#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2013974.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013974_Fobs loop_ _publ_author_name 'Barich, Dewey H.' 'Zell, Mark T.' 'Powell, Douglas R.' 'Munson, Eric J.' _publ_section_title ; 2,4-Dimethoxybenzoic acid and 2,5-dimethoxybenzoic acid ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o261 _journal_page_last o262 _journal_volume 60 _journal_year 2004 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 94.995 _cell_angle_beta 95.894 _cell_angle_gamma 96.759 _cell_length_a 6.7602 _cell_length_b 7.7124 _cell_length_c 8.0237 _exptl_crystal_F_000 192.00 _reflns_d_resolution_high 0.8108 _[local]_cod_data_source_file fr1460Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 03083 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 127.27 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 16.91 20.16 0.48 o 2 0 0 130.78 157.66 2.00 o 3 0 0 1396.54 1779.81 14.46 o 4 0 0 11.66 13.35 0.82 o 5 0 0 2.21 2.23 1.04 o 6 0 0 24.14 20.92 1.21 o 7 0 0 0.35 -1.24 1.24 o 8 0 0 23.61 22.55 2.38 o -8 1 0 31.37 31.89 2.60 o -7 1 0 21.30 21.77 2.28 o -6 1 0 44.63 42.40 2.57 o -5 1 0 151.95 149.69 4.56 o -4 1 0 221.62 228.04 3.07 o -3 1 0 98.92 96.46 2.55 o -2 1 0 284.98 291.41 4.25 o -1 1 0 873.05 949.64 12.79 o 0 1 0 856.11 820.02 7.93 o 1 1 0 866.42 1098.70 8.93 o 2 1 0 0.39 0.16 0.32 o 3 1 0 221.65 291.52 3.04 o 4 1 0 8.55 11.24 1.09 o 5 1 0 24.52 24.07 1.61 o 6 1 0 59.22 53.30 1.45 o 7 1 0 148.79 120.99 4.19 o 8 1 0 3.44 3.48 1.59 o -8 2 0 1.45 1.18 1.44 o -7 2 0 15.99 17.18 2.09 o -6 2 0 601.22 569.59 10.80 o -5 2 0 41.19 38.52 1.31 o -4 2 0 37.89 34.79 1.37 o -3 2 0 71.52 58.36 1.57 o -2 2 0 364.22 388.78 5.50 o -1 2 0 652.69 624.46 6.18 o 0 2 0 64.23 46.26 0.92 o 1 2 0 309.30 332.99 3.03 o 2 2 0 20.58 17.25 0.68 o 3 2 0 13.39 18.14 0.78 o 4 2 0 94.07 98.77 1.67 o 5 2 0 1.33 0.98 0.56 o 6 2 0 329.30 290.05 3.65 o 7 2 0 4.90 4.42 0.80 o -8 3 0 3.48 5.12 1.97 o -7 3 0 30.77 31.08 2.54 o -6 3 0 463.63 447.40 9.12 o -5 3 0 118.02 104.71 3.44 o -4 3 0 24.21 21.89 0.95 o -3 3 0 338.46 344.61 4.02 o -2 3 0 83.09 82.45 1.49 o -1 3 0 75.75 67.65 0.97 o 0 3 