#------------------------------------------------------------------------------
#$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $
#$Revision: 26848 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/40/2014024.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2014024_Fobs
loop_
_publ_author_name
'Vertruyen, B\'en\'edicte'
'Robertz, B\'en\'edicte'
'Guillaume, Bernard'
'Rulmont, Andr\'e'
'Spirlet, Marie-Rose'
_publ_section_title
;
 Dibarium zirconium tetraoxalate trihydrate
;
_journal_issue                   6
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              m233
_journal_page_last               m234
_journal_volume                  60
_journal_year                    2004
_space_group_IT_number           15
_symmetry_space_group_name_Hall  '-I 2ya'
_symmetry_space_group_name_H-M   'I 1 2/a 1'
_[local]_cod_data_source_file    iz1040Isup2.hkl
_[local]_cod_data_source_block   I
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 60921.98 58300.51 4400.02 o
4 0 0 206680.72 206024.09 13543.33 o
6 0 0 40797.59 41257.27 968.57 o
8 0 0 29767.26 30888.79 1824.72 o
1 1 0 1260.09 438.93 144.79 o
3 1 0 1412.02 317.69 303.19 o
5 1 0 1011.29 404.22 359.57 o
7 1 0 723.34 614.84 247.46 o
9 1 0 5.53 -67.24 416.24 o
0 2 0 9536.04 467.78 2496.63 o
2 2 0 19.26 249.97 170.75 o
4 2 0 8193.10 9149.25 452.90 o
6 2 0 375.20 742.23 269.93 o
8 2 0 95.71 146.96 320.72 o
1 3 0 250427.36 228609.13 16000.25 o
3 3 0 90536.43 90141.10 5078.31 o
5 3 0 50531.31 48179.57 2024.03 o
7 3 0 25956.41 24349.37 693.91 o
9 3 0 11624.80 11975.34 756.65 o
0 4 0 34878.16 43781.63 2863.69 o
2 4 0 19577.19 20458.71 1803.66 o
4 4 0 19782.88 20028.98 563.83 o
6 4 0 7030.21 8645.35 466.44 o
8 4 0 4065.99 5136.57 544.82 o
1 5 0 32013.40 16674.40 2339.83 o
3 5 0 563.84 1150.38 191.72 o
5 5 0 711.43 326.31 211.72 o
7 5 0 27.98 183.62 255.69 o
9 5 0 51.11 939.55 474.30 o
0 6 0 6033.13 5831.60 312.73 o
2 6 0 8405.49 12255.12 1839.36 o
4 6 0 7771.07 9081.35 857.12 o
6 6 0 296.82 406.84 261.96 o
8 6 0 69.30 262.50 381.73 o
1 7 0 13248.51 8228.82 777.23 o
3 7 0 18428.22 18285.49 2200.71 o
5 7 0 10579.01 9580.50 573.81 o
7 7 0 11524.55 11406.43 672.96 o
9 7 0 1818.33 515.16 561.04 o
0 8 0 8001.17 8919.05 380.85 o
2 8 0 171337.55 186350.27 24420.14 o
4 8 0 6578.19 5782.73 649.50 o
6 8 0 21450.29 22671.51 1532.00 o
8 8 0 8602.68 8864.51 646.79 o
1 9 0 14574.00 16444.83 514.69 o
3 9 0 10700.06 13027.56 1470.05 o
5 9 0 9991.05 12074.97 796.00 o
7 9 0 13576.46 13761.12 696.89 o
9 9 0 3941.59 4152.10 570.92 o
0 10 0 23299.99 42282.14 8762.15 o
2 10 0 673.70 109.63 244.92 o
4 10 0 809.66 783.13 234.87 o
6 10 0 86.25 -73.65 266.34 o
8 10 0 124.99 -78.48 434.79 o
1 11 0 26978.95 34736.06 1749.97 o
3 11 0 101479.66 100149.66 4225.50 o
5 11 0 38824.76 40243.86 2404.16 o
7 11 0 30098.58 29704.25 1261.03 o
9 11 0 8396.29 8813.37 705.15 o
