#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/38/2013830.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013830_Fobs loop_ _publ_author_name 'Yilmaz, Veysel T.' 'Caglar, Sema' 'Harrison, William T. A.' _publ_section_title ; Bis(saccharinato-\kN)zinc(II) complexes with N,N'-bidentate 2-aminomethylpyridine and 2-aminoethylpyridine ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m35 _journal_page_last m38 _journal_volume 60 _journal_year 2004 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.522 _cell_angle_gamma 90.000 _cell_length_a 9.1654 _cell_length_b 13.9784 _cell_length_c 17.4679 _exptl_crystal_F_000 1128.00 _reflns_d_resolution_high 0.7099 _[local]_cod_data_source_file ob1151IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' vty16 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 240.18 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 9994.72 10346.30 72.25 o 4 0 0 3425.59 3532.91 71.05 o 6 0 0 12995.00 13032.91 97.77 o 8 0 0 336.52 279.57 19.50 o 10 0 0 156.58 161.94 33.05 o 12 0 0 184.49 206.22 42.30 o 1 1 0 549.33 583.40 7.69 o 2 1 0 53.94 51.00 5.02 o 3 1 0 8959.58 8649.96 52.69 o 4 1 0 1198.69 1243.47 14.12 o 5 1 0 115.48 101.54 7.55 o 6 1 0 894.69 810.07 15.46 o 7 1 0 3.00 -4.49 9.52 o 8 1 0 1041.68 1019.74 21.83 o 9 1 0 502.76 455.14 29.56 o 10 1 0 25.60 57.47 28.09 o 11 1 0 87.47 73.57 24.35 o 12 1 0 63.83 54.28 24.98 o 0 2 0 17244.74 17160.41 130.87 o 1 2 0 5667.60 5522.85 64.78 o 2 2 0 10781.78 10945.57 54.61 o 3 2 0 3155.77 3281.91 24.58 o 4 2 0 969.30 913.24 12.84 o 5 2 0 34.92 28.57 6.74 o 6 2 0 148.26 112.31 9.00 o 7 2 0 3494.73 3488.32 31.44 o 8 2 0 192.61 201.99 15.73 o 9 2 0 124.80 116.81 21.26 o 10 2 0 25.55 41.53 20.33 o 11 2 0 0.15 0.00 21.81 o 12 2 0 153.82 166.34 28.38 o 1 3 0 3327.72 3454.50 40.60 o 2 3 0 305.84 335.42 10.30 o 3 3 0 7306.01 7352.48 47.62 o 4 3 0 1625.51 1533.56 19.55 o 5 3 0 2174.71 2126.96 25.02 o 6 3 0 1035.84 984.10 22.04 o 7 3 0 107.21 92.35 11.97 o 8 3 0 158.82 144.27 15.11 o 9 3 0 897.08 881.35 27.87 o 10 3 0 71.89 64.88 22.31 o 11 3 0 150.31 151.02 25.47 o 12 3 0 7.74 9.85 27.10 o 0 4 0 12.27 24.11 9.00 o 1 4 0 14.94 17.85 5.95 o 2 4 0 6224.02 6491.06 65.82 o 3 4 0 5189.39 5350.81 40.67 o 4 4 0 1413.39 1573.67 24.38 o 5 4 0 