0 90.41 92.14 1.17 o 1 3 0 341.12 407.09 6.58 o 2 3 0 353.86 402.50 3.82 o 3 3 0 0.00 0.08 0.39 o 4 3 0 76.98 86.72 1.65 o 5 3 0 159.94 158.49 2.43 o 6 3 0 11.96 13.56 0.97 o 7 3 0 3.45 2.20 0.76 o -7 4 0 2.99 1.83 1.57 o -6 4 0 0.00 -1.16 1.16 o -5 4 0 143.79 136.97 4.00 o -4 4 0 3.17 3.06 0.55 o -3 4 0 28.27 29.69 1.51 o -2 4 0 57.50 47.87 1.02 o -1 4 0 91.26 82.66 1.17 o 0 4 0 1039.10 1119.69 9.70 o 1 4 0 221.37 227.57 4.40 o 2 4 0 2.19 3.01 0.58 o 3 4 0 131.58 120.35 5.47 o 4 4 0 335.07 341.25 3.84 o 5 4 0 36.77 34.60 1.57 o 6 4 0 39.98 32.04 1.63 o 7 4 0 119.35 122.40 3.05 o -7 5 0 96.48 103.30 4.20 o -6 5 0 1.94 2.73 1.37 o -5 5 0 32.54 32.92 2.43 o -4 5 0 6.85 7.20 0.62 o -3 5 0 9.00 9.55 0.69 o -2 5 0 171.58 146.93 1.86 o -1 5 0 6.97 5.18 0.65 o 0 5 0 60.68 70.52 1.28 o 1 5 0 479.34 489.08 5.78 o 2 5 0 0.10 0.60 0.92 o 3 5 0 208.89 202.01 3.37 o 4 5 0 0.04 -0.28 0.65 o 5 5 0 22.89 24.55 1.48 o 6 5 0 15.06 15.14 1.35 o -7 6 0 0.69 1.51 1.56 o -6 6 0 51.84 49.50 2.01 o -5 6 0 4.80 5.18 1.04 o -4 6 0 1.52 2.53 0.82 o -3 6 0 0.01 -0.29 0.46 o -2 6 0 74.79 75.88 1.79 o -1 6 0 40.33 39.32 1.06 o 0 6 0 4.15 3.91 0.59 o 1 6 0 3.86 4.58 0.78 o 2 6 0 44.64 42.14 2.11 o 3 6 0 144.34 133.70 2.81 o 4 6 0 96.17 90.17 2.42 o 5 6 0 4.07 4.12 0.99 o -6 7 0 57.43 50.77 2.86 o -5 7 0 15.10 17.18 1.99 o -4 7 0 20.98 21.20 1.94 o -3 7 0 135.06 127.23 1.87 o -2 7 0 30.37 29.86 1.03 o -1 7 0 4.08 4.93 0.67 o 0 7 0 21.37 18.01 1.70 o 1 7 0 7.42 8.21 1.02 o 2 7 0 4.25 4.14 0.92 o 3 7 0 13.28 11.78 1.24 o 4 7 0 11.51 11.88 1.23 o -5 8 0 64.10 59.72 2.99 o -4 8 0 16.91 14.19 1.88 o -3 8 0 87.93 89.57 3.33 o -2 8 0 17.68 17.30 0.95 o -1 8 0 1.93 3.68 1.39 o 0 8 0 87.47 85.02 2.28 o 1 8 0 40.67 33.25 1.62 o 2 8 0 3.39 2.63 1.03 o 3 8 0 1.14 1.26 1.10 o -3 9 0 30.28 28.30 2.26 o -2 9 0 17.87 17.57 2.00 o -1 9 0 10.25 11.23 1.14 o 0 9 0 65.58 59.14 2.80 o 1 9 0 0.05 1.13 0.87 o -1 -9 1 2.67 5.34 1.04 o 0 -9 1 6.98 8.86 1.60 o 1 -9 1 12.22 12.25 0.98 o 2 -9 1 27.24 35.06 1.29 o 3 -9 1 66.71 73.44 3.16 o -3 -8 1 6.34 7.43 1.12 o -2 -8 1 8.72 9.11 1.11 o -1 -8 1 7.91 10.04 1.12 o 0 -8 1 7.40 7.14 0.81 o 1 -8 1 35.75 39.74 1.27 o 2 -8 1 32.23 34.98 1.17 o 3 -8 1 50.27 53.37 1.76 o 4 -8 1 28.38 26.85 2.20 o 5 -8 1 22.21 23.16 2.15 o -4 -7 1 0.07 0.12 0.80 o -3 -7 1 0.31 0.99 1.25 o -2 -7 1 0.03 1.06 0.75 o -1 -7 1 210.15 193.99 2.65 o 0 -7 1 2.12 3.12 0.61 o 1 -7 1 7.26 7.44 0.71 o 2 -7 1 813.92 869.09 9.56 o 3 -7 1 73.74 74.73 1.88 o 4 -7 1 2.34 2.03 1.31 o 5 -7 1 7.91 6.86 1.60 o 6 -7 1 32.38 28.60 3.25 o -5 -6 1 18.36 19.73 1.41 o -4 -6 1 2.66 4.02 0.87 o -3 -6 1 0.20 0.29 0.66 o -2 -6 1 107.19 98.84 2.21 o -1 -6 1 0.86 1.46 0.53 o 0 -6 1 7.62 7.37 0.63 o 1 -6 1 13.61 16.15 1.00 o 2 -6 1 193.67 194.12 7.55 o 3 -6 1 41.37 37.43 2.40 o 4 -6 1 7.33 7.05 0.71 o 5 -6 1 16.34 16.23 1.30 o 6 -6 1 4.98 5.23 1.13 o -6 -5 1 6.33 7.78 1.11 o -5 -5 1 4.46 4.78 1.35 o -4 -5 1 296.77 296.46 4.48 o -3 -5 1 350.09 368.18 4.93 o -2 -5 1 29.48 32.76 1.79 o -1 -5 1 13.30 12.84 0.82 o 0 -5 1 379.40 425.90 5.03 o 1 -5 1 91.28 86.51 1.71 o 2 -5 1 68.99 66.68 1.51 o 3 -5 1 21.42 23.64 1.04 o 4 -5 1 114.21 110.66 1.77 o 5 -5 1 7.39 6.47 1.02 o 6 -5 1 5.34 6.83 1.70 o 7 -5 1 19.33 17.61 2.31 o -7 -4 1 124.31 136.10 3.15 o -6 -4 1 15.86 16.29 2.18 o -5 -4 1 29.95 32.73 1.35 o -4 -4 1 1472.49 1564.63 13.39 o -3 -4 1 87.12 83.14 2.25 o -2 -4 1 125.76 108.57 1.29 o -1 -4 1 365.26 431.97 3.92 o 0 -4 1 11.69 10.78 0.68 o 1 -4 1 33.69 30.43 0.98 o 2 -4 1 13.60 14.05 0.79 o 3 -4 1 133.24 141.22 2.14 o 4 -4 1 123.01 129.15 2.86 o 5 -4 1 0.64 0.07 0.67 o 6 -4 1 7.62 8.84 1.74 o 7 -4 1 13.89 14.16 2.05 o -7 -3 1 23.70 23.29 1.54 o -6 -3 1 11.91 11.88 0.94 o -5 -3 1 12.39 11.43 0.85 o -4 -3 1 47.70 50.92 1.26 o -3 -3 1 346.57 400.17 3.98 o -2 -3 1 0.68 0.82 0.31 o -1 -3 1 42.36 49.22 1.15 o 0 -3 1 0.90 0.58 0.35 o 1 -3 1 161.25 153.75 2.52 o 2 -3 1 426.21 498.85 5.25 o 3 -3 1 768.12 998.28 13.76 o 4 -3 1 1.55 2.41 0.81 o 5 -3 1 7.96 5.67 1.05 o 6 -3 1 555.10 548.90 10.89 o 7 -3 1 76.16 73.67 3.44 o 8 -3 1 23.54 25.72 2.76 o -7 -2 1 3.57 6.22 1.56 o -6 -2 1 5.92 7.29 0.79 o -5 -2 1 84.93 89.24 1.73 o -4 -2 1 6.95 10.20 0.69 o -3 -2 1 46.15 38.34 0.97 o -2 -2 1 94.22 100.54 1.14 o -1 -2 1 13.14 9.22 0.45 o 0 -2 1 271.25 270.04 2.92 o 1 -2 1 52.19 49.57 0.93 o 2 -2 1 841.36 