o 3 6 6 608.68 587.03 17.87 o 4 6 6 164.89 158.31 13.48 o 0 7 6 2010.20 2153.74 66.51 o 1 7 6 18.86 12.79 7.05 o 2 7 6 3477.89 3434.52 52.54 o 3 7 6 15.86 9.87 7.88 o 4 7 6 476.73 540.85 39.95 o 0 8 6 246.84 230.26 24.00 o 1 8 6 31.21 31.10 10.24 o 2 8 6 149.54 133.26 12.47 o 3 8 6 814.02 832.61 26.61 o 0 9 6 2068.59 2215.68 151.48 o 1 9 6 21.14 16.25 10.01 o 2 9 6 899.55 940.02 26.59 o 1 0 7 2564.80 2456.96 126.98 o 2 0 7 230.04 220.76 15.99 o 3 0 7 277.13 267.47 13.92 o 4 0 7 1375.75 1354.22 63.35 o 5 0 7 55.70 48.13 12.67 o 1 1 7 12087.36 11474.14 145.27 o 2 1 7 65.96 66.82 6.36 o 3 1 7 3926.71 3996.56 109.40 o 4 1 7 5.32 5.27 6.11 o 5 1 7 587.05 600.80 18.69 o 1 2 7 651.48 576.75 12.84 o 2 2 7 530.27 541.37 14.42 o 3 2 7 16.18 8.83 6.82 o 4 2 7 361.14 376.91 15.29 o 5 2 7 3.42 -6.36 8.29 o 1 3 7 1147.32 1090.18 21.27 o 2 3 7 88.39 90.75 7.48 o 3 3 7 53.59 61.08 9.23 o 4 3 7 113.77 122.54 11.19 o 5 3 7 159.83 186.28 16.28 o 1 4 7 272.60 258.24 9.84 o 2 4 7 107.89 124.65 9.10 o 3 4 7 22.37 24.28 7.51 o 4 4 7 631.66 647.62 29.42 o 5 4 7 13.48 5.58 10.73 o 1 5 7 10722.49 10678.18 106.97 o 2 5 7 21.34 21.70 6.59 o 3 5 7 4665.33 4287.13 69.12 o 4 5 7 7.31 -1.69 8.30 o 1 6 7 107.09 100.67 10.43 o 2 6 7 401.23 411.99 17.44 o 3 6 7 389.04 382.47 16.92 o 4 6 7 464.66 464.97 22.44 o 1 7 7 1314.92 1245.77 27.34 o 2 7 7 31.87 26.42 8.73 o 3 7 7 273.51 271.35 17.53 o 4 7 7 51.81 63.01 21.94 o 1 8 7 46.29 34.14 10.19 o 2 8 7 24.20 21.72 9.40 o 3 8 7 267.58 283.30 19.19 o 1 9 7 695.29 722.28 30.70 o 2 9 7 10.65 9.14 10.40 o 0 0 8 11543.69 11428.48 807.88 o 1 0 8 11.27 16.46 8.36 o 2 0 8 3891.94 3833.94 172.47 o 3 0 8 2553.89 2386.62 133.03 o 4 0 8 825.66 893.73 28.14 o 5 0 8 99.58 84.12 17.25 o 0 1 8 5207.67 5476.19 155.21 o 1 1 8 4.71 2.16 4.81 o 2 1 8 4237.19 4184.91 99.93 o 3 1 8 45.27 46.24 8.83 o 4 1 8 631.93 621.58 19.53 o 5 1 8 94.11 93.57 11.37 o 0 2 8 1148.90 1060.43 51.69 o 1 2 8 313.71 337.47 12.34 o 2 2 8 416.15 415.55 14.18 o 3 2 8 61.90 72.81 10.10 o 4 2 8 494.88 483.51 17.91 o 5 2 8 1336.74 1344.75 50.33 o 0 3 8 6320.41 5990.61 98.67 o 1 3 8 31.22 26.47 6.69 o 2 3 8 1341.85 1362.28 23.82 o 3 3 8 7.42 8.63 