4774.76 4743.58 38.69 o 6 4 0 905.78 884.46 19.65 o 7 4 0 1248.61 1185.23 23.63 o 8 4 0 730.48 726.08 24.58 o 9 4 0 1487.74 1504.99 35.21 o 10 4 0 91.37 110.32 22.06 o 11 4 0 131.12 169.90 25.32 o 12 4 0 0.34 23.01 24.65 o 1 5 0 1646.70 1435.43 14.51 o 2 5 0 8495.57 8258.80 67.30 o 3 5 0 3503.76 3638.30 33.87 o 4 5 0 3217.07 3042.46 54.06 o 5 5 0 4730.13 4807.78 49.69 o 6 5 0 826.51 756.31 19.18 o 7 5 0 48.69 36.82 11.77 o 8 5 0 362.86 345.69 16.14 o 9 5 0 73.08 78.33 14.87 o 10 5 0 360.88 352.38 28.98 o 11 5 0 90.79 100.98 23.32 o 12 5 0 79.24 101.96 25.19 o 0 6 0 13412.47 14233.33 175.49 o 1 6 0 6491.70 6567.70 35.80 o 2 6 0 354.30 433.27 10.73 o 3 6 0 5.58 10.48 8.56 o 4 6 0 178.89 165.20 12.34 o 5 6 0 230.85 219.78 15.73 o 6 6 0 59.35 44.92 11.24 o 7 6 0 1490.80 1508.94 27.19 o 8 6 0 131.71 130.25 13.61 o 9 6 0 15.81 -6.27 13.65 o 10 6 0 0.72 8.93 17.88 o 11 6 0 59.93 96.13 23.70 o 12 6 0 11.07 30.69 22.53 o 1 7 0 311.77 367.21 9.88 o 2 7 0 6080.89 6247.27 39.65 o 3 7 0 135.49 140.37 10.80 o 4 7 0 962.33 831.25 20.10 o 5 7 0 1.32 -3.21 11.49 o 6 7 0 8.33 16.18 10.84 o 7 7 0 223.31 196.89 13.95 o 8 7 0 17.51 18.82 11.45 o 9 7 0 104.55 111.87 16.47 o 10 7 0 100.68 110.12 22.19 o 11 7 0 13.82 9.09 21.27 o 0 8 0 3860.55 3967.80 38.35 o 1 8 0 8173.53 8126.75 43.50 o 2 8 0 148.83 148.13 9.05 o 3 8 0 108.77 125.61 10.02 o 4 8 0 1224.12 1207.84 24.11 o 5 8 0 2075.46 2019.79 33.99 o 6 8 0 187.78 161.34 15.00 o 7 8 0 470.17 488.58 18.33 o 8 8 0 5.67 -7.01 11.08 o 9 8 0 234.13 256.71 19.65 o 10 8 0 10.83 29.07 19.36 o 11 8 0 7.65 -12.93 19.83 o 1 9 0 62.76 79.40 12.91 o 2 9 0 2214.42 2252.26 23.61 o 3 9 0 1480.18 1517.73 34.20 o 4 9 0 3859.71 3933.16 42.55 o 5 9 0 2.56 9.94 10.63 o 6 9 0 101.19 98.18 13.72 o 7 9 0 5.67 -2.50 10.52 o 8 9 0 5.82 0.34 11.87 o 9 9 0 104.63 128.89 17.65 o 10 9 0 566.47 592.52 34.70 o 11 9 0 23.17 43.37 22.44 o 0 10 0 44.85 50.23 27.43 o 1 10 0 2143.67 2103.29 47.18 o 2 10 0 3759.68 3495.06 58.82 o 3 10 0 12.33 20.62 13.14 o 4 10 0 2555.96 2567.14 49.14 o 5 10 0 4.76 -10.31 12.28 o 6 10 0 526.50 513.80 21.79 o 7 10 0 1231.49 1238.95 32.37 o 8 10 0 744.84 798.27 28.68 o 9 10 0 21.30 8.24 19.57 o 10 10 0 5.50 -1.32 28.42 o 1 11 0 1126.49 1112.24 39.08 o 2 11 0 232.86 216.38 23.76 o 3 11 0 57.50 