980.69 13.32 o 3 -2 1 136.07 173.55 3.18 o 4 -2 1 5.82 4.20 0.84 o 5 -2 1 336.79 377.00 6.25 o 6 -2 1 22.31 24.05 1.33 o 7 -2 1 23.21 21.06 2.40 o 8 -2 1 30.39 33.04 2.64 o -8 -1 1 7.50 9.64 1.82 o -7 -1 1 1.34 0.63 1.42 o -6 -1 1 37.46 32.95 1.50 o -5 -1 1 59.89 47.63 2.48 o -4 -1 1 45.67 43.23 1.08 o -3 -1 1 567.20 697.29 6.12 o -2 -1 1 232.77 270.66 3.65 o -1 -1 1 384.98 400.46 3.45 o 0 -1 1 1744.20 1661.67 16.31 o 1 -1 1 728.22 825.04 11.10 o 2 -1 1 105.95 145.26 2.67 o 3 -1 1 12.68 13.72 1.12 o 4 -1 1 39.13 39.59 1.56 o 5 -1 1 34.12 30.87 1.65 o 6 -1 1 1.80 2.58 0.81 o 7 -1 1 0.44 -1.22 1.39 o 8 -1 1 18.18 24.20 2.51 o -8 0 1 11.15 14.97 2.05 o -7 0 1 59.82 46.56 2.87 o -6 0 1 30.96 25.52 2.20 o -5 0 1 25.28 22.44 1.07 o -4 0 1 349.97 381.92 4.55 o -3 0 1 491.60 533.05 5.78 o -2 0 1 193.40 187.74 2.28 o -1 0 1 225.78 225.30 2.46 o 0 0 1 208.81 215.58 2.32 o 1 0 1 52.71 66.13 1.03 o 2 0 1 1520.66 2030.11 19.32 o 3 0 1 295.30 390.14 4.46 o 4 0 1 15.27 18.87 1.96 o 5 0 1 62.19 70.49 2.35 o 6 0 1 10.11 11.00 1.30 o 7 0 1 0.03 -0.78 1.27 o 8 0 1 8.42 4.43 1.59 o -8 1 1 0.10 -0.95 1.47 o -7 1 1 5.76 4.83 1.63 o -6 1 1 42.46 37.15 2.35 o -5 1 1 1.52 1.81 0.54 o -4 1 1 172.70 170.08 2.36 o -3 1 1 853.54 888.19 9.09 o -2 1 1 44.76 40.86 1.62 o -1 1 1 243.06 236.49 2.75 o 0 1 1 347.22 346.13 5.05 o 1 1 1 151.36 162.32 3.28 o 2 1 1 684.73 880.39 8.88 o 3 1 1 645.53 887.82 9.20 o 4 1 1 56.61 68.29 1.64 o 5 1 1 59.26 62.23 1.49 o 6 1 1 66.03 45.57 1.39 o 7 1 1 8.58 7.37 1.06 o -8 2 1 0.32 -0.03 1.44 o -7 2 1 0.95 1.63 1.39 o -6 2 1 12.59 11.15 1.62 o -5 2 1 43.30 33.93 2.14 o -4 2 1 10.02 11.32 0.69 o -3 2 1 3.39 3.35 0.31 o -2 2 1 607.50 579.64 6.03 o -1 2 1 1799.25 1752.68 34.87 o 0 2 1 424.97 394.14 4.18 o 1 2 1 386.67 440.65 4.79 o 2 2 1 784.91 1004.31 16.44 o 3 2 1 49.81 50.28 1.38 o 4 2 1 118.09 121.42 1.94 o 5 2 1 15.24 11.05 0.83 o 6 2 1 3.16 4.80 0.75 o 7 2 1 22.24 21.68 1.21 o -7 3 1 19.16 20.59 2.28 o -6 3 1 262.45 251.78 6.08 o -5 3 1 1.51 0.82 1.04 o -4 3 1 40.05 34.91 0.83 o -3 3 1 421.33 391.61 4.34 o -2 3 1 0.11 0.00 0.24 o -1 3 1 118.42 121.70 1.41 o 0 3 1 1.67 3.12 0.46 o 1 3 1 153.85 157.49 