0 12 0 47746.34 55455.49 6325.00 o
2 12 0 22357.49 26334.97 1378.30 o
4 12 0 22897.77 20633.74 1806.09 o
6 12 0 8647.99 8281.94 472.16 o
8 12 0 7140.64 7070.07 648.19 o
1 13 0 19881.54 26332.95 1039.54 o
3 13 0 3139.82 5522.25 829.20 o
5 13 0 12896.06 11930.57 763.87 o
7 13 0 3897.98 4512.09 573.35 o
9 13 0 2670.16 2451.04 615.41 o
0 14 0 16486.13 16760.19 554.74 o
2 14 0 15004.85 16779.48 638.22 o
4 14 0 25513.20 29219.54 2663.82 o
6 14 0 10174.26 9679.85 668.07 o
8 14 0 5343.97 4806.18 594.33 o
1 15 0 2282.23 3665.03 359.66 o
3 15 0 10085.70 11378.70 847.57 o
5 15 0 2174.21 1970.79 375.67 o
7 15 0 5533.41 5912.34 556.98 o
0 16 0 22711.67 28518.11 2217.68 o
2 16 0 35318.91 36611.86 796.37 o
4 16 0 2920.32 1567.78 493.90 o
6 16 0 5572.79 6235.22 798.04 o
8 16 0 4814.82 4442.38 726.44 o
1 17 0 12545.39 13302.07 384.59 o
3 17 0 4852.78 4825.45 415.89 o
5 17 0 1357.50 1360.58 394.12 o
7 17 0 97.67 1079.49 473.40 o
0 18 0 1931.96 2022.12 436.57 o
2 18 0 20.79 277.18 365.48 o
4 18 0 493.79 87.15 333.69 o
6 18 0 1882.33 2086.12 544.42 o
8 18 0 29.74 -203.57 433.74 o
1 19 0 955.33 518.50 330.68 o
3 19 0 2962.12 2848.57 397.78 o
5 19 0 57.58 -54.41 465.23 o
7 19 0 2220.30 1772.55 564.54 o
0 20 0 57930.13 67479.73 9557.19 o
2 20 0 59915.79 61417.19 1226.50 o
4 20 0 33711.30 34430.60 3002.20 o
6 20 0 18672.83 18732.43 1315.12 o
8 20 0 9511.74 9458.98 735.03 o
1 21 0 6288.12 6272.85 360.10 o
3 21 0 2518.03 2880.25 508.44 o
5 21 0 423.53 244.73 520.52 o
7 21 0 651.83 508.00 706.49 o
0 22 0 1818.65 664.35 845.70 o
2 22 0 3053.90 3971.74 723.62 o
4 22 0 690.50 799.61 543.19 o
6 22 0 1496.22 1552.62 540.24 o
1 23 0 63471.31 70010.59 3472.13 o
3 23 0 39192.29 40086.39 943.66 o
5 23 0 37848.58 37130.36 1852.35 o
7 23 0 13473.59 13558.19 795.17 o
0 24 0 11694.40 15146.00 1296.96 o
2 24 0 10951.09 13489.12 1209.68 o
4 24 0 8212.16 8055.94 716.53 o
6 24 0 5551.49 5856.74 807.39 o
1 25 0 2623.02 3113.72 493.25 o
3 25 0 1253.06 1389.29 530.83 o
5 25 0 872.76 873.03 642.34 o
0 26 0 27702.38 29036.19 1301.86 o
2 26 0 21086.13 21412.52 866.44 o
4 26 0 12472.99 11994.25 785.10 o
6 26 0 3355.12 4490.00 917.32 o
1 27 0 10408.20 10585.98 590.87 o
3 27 0 9979.11 9999.81 882.69 o
5 27 0 11453.24 10411.13 977.26 o
0 28 0 726.21 906.95 607.25 o
2 28 0 409.90 972.70 539.90 o
4 28 0 1297.29 1224.93 566.13 o
1 29 0 1455.49 1472.78 447.04 o
3 29 0 1016.76 1179.13 569.17 o
5 29 0 61.65 150.46 558.54 o
0 30 0 602.45 298.69 602.58 o
2 30 0 2615.98 2006.06 1152.65 o
4 30 0 1890.34 1356.97 657.85 o
1 31 0 11032.61 11002.49 696.85 o
3 31 0 10827.99 11344.25 823.08 o
0 32 0 366.36 355.32 592.54 o
2 32 0 142.76 507.29 574.31 o
1 33 0 1912.61 1801.91 471.70 o
0 34 0 11388.42 12179.09 836.36 o
-10 1 1 889.40 911.16 486.49 o
-8 1 1 4502.80 4053.22 555.84 o
-6 1 1 2727.59 2888.33 286.18 o
-4 1 1 26828.88 25515.00 1064.30 o
-2 1 1 33116.53 28068.51 2217.59 o
