#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2013827.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013827_Fobs loop_ _publ_author_name 'Sonar, Vijayakumar N.' 'Parkin, Sean' 'Crooks, Peter A.' _publ_section_title ; (Z)-3-(1-Methyl-1H-indol-3-yl)-2-(thiophen-3-yl)acrylonitrile ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o217 _journal_page_last o218 _journal_volume 60 _journal_year 2004 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 113.237 _cell_angle_gamma 90.000 _cell_length_a 15.4031 _cell_length_b 5.8621 _cell_length_c 15.4902 _exptl_crystal_F_000 552.00 _reflns_d_resolution_high 0.8410 _[local]_cod_data_source_file na1640Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' k03223 - P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 167.70 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 120.35 108.67 4.47 o 2 0 0 23831.84 18187.85 800.00 o 3 0 0 1359.68 1058.89 43.15 o 4 0 0 454.45 436.60 11.19 o 5 0 0 98.52 108.03 3.84 o 6 0 0 559.99 505.00 12.15 o 7 0 0 36.90 36.76 3.20 o 8 0 0 2125.30 2345.99 55.29 o 9 0 0 1552.42 1471.52 34.84 o 10 0 0 696.92 663.85 17.90 o 11 0 0 93.46 70.64 6.07 o 12 0 0 149.36 135.84 8.31 o 13 0 0 68.92 78.31 11.83 o 14 0 0 375.96 322.81 33.24 o 15 0 0 39.25 32.60 21.73 o 16 0 0 55.95 41.55 19.50 o 1 1 0 1751.07 1784.56 39.58 o 2 1 0 379.21 368.38 12.15 o 3 1 0 1630.12 1443.98 31.64 o 4 1 0 1183.79 1050.65 21.89 o 5 1 0 77.31 76.19 5.75 o 6 1 0 258.96 202.79 10.23 o 7 1 0 737.39 687.48 12.63 o 8 1 0 1.27 14.49 14.06 o 9 1 0 107.35 109.02 3.58 o 10 1 0 0.23 -0.29 3.17 o 11 1 0 43.62 40.99 4.63 o 12 1 0 124.56 96.41 5.55 o 13 1 0 0.79 -9.26 31.96 o 14 1 0 19.75 15.87 9.24 o 15 1 0 1.14 -12.24 12.24 o 16 1 0 48.78 69.75 31.32 o 0 2 0 9.49 13.62 2.86 o 1 2 0 496.23 494.26 9.04 o 2 2 0 671.39 703.74 16.48 o 3 2 0 76.08 80.23 5.43 o 4 2 0 371.01 388.10 10.23 o 5 2 0 948.84 948.83 19.06 o 6 2 0 57.67 65.95 6.23 o 7 2 0 701.68 706.53 15.94 o 8 2 0 348.39 348.99 14.22 o 9 2 0 787.35 778.51 21.34 o 10 2 0 224.74 227.33 19.98 o 11 2 0 731.51 742.85 28.00 o 12 2 0 4.95 23.26 11.82 o 13 2 0 0.05 23.01 16.94 o 14 2 0 141.32 169.61 15.13 o 15 2 0 12.79 11.33 12.28 o 16 2 0 7.96 -1.35 15.02 o 1 3 0 2879.58 3218.08 70.65 o 2 3 0 320.24 268.72 14.06 o 3 3 0 215.85 229.98 7.99 o 4 3 0 17.48 16.61 