#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/36/2013650.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013650_Fobs loop_ _publ_author_name 'Wang, Cheng' 'Zheng, Qitai' 'Lu, Yang' 'Xiao, Ying' 'Li, Jianbei' 'Ding, Yi' _publ_section_title ; Dibothrioclinin I and II, epimers from Gerbera piloselloides (L.) Cass ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o593 _journal_page_last o595 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 102.905 _cell_angle_gamma 90.000 _cell_length_a 15.5167 _cell_length_b 19.4112 _cell_length_c 7.9627 _exptl_crystal_F_000 1024.00 _reflns_d_resolution_high 0.7721 _[local]_cod_data_source_file ln1173IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' II in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 207.38 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1.13 -1.99 1.99 o 2 0 0 8897.48 5433.66 497.77 o 3 0 0 13.19 11.95 5.97 o 4 0 0 39792.32 35461.14 501.75 o 5 0 0 1.78 1.99 39.82 o 6 0 0 305.20 274.77 23.89 o 7 0 0 519.79 541.57 27.88 o 8 0 0 415.97 487.81 21.90 o 9 0 0 148.55 169.24 43.80 o 10 0 0 86.73 75.66 21.90 o 11 0 0 312.23 336.49 25.88 o 12 0 0 2084.00 2134.44 73.67 o 13 0 0 3318.21 4099.63 165.26 o 15 0 0 3251.16 3271.34 155.30 o 16 0 0 333.22 473.88 61.72 o 17 0 0 84.79 117.47 47.79 o 18 0 0 465.01 489.81 65.71 o 19 0 0 24.67 31.86 67.70 o 1 1 0 4645.88 0.00 3.98 o 2 1 0 282.07 284.72 11.95 o 3 1 0 10.47 15.93 9.96 o 4 1 0 1600.63 1541.10 51.77 o 5 1 0 315.30 278.75 47.79 o 6 1 0 531.35 549.54 63.71 o 7 1 0 669.81 619.23 45.79 o 8 1 0 0.84 11.95 17.92 o 9 1 0 34.70 53.76 19.91 o 10 1 0 1185.96 1216.55 67.70 o 11 1 0 4.29 55.75 35.84 o 12 1 0 430.81 615.24 141.37 o 13 1 0 3601.21 4087.69 149.33 o 14 1 0 16.66 43.80 55.75 o 15 1 0 815.43 1230.49 278.75 o 16 1 0 490.92 603.30 89.60 o 17 1 0 140.49 179.20 45.79 o 18 1 0 24.73 91.59 69.69 o 19 1 0 12.71 47.79 51.77 o 0 2 0 42.07 17.92 13.94 o 1 2 0 11477.65 9714.48 517.68 o 2 2 0 265.70 226.98 17.92 o 3 2 0 1347.33 1138.90 69.69 o 4 2 0 118.16 99.55 13.94 o 5 2 0 1902.93 1927.37 37.83 o 6 2 0 428.60 396.22 31.86 o 7 2 0 508.70 738.69 101.55 o 8 2 0 70.41 99.55 23.89 o 9 2 0 446.74 438.04 37.83 o 10 2 0 38.58 129.42 89.60 o 11 2 0 56.44 59.73 37.83 o 12 2 0 103.22 95.57 23.89 o 13 2 0 43.26 619.23 167.25 o 14 2 0 750.91 836.25 89.60 o 15 2 0 