#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/40/2014027.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014027_Fobs loop_ _publ_author_name 'Seela, Frank' 'Jawalekar, Anup M.' 'Eickmeier, Henning' _publ_section_title ; 1-(2-Deoxy-\b-D-erythro-pentofuranosyl)-4-nitro-1H-indazole ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o387 _journal_page_last o389 _journal_volume 60 _journal_year 2004 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.7444 _cell_length_b 11.7177 _cell_length_c 15.7337 _exptl_crystal_F_000 584.00 _reflns_d_resolution_high 0.7108 _[local]_cod_data_source_file jz1612Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' N4nitroc in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 126.96 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 8573.28 7907.00 43.80 o 4 0 0 2918.10 2911.63 37.99 o 6 0 0 300.76 231.55 8.68 o 8 0 0 0.74 0.48 0.77 o 1 1 0 2354.20 2392.86 52.53 o 2 1 0 1242.11 1290.41 17.72 o 3 1 0 1011.56 984.80 30.38 o 4 1 0 156.25 161.35 4.09 o 5 1 0 26.02 27.45 0.65 o 6 1 0 464.81 409.15 12.22 o 7 1 0 16.67 13.46 0.64 o 8 1 0 43.95 47.41 1.71 o 9 1 0 0.40 -0.23 0.62 o 0 2 0 4911.14 4636.23 23.98 o 1 2 0 5245.73 5005.41 618.68 o 2 2 0 504.54 518.74 11.66 o 3 2 0 9.73 9.90 0.42 o 4 2 0 56.73 47.23 2.10 o 5 2 0 84.67 84.74 2.98 o 6 2 0 1.27 0.93 0.54 o 7 2 0 2.72 1.19 0.69 o 8 2 0 15.19 10.94 1.33 o 9 2 0 1.42 1.28 1.12 o 1 3 0 6641.01 6653.19 216.45 o 2 3 0 311.58 313.45 10.25 o 3 3 0 1129.43 1110.68 21.95 o 4 3 0 1.27 1.73 0.37 o 5 3 0 418.92 372.75 16.68 o 6 3 0 43.17 37.43 2.00 o 7 3 0 0.70 1.62 0.66 o 8 3 0 6.72 7.45 1.03 o 9 3 0 15.59 18.15 1.47 o 0 4 0 65.51 51.21 1.81 o 1 4 0 110.75 101.13 7.69 o 2 4 0 176.10 178.40 5.72 o 3 4 0 93.26 103.31 4.45 o 4 4 0 310.28 323.59 15.08 o 5 4 0 436.37 440.79 12.69 o 6 4 0 83.07 73.83 2.98 o 7 4 0 13.08 13.36 0.95 o 8 4 0 0.12 0.13 0.83 o 9 4 0 14.04 14.24 1.28 o 1 5 0 754.62 762.37 44.68 o 2 5 0 0.43 0.42 0.29 o 3 5 0 57.50 65.59 2.82 o 4 5 0 66.26 81.60 3.06 o 5 5 0 374.67 361.24 12.14 o 6 5 0 21.52 15.48 1.04 o 7 5 0 8.16 4.81 0.77 o 8 5 0 0.30 -0.24 0.83 o 9 5 0 68.40 74.16 4.55 o 0 6 0 645.31 592.63 16.25 o 1 6 0 11.48 16.85 2.76 o 2 6 0 148.85 162.43 5.45 o 3 6 0 82.56 87.82 3.48 o 4 6 0 75.03 68.77 3.03 o 5 6 0 525.25 518.26 21.26 o 7 6 0 0.15 0.21 0.72 o 8 6 0 5.24 5.91 0.98 o 1 7 0 219.59 256.43 5.68 o 2 7 0 17.16 12.00 0.59 o 3 7 0 18.68 