2.32 o 2 3 1 30.17 24.12 0.98 o 3 3 1 5.62 8.95 0.62 o 4 3 1 67.43 74.43 1.57 o 5 3 1 2.56 4.74 0.70 o 6 3 1 0.11 0.54 0.61 o 7 3 1 4.47 5.03 0.85 o -7 4 1 271.85 256.37 6.66 o -6 4 1 0.20 0.09 1.30 o -5 4 1 0.19 0.02 1.05 o -4 4 1 245.47 240.37 3.60 o -3 4 1 195.70 188.74 2.14 o -2 4 1 19.54 16.98 0.54 o -1 4 1 4.89 5.81 0.52 o 0 4 1 17.08 19.72 1.21 o 1 4 1 0.21 0.01 0.48 o 2 4 1 225.98 232.65 2.59 o 3 4 1 26.62 25.78 1.38 o 4 4 1 36.92 33.41 1.14 o 5 4 1 29.55 27.68 2.12 o 6 4 1 26.59 25.88 1.55 o -7 5 1 5.26 6.25 1.76 o -6 5 1 3.19 2.60 1.02 o -5 5 1 54.64 51.17 1.84 o -4 5 1 42.93 45.55 2.46 o -3 5 1 9.16 9.39 0.49 o -2 5 1 27.79 23.98 0.68 o -1 5 1 0.09 0.53 0.87 o 0 5 1 256.10 266.85 5.01 o 1 5 1 125.22 114.15 3.09 o 2 5 1 67.08 61.23 1.72 o 3 5 1 1381.19 1377.85 14.50 o 4 5 1 14.88 14.26 1.15 o 5 5 1 13.57 12.52 1.20 o 6 5 1 123.72 130.44 3.17 o -7 6 1 4.24 4.44 1.09 o -6 6 1 9.80 9.75 1.27 o -5 6 1 56.34 52.28 1.83 o -4 6 1 8.54 9.86 1.02 o -3 6 1 33.82 35.55 0.97 o -2 6 1 43.50 38.07 1.27 o -1 6 1 176.82 175.02 2.86 o 0 6 1 0.05 -0.18 0.61 o 1 6 1 20.45 19.15 1.17 o 2 6 1 181.40 182.99 3.27 o 3 6 1 302.45 290.12 10.04 o 4 6 1 5.21 5.21 0.97 o 5 6 1 1.69 2.46 0.91 o -6 7 1 2.86 3.25 1.59 o -5 7 1 1.44 1.05 1.41 o -4 7 1 17.68 16.19 1.82 o -3 7 1 82.80 80.10 3.04 o -2 7 1 32.57 32.97 2.36 o -1 7 1 2.47 3.36 0.80 o 0 7 1 8.67 8.13 0.97 o 1 7 1 94.96 90.88 4.28 o 2 7 1 0.12 0.53 0.78 o 3 7 1 4.17 4.77 1.60 o 4 7 1 13.70 13.41 1.34 o -5 8 1 1.19 0.34 1.36 o -4 8 1 38.60 33.30 2.40 o -3 8 1 409.58 388.62 7.87 o -2 8 1 6.94 7.15 0.97 o -1 8 1 0.02 -0.17 0.71 o 0 8 1 104.16 103.08 2.55 o 1 8 1 0.27 0.30 1.52 o 2 8 1 1.34 0.98 0.90 o 3 8 1 0.38 0.88 0.87 o -3 9 1 9.79 9.23 1.74 o -2 9 1 26.45 28.12 2.32 o -1 9 1 4.54 4.74 0.99 o 0 9 1 0.95 1.32 0.88 o 1 9 1 3.68 4.60 1.00 o -1 -9 2 0.06 0.32 1.10 o 0 -9 2 44.71 51.26 1.56 o 1 -9 2 0.03 0.39 0.67 o 2 -9 2 3.04 1.66 0.71 o 3 -9 2 2.09 2.12 0.87 o -3 -8 2 18.01 17.78 1.38 o -2 -8 2 0.73 1.15 1.04 o -1 -8 2 103.60 97.27 1.95 o 0 -8 2 7.86 8.23 0.82 o 1 -8 2 43.49 46.33 1.65 o 2 -8 2 35.82 38.97 1.57 o 3 -8 2 0.06 -0.71 0.71 o 4 -8 2 6.52 6.37 1.56 o 5 -8 2 1.63 