80.93 161.28 77.65 o 16 2 0 1447.96 1515.21 187.16 o 17 2 0 4.75 27.88 43.80 o 18 2 0 12.28 1.99 43.80 o 19 2 0 67.96 61.72 49.78 o 1 3 0 674.80 667.01 35.84 o 2 3 0 133.39 135.39 9.96 o 3 3 0 456.26 447.99 29.87 o 4 3 0 766.84 702.85 27.88 o 5 3 0 1564.71 1403.71 105.53 o 6 3 0 320.96 286.72 15.93 o 7 3 0 342.52 348.44 15.93 o 8 3 0 2183.39 2192.18 149.33 o 9 3 0 0.15 5.97 19.91 o 10 3 0 190.73 161.28 25.88 o 11 3 0 4.52 3.98 19.91 o 12 3 0 452.66 459.94 25.88 o 13 3 0 2142.81 2243.95 99.55 o 14 3 0 837.40 814.35 89.60 o 15 3 0 26.12 63.71 47.79 o 16 3 0 253.37 288.71 45.79 o 17 3 0 17.72 31.86 39.82 o 18 3 0 0.03 7.96 35.84 o 19 3 0 25.00 25.88 41.81 o 0 4 0 150.77 151.32 7.96 o 1 4 0 11102.82 10516.88 340.47 o 2 4 0 39.70 49.78 11.95 o 3 4 0 527.01 461.93 37.83 o 4 4 0 1398.72 1345.97 71.68 o 5 4 0 66.60 75.66 17.92 o 6 4 0 311.85 270.79 17.92 o 7 4 0 108.58 99.55 15.93 o 8 4 0 1385.71 1268.32 91.59 o 9 4 0 0.00 3.98 23.89 o 10 4 0 45.91 37.83 39.82 o 11 4 0 448.74 416.14 25.88 o 12 4 0 0.11 21.90 39.82 o 13 4 0 48.24 141.37 131.41 o 14 4 0 139.46 151.32 67.70 o 15 4 0 24.86 29.87 37.83 o 16 4 0 114.83 105.53 39.82 o 17 4 0 193.46 223.00 47.79 o 18 4 0 4.82 35.84 51.77 o 19 4 0 18.16 27.88 39.82 o 1 5 0 1892.47 1975.15 27.88 o 2 5 0 99.64 101.55 13.94 o 3 5 0 57.80 61.72 17.92 o 4 5 0 81.44 65.71 19.91 o 5 5 0 539.18 559.49 29.87 o 6 5 0 1799.93 1776.04 73.67 o 7 5 0 475.62 447.99 33.85 o 8 5 0 792.73 814.35 45.79 o 9 5 0 0.38 5.97 19.91 o 10 5 0 132.34 117.47 19.91 o 11 5 0 19.46 11.95 27.88 o 12 5 0 2256.97 2188.20 43.80 o 13 5 0 109.71 109.51 37.83 o 14 5 0 95.57 95.57 43.80 o 15 5 0 5.93 23.89 27.88 o 16 5 0 217.97 223.00 57.74 o 17 5 0 0.19 51.77 67.70 o 18 5 0 42.77 49.78 37.83 o 19 5 0 43.92 29.87 39.82 o 0 6 0 757.63 690.90 21.90 o 1 6 0 1628.30 1453.49 129.42 o 2 6 0 2122.97 2132.45 115.48 o 3 6 0 379.88 386.27 29.87 o 4 6 0 37.83 35.84 15.93 o 5 6 0 544.38 549.54 35.84 o 6 6 0 310.40 300.65 21.90 o 7 6 0 80.86 89.60 13.94 o 8 6 0 191.98 223.00 23.89 o 9 6 0 811.23 748.65 33.85 o 10 6 0 20.33 11.95 45.79 o 11 6 0 1.27 -1.99 23.89 o 12 6 0 2.61 9.96 87.61 o 13 6 0 57.44 53.76 37.83 o 14 6 0 0.07 23.89 39.82 o 15 6 0 11.51 59.73 33.85 o 16 6 0 63.06 91.59 43.80 o 17 6 0 489.40 334.50 75.66 o 18 6 0 0.23 0.00 43.80 o 19 6 0 104.37 121.46 69.69 o 1 7 0 48.00 