#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/40/2014026.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014026_Fobs loop_ _publ_author_name 'Reddy, C. Malla' 'Nangia, Ashwini' 'Jetti, Ram K. R.' 'Boese, Roland' _publ_section_title ; Triphenyl(3,4,5-triiodophenyl)methane ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o331 _journal_page_last o333 _journal_volume 60 _journal_year 2004 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 108.031 _cell_angle_beta 95.774 _cell_angle_gamma 111.805 _cell_length_a 11.5670 _cell_length_b 12.8327 _cell_length_c 17.5717 _exptl_crystal_F_000 1304.00 _reflns_d_resolution_high 0.7472 _[local]_cod_data_source_file jz1609Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' tphdju0m in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 460.50 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 42845.22 41278.85 1571.90 o 2 0 0 2401.61 3091.86 86.90 o 3 0 0 4893.30 3807.38 130.77 o 4 0 0 10015.52 7395.02 303.19 o 5 0 0 9418.92 7248.60 186.46 o 6 0 0 29836.55 32256.27 811.29 o 7 0 0 7887.88 7396.94 194.17 o 8 0 0 1065.40 1044.06 47.88 o 9 0 0 413.72 497.45 37.76 o 10 0 0 36.18 40.34 39.03 o 11 0 0 114.77 84.63 33.33 o 12 0 0 2554.99 2647.81 270.85 o 13 0 0 166.88 56.59 43.74 o -14 1 0 12.76 64.85 59.14 o -13 1 0 57.98 54.31 39.73 o -12 1 0 1018.57 856.07 76.88 o -11 1 0 853.80 824.40 59.22 o -10 1 0 91.63 100.26 54.41 o -9 1 0 3442.76 3495.24 186.08 o -8 1 0 1276.44 1260.17 47.14 o -7 1 0 7457.43 7518.09 174.78 o -6 1 0 3640.66 2427.57 61.90 o -5 1 0 10929.88 8275.93 188.08 o -3 1 0 57370.77 74940.05 3896.00 o -2 1 0 9832.76 9150.72 351.74 o -1 1 0 86798.97 84969.13 2484.09 o 0 1 0 43438.90 39575.08 1892.41 o 1 1 0 1084.72 2384.85 62.01 o 2 1 0 30986.46 34588.62 863.73 o 3 1 0 195.41 99.99 16.73 o 4 1 0 384.57 179.12 25.42 o 5 1 0 50759.02 56752.50 1649.12 o 6 1 0 31559.84 33358.78 833.83 o 7 1 0 3415.05 2906.14 85.07 o 8 1 0 5522.36 5651.77 154.36 o 9 1 0 28.83 10.02 19.57 o 10 1 0 235.20 307.54 38.47 o 11 1 0 4720.97 5166.52 238.92 o 12 1 0 1625.46 1506.11 210.53 o 13 1 0 52.27 20.43 48.49 o -14 2 0 225.83 196.41 100.53 o -13 2 0 374.17 235.25 49.68 o -12 2 0 16.57 44.72 35.01 o -11 2 0 198.58 144.30 36.68 o -10 2 0 1685.66 1479.53 65.37 o -9 2 0 784.90 681.48 36.52 o -8 2 0 434.24 512.66 25.46 o -7 2 0 505.63 