0 1 1 856.89 5537.96 578.20 o
2 1 1 24799.73 25883.33 1204.95 o
4 1 1 3554.83 2978.47 246.03 o
6 1 1 9107.80 9130.33 415.43 o
8 1 1 2683.25 3046.12 487.38 o
-9 2 1 593.43 -222.96 458.93 o
-7 2 1 1902.38 2075.64 292.50 o
-5 2 1 7534.02 7363.31 332.14 o
-3 2 1 3933.70 2188.41 507.97 o
-1 2 1 39449.66 39177.64 1025.25 o
1 2 1 2870.84 7159.08 851.47 o
3 2 1 697.47 749.46 194.18 o
5 2 1 2745.42 2238.50 304.60 o
7 2 1 25.46 -15.35 371.26 o
9 2 1 1754.93 2367.41 489.82 o
-10 3 1 1766.58 1656.09 531.32 o
-8 3 1 10847.15 10845.78 656.21 o
-6 3 1 13148.94 13356.53 466.55 o
-4 3 1 16778.32 17071.60 809.55 o
-2 3 1 1272.52 6839.41 1776.90 o
0 3 1 122933.20 90926.83 11517.93 o
2 3 1 1707.66 1121.61 192.88 o
4 3 1 20290.85 20299.65 472.34 o
6 3 1 3816.30 3660.91 346.01 o
8 3 1 4594.46 4659.97 539.12 o
-9 4 1 6403.80 6890.79 632.98 o
-7 4 1 10349.35 8618.49 657.35 o
-5 4 1 2768.57 2821.05 258.88 o
-3 4 1 20299.99 16675.97 2366.32 o
-1 4 1 12457.25 14424.28 668.06 o
1 4 1 72016.08 64206.47 3525.97 o
3 4 1 40843.08 38124.77 3249.62 o
5 4 1 19032.84 20424.59 883.82 o
7 4 1 7256.53 5979.06 672.24 o
9 4 1 346.64 238.24 441.16 o
-10 5 1 8797.17 9420.40 841.38 o
-8 5 1 13228.18 12863.04 686.35 o
-6 5 1 34016.57 34474.71 1396.75 o
-4 5 1 101846.02 105297.27 8673.77 o
-2 5 1 179106.92 182244.05 12509.00 o
0 5 1 71144.63 90708.43 5653.94 o
2 5 1 68710.84 61506.00 4607.66 o
4 5 1 39205.86 37069.94 2679.83 o
6 5 1 24296.20 24148.58 594.79 o
8 5 1 15083.46 15096.64 736.52 o
-9 6 1 6669.96 6424.94 666.01 o
-7 6 1 11838.28 11816.59 475.41 o
-5 6 1 6915.17 7566.21 490.93 o
-3 6 1 128.35 254.74 200.04 o
-1 6 1 5979.19 16647.60 1975.20 o
1 6 1 58430.17 81379.35 6700.01 o
3 6 1 23938.20 26210.55 1503.87 o
5 6 1 8315.96 8282.79 397.34 o
7 6 1 5489.74 5602.75 572.15 o
9 6 1 2815.50 2858.85 598.77 o
-10 7 1 510.05 129.51 446.76 o
-8 7 1 4009.03 3485.87 508.22 o
-6 7 1 1636.39 2289.38 306.24 o
-4 7 1 502.71 526.48 219.52 o
-2 7 1 16022.26 17044.57 1286.62 o
0 7 1 3406.54 3003.27 333.96 o
2 7 1 33961.17 31480.22 1497.72 o
4 7 1 6030.61 5181.17 576.96 o
6 7 1 5734.02 6599.34 564.01 o
8 7 1 38.58 74.62 426.24 o
-9 8 1 17982.96 19762.46 1723.64 o
-7 8 1 25077.64 24630.60 1125.31 o
-5 8 1 60810.00 59056.34 3568.03 o
-3 8 1 194639.81 213240.20 27437.47 o
-1 8 1 117136.18 127141.62 7557.67 o
1 8 1 124784.59 107235.24 10483.81 o
3 8 1 82205.54 80887.55 2024.98 o
5 8 1 58476.78 58445.44 2381.37 o
7 8 1 28667.12 28482.69 875.21 o
9 8 1 8383.34 8911.25 942.68 o
-8 9 1 20.81 -90.20 388.70 o
-6 9 1 350.35 714.73 259.91 o
-4 9 1 56.32 256.60 218.23 o
-2 9 1 4862.43 8600.53 1661.70 o
0 9 1 14845.85 18252.43 812.14 o
2 9 1 443.63 239.83 255.56 o
4 9 1 4403.01 3492.99 317.22 o
6 9 1 18.67 307.49 288.79 o
8 9 1 251.07 -236.55 436.23 o
-9 10 1 137.85 730.80 453.09 o
-7 10 1 298.85 358.41 395.42 o
-5 10 1 385.67 413.19 242.00 o
-3 10 1 10867.79 12806.12 1690.40 o