76.07 22.78 o 4 11 0 179.88 212.65 23.34 o 5 11 0 2108.93 1996.92 61.97 o 6 11 0 195.88 203.41 20.76 o 7 11 0 21.32 42.00 14.48 o 8 11 0 201.42 219.33 20.15 o 9 11 0 67.85 60.27 21.44 o 10 11 0 2.14 -6.91 20.19 o 0 12 0 1879.18 1916.81 71.38 o 1 12 0 409.18 346.50 27.74 o 2 12 0 323.05 366.58 29.31 o 3 12 0 89.52 94.30 22.39 o 4 12 0 31.57 13.63 19.09 o 5 12 0 18.53 12.20 18.39 o 6 12 0 764.41 747.48 35.38 o 7 12 0 152.95 196.83 25.00 o 8 12 0 329.07 342.44 28.98 o 9 12 0 2.47 33.38 31.40 o 10 12 0 0.45 0.00 32.39 o 1 13 0 736.75 709.47 57.50 o 2 13 0 6.65 12.12 22.02 o 3 13 0 1015.15 1050.25 41.17 o 4 13 0 112.51 139.60 24.53 o 5 13 0 802.78 775.10 37.03 o 6 13 0 15.25 0.33 27.43 o 7 13 0 15.21 47.59 33.71 o 8 13 0 36.05 24.42 20.48 o 9 13 0 94.79 106.75 35.69 o 0 14 0 2228.51 2072.80 77.33 o 1 14 0 49.53 53.63 24.35 o 2 14 0 894.06 836.73 48.09 o 3 14 0 52.34 54.08 22.95 o 4 14 0 67.47 86.47 22.81 o 5 14 0 153.78 150.03 24.53 o 6 14 0 337.62 337.09 45.28 o 7 14 0 131.20 183.09 41.31 o 8 14 0 31.42 73.80 23.48 o 1 15 0 69.50 40.37 23.01 o 2 15 0 138.55 93.51 24.07 o 3 15 0 596.22 589.53 35.40 o 4 15 0 912.14 805.02 39.82 o 5 15 0 9.92 -2.21 21.11 o 6 15 0 5.05 -17.85 29.74 o 7 15 0 99.28 120.96 39.00 o 8 15 0 11.83 45.87 23.19 o 0 16 0 1834.06 1726.45 78.99 o 1 16 0 505.00 446.79 34.81 o 2 16 0 139.49 107.21 25.24 o 3 16 0 14.35 17.21 23.65 o 4 16 0 8.75 9.19 23.52 o 5 16 0 17.57 12.64 24.75 o 6 16 0 110.56 70.72 37.68 o 7 16 0 17.07 35.69 36.68 o 1 17 0 19.19 11.09 24.99 o 2 17 0 101.18 81.79 26.17 o 3 17 0 194.69 213.03 30.52 o 4 17 0 145.73 164.64 29.63 o 5 17 0 19.08 17.33 24.98 o 6 17 0 5.90 14.54 38.34 o 0 18 0 253.40 233.65 46.93 o 1 18 0 241.01 209.13 31.20 o 2 18 0 15.49 21.08 26.50 o 3 18 0 8.49 -20.23 24.84 o 4 18 0 19.80 -0.98 25.08 o 5 18 0 15.43 41.97 39.00 o 1 19 0 110.94 159.24 31.41 o 2 19 0 162.71 215.98 36.52 o 3 19 0 5.50 12.41 26.86 o -11 0 1 0.29 19.83 29.41 o -9 0 1 234.39 201.27 33.38 o -7 0 1 5282.71 5122.17 62.85 o -5 0 1 752.81 754.04 25.61 o -3 0 1 1395.39 1433.55 15.86 o -1 0 1 30607.46 28292.85 165.24 o 1 0 1 939.10 1126.74 136.99 o 3 0 1 7078.45 7494.19 59.98 o 5 0 1 158.13 169.29 12.26 o 7 0 1 590.12 590.87 38.83 o 9 0 1 131.14 115.67 30.40 o 11 0 1 187.90 169.54 36.68 o -12 1 1 308.47 