#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:53:42 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180808 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/39/2013936.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013936_Fobs loop_ _publ_author_name 'Byres, Maureen' 'Cox, Philip J.' _publ_section_title ; The supramolecular structure of 6-hydroxy-1,3-benzoxathiol-2-one (tioxolone) ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o395 _journal_page_last o396 _journal_volume 60 _journal_year 2004 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.424 _cell_angle_gamma 90.000 _cell_length_a 3.7620 _cell_length_b 10.6860 _cell_length_c 16.4470 _exptl_crystal_F_000 344.00 _reflns_d_resolution_high 0.7700 _cod_data_source_file bm1566Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' C7H4O3S in P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 173.37 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 6023.80 5893.95 172.08 o 2 0 0 737.65 705.31 18.00 o 3 0 0 1252.77 1331.29 32.47 o 4 0 0 13.56 -11.25 11.51 o 1 1 0 1142.58 1135.55 18.62 o 2 1 0 54.09 60.18 3.17 o 3 1 0 4.75 7.49 4.02 o 4 1 0 23.61 14.06 8.13 o 0 2 0 11403.88 10987.02 195.70 o 1 2 0 17.37 32.35 3.40 o 2 2 0 6.90 9.05 3.01 o 3 2 0 11.51 18.07 3.90 o 4 2 0 4.05 10.75 8.32 o 1 3 0 154.30 140.72 2.74 o 2 3 0 328.33 322.39 9.66 o 3 3 0 111.98 95.05 7.46 o 4 3 0 173.09 169.90 10.46 o 0 4 0 7665.81 8241.50 182.91 o 1 4 0 1475.34 1531.93 20.14 o 2 4 0 781.68 730.47 16.52 o 3 4 0 553.20 541.28 13.14 o 4 4 0 78.82 65.53 12.13 o 1 5 0 168.40 153.94 2.95 o 2 5 0 140.27 133.56 4.02 o 3 5 0 14.72 19.31 4.12 o 4 5 0 15.77 17.13 8.35 o 0 6 0 1450.32 1642.33 50.40 o 1 6 0 14.62 22.22 3.37 o 2 6 0 0.63 -2.63 2.63 o 3 6 0 4.38 11.39 5.64 o 4 6 0 232.17 211.87 12.63 o 1 7 0 481.31 469.98 9.59 o 2 7 0 92.43 93.21 4.16 o 3 7 0 267.89 262.87 12.57 o 4 7 0 304.48 258.70 13.94 o 0 8 0 471.12 422.24 8.89 o 1 8 0 260.37 265.48 8.19 o 2 8 0 727.42 688.21 11.17 o 3 8 0 78.74 85.35 6.84 o 1 9 0 211.20 186.05 6.46 o 2 9 0 48.23 54.33 6.94 o 3 9 0 10.57 15.54 5.60 o 0 10 0 18.82 14.81 3.95 o 1 10 0 21.79 16.12 4.12 o 2 10 0 85.71 96.21 8.67 o 3 10 0 129.51 167.61 22.31 o 1 11 0 355.11 377.98 13.03 o 2 11 0 194.84 216.33 19.60 o 0 12 0 140.47 164.71 27.50 