#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:51:04 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180806 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/37/2013713.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013713_Fobs loop_ _publ_author_name 'Bernhardt, Paul V.' 'Macpherson, Brendan P.' _publ_section_title ; Geometric isomers of chloro(6-methyl-1,4,8,11-tetraazacyclotetradecane-6-amine)cobalt(III) tetrachlorozincate(II) ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m467 _journal_page_last m470 _journal_volume 59 _journal_year 2003 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2bc 2ac' _symmetry_space_group_name_H-M 'P c a b' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.6190 _cell_length_b 14.1090 _cell_length_c 23.5170 _exptl_crystal_F_000 2160.00 _reflns_d_resolution_high 0.8419 _cod_data_source_file ta1423Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1444bm1 in P c a b' _shelx_refln_list_code 4 _shelx_f_calc_maximum 583.35 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y+1/2, z+1/2' 'x+1/2, -y, -z+1/2' '-x+1/2, y+1/2, -z' '-x, -y, -z' 'x, y-1/2, -z-1/2' '-x-1/2, y, z-1/2' 'x-1/2, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 111576.77 103073.11 892.80 o 4 0 0 237.40 344.07 14.23 o 6 0 0 33759.66 34632.95 232.04 o 8 0 0 17514.67 18246.35 174.75 o 10 0 0 513.52 549.82 30.38 o 12 0 0 5773.11 5561.72 89.33 o 0 2 0 147851.33 159955.31 1045.99 o 1 2 0 182994.66 192761.33 1261.48 o 2 2 0 4406.87 4776.11 49.06 o 3 2 0 5940.69 5841.86 56.25 o 4 2 0 30024.94 29255.29 193.67 o 5 2 0 23256.10 24030.17 181.78 o 6 2 0 23748.14 24346.09 199.12 o 7 2 0 42151.52 44141.93 294.60 o 8 2 0 1914.75 1877.73 39.98 o 9 2 0 147.56 129.04 22.20 o 10 2 0 4307.19 4282.07 70.46 o 11 2 0 49.92 72.64 22.83 o 12 2 0 101.70 92.08 47.79 o 13 2 0 1636.35 1623.48 63.23 o 0 4 0 37563.99 37936.71 174.95 o 1 4 0 3955.69 4290.58 43.37 o 2 4 0 39572.50 39737.71 194.26 o 3 4 0 2105.88 2246.70 28.64 o 4 4 0 26441.26 27980.32 190.56 o 5 4 0 103692.23 105464.24 414.47 o 6 4 0 54261.45 52945.82 319.10 o 7 4 0 6878.27 6853.82 76.28 o 8 4 0 4687.84 4788.94 70.82 o 9 4 0 8186.72 8849.97 95.58 o 10 4 0 16583.96 17358.52 170.60 o 11 4 0 227.80 242.90 31.22 o 12 4 0 296.79 246.19 37.17 o 13 4 0 18.22 102.16 33.13 o 0 6 0 5363.30 5500.95 54.03 o 1 6 0 2086.90 2163.77 29.80 o 2 6 0 9566.94 10180.18 101.49 o 3 6 0 14917.17 15565.92 151.18 o 4 6 0 7625.38 7071.11 71.81 o 5 6 0 7409.11 7281.48 72.72 o 6 6 0 3965.65 3804.40 51.22 o 7 6 0 6588.70 6690.54 70.80 o 8 6 0 3191.81 3133.21 57.45 o 9 6 0 5184.06 5321.48 78.69 o 10 6 0 377.59 488.80 37.28 o 11 6 0 9615.64 10285.93 142.39 o 12 6 0 61.31 52.25 60.32 o 0 8 0 278.74 287.85 17.00 o 1 8 0 7878.77 8328.58 85.80 o 2 8 0 7997.46 8100.84 80.34 o 3 8 0 1783.76 1646.66 34.35 o 4 8 0 26167.43 25947.62 234.18 o 5 8 0 8559.99 8306.47 81.25 o 6 8 0 688.48 733.48 31.45 o 7 8 0 165.13 167.49 26.87 o 8 8 0 1230.98 1209.60 42.19 o 9 8 0 12330.15 12266.27 121.36 o 10 8 0 13317.77 13009.56 132.59 