312.49 18.60 o -6 2 0 4905.59 3044.42 165.59 o -5 2 0 615.46 296.45 17.41 o -4 2 0 64232.88 84329.92 2040.40 o -3 2 0 18582.62 26444.43 661.01 o -2 2 0 45598.00 52893.47 1541.45 o -1 2 0 21266.81 22751.71 794.81 o 1 2 0 6332.64 4234.44 109.03 o 2 2 0 37725.92 53055.97 1334.88 o 3 2 0 22110.89 28192.61 711.45 o 4 2 0 8538.24 7563.82 196.02 o 5 2 0 18390.32 18070.26 456.67 o 6 2 0 6741.77 6045.99 160.47 o 7 2 0 375.41 371.16 25.11 o 8 2 0 1632.10 1417.81 72.04 o 9 2 0 1098.41 849.91 44.65 o 10 2 0 2283.67 2151.65 145.48 o 11 2 0 1118.16 999.88 127.74 o 12 2 0 8.50 -40.04 40.04 o -14 3 0 5.08 -41.42 41.42 o -13 3 0 571.02 492.75 53.21 o -12 3 0 1413.07 1407.92 85.16 o -11 3 0 27.78 22.65 27.95 o -10 3 0 22.62 52.98 21.35 o -9 3 0 492.08 442.65 28.29 o -8 3 0 881.69 690.20 34.65 o -6 3 0 8248.89 7329.19 179.99 o -5 3 0 4670.33 5796.53 192.60 o -4 3 0 165.52 536.72 22.11 o -3 3 0 20078.49 21942.18 645.52 o -2 3 0 462.56 930.48 62.08 o -1 3 0 12254.91 10253.95 259.83 o 0 3 0 67459.10 70086.41 2370.94 o 1 3 0 1268.47 1804.98 54.67 o 2 3 0 37737.68 45565.41 1142.96 o 3 3 0 573.36 988.07 34.69 o 4 3 0 2407.81 1343.11 63.51 o 5 3 0 5743.19 4911.99 131.85 o 6 3 0 2295.99 1928.87 63.36 o 7 3 0 5716.52 5390.79 147.39 o 8 3 0 6114.21 5946.62 163.48 o 9 3 0 0.28 -5.81 26.60 o 10 3 0 1.37 -2.36 31.78 o 11 3 0 58.63 -9.46 40.14 o 12 3 0 260.53 257.17 54.19 o -15 4 0 0.53 1.88 85.16 o -14 4 0 68.99 63.96 47.31 o -13 4 0 968.79 987.18 70.25 o -12 4 0 58.93 90.09 34.06 o -11 4 0 1952.20 1933.46 83.99 o -10 4 0 4967.47 5349.30 149.02 o -8 4 0 12005.62 11479.07 325.32 o -7 4 0 21519.02 23296.75 646.16 o -6 4 0 3.13 167.18 16.35 o -5 4 0 20517.00 20086.49 508.27 o -4 4 0 18970.40 19855.37 588.46 o -3 4 0 179.67 311.74 19.40 o -2 4 0 24296.84 24560.62 867.68 o -1 4 0 178070.56 188862.42 4450.10 o 0 4 0 5582.82 3937.23 165.59 o 1 4 0 16248.25 20479.19 563.36 o 2 4 0 23.43 51.43 10.65 o 3 4 0 11838.81 10774.26 277.83 o 4 4 0 20937.70 20553.15 573.61 o 5 4 0 19682.84 21717.73 551.64 o 6 4 0 1106.02 930.08 42.37 o 7 4 0 86.81 93.91 25.24 o 8 4 0 0.90 15.38 26.26 o 9 4 0 500.72 481.65 41.23 o 10 4 0 127.86 139.39 44.09 o 11 4 0 720.59 853.95 96.99 o -15 5 0 4.29 -43.69 43.69 o -14 5 0 322.07 240.00 68.60 o -13 5 0 1256.86 1157.22 75.16 o -12 5 0 64.98 42.12 31.24 o -11 5 0 2663.75 2458.71 110.24 o -10 5 0 166.85 155.38 32.99 o -9 5 0 2911.74 2403.36 149.03 o -8 5 0 2023.35 1776.50 115.91 o -7 5 0 831.65 653.54 33.32 o -6 5 0 9276.37 6809.51 178.59 o -5 5 0 4216.19 3345.25 106.06 o -4 5 0 14047.77 19215.04 570.37 o -3 5 0 25964.60 29417.08 1131.39 o -2 5 0 100994.78 113970.24 2680.08 o -1 5 0 7406.33 5559.24 196.49 o 0 5 0 35.55 234.38 21.23 o 1 5 0 7464.78 6877.45 193.66 o 2 5 0 10.59 179.31 22.75 o 3 5 0 13985.87 13659.78 501.50 o 4 5 0 33969.04 38361.54 1086.12 o 5 5 0 20500.69 23399.18 594.18 o 6 5 0 1101.31 1246.23 52.16 o 7 5 0 649.59 662.09 37.60 o 8 5 0 6.79 28.09 27.63 o 9 5 0 1034.19 1337.45 87.47 o 10 5 0 3259.25 4264.37 180.28 o 11 5 0 287.59 324.08 80.43 o -15 6 0 195.20 147.94 53.88 o -14 6 0 2517.49 2498.16 181.80 o -13 6 0 180.03 185.09 37.77 o -12 6 0 63.68 138.07 33.67 o -11 6 0 3.70 -21.10 23.61 o -10 6 0 181.55 104.27 43.31 o -9 6 0 641.20 545.96 35.34 o -8 6 0 2864.29 3139.43 91.49 o -7 6 0 1599.45 939.95 38.00 o -6 6 0 177.09 81.16 15.47 o -5 6 0 13920.42 15607.22 556.55 o -4 6 0 1454.16 1234.16 60.92 o -3 6 0 25254.77 27418.59 798.45 o -2 6 0 33.78 138.51 78.92 o -1 6 0 1108.79 724.97 46.57 o 0 6 0 1552.20 988.74 81.39 o 1 6 0 1803.40 2224.14 70.07 o 2 6 0 181.57 113.11 24.99 o 3 6 0 14478.01 15185.69 422.66 o 4 6 0 3255.83 3097.76 99.95 o 5 6 0 435.08 509.87 42.68 o 6 6 0 309.63 323.12 66.23 o 7 6 0 2538.75 2588.41 215.26 o 8 6 0 348.77 406.71 54.89 o 9 6 0 4686.35 5849.96 302.79 o 10 6 0 1016.40 1131.76 86.55 o -15 7 0 1522.49 1637.81 82.30 o -14 7 0 81.69 108.54 40.93 o -13 7 0 74.53 105.44 35.95 o -12 7 0 136.96 118.64 34.58 o -11 7 0 1271.63 1061.83 69.04 o -10 7 0 104.60 18.46 22.58 o -9 7 0 1306.81 1193.59 49.97 o -8 7 0 1008.62 866.83 40.97 o -7 7 0 18.24 61.54 15.16 o -6 7 0 6910.28 7844.76 259.83 o -5 7 0 807.76 644.66 36.30 o -4 7 0 7857.06 8567.32 241.52 o -3 7 0 2885.69 2633.38 69.99 o -2 7 0 710.88 1005.60 62.39 o -1 7 0 3386.73 2535.69 166.77 o 0 7 0 6929.55 7725.09 397.41 o 1 7 0 5551.85 6046.10 248.08 o 2 7 0 896.07 868.90 89.89 o 3 7 0 1809.45 1669.71 83.47 o 4 7 0 5280.98 5466.91 242.47 o 5 7 0 116.49 111.59 52.04 o 6 7 0 6669.46 6594.88 248.35 o 7 7 0 1700.38 1356.46 106.45 o 8 7 0 1080.73 1098.38 93.44 o 9 7 0 128.51 193.97 94.62 o -15 8 0 23.93 12.13 44.06 o -14 8 0 249.06 245.10 43.66 o -13 8 0 446.04 421.85 44.94 o -11 8 0 2052.61 1973.52 94.23 o -10 8 0 3.83 -10.77 22.58 o -9 8 0 1065.96 851.20 41.87 o -8 8 0 844.33 796.40 37.93 o -7 8 0 1350.04 1485.76 52.18 o -6 8 0 14614.23 15080.00 386.36 o -5 8 0 9833.83 10698.91 301.09 o -4 8 0 5133.08 5685.96 141.03 o -3 8 0 1560.46 1415.93 48.14 o -2 8 0 11949.80 11421.34 399.76 o -1 8 0 915.90 1099.87 62.51 o 0 8 0 818.33 806.56 75.70 o 1 8 0 0.69 24.05 28.87 o 2 8 0 257.10 168.56 36.29 o 3 8 0 3212.68 2975.10 126.60 o 4 8 0 304.00 235.72 41.46 o 5 8 0 4775.69 4334.16 192.79 o 6 8 0 1468.91 1117.10 173.87 o 7 8 0 118.66 68.37 50.50 o 8 8 0 26.00 66.23 80.43 o -15 9 0 139.71 64.86 49.61 o -14 9 0 406.21 352.00 48.24 o -13 9 0 1827.69 1675.41 178.57 o -12 9 0 2492.05 2422.96 113.41 o -11 9 0 832.34 757.37 44.05 o -10 9 0 1103.04 989.61 47.88 o -9 9 0 710.21 629.23 35.60 o -8 9 0 13.69 24.79 23.23 o -7 9 0 13812.84 13858.72 357.47 o -6 9 0 14256.48 15110.07 386.32 o -5 9 0 9.99 5.54 16.50 o -4 9 0 9458.96 10119.05 357.94 o -3 9 0 22622.70 24934.04 857.24 o -2 9 0 413.21 313.14 36.94 o -1 9 0 145.88 83.91 37.85 o 0 9 0 2451.86 2276.20 103.34 o 1 9 0 1130.81 1103.46 72.69 o 2 9 0 7540.29 7397.26 315.80 o 3 9 0 5572.69 5797.89 620.95 o 4 9 0 25.90 -40.34 40.34 o 5 9 0 24.40 21.08 46.03 o 6 9 0 4.76 16.56 80.43 o 7 9 0 60.16 151.39 87.52 o -14 10 0 187.09 182.99 50.29 o -13 10 0 442.91 357.69 49.13 o -12 10 0 308.08 289.47 37.51 o -11 10 0 0.25 -30.83 30.83 o -10 10 0 3201.62 2984.21 124.96 o -9 10 0 5124.30 5179.82 145.66 o -8 10 0 3370.72 3297.31 114.18 o -7 10 0 2431.99 2300.83 74.84 o -6 10 0 392.72 454.39 46.48 o -5 10 0 1803.03 1592.62 85.11 o -4 10 0 6593.64 6844.29 251.70 o -3 10 0 35.45 85.34 32.34 o -2 10 0 665.45 655.35 51.53 o -1 10 0 2949.22 2710.54 145.48 o 0 10 0 45.24 52.19 39.21 o 1 10 0 3454.52 3318.86 141.16 o 2 10 0 4557.43 4373.16 254.29 o 3 10 0 425.69 568.47 62.69 o 4 10 0 266.25 364.38 58.47 o 5 10 0 249.39 210.53 85.16 o 6 10 0 72.68 101.72 89.89 o -14 11 0 7.10 -25.72 51.78 o -13 11 0 306.51 237.11 51.56 o -12 11 0 442.58 410.30 44.13 o -11 11 0 2292.16 2362.19 85.20 o -10 11 0 4771.90 5105.28 146.57 o -9 11 0 23.76 6.88 28.95 o -8 11 0 33.58 33.29 54.41 o -7 11 0 1100.91 1106.50 61.72 o -6 11 0 1295.18 1133.08 76.72 o -5 11 0 8.36 -34.69 35.01 o -4 11 0 3808.40 3594.07 147.97 o -3 11 0 1000.34 967.77 71.69 o -2 11 0 