o 1 12 0 6.01 0.00 9.08 o 2 12 0 66.56 50.61 18.61 o 1 13 0 192.48 215.81 24.24 o -4 1 1 117.72 100.02 11.42 o -3 1 1 1.42 4.99 5.42 o -2 1 1 75.64 63.12 3.17 o -1 1 1 80.75 84.43 3.17 o 1 1 1 78.22 91.53 3.18 o 2 1 1 355.63 343.87 7.50 o 3 1 1 27.01 22.10 4.37 o 4 1 1 217.22 217.79 13.11 o -4 2 1 102.26 85.65 9.34 o -3 2 1 798.36 826.20 13.85 o -2 2 1 684.52 667.26 12.21 o -1 2 1 1341.61 1361.33 20.04 o 0 2 1 697.43 691.65 10.41 o 1 2 1 3071.82 3171.61 49.77 o 2 2 1 47.57 41.39 3.91 o 3 2 1 501.83 514.65 15.54 o 4 2 1 49.52 38.82 8.68 o -4 3 1 152.53 157.21 12.00 o -3 3 1 2.13 6.03 4.28 o -2 3 1 63.09 53.96 2.85 o -1 3 1 176.45 189.84 3.13 o 0 3 1 449.34 449.23 5.93 o 1 3 1 1483.58 1562.22 21.52 o 2 3 1 837.38 794.91 15.00 o 3 3 1 1.03 2.79 3.96 o 4 3 1 46.78 45.41 8.74 o -4 4 1 6.61 6.49 7.24 o -3 4 1 149.29 149.00 5.61 o -2 4 1 29.63 28.85 2.61 o -1 4 1 867.66 897.68 12.38 o 0 4 1 2007.55 2088.73 38.42 o 1 4 1 0.01 3.03 3.71 o 2 4 1 41.30 36.98 2.87 o 3 4 1 0.76 1.94 5.27 o 4 4 1 2.98 -0.69 9.24 o -4 5 1 12.99 29.32 7.89 o -3 5 1 0.23 0.65 4.28 o -2 5 1 213.47 204.52 5.24 o -1 5 1 156.47 133.74 3.01 o 0 5 1 106.94 132.61 34.08 o 1 5 1 2839.42 2993.95 36.93 o 2 5 1 24.63 20.92 2.88 o 3 5 1 50.92 49.25 5.17 o 4 5 1 583.88 629.99 24.47 o -4 6 1 96.38 89.61 9.89 o -3 6 1 947.26 986.93 15.38 o -2 6 1 191.61 182.13 5.27 o -1 6 1 8.38 4.53 2.86 o 0 6 1 2660.98 2862.65 55.63 o 1 6 1 437.81 484.72 9.58 o 2 6 1 13.66 12.31 2.97 o 3 6 1 452.81 461.13 11.79 o 4 6 1 97.22 109.12 11.58 o -4 7 1 6.20 25.08 15.03 o -3 7 1 198.04 183.05 10.52 o -2 7 1 126.99 123.92 3.85 o -1 7 1 33.32 31.50 4.19 o 0 7 1 33.02 23.83 2.98 o 1 7 1 249.93 264.96 6.46 o 2 7 1 98.02 88.69 4.42 o 3 7 1 13.65 15.71 5.45 o 4 7 1 145.34 176.16 16.46 o -3 8 1 15.01 20.40 6.84 o -2 8 1 103.65 94.92 3.78 o -1 8 1 0.33 13.70 4.79 o 0 8 1 0.07 3.63 3.35 o 1 8 1 0.88 1.43 2.98 o 2 8 1 9.82 7.27 4.84 o 3 8 1 6.09 8.32 5.54 o -3 9 1 270.01 235.60 11.88 o -2 9 1 217.94 222.00 5.32 o -1 9 1 366.28 367.91 8.10 o 0 9 1 10.32 3.16 2.93 o 1 9 1 160.72 164.02 6.11 o 2 9 1 80.16 85.41 6.91 o 3 9 1 56.22 50.35 8.25 o -3 10 1 362.86 398.46 25.81 o -2 10 1 110.69 113.45 10.64 o -1 10 1 0.45 6.79 4.05 o 0 10 1 101.08 113.40 5.58 o 1 10 1 1.05 2.63 4.01 o 2 10 1 82.47 84.59 11.05 o 