23.87 0.93 o 4 7 0 28.00 27.37 0.90 o 5 7 0 114.32 131.39 4.85 o 6 7 0 3.27 1.36 0.67 o 7 7 0 10.84 10.57 1.03 o 8 7 0 3.89 4.85 1.07 o 0 8 0 383.42 375.52 14.66 o 1 8 0 28.15 26.84 0.99 o 2 8 0 2.40 2.23 0.50 o 3 8 0 12.47 11.95 0.67 o 4 8 0 55.94 57.33 3.19 o 5 8 0 75.09 73.64 2.15 o 6 8 0 10.52 8.94 0.90 o 7 8 0 27.89 32.35 1.36 o 8 8 0 38.28 43.26 1.59 o 1 9 0 0.01 0.16 0.30 o 2 9 0 6.53 5.46 0.61 o 3 9 0 3.18 2.19 0.51 o 4 9 0 47.50 57.45 2.40 o 5 9 0 7.45 7.35 0.75 o 6 9 0 67.76 72.03 2.42 o 7 9 0 0.41 2.52 0.88 o 0 10 0 66.07 59.46 3.38 o 1 10 0 79.61 72.63 6.23 o 2 10 0 41.60 46.25 1.78 o 3 10 0 5.33 4.89 0.91 o 4 10 0 111.21 120.42 4.44 o 5 10 0 0.79 0.98 0.67 o 6 10 0 2.15 2.56 0.82 o 7 10 0 7.87 6.67 0.99 o 1 11 0 2.60 2.49 1.15 o 2 11 0 2.63 1.23 0.61 o 3 11 0 1.62 1.36 0.59 o 4 11 0 7.33 6.01 0.79 o 5 11 0 15.89 15.94 1.01 o 6 11 0 0.01 0.80 0.79 o 7 11 0 0.62 1.94 0.91 o 0 12 0 83.11 74.44 3.28 o 1 12 0 46.73 46.01 4.99 o 2 12 0 1.54 1.91 0.66 o 3 12 0 3.48 1.59 0.67 o 4 12 0 10.49 12.40 0.98 o 5 12 0 15.36 13.14 1.07 o 6 12 0 0.14 0.72 0.82 o 1 13 0 1.42 1.16 0.58 o 2 13 0 38.50 33.00 2.18 o 3 13 0 20.49 19.43 1.06 o 4 13 0 17.54 16.97 1.15 o 5 13 0 40.35 43.55 1.59 o 0 14 0 10.54 10.72 0.99 o 1 14 0 127.05 125.85 6.75 o 2 14 0 5.05 2.80 0.88 o 3 14 0 3.78 2.13 0.83 o 4 14 0 14.83 17.13 1.38 o 1 15 0 10.18 7.53 0.74 o 2 15 0 27.26 29.02 1.36 o 3 15 0 3.86 3.62 0.91 o 0 16 0 12.16 10.72 1.09 o 1 16 0 2.79 1.83 0.73 o 2 16 0 2.45 1.54 0.90 o 1 0 1 3468.46 3292.84 24.36 o 2 0 1 2849.06 2828.67 32.83 o 3 0 1 252.03 236.98 6.90 o 4 0 1 528.23 515.80 14.23 o 5 0 1 5.21 3.86 0.54 o 6 0 1 51.41 54.29 1.43 o 7 0 1 0.63 -0.04 0.48 o 8 0 1 5.25 6.00 0.78 o 9 0 1 5.31 2.90 0.75 o 0 1 1 78.45 84.04 7.39 o 1 1 1 2244.95 2286.90 23.83 o 2 1 1 792.46 763.67 16.15 o 3 1 1 55.10 44.49 1.62 o 4 1 1 324.24 317.01 5.11 o 5 1 1 32.11 33.62 0.62 o 6 1 1 52.39 49.58 1.14 o 7 1 1 38.33 36.10 1.57 o 8 1 1 1.98 0.84 0.47 o 9 1 1 29.40 29.61 1.89 o 0 2 1 881.71 877.59 49.36 o 1 2 1 10365.84 9122.83 626.52 o 2 2 1 639.31 685.51 9.90 o 3 2 1 755.16 772.58 12.91 o 4 2 1 19.97 23.28 1.95 o 5 2 1 186.75 182.59 7.86 o 6 2 1 22.93 18.87 0.64 o 7 2 1 148.24 123.38 4.14 o 8 2 1 18.98 19.12 0.79 o 9 2 1 19.90 20.37 1.14 o 0 3 1 16117.95 14675.02 990.62 o 1 3 1 5421.43 5609.51 55.34 o 2 3 1 310.84 341.32 9.12 o 3 3 1 424.17 450.45 10.39 o 4 3 1 308.22 330.55 20.44 o 