6.39 o 5 3 0 0.11 -1.47 4.18 o 6 3 0 35.26 38.06 4.47 o 7 3 0 33.96 55.37 18.38 o 8 3 0 0.03 -6.51 16.14 o 9 3 0 128.77 149.56 10.73 o 10 3 0 435.58 510.83 23.18 o 11 3 0 7.31 12.02 15.50 o 12 3 0 34.69 9.11 10.62 o 13 3 0 63.34 69.08 13.89 o 14 3 0 13.23 16.85 18.74 o 15 3 0 17.22 30.22 18.01 o 0 4 0 7.85 6.39 4.79 o 1 4 0 0.00 0.96 4.47 o 2 4 0 4.14 -0.26 3.33 o 3 4 0 88.95 75.66 14.70 o 4 4 0 58.89 50.72 4.15 o 5 4 0 32.55 24.75 6.14 o 6 4 0 167.62 149.69 9.91 o 7 4 0 315.16 289.82 16.78 o 8 4 0 1.03 -16.37 21.89 o 9 4 0 903.79 1135.93 79.43 o 10 4 0 174.97 191.28 29.72 o 11 4 0 200.30 193.74 14.44 o 12 4 0 8.48 7.45 15.05 o 13 4 0 0.51 15.87 20.35 o 1 5 0 5.41 -3.84 7.99 o 2 5 0 23.88 32.28 16.62 o 3 5 0 111.92 104.95 19.82 o 4 5 0 498.71 487.75 40.27 o 5 5 0 1.56 6.00 6.82 o 6 5 0 0.19 3.38 24.93 o 7 5 0 1.02 4.15 31.16 o 8 5 0 8.04 -1.01 17.73 o 9 5 0 41.68 39.37 26.85 o 10 5 0 34.98 79.77 20.78 o 11 5 0 5.47 68.60 18.86 o 0 6 0 755.87 787.54 67.76 o 1 6 0 35.04 39.95 13.42 o 2 6 0 821.37 796.49 31.00 o 3 6 0 0.09 19.82 10.55 o 4 6 0 147.25 147.02 26.85 o 5 6 0 72.32 78.65 12.54 o 6 6 0 8.72 38.35 19.50 o 7 6 0 43.07 39.25 24.61 o 8 6 0 82.54 69.39 20.78 o -17 1 1 27.29 37.67 22.69 o -16 1 1 13.21 2.56 20.93 o -15 1 1 7.92 -4.92 25.73 o -14 1 1 0.19 -0.64 8.76 o -13 1 1 58.95 52.34 20.93 o -12 1 1 371.20 368.25 9.22 o -11 1 1 39.92 51.28 3.67 o -10 1 1 11.06 14.53 4.31 o -9 1 1 985.76 986.88 67.60 o -8 1 1 432.34 409.26 13.90 o -7 1 1 2623.01 2546.77 101.64 o -6 1 1 64.61 60.65 3.52 o -5 1 1 1991.74 1851.39 38.46 o -4 1 1 1870.59 1650.24 111.23 o -3 1 1 1896.20 1693.34 66.80 o -2 1 1 428.61 421.50 28.61 o -1 1 1 158.30 143.39 5.43 o 0 1 1 1007.60 997.80 20.61 o 1 1 1 5454.36 5619.58 138.56 o 2 1 1 1635.11 1485.11 29.47 o 3 1 1 338.33 302.95 8.95 o 4 1 1 8.52 3.93 1.46 o 5 1 1 262.32 262.20 14.22 o 6 1 1 43.20 47.90 6.71 o 7 1 1 257.39 268.99 7.30 o 8 1 1 18.55 30.39 3.30 o 9 1 1 13.09 17.21 6.71 o 10 1 1 17.93 15.12 7.35 o 11 1 1 214.83 200.92 11.03 o 12 1 1 578.37 561.45 18.41 o 13 1 1 1.21 12.87 9.90 o 14 1 1 40.36 16.21 11.81 o 15 1 1 5.07 21.17 13.90 o 16 1 1 3.15 17.75 16.43 o -16 2 1 1.36 -13.74 19.18 o -15 2 1 77.77 73.36 11.03 o -14 2 1 82.63 98.60 25.41 o -13 2 1 207.60 221.16 15.48 o -12 2 1 159.51 130.95 11.01 o -11 2 1 29.58 17.54 7.27 