368.14 34.45 o -11 1 1 0.21 -19.77 30.40 o -10 1 1 281.43 298.98 29.91 o -9 1 1 57.44 53.26 14.13 o -8 1 1 8.68 15.90 9.65 o -7 1 1 287.75 285.29 14.12 o -6 1 1 2694.11 2694.40 24.94 o -5 1 1 735.23 706.81 12.44 o -4 1 1 3546.17 3250.48 22.56 o -3 1 1 1899.11 1901.51 15.97 o -2 1 1 75.80 92.11 6.32 o -1 1 1 2421.51 2465.00 46.56 o 1 1 1 4032.44 4187.89 25.73 o 2 1 1 22938.78 22625.06 122.62 o 3 1 1 10011.28 10696.15 102.28 o 4 1 1 1061.55 1243.03 14.16 o 5 1 1 2630.59 2659.01 23.80 o 6 1 1 1717.49 1798.61 23.59 o 7 1 1 1.08 1.13 9.04 o 8 1 1 891.61 848.64 25.56 o 9 1 1 112.70 124.48 21.62 o 10 1 1 99.73 74.96 21.37 o 11 1 1 120.88 167.90 28.59 o 12 1 1 327.12 359.54 49.08 o -12 2 1 103.95 80.74 25.82 o -11 2 1 21.37 19.02 24.13 o -10 2 1 357.72 357.45 28.97 o -9 2 1 1014.25 1031.44 29.02 o -8 2 1 45.07 61.77 10.93 o -7 2 1 1409.29 1375.44 20.37 o -6 2 1 1093.10 1075.99 16.88 o -5 2 1 5317.69 5537.68 44.87 o -4 2 1 5053.76 5256.62 35.65 o -3 2 1 4790.68 4903.90 67.81 o -2 2 1 26316.50 26382.39 106.70 o -1 2 1 42796.69 39266.62 266.89 o 0 2 1 17886.51 18297.67 101.84 o 1 2 1 452.65 420.17 7.41 o 2 2 1 937.39 1013.03 13.42 o 3 2 1 681.71 683.38 14.02 o 4 2 1 4608.89 4835.82 34.12 o 5 2 1 7229.80 7328.66 73.60 o 6 2 1 4551.41 4429.46 38.54 o 7 2 1 69.14 56.52 10.99 o 8 2 1 33.30 21.55 14.00 o 9 2 1 357.40 355.08 27.22 o 10 2 1 0.29 6.30 18.46 o 11 2 1 295.72 307.41 36.19 o 12 2 1 22.91 13.51 23.48 o -12 3 1 32.78 49.92 24.74 o -11 3 1 127.52 112.88 23.84 o -10 3 1 515.97 527.98 32.78 o -9 3 1 695.16 677.63 25.19 o -8 3 1 521.46 543.77 21.83 o -7 3 1 565.01 547.95 17.34 o -6 3 1 420.55 429.32 17.94 o -5 3 1 170.49 172.29 10.24 o -4 3 1 1051.32 967.93 29.07 o -3 3 1 2205.41 1674.42 21.44 o -2 3 1 8530.61 8803.57 66.96 o -1 3 1 5980.67 6212.43 35.51 o 0 3 1 189.78 200.79 9.27 o 1 3 1 5704.51 5791.38 52.90 o 2 3 1 257.89 270.42 10.23 o 3 3 1 10302.43 9973.02 105.01 o 4 3 1 5251.60 5403.77 37.58 o 5 3 1 585.30 553.63 14.70 o 6 3 1 511.50 497.21 15.52 o 7 3 1 0.16 9.89 10.79 o 8 3 1 3.35 4.38 11.69 o 9 3 1 203.13 180.08 23.24 o 10 3 1 604.96 638.65 48.58 o 11 3 1 10.22 14.21 21.48 o 12 3 1 34.84 28.44 24.94 o -12 4 1 37.95 43.62 32.39 o -11 4 1 49.56 27.89 22.31 o -10 4 1 91.71 100.34 21.10 o -9 4 1 91.03 97.37 20.69 o -8 