5 3 1 224.28 210.18 9.28 o 6 3 1 106.69 86.77 4.25 o 7 3 1 6.31 5.43 0.63 o 8 3 1 8.75 8.18 0.88 o 9 3 1 60.14 67.78 1.96 o 0 4 1 4308.30 3944.38 77.59 o 1 4 1 1610.13 1522.98 85.82 o 2 4 1 832.05 891.86 13.19 o 3 4 1 440.26 474.60 11.01 o 4 4 1 240.50 240.06 6.33 o 5 4 1 137.77 118.12 3.50 o 6 4 1 159.46 136.75 3.87 o 7 4 1 28.86 29.84 1.82 o 8 4 1 28.62 33.57 1.02 o 9 4 1 35.71 39.39 1.25 o 0 5 1 777.82 763.38 12.36 o 1 5 1 429.47 437.66 25.32 o 2 5 1 158.35 163.49 4.11 o 3 5 1 209.84 208.79 5.28 o 4 5 1 94.64 98.67 2.69 o 5 5 1 5.93 7.05 0.45 o 6 5 1 104.73 100.89 3.26 o 7 5 1 55.35 62.44 1.78 o 8 5 1 9.79 10.96 0.75 o 9 5 1 1.51 2.41 0.77 o 0 6 1 3.77 2.41 0.26 o 1 6 1 2042.81 1915.60 111.03 o 2 6 1 94.85 100.06 2.90 o 3 6 1 129.66 130.39 3.44 o 4 6 1 289.32 299.01 7.06 o 5 6 1 63.46 68.17 2.72 o 6 6 1 79.34 87.97 3.32 o 7 6 1 15.60 15.77 0.72 o 8 6 1 4.10 3.59 0.67 o 0 7 1 45.02 44.72 1.08 o 1 7 1 382.07 384.33 19.03 o 2 7 1 14.20 17.61 0.80 o 3 7 1 12.01 14.30 0.45 o 4 7 1 70.69 74.28 1.51 o 5 7 1 153.48 158.08 4.13 o 6 7 1 81.65 79.35 3.01 o 7 7 1 7.94 9.80 0.67 o 8 7 1 4.95 4.77 0.76 o 0 8 1 585.07 578.30 36.59 o 1 8 1 14.77 14.35 0.81 o 2 8 1 19.75 22.86 0.75 o 3 8 1 1.25 0.43 0.40 o 4 8 1 207.64 206.70 7.51 o 5 8 1 49.66 52.92 1.61 o 6 8 1 5.98 5.93 0.57 o 7 8 1 5.09 5.08 0.63 o 8 8 1 14.15 17.63 0.93 o 0 9 1 27.69 28.49 0.98 o 1 9 1 47.30 47.22 1.61 o 2 9 1 89.99 91.62 2.86 o 3 9 1 42.96 41.98 1.46 o 4 9 1 0.41 -0.39 0.39 o 5 9 1 11.29 10.14 0.57 o 6 9 1 4.95 6.10 1.63 o 7 9 1 5.02 6.05 0.97 o 0 10 1 227.90 219.28 5.87 o 1 10 1 71.26 70.41 1.97 o 2 10 1 71.92 71.45 1.74 o 3 10 1 30.25 28.59 1.23 o 4 10 1 36.60 38.50 0.98 o 5 10 1 26.73 27.34 0.81 o 6 10 1 15.79 16.31 0.78 o 7 10 1 16.72 18.69 0.91 o 0 11 1 13.42 13.81 1.91 o 1 11 1 5.21 6.22 0.62 o 2 11 1 16.46 17.50 0.70 o 3 11 1 24.16 24.42 1.91 o 4 11 1 40.00 43.65 1.47 o 5 11 1 6.20 7.00 0.60 o 6 11 1 18.22 17.85 1.10 o 7 11 1 0.09 0.38 0.60 o 0 12 1 22.52 16.85 0.72 o 1 12 1 14.58 10.06 0.44 o 2 12 1 47.54 47.58 1.09 o 3 12 1 30.74 31.02 1.14 o 4 12 1 0.11 -0.08 0.50 o 5 12 1 15.94 17.88 0.83 o 6 12 1 10.92 12.95 1.36 o 0 13 1 1.91 0.49 0.58 o 1 13 1 16.11 14.59 0.87 o 2 13 1 8.61 8.77 1.05 o 3 13 1 12.65 11.98 0.75 o 4 13 1 10.74 9.30 0.70 o 5 13 1 6.45 5.45 0.69 o 0 14 1 16.38 16.86 0.79 o 1 14 1 1.64 0.65 0.38 o 2 14 1 5.46 3.74 0.63 o 3 14 1 2.91 1.80 1.15 o 4 14 1 0.40 0.70 