o -10 2 1 1845.29 1916.78 48.91 o -9 2 1 0.07 -0.73 3.84 o -8 2 1 1261.29 1384.71 48.26 o -7 2 1 380.93 401.92 10.06 o -6 2 1 314.88 298.06 8.37 o -5 2 1 5.24 3.67 1.53 o -4 2 1 9.31 6.71 2.56 o -3 2 1 44.32 45.31 6.23 o -2 2 1 259.03 248.96 18.70 o -1 2 1 1833.33 1790.27 35.05 o 0 2 1 2970.31 2898.54 53.92 o 1 2 1 92.41 76.05 2.95 o 2 2 1 113.41 137.75 4.53 o 3 2 1 3.97 7.80 2.72 o 4 2 1 55.88 56.90 3.52 o 5 2 1 3.16 11.75 10.23 o 6 2 1 181.47 181.20 4.31 o 7 2 1 0.11 -0.47 10.07 o 8 2 1 2.19 2.26 5.91 o 9 2 1 560.52 555.09 17.02 o 10 2 1 6.05 0.40 8.45 o 11 2 1 40.53 23.74 11.99 o 12 2 1 47.15 54.10 12.73 o 13 2 1 109.54 61.51 26.21 o 14 2 1 7.79 5.08 10.72 o 15 2 1 153.23 164.14 61.85 o -15 3 1 4.81 4.01 13.78 o -14 3 1 64.58 81.59 15.24 o -13 3 1 1.83 -3.85 16.78 o -12 3 1 124.94 135.70 12.77 o -11 3 1 91.16 96.70 12.82 o -10 3 1 299.49 290.51 22.21 o -9 3 1 71.25 61.39 7.82 o -8 3 1 30.73 30.01 6.09 o -7 3 1 628.35 606.88 36.60 o -6 3 1 326.55 317.02 8.60 o -5 3 1 30.27 23.98 7.19 o -4 3 1 758.30 829.68 25.11 o -3 3 1 221.77 234.98 12.31 o -2 3 1 251.29 250.36 10.23 o -1 3 1 193.18 165.51 12.94 o 0 3 1 238.32 226.03 8.63 o 1 3 1 793.62 771.20 15.82 o 2 3 1 2182.25 2401.60 106.27 o 3 3 1 1408.18 1522.04 57.05 o 4 3 1 834.70 910.99 24.01 o 5 3 1 495.50 496.18 11.67 o 6 3 1 310.27 289.49 16.46 o 7 3 1 315.98 300.52 8.37 o 8 3 1 76.99 81.43 8.03 o 9 3 1 167.43 165.35 18.86 o 10 3 1 495.49 521.97 24.84 o 11 3 1 293.30 273.32 34.52 o 12 3 1 232.10 263.46 17.32 o 13 3 1 26.63 30.31 14.27 o 14 3 1 2.86 -15.02 15.02 o -14 4 1 9.94 6.97 21.57 o -13 4 1 10.26 -20.62 20.62 o -12 4 1 0.26 15.33 13.07 o -11 4 1 19.24 9.12 23.01 o -10 4 1 348.35 403.30 69.68 o -9 4 1 50.67 60.45 19.98 o -8 4 1 1479.25 1772.42 146.23 o -7 4 1 0.01 -6.01 6.03 o -6 4 1 772.07 782.79 27.12 o -5 4 1 433.21 401.75 23.17 o -4 4 1 331.85 288.48 19.66 o -3 4 1 367.74 360.31 28.13 o -2 4 1 439.51 396.36 26.85 o -1 4 1 571.55 514.90 14.38 o 0 4 1 271.07 255.69 9.27 o 1 4 1 1127.84 1133.18 48.10 o 2 4 1 795.11 779.62 26.05 o 3 4 1 53.33 47.02 7.03 o 4 4 1 55.57 59.91 4.85 o 5 4 1 28.62 34.01 4.51 o 6 4 1 107.01 81.12 27.01 o 7 4 1 310.91 373.39 14.88 o 8 4 1 248.55 252.52 26.69 o 9 4 1 31.02 28.99 11.59 o 10 4 1 125.87 96.56 16.47 o 11 4 1 298.95 312.72 21.87 o 12 4 1 45.02 30.27 15.34 