#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2013653.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013653_Fobs loop_ _publ_author_name 'Qiao, Shan-Bao' 'Jiao, Chang-Mei' 'Xu, Qing-Feng' 'Zhang, Yong' 'Li, Bao-Long' 'Lang, Jian-Ping' _publ_section_title ; Bis(tetraphenylphosphonium) (\m-tetrathiotungstenio-\k^4^S,S':S'':S''')bis[(cyano-\kC)cuprate](2--) acetonitrile solvate monohydrate ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m465 _journal_page_last m466 _journal_volume 59 _journal_year 2003 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 72.922 _cell_angle_beta 76.449 _cell_angle_gamma 77.159 _cell_length_a 10.6193 _cell_length_b 12.7441 _cell_length_c 20.7526 _exptl_crystal_F_000 1224.00 _reflns_d_resolution_high 0.7701 _[local]_cod_data_source_file ln1179Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' _L030108a' _shelx_refln_list_code 4 _shelx_f_calc_maximum 242.56 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 16923.78 16756.95 397.06 o 3 0 0 9222.82 9875.65 151.63 o 4 0 0 18.63 19.38 8.60 o 5 0 0 17232.54 18022.14 200.78 o 6 0 0 17370.05 17451.49 185.91 o 7 0 0 7333.34 7367.42 101.87 o 8 0 0 6015.93 5815.35 119.03 o 9 0 0 111.12 70.50 15.41 o 10 0 0 379.51 378.76 27.88 o 11 0 0 695.65 682.60 37.17 o 12 0 0 1709.63 1625.43 104.23 o 13 0 0 1637.83 1663.03 136.92 o -13 1 0 1118.22 1187.93 70.38 o -12 1 0 1169.61 1068.46 45.14 o -11 1 0 1302.95 1397.09 104.31 o -10 1 0 3421.44 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