7.30 o 4 3 8 992.18 1013.25 27.32 o 5 3 8 1.63 2.92 10.34 o 0 4 8 1186.32 1009.25 44.01 o 1 4 8 158.26 155.68 9.06 o 2 4 8 84.07 75.41 8.06 o 3 4 8 1133.28 1177.48 25.81 o 4 4 8 53.85 50.09 12.08 o 5 4 8 159.64 150.51 37.87 o 0 5 8 2117.29 1804.75 37.13 o 1 5 8 36.82 29.70 7.75 o 2 5 8 3659.50 3541.32 70.79 o 3 5 8 76.12 74.01 9.38 o 4 5 8 199.65 180.56 21.11 o 0 6 8 1399.04 1411.89 48.00 o 1 6 8 2.02 -0.34 7.41 o 2 6 8 1290.24 1339.99 28.18 o 3 6 8 279.26 300.70 17.42 o 4 6 8 475.39 484.40 23.65 o 0 7 8 2712.47 2484.18 63.46 o 1 7 8 13.47 7.40 7.81 o 2 7 8 601.69 595.36 22.05 o 3 7 8 1.51 4.23 12.22 o 0 8 8 267.96 290.74 29.16 o 1 8 8 268.01 287.52 19.47 o 2 8 8 541.93 511.84 21.05 o 3 8 8 140.79 171.25 21.77 o 0 9 8 760.63 821.91 51.95 o 1 9 8 4.72 5.05 12.86 o 2 9 8 834.68 762.97 36.63 o 1 0 9 15.14 29.16 9.42 o 2 0 9 6.73 0.17 9.50 o 3 0 9 33.07 31.11 20.88 o 4 0 9 584.91 541.67 33.98 o 5 0 9 95.08 77.79 16.44 o 1 1 9 1053.33 1046.05 23.23 o 2 1 9 175.81 184.41 13.96 o 3 1 9 618.63 561.89 20.61 o 4 1 9 283.55 309.47 16.11 o 5 1 9 71.73 51.95 11.56 o 1 2 9 1443.82 1316.63 37.27 o 2 2 9 2187.07 2131.02 72.89 o 3 2 9 225.61 222.61 15.27 o 4 2 9 602.20 605.83 21.30 o 5 2 9 108.36 96.10 17.77 o 1 3 9 8622.64 8253.96 80.54 o 2 3 9 330.84 320.23 13.67 o 3 3 9 4638.75 4407.03 88.81 o 4 3 9 207.04 212.46 16.29 o 1 4 9 277.36 285.25 15.76 o 2 4 9 49.27 71.25 9.07 o 3 4 9 182.28 197.70 13.69 o 4 4 9 643.33 675.76 24.77 o 1 5 9 42.87 38.99 8.49 o 2 5 9 46.64 49.01 9.84 o 3 5 9 30.31 31.72 9.14 o 4 5 9 220.58 194.23 18.68 o 1 6 9 91.68 91.93 11.30 o 2 6 9 600.50 614.37 21.06 o 3 6 9 2.60 -0.86 8.90 o 4 6 9 157.69 145.74 25.00 o 1 7 9 2173.16 2091.82 52.34 o 2 7 9 158.47 150.16 14.84 o 3 7 9 1002.26 924.09 45.85 o 1 8 9 426.86 416.41 22.88 o 2 8 9 101.03 118.49 14.09 o 0 0 10 726.10 779.42 35.62 o 1 0 10 1443.08 1454.54 39.52 o 2 0 10 13.87 16.17 12.40 o 3 0 10 184.26 269.49 28.44 o 4 0 10 217.82 243.73 27.44 o 0 1 10 5209.27 5201.35 161.46 o 1 1 10 92.69 133.90 11.01 o 2 1 10 2428.69 2166.29 39.66 o 3 1 10 524.12 537.72 24.09 o 4 1 10 954.37 865.61 30.48 o 5 1 10 152.71 132.06 30.10 o 0 2 10 5016.82 5051.44 66.71 