o 13 4 1 19.02 31.59 21.84 o -12 5 1 66.08 69.16 22.56 o -11 5 1 62.07 106.57 15.71 o -10 5 1 3.43 26.35 21.73 o -9 5 1 462.25 540.63 85.98 o -8 5 1 80.42 123.66 23.81 o -7 5 1 423.35 476.89 26.85 o -6 5 1 102.03 94.22 13.90 o -5 5 1 210.20 218.30 30.04 o -4 5 1 135.00 127.56 26.53 o -3 5 1 122.95 92.89 7.59 o -2 5 1 93.79 82.46 8.31 o -1 5 1 215.36 206.47 11.19 o 0 5 1 3.67 10.87 8.63 o 1 5 1 526.37 475.59 19.18 o 2 5 1 27.39 19.73 5.59 o 3 5 1 13.10 21.09 9.27 o 4 5 1 2.49 12.42 8.47 o 5 5 1 0.47 14.50 5.87 o 6 5 1 22.22 16.41 17.90 o 7 5 1 21.00 21.78 11.47 o 8 5 1 3.93 7.49 17.42 o 9 5 1 5.20 -15.67 15.67 o 10 5 1 70.83 90.11 22.78 o 11 5 1 15.85 42.41 29.25 o -8 6 1 77.19 90.40 28.93 o -7 6 1 97.87 96.28 25.41 o -6 6 1 31.34 39.66 11.90 o -5 6 1 222.12 201.74 56.57 o -4 6 1 95.31 103.56 14.38 o -3 6 1 144.78 123.05 17.26 o -2 6 1 0.75 2.56 10.23 o 0 6 1 176.95 125.61 22.05 o 1 6 1 95.71 94.93 15.34 o 2 6 1 54.34 56.89 10.23 o 3 6 1 11.51 16.30 16.30 o 4 6 1 170.45 181.10 46.98 o 5 6 1 86.80 84.44 16.81 o 6 6 1 299.48 286.52 28.77 o 7 6 1 10.41 -9.42 14.22 o 8 6 1 72.95 52.70 15.92 o -17 0 2 169.88 245.15 36.12 o -16 0 2 65.90 74.47 17.26 o -15 0 2 4.99 -2.88 11.19 o -14 0 2 42.07 14.70 8.63 o -13 0 2 333.48 329.21 14.70 o -12 0 2 690.01 681.74 20.78 o -11 0 2 48.74 61.37 7.03 o -10 0 2 203.53 188.57 7.67 o -9 0 2 199.26 145.11 7.35 o -8 0 2 1283.63 1099.17 31.64 o -7 0 2 263.13 268.48 11.83 o -6 0 2 824.30 752.38 26.53 o -5 0 2 1333.93 1121.54 36.12 o -4 0 2 2244.08 1735.84 49.22 o -3 0 2 2293.78 2010.08 55.61 o -2 0 2 22.90 15.98 0.96 o -1 0 2 602.58 602.16 15.34 o 0 0 2 108.64 100.36 2.56 o 1 0 2 1999.17 1699.41 45.71 o 2 0 2 2122.14 1846.75 52.74 o 3 0 2 884.52 681.74 19.18 o 4 0 2 362.44 338.48 9.59 o 5 0 2 5606.75 5225.11 134.56 o 6 0 2 1193.04 1143.91 27.81 o 7 0 2 1501.52 1438.92 30.68 o 8 0 2 1643.06 1646.35 37.08 o 9 0 2 1352.52 1421.98 36.44 o 10 0 2 62.77 64.24 7.03 o 11 0 2 618.80 673.12 23.01 o 12 0 2 4.90 -10.23 10.23 o 13 0 2 883.35 941.27 49.86 o 14 0 2 83.62 128.49 17.26 o 15 0 2 3.95 -23.65 23.65 o -17 1 2 285.44 378.97 23.17 o -16 1 2 14.86 15.35 11.64 o -15 1 2 232.33 264.22 14.58 o -14 1 2 381.03 389.08 12.60 o -13 1 2 148.39 131.40 15.02 o -12 1 2 648.82 674.52 29.25 o -11 1 2 6.79 4.68 4.63 o -10 1 2 235.47 220.48 4.90 o -9 1 2 921.35 831.05 18.54 o -8 1 2 352.97 327.61 6.91 o -7 1 2 1005.62 999.98 17.20 o -6 1 2 1238.62 1184.19 58.01 o -5 1 2 614.06 561.09 9.34 o -4 1 2 5.70 8.32 2.24 o -3 1 2 1197.95 1176.85 19.70 o -2 1 2 143.09 171.54 7.35 o -1 1 2 1778.80 1904.61 46.77 o 0 1 2 236.79 243.55 4.60 o 1 1 2 2.67 7.75 1.00 o 2 1 2 3261.83 2909.55 42.78 o 3 1 2 802.58 703.46 19.50 o 4 1 2 892.10 822.05 30.52 o 5 1 2 935.67 919.82 35.00 o 6 1 2 0.68 1.08 3.04 o 7 1 2 1142.35 1116.70 27.17 o 8 1 2 322.24 281.29 12.31 o 9 1 2 112.86 111.83 14.38 o 10 1 2 1007.04 979.76 26.34 o 11 1 2 8.90 -0.81 6.95 o 12 1 2 230.49 223.22 14.24 o 13 1 2 103.50 80.13 13.90 o 14 1 2 7.53 5.43 16.94 o 15 1 2 114.20 127.12 18.70 o -16 2 2 158.01 158.14 15.92 o -15 2 2 108.26 104.21 14.84 o -14 2 2 17.22 10.47 8.60 o -13 2 2 404.99 416.86 25.50 o -12 2 2 22.35 14.45 16.94 o -11 2 2 1326.78 1347.47 49.20 o -10 2 2 5.51 4.51 5.30 o -9 2 2 40.76 66.47 12.62 o -8 2 2 363.22 336.90 9.91 o -7 2 2 92.79 84.82 13.90 o -6 2 2 15.25 8.77 2.37 o -5 2 2 2863.92 3076.26 117.30 o -4 2 2 398.48 400.06 10.60 o -3 2 2 1639.06 1780.92 51.46 o -2 2 2 235.89 218.68 12.94 o -1 2 2 133.61 106.20 4.63 o 0 2 2 281.25 310.80 22.37 o 1 2 2 139.72 143.09 12.94 o 2 2 2 433.65 505.01 41.87 o 3 2 2 38.49 29.66 2.18 o 4 2 2 403.47 420.91 7.38 o 5 2 2 10.39 13.94 3.84 o 6 2 2 634.85 584.08 22.53 o 7 2 2 244.15 191.60 5.72 o 8 2 2 117.13 113.66 7.26 o 9 2 2 96.43 95.15 16.94 o 10 2 2 222.87 258.78 32.28 o 11 2 2 147.79 195.27 15.87 o 12 2 2 519.54 605.26 34.44 o 13 2 2 1.92 -7.18 22.85 o 14 2 2 182.71 181.65 21.66 o 15 2 2 0.03 -14.53 16.61 o -15 3 2 67.41 67.29 14.34 o -14 3 2 8.42 0.56 11.19 o -13 3 2 18.38 23.22 12.53 o -12 3 2 221.53 232.99 22.69 o -11 3 2 2.85 -6.80 20.93 o -10 3 2 13.98 21.75 8.78 o -9 3 2 3.84 -3.73 6.33 o -8 3 2 1.22 0.00 10.55 o -7 3 2 651.30 678.06 31.48 o -6 3 2 5.20 5.96 10.23 o -5 3 2 6.55 8.67 3.13 o -4 3 2 120.79 123.64 6.87 o -3 3 2 53.77 45.69 13.10 o -2 3 2 110.47 98.19 12.15 o -1 3 2 890.63 986.37 41.71 o 0 3 2 199.27 227.82 22.21 o 1 3 2 94.60 98.87 11.51 o 2 3 2 35.16 26.33 2.84 o 3 3 2 1012.88 1074.65 29.56 o 4 3 2 10.00 7.35 3.14 o 5 3 2 6.29 3.20 5.11 o 6 3 2 71.17 50.95 5.75 o 7 3 2 144.73 146.96 16.94 o 8 3 2 17.95 29.22 8.26 o 9 3 2 0.56 4.01 32.12 o 10 3 2 1.58 26.21 12.82 o 11 3 