4 1 902.83 902.38 26.98 o -7 4 1 3083.26 3106.96 46.13 o -6 4 1 174.41 139.35 11.70 o -5 4 1 2093.26 2140.94 25.61 o -4 4 1 3341.09 3533.41 42.65 o -3 4 1 462.21 497.42 13.25 o -2 4 1 4027.35 4155.45 51.19 o -1 4 1 495.20 501.65 9.28 o 0 4 1 3364.68 3574.85 41.31 o 1 4 1 10475.01 10506.13 65.49 o 2 4 1 4433.29 4598.29 33.97 o 3 4 1 465.44 453.20 13.58 o 4 4 1 4888.19 5017.18 37.47 o 5 4 1 593.55 572.05 17.12 o 6 4 1 2609.89 2522.12 32.53 o 7 4 1 2020.05 1897.57 46.60 o 8 4 1 323.50 297.29 15.32 o 9 4 1 25.84 40.12 18.78 o 10 4 1 3.82 -8.38 18.92 o 11 4 1 13.93 4.12 21.22 o 12 4 1 214.16 243.39 30.02 o -12 5 1 27.40 25.39 22.38 o -11 5 1 49.03 61.17 22.11 o -10 5 1 18.31 10.59 18.42 o -9 5 1 407.76 389.16 21.18 o -8 5 1 0.36 -0.68 12.71 o -7 5 1 165.31 153.02 13.08 o -6 5 1 375.51 377.18 15.27 o -5 5 1 1329.33 1223.95 24.75 o -4 5 1 19.23 19.26 8.98 o -3 5 1 7099.44 7015.68 47.97 o -2 5 1 468.45 547.46 19.82 o -1 5 1 4.55 11.47 5.32 o 0 5 1 839.21 906.35 15.29 o 1 5 1 3154.53 3192.80 40.31 o 2 5 1 1467.63 1487.00 17.22 o 3 5 1 8220.92 7978.00 88.67 o 4 5 1 1409.94 1447.07 24.66 o 5 5 1 1727.96 1679.15 24.71 o 6 5 1 16.00 16.53 10.85 o 7 5 1 98.81 93.90 12.65 o 8 5 1 853.53 842.55 23.32 o 9 5 1 619.67 598.39 32.24 o 10 5 1 12.33 12.65 18.68 o 11 5 1 64.75 90.83 23.68 o 12 5 1 4.58 3.67 22.22 o -12 6 1 0.78 7.52 22.55 o -11 6 1 0.54 0.35 19.74 o -10 6 1 69.30 19.01 19.59 o -9 6 1 8.47 2.61 12.76 o -8 6 1 1746.76 1693.72 35.99 o -7 6 1 367.37 376.30 16.37 o -6 6 1 3964.30 3869.57 41.45 o -5 6 1 89.83 80.15 12.41 o -4 6 1 151.26 145.22 11.95 o -3 6 1 80.74 97.45 9.54 o -2 6 1 1979.96 2110.11 22.50 o -1 6 1 1705.57 1850.43 22.63 o 0 6 1 25085.78 26455.11 197.12 o 1 6 1 436.56 407.58 9.44 o 2 6 1 3846.85 4268.32 30.42 o 3 6 1 1305.92 1367.75 30.74 o 4 6 1 22.67 27.75 10.28 o 5 6 1 52.85 41.36 10.44 o 6 6 1 439.94 399.76 16.46 o 7 6 1 1195.27 1203.70 24.91 o 8 6 1 794.93 793.29 22.25 o 9 6 1 120.73 148.34 17.19 o 10 6 1 66.16 68.76 20.78 o 11 6 1 0.87 -2.55 20.28 o -11 7 1 478.31 487.51 49.57 o -10 7 1 121.86 127.49 17.72 o -9 7 1 114.08 103.30 16.82 o -8 7 1 48.46 40.83 11.77 o -7 7 1 0.20 -4.00 10.27 o -6 7 1 1.68 -0.21 12.77 o -5 7 1 6292.61 6280.01 56.20 o -4 7 1 670.18 659.79 19.20 o -3 7 1 2294.73 2319.89 27.73 o -2 7 1 523.13 598.35 12.24 o -1 7 1 60.40 148.51 16.64 o 0 7 1 1444.31 1645.08 25.45 o 1 7 1 8484.34 8321.38 84.05 o 2 7 1 4117.98 4605.11 41.60 o 3 7 1 965.64 903.66 16.73 o 4 7 1 2802.83 2622.52 33.93 o 5 7 1 911.68 968.66 27.65 o 6 7 1 479.03 450.23 17.02 o 7 7 1 271.98 276.70 15.23 o 8 7 1 297.14 297.12 16.52 o 9 7 1 475.34 483.82 23.75 o 10 7 1 171.69 195.41 24.98 o 11 7 1 174.60 188.62 26.61 o -11 8 1 11.91 -7.68 19.09 o -10 8 1 21.90 4.51 15.17 o -9 8 1 10.01 7.71 13.80 o -8 8 1 1336.84 1401.41 28.98 o -7 8 1 482.53 464.55 17.92 o -6 8 1 58.94 37.22 16.78 o -5 8 1 0.16 -10.73 11.53 o -4 8 1 3705.64 3697.33 39.62 o -3 8 1 107.65 105.38 10.57 o -2 8 1 9116.47 8627.76 91.44 o -1 8 1 765.98 853.88 18.99 o 0 8 1 1013.07 953.24 32.90 o 1 8 1 1729.69 1829.61 18.94 o 2 8 1 6894.41 6978.12 42.84 o 3 8 1 94.66 88.92 10.15 o 4 8 1 3757.96 3790.06 36.19 o 5 8 1 127.74 98.56 12.03 o 6 8 1 63.40 73.08 11.66 o 7 8 1 10.94 21.00 11.17 o 8 8 1 80.99 90.85 13.29 o 9 8 1 0.43 -3.37 13.77 o 10 8 1 104.90 125.10 24.18 o 11 8 1 0.02 0.52 20.97 o -11 9 1 207.15 243.90 39.66 o -10 9 1 497.82 522.84 26.45 o -9 9 1 1.23 6.65 14.73 o -8 9 1 454.71 442.99 19.53 o -7 9 1 130.04 122.03 13.35 o -6 9 1 307.42 332.24 18.19 o -5 9 1 1267.33 1248.58 26.86 o -4 9 1 2051.31 1993.83 30.21 o -3 9 1 1236.88 1265.20 19.94 o -2 9 1 16.45 28.68 7.73 o -1 9 1 1886.04 1867.71 27.35 o 0 9 1 95.92 77.42 12.03 o 1 9 1 3966.91 3857.30 44.51 o 2 9 1 436.83 425.70 13.07 o 3 9 1 146.45 110.52 10.50 o 4 9 1 2458.11 2317.07 29.26 o 5 9 1 692.54 652.24 18.74 o 6 9 1 33.36 17.85 9.84 o 7 9 1 212.75 218.88 15.52 o 8 9 1 37.89 27.85 12.29 o 9 9 1 40.37 51.55 15.52 o 10 9 1 254.14 282.94 28.50 o 11 9 1 367.27 421.18 32.93 o -11 10 1 4.90 16.52 31.07 o -10 10 1 174.71 180.36 25.23 o -9 10 1 562.22 601.22 34.06 o -8 10 1 928.79 922.63 30.02 o -7 10 1 902.61 873.62 35.16 o -6 10 1 152.14 152.05 20.10 o -5 10 1 1125.51 1108.48 28.01 o -4 10 1 52.04 48.99 14.80 o -3 10 1 59.04 42.02 13.60 o -2 10 1 1664.78 1668.88 29.28 o -1 10 1 127.17 119.15 23.10 o 0 10 1 987.46 973.06 59.16 o 1 10 1 772.75 719.80 31.97 o 2 10 1 368.60 371.57 27.13 o 3 10 1 179.92 187.42 15.35 o 4 10 1 105.90 109.12 12.75 o 5 10 1 1063.00 1067.06 22.66 o 6 10 1 3.86 5.12 10.40 o 7 10 1 317.48 329.62 