o 11 8 0 1715.90 1775.00 61.11 o 12 8 0 373.34 450.66 43.44 o 0 10 0 258.66 264.26 19.44 o 1 10 0 14.46 50.44 29.95 o 2 10 0 37.17 47.58 30.69 o 3 10 0 1293.08 1257.59 35.71 o 4 10 0 5837.48 5849.19 73.52 o 5 10 0 799.31 847.39 36.76 o 6 10 0 4746.72 4821.38 73.78 o 7 10 0 3635.21 3395.81 65.22 o 8 10 0 13020.40 12982.08 127.68 o 9 10 0 435.40 555.83 35.26 o 10 10 0 5012.12 5218.26 96.63 o 11 10 0 265.53 289.10 38.66 o 0 12 0 12667.77 13132.46 129.80 o 1 12 0 298.07 342.86 27.83 o 2 12 0 3901.98 3887.89 65.98 o 3 12 0 12767.15 12950.23 133.94 o 4 12 0 2759.07 2698.15 58.17 o 5 12 0 1173.54 1215.47 44.95 o 6 12 0 2274.59 2267.69 57.94 o 7 12 0 3408.99 3297.57 70.94 o 8 12 0 674.77 643.52 40.68 o 9 12 0 3991.37 3993.97 87.44 o 0 14 0 2107.88 2295.15 58.36 o 1 14 0 1246.01 1245.77 46.01 o 2 14 0 16752.31 16757.17 167.38 o 3 14 0 5155.41 4937.64 83.88 o 4 14 0 472.45 377.61 36.22 o 5 14 0 485.97 503.37 38.56 o 6 14 0 1396.98 1481.15 56.74 o 7 14 0 29.39 29.95 49.38 o 0 16 0 63.46 32.82 52.57 o 1 16 0 15513.07 15881.94 168.24 o 2 16 0 490.48 538.42 39.94 o 3 16 0 549.78 590.69 41.74 o 4 16 0 290.36 347.73 39.51 o 2 0 1 129731.39 131005.80 1029.37 o 4 0 1 4625.41 4994.32 50.53 o 6 0 1 16.10 39.93 23.04 o 8 0 1 6963.00 7247.77 75.10 o 10 0 1 7345.18 7163.23 87.85 o 12 0 1 879.71 718.38 39.52 o 1 1 1 20492.35 20776.45 211.87 o 2 1 1 133.20 138.84 13.70 o 3 1 1 1800.74 1729.87 22.05 o 4 1 1 3903.96 4101.57 40.23 o 5 1 1 331.06 287.14 15.51 o 6 1 1 387.79 328.25 17.00 o 7 1 1 56675.34 57663.16 332.97 o 8 1 1 3269.78 3165.84 48.63 o 9 1 1 1033.48 1055.06 37.40 o 10 1 1 7021.53 7147.96 87.19 o 11 1 1 3909.88 4561.43 74.59 o 12 1 1 9.82 10.51 47.26 o 13 1 1 2587.82 2551.51 73.57 o 1 2 1 28292.59 29974.10 293.07 o 2 2 1 15621.80 15944.90 101.92 o 3 2 1 2022.76 1861.21 24.50 o 4 2 1 6178.65 6115.30 60.12 o 5 2 1 9613.95 10055.42 100.76 o 6 2 1 799.41 806.24 23.59 o 7 2 1 4000.81 4189.29 51.01 o 8 2 1 262.80 322.04 21.46 o 9 2 1 2780.23 2918.49 54.03 o 10 2 1 1639.78 1640.76 46.45 o 11 2 1 1830.33 1948.30 52.61 o 12 2 1 52.39 91.97 47.68 o 13 2 1 683.36 670.50 47.91 o 1 3 1 783.62 775.74 15.95 o 2 3 1 19759.52 20967.98 128.75 o 3 3 1 40349.98 41169.32 200.32 o 4 3 1 2641.31 2558.78 31.52 o 5 3 1 236.95 267.88 17.10 o 6 3 1 4113.26 3980.48 46.99 o 7 3 1 47.07 23.79 31.44 o 8 3 1 5207.84 5059.81 61.79 o 9 3 1 3813.53 3641.14 61.09 o 10 3 1 222.79 241.09 27.08 o 11 3 1 89.43 115.44 25.49 o 12 3 1 2807.98 2934.05 72.41 o 13 3 1 171.00 105.99 55.97 o 1 4 1 2856.12 3189.00 31.03 o 2 4 1 2506.61 2886.98 30.05 o 3 4 1 18283.78 17815.69 140.48 o 4 4 1 17872.73 18069.96 153.44 o 5 4 1 5989.26 6216.04 61.59 o 6 4 1 1481.58 1502.76 32.11 o 7 4 1 2153.97 2130.09 40.63 o 8 4 1 1354.10 1517.30 39.96 o 9 4 1 1127.81 1218.30 39.64 o 10 4 1 1152.14 1198.38 43.03 o 11 4 1 5513.85 5367.81 85.50 o 12 4 1 5225.50 5727.47 99.63 o 13 4 1 12.62 16.67 53.74 o 1 5 1 16488.79 16949.09 133.95 o 2 5 1 6408.05 6642.31 68.13 o 3 5 1 7161.23 7286.35 75.08 o 4 5 1 13105.67 13171.28 120.87 o 5 5 1 