2 30.10 6.15 12.88 o 12 3 2 156.90 175.89 16.07 o 13 3 2 20.86 1.34 18.27 o 14 3 2 3.67 -20.90 20.90 o -14 4 2 1.62 7.84 30.52 o -13 4 2 20.88 35.58 16.62 o -12 4 2 30.71 52.62 35.00 o -11 4 2 42.82 47.62 19.50 o -10 4 2 6.66 13.40 12.78 o -9 4 2 3.23 6.39 9.60 o -8 4 2 18.23 26.41 7.67 o -7 4 2 7.15 14.81 6.39 o -6 4 2 35.29 28.18 4.73 o -5 4 2 101.88 84.55 13.42 o -4 4 2 321.08 311.59 11.13 o -3 4 2 213.06 207.18 7.51 o -2 4 2 366.67 343.81 10.31 o -1 4 2 256.33 238.48 22.69 o 0 4 2 36.83 33.27 6.07 o 1 4 2 16.45 10.23 8.15 o 2 4 2 71.73 73.97 5.26 o 3 4 2 64.45 50.20 8.20 o 4 4 2 24.93 23.18 6.71 o 5 4 2 65.63 58.51 4.66 o 6 4 2 87.95 83.71 23.49 o 7 4 2 153.43 142.79 7.81 o 8 4 2 26.40 4.81 9.01 o 9 4 2 56.98 81.88 10.72 o 10 4 2 15.33 4.09 12.83 o 11 4 2 43.48 46.39 19.85 o 12 4 2 31.72 16.25 32.28 o -12 5 2 12.93 32.99 18.38 o -11 5 2 3.31 -14.96 14.96 o -10 5 2 94.54 88.27 14.29 o -9 5 2 53.67 71.52 30.36 o -8 5 2 984.89 1125.38 37.51 o -7 5 2 168.69 153.10 10.98 o -6 5 2 734.51 819.05 27.64 o -5 5 2 160.58 140.81 9.15 o -4 5 2 168.17 161.43 9.39 o -3 5 2 204.45 178.78 24.29 o -2 5 2 30.93 41.87 7.03 o -1 5 2 779.91 833.24 41.23 o 0 5 2 320.83 327.61 15.66 o 1 5 2 7.69 -4.47 7.35 o 2 5 2 73.41 67.35 8.91 o 3 5 2 2.63 2.16 13.58 o 4 5 2 10.04 29.18 14.38 o 5 5 2 71.48 72.08 42.99 o 6 5 2 4.74 -11.01 16.02 o 7 5 2 32.69 -12.40 17.11 o 8 5 2 111.64 117.79 19.70 o 9 5 2 0.10 2.22 23.49 o 10 5 2 24.98 23.22 19.73 o -9 6 2 12.74 -1.86 15.00 o -8 6 2 34.60 31.86 14.64 o -7 6 2 1.66 22.35 16.78 o -6 6 2 23.88 11.54 10.04 o -5 6 2 8.37 28.96 10.33 o -4 6 2 0.46 13.70 8.54 o -3 6 2 30.15 6.39 9.59 o -2 6 2 31.86 16.30 13.42 o 0 6 2 0.83 -13.10 13.10 o 1 6 2 4.61 -1.92 10.87 o 2 6 2 65.05 54.97 14.06 o 3 6 2 193.04 185.57 27.33 o 4 6 2 34.06 13.75 15.57 o 5 6 2 200.16 190.00 20.23 o 6 6 2 22.82 9.14 19.18 o 7 6 2 126.62 126.12 19.83 o -17 1 3 112.56 158.68 23.33 o -16 1 3 70.41 95.75 14.70 o -15 1 3 0.02 2.92 9.97 o -14 1 3 846.18 863.51 25.11 o -13 1 3 264.71 261.22 23.17 o -12 1 3 169.99 174.94 12.78 o -11 1 3 43.66 41.20 4.16 o -10 1 3 6.95 3.28 3.27 o -9 1 3 92.12 102.32 5.91 o -8 1 3 215.37 218.08 8.63 o -7 1 3 733.76 685.74 27.17 o -6 1 3 5.17 -0.21 1.68 o -5 1 3 70.75 61.47 2.00 o -4 1 3 128.13 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