119.04 193.49 80.43 o -1 11 0 437.31 422.75 50.50 o 0 11 0 616.70 458.31 53.21 o 1 11 0 637.72 584.36 60.62 o 2 11 0 45.41 81.72 51.13 o 3 11 0 417.36 494.39 96.99 o 4 11 0 0.57 -52.04 75.70 o 5 11 0 704.83 896.53 123.01 o -14 12 0 534.79 619.75 67.61 o -13 12 0 2156.83 2212.03 113.12 o -12 12 0 47.12 -17.96 44.90 o -11 12 0 1209.80 1361.74 75.54 o -10 12 0 97.59 92.20 46.29 o -9 12 0 34.95 6.26 40.21 o -8 12 0 54.03 32.53 39.21 o -7 12 0 5131.55 5269.94 196.72 o -6 12 0 285.59 332.14 50.18 o -5 12 0 6237.63 6405.82 243.34 o -4 12 0 678.10 650.76 58.26 o -3 12 0 16.16 -0.14 53.22 o -2 12 0 402.45 428.13 92.26 o -1 12 0 120.30 89.97 48.42 o 0 12 0 4.40 -4.01 49.15 o 1 12 0 295.65 247.22 59.94 o 2 12 0 169.65 144.30 85.16 o 3 12 0 166.39 101.72 89.89 o 4 12 0 1469.26 1310.50 149.03 o -13 13 0 742.65 771.64 69.17 o -12 13 0 15.67 9.59 43.12 o -11 13 0 199.16 147.67 41.50 o -10 13 0 278.67 298.72 43.55 o -9 13 0 93.07 140.10 45.06 o -8 13 0 9814.75 11130.68 447.30 o -7 13 0 2368.83 2316.23 121.97 o -6 13 0 1339.06 1194.03 133.65 o -5 13 0 93.34 115.48 51.00 o -4 13 0 47.02 44.36 47.65 o -3 13 0 7.95 5.69 50.86 o -2 13 0 841.14 842.29 74.31 o -1 13 0 1080.87 1078.88 83.58 o 0 13 0 0.76 -61.50 82.79 o 1 13 0 283.75 338.27 101.72 o 2 13 0 2.06 4.73 89.89 o 3 13 0 432.34 399.77 106.45 o -12 14 0 3.33 -21.29 44.00 o -11 14 0 2099.00 2145.93 142.27 o -10 14 0 517.43 548.05 56.80 o -9 14 0 2744.73 2693.20 142.06 o -8 14 0 4141.01 4112.99 192.65 o -7 14 0 99.56 102.53 45.47 o -6 14 0 174.93 163.95 59.36 o -5 14 0 45.44 120.64 56.87 o -4 14 0 213.51 245.57 61.04 o -3 14 0 1581.78 1560.93 108.69 o -2 14 0 1676.91 1619.07 110.24 o -1 14 0 146.21 156.12 94.62 o 0 14 0 852.60 979.32 132.47 o 1 14 0 175.30 75.70 94.62 o -11 15 0 1579.37 1812.83 101.48 o -10 15 0 336.92 254.18 58.38 o -9 15 0 370.33 337.54 62.45 o -8 15 0 66.32 51.03 56.77 o -7 15 0 65.19 2.17 45.33 o -6 15 0 496.25 446.53 76.09 o -5 15 0 2656.21 2606.22 143.01 o -4 15 0 26.43 -9.71 72.15 o -3 15 0 292.65 331.17 106.45 o -2 15 0 160.46 89.89 101.72 o -1 15 0 246.10 246.01 108.81 o -9 16 0 131.34 76.88 61.97 o -8 16 0 561.15 588.63 79.48 o -7 16 0 86.71 41.25 56.77 o -6 16 0 2747.33 2796.04 227.09 o -5 16 0 197.39 193.97 108.81 o -4 16 0 131.93 66.23 108.81 o 3 -16 1 315.11 231.82 106.45 o 4 -16 1 288.37 43.13 75.05 o 5 -16 1 