16469.94 17114.92 147.93 o 6 5 1 7864.82 7832.55 77.00 o 7 5 1 2861.68 2917.27 47.56 o 8 5 1 707.79 701.40 30.60 o 9 5 1 2242.82 2360.29 59.54 o 10 5 1 192.07 185.65 29.53 o 11 5 1 210.22 92.72 54.91 o 12 5 1 1458.12 1563.56 60.57 o 13 5 1 3501.81 3790.47 89.76 o 1 6 1 1002.64 994.05 22.00 o 2 6 1 3527.25 3386.68 38.47 o 3 6 1 931.07 965.16 23.49 o 4 6 1 12038.16 11756.92 121.17 o 5 6 1 25440.76 25538.37 220.79 o 6 6 1 1280.93 1203.60 31.67 o 7 6 1 1917.71 1728.03 39.98 o 8 6 1 2113.48 2045.75 46.78 o 9 6 1 1133.62 1042.50 40.59 o 10 6 1 161.99 199.45 29.63 o 11 6 1 10258.48 10972.22 146.59 o 12 6 1 420.39 485.83 45.35 o 1 7 1 3.30 31.86 22.19 o 2 7 1 16265.17 15906.23 157.70 o 3 7 1 44815.87 44624.89 277.23 o 4 7 1 5487.86 5340.72 55.45 o 5 7 1 271.57 349.13 20.92 o 6 7 1 253.56 273.39 22.09 o 7 7 1 3390.64 3457.65 58.31 o 8 7 1 873.01 919.03 37.08 o 9 7 1 4851.63 4975.49 76.86 o 10 7 1 291.42 273.60 30.48 o 11 7 1 104.17 219.84 33.77 o 12 7 1 195.12 228.23 37.07 o 1 8 1 3500.56 3643.91 44.83 o 2 8 1 422.66 435.22 19.65 o 3 8 1 818.41 828.60 25.40 o 4 8 1 573.39 605.13 24.01 o 5 8 1 1300.85 1357.88 34.86 o 6 8 1 17789.14 17238.67 165.69 o 7 8 1 18148.52 18084.46 176.54 o 8 8 1 1321.04 1287.12 43.57 o 9 8 1 326.36 311.10 32.71 o 10 8 1 196.16 216.55 33.14 o 11 8 1 1186.62 1167.58 53.66 o 12 8 1 2827.98 2879.96 81.23 o 1 9 1 17058.33 17189.10 162.36 o 2 9 1 1366.94 1434.76 32.95 o 3 9 1 42947.16 43262.84 312.26 o 4 9 1 3973.29 3736.28 54.08 o 5 9 1 568.66 513.63 30.70 o 6 9 1 371.65 392.58 29.10 o 7 9 1 540.95 545.79 33.04 o 8 9 1 77.49 18.16 46.83 o 9 9 1 4982.81 4676.13 81.00 o 10 9 1 596.48 566.39 40.58 o 11 9 1 152.51 231.52 36.11 o 1 10 1 2705.88 2558.60 44.47 o 2 10 1 163.03 222.50 19.65 o 3 10 1 3396.99 3384.99 55.23 o 4 10 1 1945.06 1941.00 45.18 o 5 10 1 12110.09 11875.49 114.81 o 6 10 1 10291.58 9901.68 103.14 o 7 10 1 1734.83 1612.92 49.32 o 8 10 1 3014.73 3155.85 66.36 o 9 10 1 209.19 226.75 30.27 o 10 10 1 2112.14 2193.76 67.07 o 11 10 1 188.31 17.31 69.35 o 1 11 1 4150.77 4077.31 62.17 o 2 11 1 8963.15 8846.90 90.41 o 3 11 1 2323.40 2240.97 49.55 o 4 11 1 12653.38 12262.76 126.48 o 5 11 1 2709.92 2788.79 58.06 o 6 11 1 1813.48 1719.48 49.96 o 7 11 1 6882.22 6700.63 94.18 o 8 11 1 232.60 263.82 30.48 o 9 11 1 221.08 293.34 36.53 o 10 11 1 780.21 801.08 46.74 o 1 12 1 4167.47 4152.50 66.63 o 2 12 1 10248.00 10434.63 104.53 o 3 12 1 1900.06 1780.11 47.84 o 4 12 1 5111.01 5012.36 76.87 o 5 12 1 4655.84 4701.53 77.06 o 6 12 1 214.28 197.76 28.36 o 7 12 1 610.84 610.69 39.94 o 8 12 1 3.13 84.11 45.66 o 9 12 1 1.57 -50.23 50.23 o 1 13 1 107.65 77.85 39.08 o 2 13 1 877.93 797.77 35.59 o 3 13 1 1638.64 1596.33 49.21 o 4 13 1 3521.52 3282.04 68.08 o 5 13 1 2761.72 2801.29 64.54 o 6 13 1 150.95 212.19 31.54 o 7 13 1 1440.13 1473.75 55.15 o 8 13 1 4511.30 4532.87 92.99 o 1 14 1 7956.87 7832.60 100.62 o 2 14 1 357.72 402.12 31.33 o 3 14 1 948.45 1008.13 43.98 o 4 14 1 3242.54 3128.94 69.66 o 5 14 1 18.15 -11.36 48.85 o 6 14 1 525.44 509.00 42.06 o 7 14 1 