37.83 17.92 o 2 7 0 341.66 370.34 39.82 o 3 7 0 988.32 1029.39 43.80 o 4 7 0 1802.58 1829.80 69.69 o 5 7 0 756.25 688.91 43.80 o 6 7 0 522.62 521.66 29.87 o 7 7 0 629.77 667.01 33.85 o 8 7 0 141.99 165.26 21.90 o 9 7 0 38.43 65.71 29.87 o 10 7 0 42.84 37.83 29.87 o 11 7 0 134.65 153.31 23.89 o 12 7 0 677.50 655.07 51.77 o 13 7 0 31.97 35.84 45.79 o 14 7 0 16.32 39.82 35.84 o 15 7 0 135.23 115.48 33.85 o 16 7 0 58.64 47.79 35.84 o 17 7 0 80.05 97.56 47.79 o 18 7 0 2.10 3.98 63.71 o 0 8 0 452.45 432.06 25.88 o 1 8 0 933.82 1015.45 57.74 o 2 8 0 147.28 147.34 29.87 o 3 8 0 682.76 672.99 47.79 o 4 8 0 383.55 428.08 41.81 o 5 8 0 126.71 137.38 17.92 o 6 8 0 37.63 33.85 15.93 o 7 8 0 83.22 113.49 27.88 o 8 8 0 159.93 169.24 17.92 o 9 8 0 710.86 692.90 49.78 o 10 8 0 217.24 223.00 21.90 o 11 8 0 144.83 145.35 35.84 o 12 8 0 3.08 1.99 31.86 o 13 8 0 0.42 25.88 55.75 o 14 8 0 152.69 175.22 57.74 o 15 8 0 341.33 318.57 45.79 o 16 8 0 29.42 47.79 29.87 o 17 8 0 60.93 69.69 51.77 o 18 8 0 12.05 43.80 45.79 o 1 9 0 398.69 446.00 41.81 o 2 9 0 2439.80 2761.63 197.12 o 3 9 0 382.93 342.47 45.79 o 4 9 0 3613.27 3832.83 215.04 o 5 9 0 1819.43 1849.71 101.55 o 6 9 0 31.59 43.80 21.90 o 7 9 0 36.06 43.80 31.86 o 8 9 0 0.68 9.96 31.86 o 9 9 0 411.89 414.14 29.87 o 10 9 0 401.23 352.42 51.77 o 11 9 0 1368.26 1413.67 73.67 o 12 9 0 265.25 294.68 55.75 o 13 9 0 1026.17 983.59 97.56 o 14 9 0 0.87 9.96 37.83 o 15 9 0 14.07 21.90 69.69 o 16 9 0 79.17 67.70 43.80 o 17 9 0 0.62 63.71 61.72 o 18 9 0 3.82 9.96 47.79 o 0 10 0 18080.86 19809.25 597.32 o 1 10 0 1920.95 2172.27 71.68 o 2 10 0 6.35 15.93 19.91 o 3 10 0 144.80 197.12 29.87 o 4 10 0 1367.54 1519.19 83.63 o 5 10 0 308.09 260.83 25.88 o 6 10 0 7.62 17.92 21.90 o 7 10 0 45.01 45.79 19.91 o 8 10 0 68.93 65.71 19.91 o 9 10 0 336.39 328.53 27.88 o 10 10 0 71.36 69.69 33.85 o 11 10 0 2.46 11.95 33.85 o 12 10 0 242.30 246.89 43.80 o 13 10 0 3.93 33.85 35.84 o 14 10 0 418.22 374.32 39.82 o 15 10 0 34.83 23.89 27.88 o 16 10 0 138.68 105.53 61.72 o 17 10 0 10.51 11.95 45.79 o 1 11 0 98.14 109.51 25.88 o 2 11 0 86.22 85.62 25.88 o 3 11 0 8.28 21.90 25.88 o 4 11 0 2955.62 3239.49 155.30 o 5 11 0 257.60 280.74 35.84 o 6 11 0 105.84 95.57 29.87 o 7 11 0 2.16 5.97 19.91 o 8 11 0 252.00 266.80 33.85 o 9 11 0 3.34 3.98 27.88 o 10 11 0 34.33 53.76 47.79 o 11 