3 10 1 433.87 440.23 24.03 o -2 11 1 244.03 289.00 33.60 o -1 11 1 78.22 68.03 9.15 o 0 11 1 267.91 231.31 7.66 o 1 11 1 48.10 42.99 5.92 o 2 11 1 15.71 9.04 13.54 o -2 12 1 153.17 157.50 16.96 o -1 12 1 22.33 15.83 11.17 o 0 12 1 218.11 185.89 18.32 o 1 12 1 108.51 88.67 14.35 o 2 12 1 36.55 65.95 25.97 o -1 13 1 425.19 447.88 26.66 o 0 13 1 24.27 11.01 15.27 o 1 13 1 426.47 422.96 28.40 o -4 0 2 226.82 234.08 56.76 o -3 0 2 20.50 29.56 6.77 o -2 0 2 116.66 104.43 6.10 o -1 0 2 423.26 452.82 15.19 o 1 0 2 537.91 563.63 19.54 o 2 0 2 622.83 633.49 19.52 o 3 0 2 15.97 27.08 9.02 o 4 0 2 52.04 30.99 17.90 o -4 1 2 30.17 23.04 8.35 o -3 1 2 277.18 272.52 8.31 o -2 1 2 594.28 603.91 11.75 o -1 1 2 1918.58 1829.83 24.62 o 0 1 2 763.08 722.13 35.72 o 1 1 2 30056.92 29201.99 536.17 o 2 1 2 1414.45 1425.63 22.53 o 3 1 2 5.72 -0.76 4.04 o 4 1 2 253.48 248.53 19.47 o -4 2 2 49.10 33.81 6.49 o -3 2 2 239.73 254.19 7.61 o -2 2 2 478.20 493.55 9.62 o -1 2 2 98.27 102.16 2.75 o 0 2 2 61.87 74.45 3.50 o 1 2 2 1044.12 1044.00 23.43 o 2 2 2 200.78 207.60 7.16 o 3 2 2 56.52 46.42 5.12 o 4 2 2 2.44 4.83 8.77 o -4 3 2 379.46 341.58 13.51 o -3 3 2 371.38 367.78 9.09 o -2 3 2 79.87 67.69 2.69 o -1 3 2 891.43 903.93 11.16 o 0 3 2 454.17 433.44 14.01 o 1 3 2 248.79 245.86 4.25 o 2 3 2 615.14 588.90 12.39 o 3 3 2 72.21 54.37 5.25 o 4 3 2 209.88 212.38 11.57 o -4 4 2 49.22 55.44 7.93 o -3 4 2 419.06 430.47 12.64 o -2 4 2 711.87 705.66 11.24 o -1 4 2 256.37 268.13 5.32 o 0 4 2 798.51 802.49 11.47 o 1 4 2 123.37 124.38 3.21 o 2 4 2 48.27 38.17 2.88 o 3 4 2 284.45 305.15 10.55 o 4 4 2 50.77 32.20 9.22 o -4 5 2 492.17 443.75 15.64 o -3 5 2 1047.27 1078.09 16.62 o -2 5 2 224.13 214.68 5.36 o -1 5 2 1243.88 1202.78 16.33 o 0 5 2 40.81 61.11 3.45 o 1 5 2 2924.60 3124.50 47.70 o 2 5 2 619.19 654.04 11.34 o 3 5 2 1.06 7.02 4.19 o 4 5 2 121.79 113.27 12.78 o -4 6 2 131.03 136.15 11.74 o -3 6 2 171.04 176.74 6.33 o -2 6 2 479.87 496.65 9.92 o -1 6 2 106.21 111.93 3.50 o 0 6 2 57.41 56.36 4.35 o 1 6 2 470.65 473.39 8.96 o 2 6 2 0.80 3.30 2.74 o 3 6 2 0.83 -4.57 4.88 o 4 6 2 36.13 49.52 19.46 o -4 7 2 35.22 7.19 11.67 o -3 7 2 25.88 25.46 5.25 o -2 7 2 12.68 17.35 3.23 o -1 7 2 689.08 680.31 20.50 o 0 7 2 9.01 5.61 3.17 o 1 7 2 6.99 4.78 3.14 o 2 7 2 223.06 