144.93 109.18 37.38 o 1 15 1 3142.92 3164.47 75.40 o 2 15 1 166.45 142.95 32.50 o 3 15 1 14.51 -3.93 46.30 o 4 15 1 1799.61 1725.31 63.34 o 5 15 1 1465.12 1431.97 57.59 o 6 15 1 2411.61 2423.44 73.24 o 1 16 1 2021.21 1953.43 66.43 o 2 16 1 4.99 -25.06 53.20 o 3 16 1 3917.04 3870.40 88.50 o 4 16 1 1835.15 1791.91 64.40 o 0 0 2 4050.64 4165.73 39.67 o 2 0 2 2574.49 2332.08 22.86 o 4 0 2 12005.59 12154.58 110.47 o 6 0 2 21919.21 22784.62 188.52 o 8 0 2 1436.30 1366.85 34.55 o 10 0 2 2005.25 1976.07 49.43 o 12 0 2 1625.74 1663.09 52.18 o 0 1 2 7999.77 8523.21 54.32 o 1 1 2 11521.89 10275.47 71.58 o 2 1 2 15856.49 16152.06 114.36 o 3 1 2 805.31 978.34 19.35 o 4 1 2 38.39 15.61 21.98 o 5 1 2 4365.22 4391.09 42.13 o 6 1 2 1178.06 1259.78 27.32 o 7 1 2 4923.03 4746.35 53.50 o 8 1 2 25542.18 25443.60 239.73 o 9 1 2 55900.18 56359.34 388.10 o 10 1 2 3591.14 3827.78 65.01 o 11 1 2 591.49 505.11 34.42 o 12 1 2 40.55 73.49 41.52 o 13 1 2 1376.42 1401.12 57.17 o 0 2 2 1774.39 1977.37 20.49 o 1 2 2 377.65 430.05 12.65 o 2 2 2 20972.07 22142.41 127.31 o 3 2 2 19578.40 20008.64 146.36 o 4 2 2 1315.33 1338.93 27.12 o 5 2 2 128.53 176.63 14.55 o 6 2 2 6676.37 7090.05 71.33 o 7 2 2 1452.24 1461.82 32.32 o 8 2 2 1467.42 1353.57 34.12 o 9 2 2 1804.65 1900.65 45.71 o 10 2 2 902.27 914.89 37.50 o 11 2 2 543.96 602.40 35.05 o 12 2 2 1.54 -47.89 47.89 o 13 2 2 1439.80 1416.67 59.19 o 0 3 2 10559.67 10069.58 80.70 o 1 3 2 23488.38 23779.87 129.61 o 2 3 2 97123.63 101214.47 958.06 o 3 3 2 8716.59 8989.16 82.68 o 4 3 2 10833.56 11357.61 104.31 o 5 3 2 8298.97 7866.84 78.11 o 6 3 2 8077.76 8081.92 79.62 o 7 3 2 1399.18 1368.50 32.74 o 8 3 2 21797.68 22327.13 198.90 o 9 3 2 874.33 850.31 35.91 o 10 3 2 10328.18 10149.10 104.95 o 11 3 2 277.22 271.69 28.46 o 12 3 2 0.35 54.05 47.89 o 13 3 2 1462.85 1422.73 59.61 o 0 4 2 3140.21 3300.16 33.29 o 1 4 2 42769.03 45127.59 201.38 o 2 4 2 1581.55 1689.82 24.05 o 3 4 2 2667.02 2739.44 31.63 o 4 4 2 4404.29 4513.41 45.75 o 5 4 2 107.62 181.61 16.57 o 6 4 2 175.73 109.61 17.21 o 7 4 2 389.21 505.20 26.98 o 8 4 2 805.72 876.23 33.68 o 9 4 2 113.21 150.70 21.24 o 10 4 2 109.77 159.30 24.96 o 11 4 2 96.19 159.51 25.70 o 12 4 2 49.83 70.20 49.59 o 13 4 2 64.43 79.22 58.83 o 0 5 2 12902.51 12821.65 115.07 o 1 5 2 16433.29 16282.54 132.91 o 2 5 2 11100.54 10528.33 96.20 o 3 5 2 19820.41 19312.31 159.15 o 4 5 2 21320.59 21234.80 178.40 o 5 5 2 27461.98 26850.13 215.45 o 6 5 2 126.76 80.93 17.31 o 7 5 2 23213.24 23044.25 201.10 o 8 5 2 588.48 564.52 30.06 o 9 5 2 221.65 238.65 32.71 o 10 5 2 1860.49 2005.45 51.77 o 11 5 2 169.32 209.97 29.74 o 12 5 2 1592.62 1553.55 58.45 o 13 5 2 2728.54 2809.47 78.67 o 0 6 2 18190.76 20031.22 157.90 o 1 6 2 4375.43 4827.26 49.06 o 2 6 2 9471.00 9496.82 99.86 o 3 6 2 1142.29 1159.34 25.62 o 4 6 2 1679.84 1880.40 32.97 o 5 6 2 1076.49 1110.62 28.91 o 6 6 2 266.18 268.83 21.35 o 7 6 2 73.59 66.48 33.88 o 8 6 2 188.16 187.14 26.13 o 9 6 2 3186.61 3076.91 61.59 o 10 6 2 124.96 111.09 26.76 o 11 6 2 814.12 944.43 52.91 o 