o 1 2 10 487.45 449.54 16.25 o 2 2 10 1671.96 1640.33 37.03 o 3 2 10 149.49 170.45 16.66 o 4 2 10 979.67 1104.89 32.31 o 5 2 10 132.84 116.52 30.10 o 0 3 10 101.87 112.86 16.11 o 1 3 10 371.03 373.98 16.70 o 2 3 10 573.41 491.72 19.72 o 3 3 10 440.85 459.08 21.71 o 4 3 10 26.96 29.78 11.30 o 0 4 10 285.12 266.38 26.06 o 1 4 10 415.51 402.21 23.62 o 2 4 10 672.76 645.13 20.79 o 3 4 10 173.60 174.55 14.60 o 4 4 10 135.24 142.26 15.56 o 0 5 10 6343.37 6058.91 134.48 o 1 5 10 3.61 2.92 8.62 o 2 5 10 1933.03 1929.99 39.31 o 3 5 10 366.83 372.19 17.38 o 4 5 10 1411.59 1298.82 55.27 o 0 6 10 35.90 33.37 14.92 o 1 6 10 2.37 -3.78 9.65 o 2 6 10 10.71 0.11 9.35 o 3 6 10 40.49 56.21 14.10 o 0 7 10 185.50 194.77 28.19 o 1 7 10 176.04 158.27 16.99 o 2 7 10 676.28 644.49 24.79 o 3 7 10 144.37 165.76 28.84 o 0 8 10 1441.46 1566.00 57.77 o 1 8 10 3.49 -2.88 11.15 o 2 8 10 1039.70 1103.42 77.20 o 1 0 11 8723.43 8711.21 395.10 o 2 0 11 1.80 0.38 14.46 o 3 0 11 1928.95 1690.49 59.84 o 4 0 11 118.49 119.67 24.69 o 1 1 11 2024.88 2102.74 45.50 o 2 1 11 230.27 269.25 18.75 o 3 1 11 861.68 819.56 31.37 o 4 1 11 344.10 384.41 24.50 o 1 2 11 55.82 62.86 10.64 o 2 2 11 125.02 140.33 14.78 o 3 2 11 86.21 70.69 14.85 o 4 2 11 89.42 90.65 15.05 o 1 3 11 246.89 259.68 18.22 o 2 3 11 44.12 58.56 11.05 o 3 3 11 54.84 21.02 11.36 o 4 3 11 173.94 221.50 19.60 o 1 4 11 1910.05 1828.58 45.46 o 2 4 11 4.30 -7.12 9.47 o 3 4 11 139.81 138.57 15.13 o 4 4 11 63.87 61.47 17.39 o 1 5 11 1960.49 1925.59 63.91 o 2 5 11 247.32 265.83 18.54 o 3 5 11 927.75 888.35 61.14 o 1 6 11 2090.63 2067.06 80.45 o 2 6 11 98.31 105.48 17.13 o 3 6 11 1377.80 1328.43 110.69 o 1 7 11 307.72 272.32 22.29 o 2 7 11 20.89 15.87 15.28 o 0 0 12 2112.93 2310.66 96.62 o 1 0 12 12.35 -1.06 11.55 o 2 0 12 878.13 893.26 133.03 o 3 0 12 137.76 133.17 25.29 o 4 0 12 1074.32 1030.92 53.34 o 0 1 12 11.87 16.26 12.68 o 1 1 12 128.12 147.14 13.76 o 2 1 12 39.66 23.14 12.61 o 3 1 12 296.27 311.41 24.14 o 4 1 12 13.07 -7.12 11.59 o 0 2 12 1876.83 2010.62 118.70 o 1 2 12 109.63 112.81 13.06 o 2 2 12 1250.73 1198.48 57.32 o 3 2 12 24.03 22.03 14.15 o 4 2 12 15.30 -1.94 16.48 o 0 3 12 3319.21 