17.27 o 8 10 1 10.60 24.61 19.67 o 9 10 1 105.85 130.09 22.19 o 10 10 1 27.10 42.30 31.07 o -10 11 1 33.72 60.17 38.83 o -9 11 1 23.82 -9.56 21.15 o -8 11 1 2.88 12.48 14.91 o -7 11 1 184.92 170.05 22.47 o -6 11 1 677.52 663.00 32.57 o -5 11 1 353.27 341.25 19.63 o -4 11 1 532.19 560.03 34.87 o -3 11 1 443.52 433.69 28.77 o -2 11 1 378.29 367.86 28.96 o -1 11 1 430.85 423.43 28.47 o 0 11 1 143.20 148.99 24.12 o 1 11 1 1442.59 1402.88 77.50 o 2 11 1 142.29 122.35 30.24 o 3 11 1 2.38 14.14 21.25 o 4 11 1 1405.27 1380.52 41.68 o 5 11 1 308.10 288.87 28.42 o 6 11 1 12.72 -4.30 28.75 o 7 11 1 81.43 85.80 21.02 o 8 11 1 218.81 239.43 26.40 o 9 11 1 10.00 30.40 29.74 o -10 12 1 13.40 27.43 31.07 o -9 12 1 8.08 18.84 32.39 o -8 12 1 10.30 6.35 19.28 o -7 12 1 1732.40 1841.46 78.32 o -6 12 1 223.97 223.90 24.32 o -5 12 1 54.31 17.70 20.72 o -4 12 1 228.58 205.35 24.77 o -3 12 1 48.72 44.64 19.93 o -2 12 1 18.03 14.62 19.29 o -1 12 1 1816.48 1795.74 48.83 o 0 12 1 1133.37 1045.95 40.43 o 1 12 1 828.13 801.17 36.76 o 2 12 1 16.90 21.24 21.97 o 3 12 1 1229.91 1153.32 40.12 o 4 12 1 2.33 0.79 19.25 o 5 12 1 236.43 261.26 26.06 o 6 12 1 515.78 554.88 48.25 o 7 12 1 1212.77 1221.01 44.41 o 8 12 1 163.95 192.26 27.00 o 9 12 1 131.85 148.72 36.02 o -9 13 1 290.73 314.29 45.61 o -8 13 1 30.47 59.88 21.80 o -7 13 1 74.74 131.86 37.01 o -6 13 1 115.61 127.75 23.50 o -5 13 1 829.74 805.82 39.49 o -4 13 1 890.22 856.92 38.68 o -3 13 1 45.96 60.17 22.87 o -2 13 1 242.63 239.32 27.15 o -1 13 1 3117.45 2883.33 62.16 o 0 13 1 154.07 159.44 24.27 o 1 13 1 1445.05 1464.36 45.09 o 2 13 1 356.03 336.10 29.01 o 3 13 1 491.36 447.23 35.36 o 4 13 1 533.48 516.62 50.89 o 5 13 1 17.85 18.33 20.33 o 6 13 1 115.62 130.54 36.68 o 7 13 1 170.58 171.52 25.33 o 8 13 1 53.25 69.57 23.84 o 9 13 1 33.07 53.21 33.38 o -9 14 1 95.22 116.99 38.01 o -8 14 1 0.28 0.74 20.96 o -7 14 1 174.68 161.61 40.98 o -6 14 1 40.76 35.66 20.87 o -5 14 1 373.88 348.32 29.48 o -4 14 1 97.49 103.24 24.29 o -3 14 1 135.15 125.18 25.06 o -2 14 1 268.90 242.75 26.33 o -1 14 1 2917.39 2865.12 65.04 o 0 14 1 91.23 74.79 37.68 o 1 14 1 794.13 770.45 38.42 o 2 14 1 6.37 5.86 22.22 o 3 14 1 29.50 16.36 21.03 o 4 14 1 74.87 77.08 23.37 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