11 0 259.08 244.90 55.75 o 12 11 0 99.33 121.46 35.84 o 13 11 0 365.76 324.55 63.71 o 14 11 0 0.87 27.88 31.86 o 15 11 0 57.41 55.75 43.80 o 16 11 0 383.87 366.36 85.62 o 17 11 0 73.02 131.41 73.67 o 0 12 0 436.49 420.12 33.85 o 1 12 0 4.94 5.97 27.88 o 2 12 0 269.59 286.72 33.85 o 3 12 0 58.64 41.81 23.89 o 4 12 0 86.67 95.57 19.91 o 5 12 0 499.05 481.84 31.86 o 6 12 0 286.63 284.72 27.88 o 7 12 0 1358.49 1405.70 67.70 o 8 12 0 1552.69 1588.88 43.80 o 9 12 0 12.99 19.91 39.82 o 10 12 0 32.17 47.79 33.85 o 11 12 0 186.44 197.12 43.80 o 12 12 0 12.33 35.84 49.78 o 13 12 0 10.92 35.84 83.63 o 14 12 0 38.71 55.75 37.83 o 15 12 0 27.85 7.96 41.81 o 16 12 0 82.06 43.80 43.80 o 17 12 0 5.14 23.89 53.76 o 1 13 0 627.15 651.08 37.83 o 2 13 0 14.45 19.91 25.88 o 3 13 0 523.18 481.84 31.86 o 4 13 0 326.02 344.46 43.80 o 5 13 0 24.79 39.82 47.79 o 6 13 0 873.91 868.11 45.79 o 7 13 0 1727.15 1596.85 85.62 o 8 13 0 554.32 543.56 57.74 o 9 13 0 335.39 298.66 43.80 o 10 13 0 387.52 418.13 51.77 o 11 13 0 215.85 217.03 41.81 o 12 13 0 13.69 19.91 41.81 o 13 13 0 77.02 87.61 53.76 o 14 13 0 0.04 7.96 49.78 o 15 13 0 8.17 21.90 39.82 o 16 13 0 12.93 17.92 41.81 o 0 14 0 222.78 205.08 47.79 o 1 14 0 26.88 15.93 25.88 o 2 14 0 2.12 1.99 31.86 o 3 14 0 180.74 191.14 33.85 o 4 14 0 72.32 89.60 25.88 o 5 14 0 348.55 344.46 65.71 o 6 14 0 419.94 406.18 45.79 o 7 14 0 476.20 440.03 37.83 o 8 14 0 2637.78 2530.66 217.03 o 9 14 0 2818.02 2785.52 97.56 o 10 14 0 147.46 125.44 37.83 o 11 14 0 103.14 87.61 29.87 o 12 14 0 218.08 209.06 39.82 o 13 14 0 50.90 53.76 55.75 o 14 14 0 43.94 37.83 47.79 o 15 14 0 37.87 83.63 75.66 o 16 14 0 28.92 3.98 61.72 o 1 15 0 89.83 79.64 27.88 o 2 15 0 663.11 617.23 33.85 o 3 15 0 53.72 49.78 29.87 o 4 15 0 207.30 183.18 35.84 o 5 15 0 67.23 75.66 55.75 o 6 15 0 22.09 39.82 27.88 o 7 15 0 168.61 175.22 53.76 o 8 15 0 194.57 195.13 27.88 o 9 15 0 0.86 7.96 41.81 o 10 15 0 322.30 284.72 33.85 o 11 15 0 2.07 65.71 37.83 o 12 15 0 248.87 244.90 61.72 o 13 15 0 0.60 5.97 55.75 o 14 15 0 23.48 41.81 37.83 o 15 15 0 5.65 27.88 69.69 o 0 16 0 110.33 115.48 55.75 o 1 16 0 106.14 95.57 33.85 o 2 16 0 1.65 -1.99 31.86 o 3 16 0 143.98 149.33 31.86 o 4 16 0 31.06 41.81 37.83 o 5 16 0 452.93 432.06 45.79 o 6 16 0 209.38 197.12 37.83 o 7 16 0 32.64 53.76 33.85 o 8 16 0 45.54 67.70 