3046.44 67.52 o 1 3 12 3.95 7.15 9.72 o 2 3 12 1974.18 1903.74 65.02 o 3 3 12 562.92 546.06 27.09 o 4 3 12 1841.89 1814.81 87.39 o 0 4 12 941.78 877.30 72.83 o 1 4 12 7.93 -3.13 9.77 o 2 4 12 666.42 654.53 29.25 o 3 4 12 119.48 123.85 17.32 o 0 5 12 552.61 554.14 39.48 o 1 5 12 189.62 222.89 21.45 o 2 5 12 89.78 89.63 15.47 o 3 5 12 75.55 106.59 23.34 o 0 6 12 1745.05 1605.86 62.75 o 1 6 12 0.06 -6.72 11.27 o 2 6 12 587.51 611.90 35.77 o 0 7 12 643.15 549.06 59.72 o 1 7 12 1.22 4.86 24.28 o 2 7 12 300.01 315.58 51.46 o 1 0 13 79.31 118.12 19.04 o 2 0 13 0.57 -7.71 16.10 o 3 0 13 188.22 241.42 31.96 o 1 1 13 247.13 249.99 17.39 o 2 1 13 313.21 329.89 23.93 o 3 1 13 217.82 231.34 23.41 o 1 2 13 2684.02 2703.24 55.94 o 2 2 13 6.47 1.89 10.33 o 3 2 13 2696.82 2489.81 59.14 o 1 3 13 15.88 11.48 11.01 o 2 3 13 361.85 398.73 37.42 o 3 3 13 3.80 -10.00 11.15 o 1 4 13 1340.54 1336.79 58.14 o 2 4 13 0.28 -7.09 11.77 o 3 4 13 230.01 218.37 30.87 o 1 5 13 258.21 245.93 23.64 o 2 5 13 183.97 219.99 22.57 o 1 6 13 24.26 28.57 14.94 o 0 0 14 1681.79 1556.52 95.16 o 1 0 14 47.99 67.16 18.83 o 2 0 14 3753.60 3448.37 93.46 o 3 0 14 62.70 73.91 26.06 o 0 1 14 262.47 305.23 28.75 o 1 1 14 13.04 14.98 12.60 o 2 1 14 174.02 167.17 21.64 o 3 1 14 294.85 354.69 28.52 o 0 2 14 1688.33 1962.61 78.78 o 1 2 14 0.18 -11.74 11.74 o 2 2 14 84.68 81.81 16.74 o 3 2 14 16.58 -1.94 28.16 o 0 3 14 430.30 550.93 63.12 o 1 3 14 174.27 198.84 21.84 o 2 3 14 278.89 344.12 26.82 o 3 3 14 35.54 57.29 38.84 o 0 4 14 534.05 489.51 40.51 o 1 4 14 65.28 87.15 17.24 o 2 4 14 989.70 1008.76 65.31 o 0 5 14 686.94 612.93 48.05 o 1 5 14 16.66 -4.04 15.38 o 2 5 14 444.94 507.84 62.14 o 1 6 14 6.34 -23.30 23.30 o 1 0 15 2508.47 2565.46 81.34 o 2 0 15 27.63 20.53 21.93 o 1 1 15 269.17 310.96 25.63 o 2 1 15 87.57 114.79 19.20 o 1 2 15 330.52 405.92 28.18 o 2 2 15 157.35 184.05 33.56 o 1 3 15 234.14 257.07 24.96 o 2 3 15 39.30 25.25 31.07 o 1 4 15 850.45 852.45 56.64 o 0 0 16 54.66 57.29 38.84 o 1 0 16 80.78 70.88 39.81 o 2 0 16 216.46 229.16 50.49 o 0 1 16 168.16 227.56 54.86 o 1 1 16 50.96 65.06 18.22 o 0 2 16 1086.05 1442.92 99.04 o 1 2 16 3.96 -14.90 14.90 o