12 6 2 32.33 -23.68 52.99 o 0 7 2 87218.13 86014.55 365.10 o 1 7 2 3784.81 3946.24 43.47 o 2 7 2 6344.93 6202.07 62.03 o 3 7 2 1249.66 1377.02 29.55 o 4 7 2 48366.50 48280.20 305.88 o 5 7 2 5109.85 4886.51 57.86 o 6 7 2 19603.02 19268.86 186.94 o 7 7 2 3283.52 3254.94 57.03 o 8 7 2 16923.89 16402.33 171.56 o 9 7 2 217.15 247.78 28.14 o 10 7 2 10.29 53.10 45.77 o 11 7 2 33.23 14.87 48.74 o 12 7 2 97.99 94.62 58.73 o 0 8 2 377.99 435.53 19.23 o 1 8 2 3540.62 3755.86 45.90 o 2 8 2 496.33 483.26 21.03 o 3 8 2 1444.72 1468.29 32.00 o 4 8 2 4842.80 4661.21 56.47 o 5 8 2 15.55 27.61 30.80 o 6 8 2 552.03 548.36 30.38 o 7 8 2 3.28 -41.84 41.84 o 8 8 2 31.91 22.62 40.67 o 9 8 2 743.25 708.37 36.86 o 10 8 2 377.22 381.52 34.84 o 11 8 2 98.31 89.74 53.95 o 12 8 2 132.63 64.57 64.57 o 0 9 2 29020.43 28879.42 241.03 o 1 9 2 42688.89 42186.89 295.97 o 2 9 2 1381.10 1443.70 33.27 o 3 9 2 6787.83 6859.82 68.69 o 4 9 2 2397.48 2580.36 45.31 o 5 9 2 27965.10 27923.90 268.42 o 6 9 2 1032.22 1010.93 37.19 o 7 9 2 9390.39 9651.10 102.13 o 8 9 2 151.21 200.19 25.81 o 9 9 2 1173.86 1149.99 44.10 o 10 9 2 62.61 -3.72 48.96 o 11 9 2 3559.24 3666.77 85.51 o 0 10 2 140.83 136.79 17.21 o 1 10 2 2466.91 2472.36 43.82 o 2 10 2 963.17 1013.29 30.07 o 3 10 2 48.64 82.73 19.33 o 4 10 2 515.49 537.51 29.53 o 5 10 2 4107.57 4109.26 66.42 o 6 10 2 761.99 791.47 35.27 o 7 10 2 437.26 438.58 31.55 o 8 10 2 47.27 39.40 46.94 o 9 10 2 484.81 481.07 39.30 o 10 10 2 141.49 159.20 34.94 o 11 10 2 227.12 271.89 40.78 o 0 11 2 10007.18 10155.58 101.58 o 1 11 2 10283.64 10349.26 102.23 o 2 11 2 6684.71 6802.20 79.95 o 3 11 2 137.34 142.63 24.00 o 4 11 2 430.54 463.01 28.57 o 5 11 2 10592.06 10523.65 107.20 o 6 11 2 6061.56 6360.48 87.34 o 7 11 2 499.30 519.31 35.37 o 8 11 2 2272.96 2321.17 61.02 o 9 11 2 7290.16 7140.58 111.86 o 10 11 2 83.06 92.18 32.50 o 0 12 2 4047.84 3857.86 64.81 o 1 12 2 36.03 132.00 19.65 o 2 12 2 487.08 464.94 29.64 o 3 12 2 176.77 139.24 24.96 o 4 12 2 382.51 382.27 30.80 o 5 12 2 196.38 254.26 27.19 o 6 12 2 0.46 70.73 39.08 o 7 12 2 299.68 284.54 32.29 o 8 12 2 249.70 297.06 36.54 o 9 12 2 3.24 -25.27 52.67 o 0 13 2 7217.76 7367.83 92.19 o 1 13 2 675.94 681.05 34.31 o 2 13 2 1532.13 1567.79 48.57 o 3 13 2 2208.33 2192.53 56.56 o 4 13 2 179.86 211.14 26.55 o 5 13 2 207.71 284.74 30.48 o 6 13 2 7739.89 7915.21 113.91 o 7 13 2 928.13 886.88 50.36 o 8 13 2 2991.90 2856.72 77.19 o 0 14 2 1468.13 1435.80 47.93 o 1 14 2 97.61 87.30 43.86 o 2 14 2 254.92 209.97 28.57 o 3 14 2 750.73 727.27 38.24 o 4 14 2 348.41 300.58 37.92 o 5 14 2 28.41 15.29 50.13 o 6 14 2 124.57 93.88 32.07 o 7 14 2 147.81 182.03 34.41 o 0 15 2 657.08 723.51 43.87 o 1 15 2 477.65 635.82 40.58 o 2 15 2 1555.13 1532.39 56.22 o 3 15 2 640.63 592.74 42.38 o 4 15 2 1838.69 1997.62 63.66 o 5 15 2 1.31 46.20 43.43 o 6 15 2 67.49 -8.81 52.67 o 0 16 2 25.10 53.63 44.28 o 1 16 2 557.31 625.75 43.02 o 2 16 2 45.32 16.78 52.04 o 3 16 2 0.47 -25.81 57.56 o 2 0 3 51447.97 53837.44 553.22 o 4 0 3 4348.61 4889.15 48.25 o 6 