2.35 1.39 o -4 -7 2 0.24 -0.01 0.76 o -3 -7 2 4.84 6.49 0.97 o -2 -7 2 26.34 20.04 1.02 o -1 -7 2 139.06 135.49 2.16 o 0 -7 2 7.16 9.94 1.02 o 1 -7 2 51.07 52.29 1.61 o 2 -7 2 144.86 151.28 2.71 o 3 -7 2 33.18 32.36 1.36 o 4 -7 2 141.71 139.63 3.46 o 5 -7 2 22.54 25.53 1.60 o 6 -7 2 3.84 2.22 1.07 o -5 -6 2 9.20 11.59 3.14 o -4 -6 2 27.95 25.56 1.40 o -3 -6 2 3.29 2.17 0.74 o -2 -6 2 1.24 1.63 0.58 o -1 -6 2 25.05 23.84 1.20 o 0 -6 2 0.46 0.08 0.79 o 1 -6 2 28.14 28.26 1.34 o 2 -6 2 223.27 227.81 3.28 o 3 -6 2 18.03 16.12 1.00 o 4 -6 2 50.05 51.04 3.07 o 5 -6 2 100.07 89.40 3.13 o 6 -6 2 0.02 1.31 1.47 o -6 -5 2 1.93 1.64 0.90 o -5 -5 2 64.75 62.90 2.05 o -4 -5 2 102.64 95.15 3.54 o -3 -5 2 69.18 70.30 2.69 o -2 -5 2 0.00 0.39 0.49 o -1 -5 2 0.33 0.10 0.52 o 0 -5 2 46.78 48.66 1.31 o 1 -5 2 143.59 130.53 2.14 o 2 -5 2 11.38 11.69 1.52 o 3 -5 2 1.87 1.43 0.65 o 4 -5 2 8.11 7.48 0.82 o 5 -5 2 82.77 70.88 1.78 o 6 -5 2 2.79 3.25 1.74 o 7 -5 2 20.98 30.87 2.83 o -7 -4 2 6.12 5.30 1.60 o -6 -4 2 30.55 30.35 1.59 o -5 -4 2 0.15 -0.20 0.80 o -4 -4 2 240.83 235.31 2.95 o -3 -4 2 0.06 -0.25 0.38 o -2 -4 2 606.22 687.31 5.91 o -1 -4 2 88.20 103.47 1.84 o 0 -4 2 5.44 3.04 0.47 o 1 -4 2 247.77 260.67 3.18 o 2 -4 2 25.85 24.21 0.91 o 3 -4 2 2.15 4.17 0.63 o 4 -4 2 35.82 37.61 1.76 o 5 -4 2 8.41 7.94 1.19 o 7 -4 2 27.58 30.37 2.86 o -7 -3 2 17.80 17.00 1.46 o -6 -3 2 33.35 34.02 1.72 o -5 -3 2 247.63 248.94 3.18 o -4 -3 2 165.99 168.36 2.31 o -3 -3 2 0.02 -0.13 0.35 o -2 -3 2 174.79 190.56 2.17 o -1 -3 2 1705.06 1930.23 18.51 o 0 -3 2 175.76 172.85 2.21 o 1 -3 2 27.30 25.37 0.76 o 2 -3 2 5.07 5.31 0.52 o 3 -3 2 2.87 4.22 0.87 o 4 -3 2 228.88 278.29 5.06 o 5 -3 2 7.32 6.84 1.25 o 6 -3 2 3.27 3.48 1.13 o 7 -3 2 23.36 26.53 2.69 o -7 -2 2 11.05 11.38 1.85 o -6 -2 2 158.16 145.36 3.31 o -5 -2 2 78.87 76.94 1.60 o -4 -2 2 0.07 -0.15 0.43 o -3 -2 2 342.12 370.25 3.14 o -2 -2 2 308.20 355.07 3.36 o -1 -2 2 143.38 157.65 2.71 o 0 -2 2 184.56 173.25 2.57 o 1 -2 2 70.87 86.42 1.24 o 2 -2 2 586.35 771.96 10.92 o 3 -2 2 50.12 39.90 1.60 o 4 -2 2 193.73 225.21 4.34 o 5 -2 2 778.50 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