43.80 o 9 16 0 309.27 252.87 43.80 o 10 16 0 212.82 199.11 31.86 o 11 16 0 7.81 45.79 65.71 o 12 16 0 22.72 57.74 49.78 o 13 16 0 21.83 51.77 49.78 o 14 16 0 3.71 -5.97 43.80 o 15 16 0 64.87 53.76 53.76 o 1 17 0 105.13 121.46 39.82 o 2 17 0 149.71 131.41 33.85 o 3 17 0 17.27 25.88 35.84 o 4 17 0 262.87 280.74 35.84 o 5 17 0 16.32 35.84 49.78 o 6 17 0 46.78 43.80 33.85 o 7 17 0 0.91 25.88 33.85 o 8 17 0 202.58 199.11 43.80 o 9 17 0 0.08 11.95 63.71 o 10 17 0 1.84 33.85 45.79 o 11 17 0 12.63 37.83 39.82 o 12 17 0 41.26 43.80 51.77 o 13 17 0 6.55 5.97 43.80 o 14 17 0 20.48 43.80 51.77 o 0 18 0 36.21 13.94 47.79 o 1 18 0 192.15 207.07 39.82 o 2 18 0 133.12 139.38 35.84 o 3 18 0 212.37 175.22 39.82 o 4 18 0 6.55 0.00 33.85 o 5 18 0 16.80 31.86 37.83 o 6 18 0 10.32 35.84 41.81 o 7 18 0 25.96 45.79 37.83 o 8 18 0 0.16 29.87 41.81 o 9 18 0 44.27 73.67 37.83 o 10 18 0 10.79 7.96 37.83 o 11 18 0 22.78 27.88 65.71 o 12 18 0 22.52 35.84 55.75 o 13 18 0 38.13 41.81 53.76 o 1 19 0 42.34 47.79 35.84 o 2 19 0 48.15 49.78 33.85 o 3 19 0 280.43 306.63 53.76 o 4 19 0 274.05 266.80 43.80 o 5 19 0 151.47 139.38 59.73 o 6 19 0 428.49 414.14 53.76 o 7 19 0 482.56 477.86 53.76 o 8 19 0 302.39 272.78 55.75 o 9 19 0 41.47 73.67 67.70 o 10 19 0 227.89 244.90 57.74 o 11 19 0 28.55 27.88 79.64 o 12 19 0 71.29 63.71 43.80 o 0 20 0 743.60 663.03 63.71 o 1 20 0 189.85 205.08 55.75 o 2 20 0 62.58 105.53 41.81 o 3 20 0 0.32 1.99 49.78 o 4 20 0 0.13 11.95 47.79 o 5 20 0 38.25 13.94 39.82 o 6 20 0 14.35 43.80 39.82 o 7 20 0 63.81 113.49 49.78 o 8 20 0 33.39 71.68 77.65 o 9 20 0 245.37 306.63 59.73 o 10 20 0 138.50 151.32 59.73 o 11 20 0 33.98 23.89 45.79 o 1 21 0 2.96 9.96 51.77 o 2 21 0 67.45 69.69 39.82 o 3 21 0 120.59 165.26 55.75 o 4 21 0 5.71 43.80 61.72 o 5 21 0 7.73 41.81 51.77 o 6 21 0 13.51 41.81 47.79 o 7 21 0 44.24 35.84 47.79 o 8 21 0 2.66 43.80 59.73 o 9 21 0 2.59 11.95 51.77 o 10 21 0 62.05 83.63 65.71 o 0 22 0 554.25 742.67 91.59 o 1 22 0 843.59 884.04 99.55 o 2 22 0 19.30 93.58 51.77 o 3 22 0 2.36 1.99 51.77 o 4 22 0 114.71 153.31 49.78 o 5 22 0 101.92 143.36 55.75 o 6 22 0 354.89 406.18 53.76 o 7 22 0 24.52 45.79 41.81 o 8 22 0 123.88 163.27 43.80 o 9 22 0 0.65 31.86 65.71 o 1 23 0 21.59 61.72 85.62 o 2 23 0 429.22 481.84 61.72 o 3 23 0 21.34 75.66 71.68 o 4 23 0 49.37 73.67 63.71 o 5 