0 3 128.12 105.89 13.49 o 8 0 3 2493.35 2655.87 44.89 o 10 0 3 1008.63 1082.18 38.04 o 12 0 3 1086.23 1143.44 46.96 o 1 1 3 1405.17 1198.83 18.23 o 2 1 3 507.92 504.50 17.54 o 3 1 3 720.87 627.76 18.82 o 4 1 3 972.85 889.67 20.09 o 5 1 3 169.90 176.10 13.91 o 6 1 3 4022.51 4235.59 46.56 o 7 1 3 4484.02 4387.54 51.67 o 8 1 3 703.83 655.42 27.20 o 9 1 3 198.40 216.03 27.61 o 10 1 3 2204.39 2155.84 51.56 o 11 1 3 9311.23 9324.73 105.93 o 12 1 3 4414.45 4427.30 80.02 o 13 1 3 1681.77 1683.13 59.51 o 1 2 3 24111.33 25531.52 128.94 o 2 2 3 1177.01 1108.68 20.43 o 3 2 3 5145.66 5130.52 52.51 o 4 2 3 1337.63 1284.77 27.65 o 5 2 3 18347.89 18940.19 174.23 o 6 2 3 24235.24 24011.39 205.70 o 7 2 3 2105.73 2340.23 39.99 o 8 2 3 11090.51 11196.05 114.96 o 9 2 3 2374.35 2405.41 49.55 o 10 2 3 1116.95 1115.50 39.63 o 11 2 3 35.25 78.16 40.57 o 12 2 3 194.52 276.98 31.33 o 13 2 3 35.76 72.43 52.14 o 1 3 3 54.94 5.74 21.03 o 2 3 3 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1124.97 48.98 o 3 6 21 17252.64 17720.63 170.51 o 4 6 21 67.31 -17.84 55.97 o 5 6 21 1237.46 1413.17 62.26 o 6 6 21 1891.70 1988.96 74.18 o 7 6 21 1725.76 1680.26 71.31 o 1 7 21 49.89 93.99 25.38 o 2 7 21 226.49 262.65 33.03 o 3 7 21 662.78 643.31 48.44 o 4 7 21 562.45 514.75 47.59 o 5 7 21 20.67 -43.97 59.26 o 6 7 21 1.56 31.01 55.43 o 7 7 21 288.22 242.79 43.86 o 1 8 21 1998.09 2189.26 70.68 o 2 8 21 5235.38 5456.08 104.21 o 3 8 21 6131.45 6436.90 117.23 o 4 8 21 9372.01 9531.97 142.55 o 5 8 21 1915.28 2090.44 75.03 o 6 8 21 721.57 761.86 56.41 o 1 9 21 141.71 9.13 59.37 o 2 9 21 491.88 544.26 44.61 o 3 9 21 2119.89 2141.03 73.77 o 4 9 21 10.21 -4.99 62.02 o 5 9 21 1006.49 1056.13 58.96 o 1 10 21 227.56 202.32 40.68 o 2 10 21 10434.93 10840.23 151.77 o 3 10 21 1513.40 1388.63 62.38 o 0 0 22 9315.86 9364.03 115.43 o 2 0 22 938.39 869.19 43.56 o 4 0 22 1086.90 1125.19 48.88 o 6 0 22 709.89 759.22 47.06 o 8 0 22 5270.75 4822.86 107.17 o 0 1 22 8770.48 9021.93 114.55 o 1 1 22 10931.39 11170.18 128.33 o 2 1 22 195.72 93.25 37.60 o 3 1 22 1410.36 1314.96 56.11 o 4 1 22 496.84 512.73 36.96 o 5 1 22 502.28 488.40 40.58 o 6 1 22 720.22 630.47 45.47 o 7 1 22 1914.77 1834.97 68.45 o 8 1 22 156.21 67.76 63.93 o 0 2 22 10870.88 11118.06 126.73 o 1 2 22 184.91 268.38 28.78 o 2 2 22 206.94 219.21 34.52 o 3 2 22 227.41 309.59 32.29 o 4 2 22 2169.48 2111.39 62.83 o 5 2 22 1260.88 1266.15 52.17 o 6 2 22 65.58 136.68 31.01 o 7 2 22 780.04 802.68 55.13 o 8 2 22 56.10 73.91 53.84 o 0 3 22 7523.08 7523.81 106.69 o 1 3 22 2148.07 2165.24 60.70 o 2 3 22 252.34 304.93 35.16 o 3 3 22 3.65 49.06 41.31 o 4 3 22 4.40 4.25 50.12 o 5 3 22 1902.91 1837.27 62.71 o 6 3 22 2858.72 3017.17 81.98 o 7 3 22 567.95 603.12 47.80 o 8 3 22 72.71 -58.94 68.50 o 0 4 22 2099.73 2094.69 60.17 o 1 4 22 1083.33 1205.94 49.19 o 2 4 22 89.34 123.72 28.89 o 3 4 22 3948.16 3798.35 81.71 o 4 4 22 18.29 8.71 45.88 o 5 4 22 4465.44 4761.77 100.34 o 6 4 22 569.50 506.89 50.35 o 7 4 22 90.39 137.32 36.43 o 0 5 22 797.27 781.68 41.01 o 1 5 22 