-1 10 1 982.76 388.11 202.63 o
1 10 1 1165.71 20.72 240.45 o
3 10 1 4929.26 6057.30 428.51 o
5 10 1 846.74 703.20 327.22 o
7 10 1 1574.53 1235.84 472.60 o
-8 11 1 7128.18 8243.10 615.04 o
-6 11 1 9022.77 10422.41 519.84 o
-4 11 1 66895.32 67439.46 6387.34 o
-2 11 1 48204.70 56205.44 6160.19 o
0 11 1 93517.70 111642.03 8817.26 o
2 11 1 1864.88 5432.76 1036.42 o
4 11 1 30032.59 27804.47 1658.28 o
6 11 1 9681.58 10096.50 804.28 o
8 11 1 4344.38 5182.69 601.61 o
-9 12 1 4007.04 5238.32 785.78 o
-7 12 1 16069.19 15155.02 710.37 o
-5 12 1 17751.89 16008.25 1756.24 o
-3 12 1 24733.16 24510.23 1872.05 o
-1 12 1 76555.60 84986.27 4513.92 o
1 12 1 44752.55 43555.57 917.63 o
3 12 1 34100.76 32340.43 908.10 o
5 12 1 19257.15 18213.70 1186.21 o
7 12 1 2905.87 2257.90 785.74 o
-8 13 1 2589.87 3496.73 578.00 o
-6 13 1 2456.31 3575.86 433.92 o
-4 13 1 5292.00 4602.42 559.02 o
-2 13 1 14751.21 17966.10 1983.93 o
0 13 1 5475.68 8162.90 474.04 o
2 13 1 24725.06 30550.76 2447.70 o
4 13 1 11059.40 10148.51 656.67 o
6 13 1 9248.42 9089.13 651.41 o
8 13 1 470.12 -3.30 494.44 o
-9 14 1 418.89 298.84 456.30 o
-7 14 1 871.95 1311.90 407.03 o
-5 14 1 11.55 255.82 273.62 o
-3 14 1 1282.61 2562.17 789.78 o
-1 14 1 2217.32 1490.55 268.24 o
1 14 1 257.35 329.99 204.49 o
3 14 1 1222.17 2336.45 366.92 o
5 14 1 20.18 -328.28 328.28 o
7 14 1 1507.08 1375.80 519.41 o
-8 15 1 8571.55 8450.23 691.13 o
-6 15 1 24760.20 26083.43 1594.54 o
-4 15 1 61042.99 64679.16 6822.84 o
-2 15 1 51711.94 56764.87 3984.23 o
0 15 1 72694.30 83057.85 5728.33 o
2 15 1 24848.40 24533.92 621.67 o
4 15 1 30836.57 29374.08 812.88 o
6 15 1 8857.62 10105.23 885.63 o
8 15 1 11647.86 11758.16 779.02 o
-9 16 1 4777.25 5223.54 653.39 o
-7 16 1 16808.19 14506.47 1222.07 o
-5 16 1 23326.33 25802.60 2299.04 o
-3 16 1 28628.41 31496.74 2630.46 o
-1 16 1 60286.17 66140.79 2492.93 o
1 16 1 32887.44 30010.01 835.79 o
3 16 1 38783.92 36079.87 1757.38 o
5 16 1 23711.45 23312.24 1161.57 o
7 16 1 8177.63 8274.94 707.00 o
-8 17 1 4668.76 5202.45 562.18 o
-6 17 1 6191.60 5334.19 620.36 o
-4 17 1 17337.30 16808.64 1201.97 o
-2 17 1 14307.32 16187.23 1024.25 o
0 17 1 10229.00 10598.91 409.95 o
2 17 1 1263.57 1160.23 382.70 o
4 17 1 9329.07 7760.74 737.79 o
6 17 1 8330.81 7994.36 677.53 o
8 17 1 4208.88 3884.41 569.96 o
-7 18 1 3443.41 2840.19 540.40 o
-5 18 1 12017.31 12687.09 844.53 o
-3 18 1 15916.80 20113.87 1381.18 o
-1 18 1 14552.65 15491.39 523.17 o
1 18 1 15839.64 14955.26 421.86 o
3 18 1 8929.25 7324.48 570.73 o
5 18 1 7140.97 6867.91 624.44 o
7 18 1 3366.90 3566.07 630.33 o
-8 19 1 9765.46 11014.26 734.66 o
-6 19 1 27841.67 27368.54 1975.46 o
-4 19 1 16897.62 19334.50 2102.15 o
-2 19 1 45014.01 52101.34 6147.53 o
0 19 1 41243.75 48632.05 2744.30 o
2 19 1 60752.98 60735.63 1866.19 o
4 19 1 26275.70 26297.72 1314.10 o
6 19 1 13406.90 13616.86 778.75 o
-7 20 1 4933.58 5458.64 659.55 o