100.59 -58.97 72.63 o 6 -16 1 1207.84 1315.83 103.06 o 7 -16 1 9.92 18.67 58.63 o 8 -16 1 355.36 316.68 67.83 o 9 -16 1 625.82 647.28 75.53 o 0 -15 1 219.42 451.81 111.18 o 1 -15 1 53.60 14.19 89.89 o 2 -15 1 40.77 6.42 66.84 o 3 -15 1 782.04 571.70 82.79 o 4 -15 1 6.85 -54.56 62.71 o 5 -15 1 3456.35 3850.68 174.79 o 6 -15 1 3254.61 3473.22 172.63 o 7 -15 1 6.84 22.30 47.63 o 8 -15 1 80.17 43.53 53.80 o 9 -15 1 1292.97 1084.61 87.52 o 10 -15 1 6.67 11.61 61.50 o 11 -15 1 376.43 568.77 99.49 o -1 -14 1 563.30 570.09 111.18 o 0 -14 1 751.18 735.68 115.91 o 1 -14 1 808.44 802.05 81.91 o 2 -14 1 1126.97 1006.75 85.11 o 3 -14 1 375.35 194.87 59.36 o 4 -14 1 2626.11 2941.02 141.33 o 5 -14 1 4825.89 5481.50 219.95 o 6 -14 1 2407.34 2714.81 112.28 o 7 -14 1 169.22 191.17 47.64 o 8 -14 1 1084.92 924.61 78.56 o 9 -14 1 17.14 78.71 45.47 o 10 -14 1 2957.91 3294.20 163.51 o 11 -14 1 1309.47 1541.10 88.92 o 12 -14 1 570.55 596.82 61.46 o -3 -13 1 5.31 101.72 92.26 o -2 -13 1 147.31 165.59 89.89 o -1 -13 1 609.99 596.51 72.75 o 0 -13 1 930.58 1008.49 81.01 o 1 -13 1 2511.68 2380.00 123.74 o 2 -13 1 3389.41 3284.36 157.31 o 3 -13 1 11.50 -16.05 46.75 o 4 -13 1 3231.14 3407.60 149.70 o 5 -13 1 4015.40 4530.46 184.82 o 6 -13 1 1310.26 1426.00 95.44 o 7 -13 1 868.08 766.99 68.58 o 8 -13 1 815.80 633.45 88.71 o 9 -13 1 547.39 534.96 57.90 o 10 -13 1 292.05 319.06 44.75 o 11 -13 1 1905.62 2307.25 103.74 o 12 -13 1 1992.76 2311.11 107.81 o 13 -13 1 44.89 -6.30 49.99 o -4 -12 1 2.74 101.72 92.26 o -3 -12 1 395.85 409.30 85.16 o -2 -12 1 281.49 236.68 59.14 o -1 -12 1 1283.38 1304.81 92.73 o 0 -12 1 3257.77 2744.56 130.34 o 1 -12 1 4517.82 4299.85 214.08 o 2 -12 1 12.32 28.81 41.42 o 3 -12 1 526.61 372.71 49.15 o 4 -12 1 3251.78 3529.91 148.84 o 5 -12 1 3555.36 3977.12 162.22 o 6 -12 1 534.87 449.78 40.00 o 7 -12 1 2164.88 1955.59 105.73 o 8 -12 1 1959.68 1969.22 106.89 o 9 -12 1 977.85 819.48 65.17 o 10 -12 1 2071.04 2251.86 97.30 o 11 -12 1 3939.57 4441.98 158.73 o 12 -12 1 132.78 62.93 47.73 o 13 -12 1 890.87 868.53 67.91 o 14 -12 1 0.47 17.28 74.88 o -6 -11 1 61.73 101.72 87.52 o -5 -11 1 13.74 -47.31 82.79 o -4 -11 1 180.09 138.90 56.80 o -3 -11 1 2177.44 2082.64 216.44 o -2 -11 1 2161.45 2308.53 134.83 o -1 -11 1 4.70 12.19 42.63 o 0 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