1697.14 1568.91 54.52 o 2 5 22 239.08 252.46 32.07 o 3 5 22 72.46 52.36 54.37 o 4 5 22 5819.57 6142.24 112.11 o 5 5 22 70.93 150.38 37.28 o 6 5 22 49.73 80.60 54.69 o 7 5 22 932.54 863.49 58.86 o 0 6 22 426.56 457.16 39.09 o 1 6 22 4907.07 5042.39 92.60 o 2 6 22 96.25 170.03 26.66 o 3 6 22 215.05 245.76 40.57 o 4 6 22 2347.38 2603.41 77.82 o 5 6 22 7411.26 7495.50 128.05 o 6 6 22 1522.16 1919.22 70.77 o 0 7 22 75.65 48.32 51.51 o 1 7 22 138.42 97.39 32.50 o 2 7 22 54.68 41.20 42.59 o 3 7 22 944.78 934.38 54.71 o 4 7 22 807.55 909.46 56.30 o 5 7 22 1234.45 1212.85 59.93 o 6 7 22 1729.72 1913.30 73.01 o 0 8 22 7896.36 8116.75 128.19 o 1 8 22 2256.10 2388.13 74.73 o 2 8 22 5700.62 5691.67 111.25 o 3 8 22 0.89 24.53 53.52 o 4 8 22 1754.91 1901.03 71.31 o 5 8 22 470.07 379.62 47.16 o 0 9 22 628.03 717.54 50.14 o 1 9 22 823.25 824.15 50.99 o 2 9 22 1646.73 1632.61 66.10 o 3 9 22 51.63 86.45 60.75 o 4 9 22 6.93 0.00 56.18 o 0 10 22 5568.48 5371.41 111.87 o 1 10 22 6559.85 6835.97 124.37 o 2 10 22 1323.82 1241.67 64.50 o 2 0 23 816.46 686.71 41.75 o 4 0 23 178.51 281.76 35.47 o 6 0 23 1258.69 1314.89 58.55 o 1 1 23 7227.06 7158.15 109.33 o 2 1 23 6514.64 6572.33 105.35 o 3 1 23 14372.58 13921.52 149.87 o 4 1 23 1784.90 1709.86 58.88 o 5 1 23 3636.16 3462.87 84.77 o 6 1 23 24.08 19.33 49.81 o 7 1 23 7356.42 6986.83 128.68 o 1 2 23 2428.19 2383.85 64.64 o 2 2 23 29.48 0.00 52.04 o 3 2 23 85.07 77.42 29.74 o 4 2 23 816.62 851.90 47.38 o 5 2 23 5222.84 4895.05 103.78 o 6 2 23 804.71 718.34 48.23 o 7 2 23 502.44 444.63 43.55 o 1 3 23 227.65 235.78 31.12 o 2 3 23 15204.42 15183.22 156.99 o 3 3 23 717.54 661.07 42.07 o 4 3 23 15090.81 14964.83 170.31 o 5 3 23 20.68 9.45 57.03 o 6 3 23 18.67 0.00 57.35 o 7 3 23 1838.55 1983.65 69.61 o 1 4 23 93.61 94.62 30.27 o 2 4 23 419.16 482.86 38.66 o 3 4 23 107.53 91.55 30.16 o 4 4 23 8.39 22.94 51.51 o 5 4 23 355.06 277.85 42.59 o 6 4 23 1114.13 1031.75 56.20 o 7 4 23 0.67 -48.53 61.17 o 1 5 23 1982.79 2048.33 64.09 o 2 5 23 6027.17 6460.17 113.83 o 3 5 23 5329.86 5491.32 107.19 o 4 5 23 642.71 493.95 45.68 o 5 5 23 2502.27 2740.64 81.86 o 6 5 23 2492.63 2485.31 82.28 o 1 6 23 783.86 818.10 50.89 o 2 6 23 464.97 466.61 42.27 o 3 6 23 8.74 23.79 54.58 o 4 6 23 112.54 120.33 35.05 o 5 6 23 242.00 262.44 43.76 o 6 6 23 103.78 49.17 71.37 o 1 7 23 1755.97 1841.24 66.95 o 2 7 23 278.65 274.55 39.93 o 3 7 23 2382.53 2454.54 80.05 o 4 7 23 2946.40 2833.71 84.64 o 5 7 23 1173.67 1205.69 65.24 o 1 8 23 57.26 54.27 49.59 o 2 8 23 170.98 249.15 39.61 o 3 8 23 788.06 700.91 52.80 o 4 8 23 0.47 31.86 58.09 o 1 9 23 0.83 40.99 50.66 o 2 9 23 561.23 620.86 49.71 o 0 0 24 1874.12 1672.22 57.50 o 2 0 24 5890.89 5846.29 98.92 o 4 0 24 1121.57 1120.28 54.19 o 6 0 24 618.40 607.81 49.71 o 0 1 24 2749.75 2799.24 70.39 o 1 1 24 3791.46 3828.52 84.04 o 2 1 24 2552.11 2623.10 73.04 o 3 1 24 633.22 525.82 52.37 o 4 1 24 376.68 377.06 41.85 o 5 1 24 1090.51 996.16 55.89 o 6 1 24 6.00 45.77 29.84 o 7 1 24 60.01 64.25 62.76 o 0 2 24 6139.91 6379.37 103.19 o 