217.05 6.51 o 3 7 2 93.66 108.53 33.74 o 4 7 2 62.58 58.95 12.63 o -3 8 2 199.58 210.69 11.98 o -2 8 2 1024.91 1021.58 14.47 o -1 8 2 6.43 10.18 2.66 o 0 8 2 620.12 625.09 8.83 o 1 8 2 262.32 303.56 8.67 o 2 8 2 185.35 163.84 8.21 o 3 8 2 167.32 182.39 9.47 o -3 9 2 276.34 247.74 10.64 o -2 9 2 2.86 2.61 3.95 o -1 9 2 1036.28 1024.28 14.06 o 0 9 2 9.18 8.47 3.30 o 1 9 2 153.67 163.25 9.91 o 2 9 2 178.98 181.55 9.01 o 3 9 2 79.23 62.10 13.47 o -3 10 2 224.86 220.18 23.13 o -2 10 2 14.20 15.16 7.87 o -1 10 2 7.87 21.30 4.07 o 0 10 2 87.30 88.95 4.30 o 1 10 2 160.63 155.77 8.78 o 2 10 2 11.34 13.70 6.37 o 3 10 2 40.35 45.30 20.92 o -2 11 2 200.12 244.15 18.73 o -1 11 2 31.34 32.61 8.11 o 0 11 2 43.61 39.79 6.18 o 1 11 2 49.29 48.89 6.05 o 2 11 2 38.20 41.90 12.32 o -2 12 2 147.50 155.45 24.42 o -1 12 2 16.49 4.52 9.04 o 0 12 2 410.84 414.66 26.27 o 1 12 2 68.06 60.73 12.71 o 2 12 2 218.58 210.86 20.80 o -1 13 2 117.95 118.90 13.18 o 0 13 2 0.00 -9.14 27.50 o 1 13 2 69.82 78.12 19.28 o -4 1 3 193.01 182.35 14.14 o -3 1 3 3.94 13.47 4.80 o -2 1 3 371.90 384.55 7.56 o -1 1 3 1835.77 1827.31 34.19 o 0 1 3 69.08 81.50 2.53 o 1 1 3 1798.95 1776.20 32.54 o 2 1 3 2929.09 2999.62 57.27 o 3 1 3 47.59 50.46 5.45 o 4 1 3 158.31 173.33 15.02 o -4 2 3 6.89 3.02 4.50 o -3 2 3 50.97 46.34 3.71 o -2 2 3 20.86 14.41 3.25 o -1 2 3 75.43 80.70 2.34 o 0 2 3 52.63 60.21 2.72 o 1 2 3 2238.19 2184.55 35.41 o 2 2 3 855.73 884.49 15.85 o 3 2 3 327.54 323.98 9.27 o 4 2 3 21.08 20.11 13.20 o -4 3 3 392.99 385.21 11.55 o -3 3 3 0.21 5.15 4.04 o -2 3 3 33.42 33.61 2.70 o -1 3 3 1501.23 1520.80 18.56 o 0 3 3 366.72 401.61 7.00 o 1 3 3 319.19 332.37 7.44 o 2 3 3 3224.09 3423.21 47.71 o 3 3 3 25.60 25.83 3.76 o 4 3 3 132.74 165.16 12.61 o -4 4 3 12.01 4.10 5.21 o -3 4 3 28.39 32.78 11.19 o -2 4 3 191.48 187.07 5.03 o -1 4 3 0.01 2.79 2.51 o 0 4 3 200.65 172.69 6.09 o 1 4 3 254.96 270.31 14.19 o 2 4 3 1076.65 1176.00 18.37 o 3 4 3 2.75 -2.12 4.56 o 4 4 3 8.12 11.88 9.22 o -4 5 3 2.13 6.06 8.72 o -3 5 3 15.55 17.54 4.98 o -2 5 3 558.84 571.98 10.97 o -1 5 3 232.41 221.32 4.73 o 0 5 3 983.37 985.67 12.99 o 1 5 3 1623.14 1639.48 25.71 o 2 5 3 233.89 216.48 5.93 o 3 5 3 39.81 36.66 4.26 o 4 5 3 123.52 83.04 11.64 o -4 6 3 16.05 5.35 13.09 o -3 6 3 0.50 3.11 8.57 o -2 6 3 4.11 6.73 2.71 o -1 6 3 0.60 3.88 2.42 o 0 6 3 319.18 275.08 5.55 o 1 6 3 292.16 245.49 7.63 o 2 6 3 339.25 345.69 10.88 o 3 6 3 245.80 249.36 11.00 o 4 6 3 26.14 48.67 13.04 o -4 7 3 73.08 54.54 18.76 o -3 7 3 13.90 15.65 6.80 o -2 7 3 74.97 68.42 6.10 o -1 7 3 112.15 100.97 2.79 o 0 7 3 273.90 256.24 6.83 o 1 7 3 730.76 760.59 22.17 o 2 7 3 492.63 500.21 10.51 o 3 7 3 22.68 23.78 4.69 o 4 7 3 68.66 75.28 16.37 o -3 8 3 723.16 717.34 15.72 o -2 8 3 1373.12 1453.67 22.74 o -1 8 3 4.06 7.36 2.84 o 0 8 3 148.85 139.51 3.59 o 1 8 3 3.97 1.93 3.60 o 2 8 3 3.95 9.01 5.56 o 3 8 3 0.23 4.80 6.88 o -3 9 3 55.39 76.41 14.15 o -2 9 3 270.68 278.77 15.45 o -1 9 3 280.31 277.60 6.14 o 0 9 3 54.90 44.97 3.69 o 1 9 3 21.95 20.06 5.45 o 2 9 3 35.08 35.26 6.03 o 3 9 3 0.08 4.54 13.61 o -3 10 3 563.85 541.57 24.54 o -2 10 3 515.62 514.64 12.11 o -1 10 3 51.60 59.41 4.53 o 0 10 3 522.49 539.42 13.63 o 1 10 3 592.98 613.17 15.14 o 2 10 3 12.66 8.18 9.70 o 3 10 3 164.95 142.34 35.53 o -2 11 3 101.04 101.64 19.44 o -1 11 3 0.23 -0.61 3.52 o 0 11 3 118.00 119.39 7.05 o 1 11 3 0.64 12.27 8.57 o 2 11 3 8.28 20.72 10.60 o -2 12 3 221.51 227.10 43.37 o -1 12 3 37.17 33.86 9.03 o 0 12 3 94.74 97.53 11.13 o 1 12 3 60.99 36.71 16.99 o 2 12 3 190.82 220.32 51.06 o -1 13 3 482.31 567.31 45.86 o 0 13 3 20.72 27.50 27.50 o 1 13 3 24.47 27.22 27.54 o -4 0 4 74.00 43.59 30.02 o -3 0 4 139.20 128.20 7.31 o -2 0 4 2807.79 2912.13 62.44 o -1 0 4 0.09 -1.81 4.05 o 0 0 4 2535.79 2369.27 43.34 o 1 0 4 154.45 127.53 7.79 o 2 0 4 5070.87 5428.34 164.75 o 3 0 4 574.07 569.44 26.16 o 4 0 4 106.74 146.64 16.96 o -4 1 4 60.93 54.68 8.94 o -3 1 4 614.86 637.17 10.36 o -2 1 4 22.16 15.29 2.84 o -1 1 4 9.42 -1.80 4.03 o 0 1 4 411.51 417.98 6.05 o 1 1 4 982.90 975.80 17.79 o 2 1 4 328.57 335.64 10.14 o 3 1 4 76.19 73.38 12.80 o 4 1 4 5.38 -11.50 11.50 o -4 2 4 11.90 0.56 5.34 o -3 2 4 53.86 46.67 3.69 o -2 2 4 0.07 -0.59 3.03 o -1 2 4 86.76 115.51 3.25 o 0 2 4 150.75 145.50 2.79 o 1 2 4 75.05 68.64 3.20 o 2 2 4 1046.14 1119.91 21.47 o 3 2 4 1.85 0.00 3.87 o 4 2 4 28.95 30.48 10.41 o -4 3 4 204.92 180.79 12.63 o -3 3 4 10.59 7.82 3.94 o -2 3 4 1167.02 1247.66 16.42 o -1 3 4 3497.27 3600.11 44.90 o 0 3 4 16.28 14.63 3.18 o 1 3 4 141.97 137.06 3.30 o 2 3 4 1063.61 1072.46 