23 0 96.02 147.34 59.73 o 6 23 0 7.32 49.78 43.80 o 7 23 0 71.89 111.50 65.71 o 0 24 0 279.34 316.58 99.55 o 1 24 0 228.77 298.66 113.49 o 2 24 0 105.11 111.50 59.73 o 3 24 0 76.61 193.13 63.71 o 4 24 0 16.23 79.64 65.71 o 5 24 0 3.70 23.89 59.73 o 1 25 0 0.24 89.60 43.80 o -19 1 1 116.68 95.57 37.83 o -18 1 1 1.04 0.00 39.82 o -17 1 1 186.78 189.15 29.87 o -16 1 1 0.69 57.74 41.81 o -15 1 1 34.32 117.47 77.65 o -14 1 1 151.65 418.13 115.48 o -13 1 1 2475.90 2598.36 99.55 o -12 1 1 125.62 135.39 31.86 o -11 1 1 27.64 37.83 23.89 o -10 1 1 6.23 5.97 35.84 o -9 1 1 565.78 374.32 81.63 o -8 1 1 253.56 264.81 17.92 o -7 1 1 522.48 531.62 21.90 o -6 1 1 1.45 -3.98 17.92 o -5 1 1 361.60 408.17 87.61 o -4 1 1 74.57 71.68 19.91 o -3 1 1 41.15 11.95 27.88 o -2 1 1 41.54 29.87 11.95 o -1 1 1 21042.16 20537.99 848.20 o 0 1 1 3579.46 3675.53 79.64 o 1 1 1 4188.96 4033.93 75.66 o 2 1 1 1226.67 1142.88 55.75 o 3 1 1 568.34 555.51 15.93 o 4 1 1 714.82 633.16 33.85 o 5 1 1 503.30 477.86 15.93 o 6 1 1 513.12 597.32 19.91 o 7 1 1 114.03 137.38 27.88 o 8 1 1 235.50 266.80 25.88 o 9 1 1 9.60 13.94 19.91 o 10 1 1 1.93 27.88 21.90 o 11 1 1 202.50 266.80 55.75 o 12 1 1 1582.60 1527.16 125.44 o 13 1 1 161.18 213.05 49.78 o 14 1 1 52.26 137.38 101.55 o 15 1 1 18.84 23.89 31.86 o 16 1 1 9.68 75.66 45.79 o 17 1 1 3.65 1.99 45.79 o 18 1 1 22.75 39.82 45.79 o 19 1 1 6.12 21.90 51.77 o -19 2 1 0.07 27.88 51.77 o -18 2 1 43.24 47.79 43.80 o -17 2 1 97.91 141.37 53.76 o -16 2 1 383.65 382.29 63.71 o -15 2 1 683.95 706.83 41.81 o -14 2 1 1848.87 1797.95 51.77 o -13 2 1 25.66 410.16 141.37 o -12 2 1 234.20 187.16 25.88 o -11 2 1 35.78 31.86 35.84 o -10 2 1 193.10 262.82 41.81 o -9 2 1 524.54 473.88 33.85 o -8 2 1 89.75 71.68 15.93 o -7 2 1 1031.86 1101.07 143.36 o -6 2 1 2860.62 2809.41 135.39 o -5 2 1 2341.13 2393.28 171.23 o -4 2 1 9.78 11.95 15.93 o -3 2 1 60.71 63.71 37.83 o -2 2 1 3325.24 3822.87 211.05 o -1 2 1 4476.81 4718.86 312.60 o 0 2 1 16567.54 16822.63 830.28 o 1 2 1 17072.03 16454.29 1045.32 o 2 2 1 1809.91 1893.52 81.63 o 3 2 1 2060.95 2062.76 101.55 o 4 2 1 1507.01 1328.05 47.79 o 5 2 1 2018.04 1899.49 123.45 o 6 2 1 36.87 23.89 15.93 o 7 2 1 50.91 43.80 15.93 o 8 2 1 49.82 19.91 25.88 o 9 2 1 106.17 95.57 17.92 o 10 2 1 398.74 366.36 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