-5 20 1 434.70 920.27 535.28 o
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1 20 1 2646.69 2724.47 301.86 o
3 20 1 3897.25 4005.16 439.93 o
5 20 1 7074.81 7304.74 641.29 o
7 20 1 596.27 153.82 543.56 o
-8 21 1 50.70 -220.24 548.91 o
-6 21 1 349.71 377.59 522.45 o
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0 21 1 933.70 1310.37 324.11 o
2 21 1 191.87 -40.14 380.96 o
4 21 1 37.54 513.19 600.00 o
6 21 1 93.57 178.83 507.68 o
-7 22 1 6306.82 6047.98 660.43 o
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1 22 1 14776.85 16031.76 475.67 o
3 22 1 19304.12 18356.08 1082.71 o
5 22 1 954.77 1374.77 500.21 o
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-2 23 1 628.46 303.31 407.61 o
0 23 1 95.46 52.15 291.72 o
2 23 1 1160.89 1917.97 404.88 o
4 23 1 8.94 -174.54 535.09 o
6 23 1 1506.66 1224.51 567.74 o
-7 24 1 727.72 1069.76 465.39 o
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1 24 1 49.38 469.72 259.37 o
3 24 1 1804.89 1515.46 768.89 o
5 24 1 1396.86 1328.75 588.51 o
-6 25 1 3200.18 2593.35 604.35 o
-4 25 1 2760.04 2141.33 760.96 o
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0 25 1 4491.60 6301.31 468.69 o
2 25 1 3477.78 3445.30 592.94 o
4 25 1 4103.50 4664.18 620.91 o
6 25 1 2191.61 2034.63 606.69 o
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1 26 1 2604.69 2238.93 489.61 o
3 26 1 2940.27 2461.86 640.57 o
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0 27 1 265.42 585.29 380.08 o
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3 30 1 191.38 495.08 471.40 o
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1 32 1 1931.54 2300.18 460.14 o
3 32 1 427.47 233.76 569.88 o
-2 33 1 86.84 10.20 556.93 o
0 33 1 209.72 -201.25 475.44 o
2 33 1 1062.73 995.04 600.79 o
-1 34 1 5032.97 5577.65 558.07 o
1 34 1 3280.36 2835.06 534.01 o
-10 0 2 15765.52 15543.77 922.96 o
-8 0 2 70366.72 69756.38 1421.39 o
-6 0 2 145903.73 148059.78 1277.38 o
-4 0 2 184643.19 186973.98 1097.94 o
-2 0 2 192254.23 184862.20 28312.32 o
0 0 2 130635.62 143686.11 10617.38 o
2 0 2 185151.25 186651.55 6217.59 o
4 0 2 154591.67 152717.16 11063.85 o
6 0 2 42589.33 43026.09 1002.15 o
8 0 2 24155.91 25751.32 2311.20 o
-9 1 2 149.80 695.66 301.92 o
-7 1 2 15.62 198.71 259.03 o
-5 1 2 1440.37 526.38 239.80 o
-3 1 2 4633.99 2519.82 686.97 o
-1 1 2 1558.35 478.92 162.25 o
1 1 2 3529.94 1296.42 338.11 o
3 1 2 3427.40 1976.19 389.34 o
5 1 2 15.84 147.29 249.34 o
7 1 2 285.48 475.34 351.24 o
-10 2 2 2020.30 1696.93 476.71 o
-8 2 2 2246.79 2139.56 439.54 o
-6 2 2 2058.27 2160.50 260.90 o
-4 2 2 653.35 555.79 186.73 o
-2 2 2 201.71 3671.34 866.75 o
0 2 2 3816.43 9290.99 717.94 o
2 2 2 327.85 1640.23 323.90 o
4 2 2 1.77 -111.87 221.70 o
6 2 2 2577.31 2384.20 322.97 o
8 2 2 2400.94 2820.42 436.31 o
-9 3 2 14184.53 15622.35 807.18 o
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