1 2 24 642.00 684.42 42.60 o 2 2 24 640.13 634.07 42.70 o 3 2 24 883.47 914.92 50.04 o 4 2 24 458.02 573.89 43.55 o 5 2 24 619.88 654.55 50.67 o 6 2 24 238.01 269.55 42.27 o 0 3 24 2769.05 3027.39 74.96 o 1 3 24 568.93 599.63 41.53 o 2 3 24 3178.09 3241.55 84.44 o 3 3 24 206.24 270.82 37.49 o 4 3 24 1867.15 1904.68 73.87 o 5 3 24 176.13 290.15 36.64 o 6 3 24 655.20 618.76 50.03 o 0 4 24 164.34 106.95 57.77 o 1 4 24 3963.48 4034.68 91.70 o 2 4 24 2392.93 2389.49 75.27 o 3 4 24 991.85 893.39 55.46 o 4 4 24 1079.18 1154.99 56.73 o 5 4 24 1351.24 1376.23 64.28 o 6 4 24 104.45 158.13 35.79 o 0 5 24 948.49 978.15 54.50 o 1 5 24 894.23 949.44 53.54 o 2 5 24 3150.68 3207.89 85.71 o 3 5 24 36.14 -52.99 52.99 o 4 5 24 1943.71 2072.73 71.95 o 5 5 24 284.33 323.62 41.42 o 0 6 24 1810.37 1734.89 66.00 o 1 6 24 773.63 817.66 51.84 o 2 6 24 1133.81 1219.29 60.24 o 3 6 24 34.27 -40.14 69.35 o 4 6 24 23.33 67.86 33.24 o 5 6 24 3616.57 3755.19 98.27 o 0 7 24 1204.16 1204.98 56.95 o 1 7 24 110.43 162.49 36.43 o 2 7 24 914.39 813.03 56.09 o 3 7 24 2961.23 2950.65 91.33 o 4 7 24 1339.56 1411.26 68.32 o 0 8 24 498.82 564.44 47.59 o 1 8 24 166.50 181.39 39.72 o 2 8 24 673.52 744.74 52.90 o 2 0 25 102.33 133.92 34.94 o 4 0 25 2550.73 2429.32 76.76 o 6 0 25 4707.07 4695.32 109.17 o 1 1 25 569.60 626.40 48.86 o 2 1 25 62.88 55.12 55.12 o 3 1 25 807.57 790.16 49.08 o 4 1 25 669.41 776.09 48.33 o 5 1 25 13.56 96.21 52.78 o 6 1 25 13.39 101.10 50.66 o 1 2 25 442.34 396.40 41.32 o 2 2 25 1435.18 1480.98 61.74 o 3 2 25 563.05 588.89 43.98 o 4 2 25 1959.95 1984.54 71.95 o 5 2 25 1792.13 1775.00 68.23 o 1 3 25 325.98 421.34 40.89 o 2 3 25 184.97 285.69 38.02 o 3 3 25 2736.36 2770.28 77.72 o 4 3 25 274.34 272.64 39.51 o 5 3 25 373.67 374.72 41.10 o 1 4 25 103.04 113.00 34.94 o 2 4 25 5324.10 5348.92 108.25 o 3 4 25 19.88 91.86 31.97 o 4 4 25 2011.88 2018.14 75.04 o 5 4 25 1915.16 2029.29 76.20 o 1 5 25 49.75 84.00 62.66 o 2 5 25 5.15 99.61 57.66 o 3 5 25 1360.75 1361.78 63.12 o 4 5 25 762.56 732.87 53.86 o 1 6 25 2789.22 2875.73 85.48 o 2 6 25 3217.59 3223.73 89.00 o 3 6 25 9167.40 9275.46 148.59 o 1 7 25 689.75 718.72 52.05 o 2 7 25 15.25 80.18 60.74 o 0 0 26 1189.84 1205.52 55.36 o 2 0 26 2828.62 2860.65 82.61 o 4 0 26 7495.43 7547.88 131.88 o 0 1 26 1615.23 1636.87 66.52 o 1 1 26 70.04 84.22 36.64 o 2 1 26 15.87 24.32 57.98 o 3 1 26 6.20 -64.57 64.57 o 4 1 26 12.64 50.66 52.14 o 0 2 26 8011.63 8267.30 131.49 o 1 2 26 3515.97 3645.22 89.23 o 2 2 26 0.21 88.25 55.01 o 3 2 26 1268.43 1378.73 62.58 o 4 2 26 173.60 107.37 70.31 o 0 3 26 2571.08 2708.18 82.39 o 1 3 26 26.89 59.05 55.12 o 2 3 26 540.97 661.86 51.30 o 3 3 26 3.55 25.17 52.04 o 4 3 26 6.11 -10.41 61.91 o 0 4 26 15642.93 16270.74 187.49 o 1 4 26 2141.74 2152.50 75.68 o 2 4 26 226.69 235.99 40.25 o 3 4 26 201.69 227.81 40.36 o 0 5 26 1342.01 1459.09 65.24 o 1 5 26 15.16 33.13 36.96 o 2 5 26 0.32 -5.20 54.16 o 0 6 26 9.11 15.82 58.51 o 1 6 26 4860.65 5190.15 112.79 o 2 0 27 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