19.18 o 3 3 4 196.55 177.01 6.71 o 4 3 4 62.27 88.48 12.87 o -4 4 4 143.56 128.53 10.30 o -3 4 4 826.79 829.70 13.36 o -2 4 4 2927.80 2971.71 39.88 o -1 4 4 0.22 4.69 2.98 o 0 4 4 1511.70 1509.02 19.85 o 1 4 4 73.38 53.42 3.60 o 2 4 4 185.26 181.87 6.93 o 3 4 4 454.78 463.69 11.89 o 4 4 4 18.12 19.46 11.32 o -4 5 4 67.82 77.25 15.42 o -3 5 4 254.65 243.64 7.14 o -2 5 4 348.72 379.18 7.87 o -1 5 4 199.01 207.64 3.94 o 0 5 4 183.06 186.34 6.75 o 1 5 4 175.24 169.17 3.46 o 2 5 4 2.62 2.72 2.87 o 3 5 4 5.73 4.47 5.24 o 4 5 4 45.90 74.82 24.20 o -4 6 4 6.29 13.93 15.64 o -3 6 4 64.08 53.67 5.49 o -2 6 4 395.98 399.00 8.57 o -1 6 4 73.30 73.00 3.04 o 0 6 4 0.06 -3.37 3.37 o 1 6 4 0.04 0.00 3.70 o 2 6 4 59.30 62.74 3.97 o 3 6 4 0.34 2.88 4.03 o 4 6 4 21.12 17.08 12.38 o -4 7 4 194.21 208.76 32.60 o -3 7 4 2.43 5.24 4.42 o -2 7 4 105.69 107.33 5.24 o -1 7 4 2128.05 2136.11 26.02 o 0 7 4 362.82 363.27 6.50 o 1 7 4 134.43 120.90 5.45 o 2 7 4 883.63 926.42 32.32 o 3 7 4 9.40 5.20 5.85 o 4 7 4 28.10 33.27 12.84 o -3 8 4 342.02 354.35 13.59 o -2 8 4 443.62 453.94 11.17 o -1 8 4 27.41 24.52 2.98 o 0 8 4 1415.71 1365.29 28.95 o 1 8 4 135.34 133.32 6.66 o 2 8 4 5.89 4.01 5.42 o 3 8 4 223.33 217.43 9.83 o -3 9 4 15.81 -1.02 12.00 o -2 9 4 2.27 5.73 3.90 o -1 9 4 628.27 598.85 10.60 o 0 9 4 0.08 2.25 4.51 o 1 9 4 3.91 9.94 4.09 o 2 9 4 2.42 12.56 6.18 o 3 9 4 29.27 27.29 17.04 o -3 10 4 115.67 116.15 14.00 o -2 10 4 138.85 120.73 7.85 o -1 10 4 10.92 6.78 3.02 o 0 10 4 158.52 123.00 6.88 o 1 10 4 15.84 24.46 6.82 o 2 10 4 5.06 3.29 9.68 o 3 10 4 1.25 7.23 18.61 o -2 11 4 66.64 54.99 18.36 o -1 11 4 209.60 199.71 6.89 o 0 11 4 178.47 191.38 10.72 o 1 11 4 159.80 148.70 29.67 o 2 11 4 304.00 284.81 21.35 o -2 12 4 30.29 43.72 15.18 o -1 12 4 20.20 6.42 6.17 o 0 12 4 243.15 246.41 11.40 o 1 12 4 172.70 201.65 16.90 o 2 12 4 14.43 4.00 28.08 o -1 13 4 61.11 54.99 27.50 o 0 13 4 22.92 44.17 15.32 o 1 13 4 3.63 22.63 19.22 o -4 1 5 210.14 237.03 46.01 o -3 1 5 87.28 81.24 6.18 o -2 1 5 61.20 70.55 2.84 o -1 1 5 86.12 79.71 2.63 o 0 1 5 519.78 507.56 8.83 o 1 1 5 7.57 8.95 4.48 o 2 1 5 758.96 738.75 14.81 o 3 1 5 231.02 221.32 13.58 o 4 1 5 23.32 25.35 12.15 o -4 2 5 106.86 118.38 58.50 o -3 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