0.58 o 0 15 1 2.50 0.79 0.79 o 1 15 1 6.12 4.09 0.53 o 2 15 1 4.88 5.45 2.15 o 3 15 1 1.44 -0.38 0.58 o 0 16 1 20.31 19.10 0.95 o 1 16 1 10.43 8.07 0.56 o 2 16 1 32.31 26.16 1.05 o 0 0 2 588.41 612.90 7.29 o 1 0 2 770.49 740.29 21.20 o 2 0 2 841.66 840.87 14.58 o 3 0 2 574.08 616.86 15.35 o 4 0 2 122.30 146.82 5.78 o 5 0 2 160.05 153.22 6.02 o 6 0 2 67.15 60.07 2.16 o 7 0 2 113.40 100.15 4.13 o 8 0 2 9.53 10.88 1.03 o 9 0 2 8.81 6.18 1.09 o 0 1 2 314.80 301.23 24.83 o 1 1 2 487.48 513.40 10.26 o 2 1 2 360.42 353.78 10.67 o 3 1 2 101.82 107.72 5.35 o 4 1 2 20.82 22.43 2.61 o 5 1 2 80.08 84.04 2.22 o 6 1 2 42.15 32.33 1.83 o 7 1 2 106.84 96.98 2.26 o 8 1 2 36.22 32.06 2.14 o 9 1 2 38.00 36.24 2.11 o 0 2 2 2837.95 2676.97 20.32 o 1 2 2 104.38 96.89 2.46 o 2 2 2 242.30 259.65 9.15 o 3 2 2 490.15 500.94 15.04 o 4 2 2 49.04 47.41 2.21 o 5 2 2 244.37 252.20 9.68 o 6 2 2 50.20 44.89 1.62 o 7 2 2 33.02 32.00 1.15 o 8 2 2 8.89 8.33 0.98 o 9 2 2 3.20 3.06 1.01 o 0 3 2 5758.11 5689.66 34.53 o 1 3 2 6855.95 6860.78 95.67 o 2 3 2 97.23 98.89 3.83 o 3 3 2 9.94 15.41 0.62 o 4 3 2 98.48 115.93 4.77 o 5 3 2 126.46 128.32 5.21 o 6 3 2 75.12 74.28 3.33 o 7 3 2 12.99 9.34 0.88 o 8 3 2 1.16 2.29 0.82 o 9 3 2 2.57 0.40 1.01 o 0 4 2 242.84 223.23 9.08 o 1 4 2 831.42 876.92 34.24 o 2 4 2 906.88 893.63 19.16 o 3 4 2 68.90 65.99 3.03 o 4 4 2 319.94 359.93 15.01 o 5 4 2 111.71 104.93 5.00 o 6 4 2 1.84 2.52 0.59 o 7 4 2 5.05 2.72 0.74 o 8 4 2 13.03 15.77 1.14 o 9 4 2 2.61 0.38 1.06 o 0 5 2 310.29 341.14 11.17 o 1 5 2 481.62 465.37 9.54 o 2 5 2 323.36 305.65 12.55 o 3 5 2 494.25 568.36 18.57 o 4 5 2 33.04 34.16 0.87 o 5 5 2 15.29 16.20 0.88 o 6 5 2 11.69 9.18 0.77 o 7 5 2 1.81 3.43 0.77 o 8 5 2 0.37 -0.13 0.83 o 0 6 2 148.69 170.02 5.66 o 1 6 2 1030.16 1056.96 32.17 o 2 6 2 958.90 991.24 24.00 o 3 6 2 48.81 53.06 2.15 o 4 6 2 70.06 84.72 3.72 o 5 6 2 225.16 229.85 8.88 o 6 6 2 7.35 8.67 0.77 o 7 6 2 33.99 34.22 1.39 o 8 6 2 32.78 33.76 1.43 o 0 7 2 27.52 30.65 1.70 o 1 7 2 389.16 385.63 10.24 o 2 7 2 534.71 560.63 19.24 o 3 7 2 89.58 88.30 4.05 o 4 7 2 262.05 265.85 9.48 o 5 7 2 115.26 107.95 4.31 o 6 7 2 50.58 50.36 1.78 o 7 7 2 12.62 15.43 1.03 o 8 7 2 5.10 4.79 0.99 o 0 8 2 0.85 0.50 0.45 o 1 8 2 83.70 88.85 2.54 o 2 8 2 41.49 49.11 1.78 o 3 8 2 20.63 21.21 0.80 o 4 8 2 24.12 24.24 0.91 o 5 8 2 32.04 29.14 1.94 o 6 8 2 37.69 37.06 1.83 o 7 8 2 6.22 6.41 0.95 o 8 8 2 48.45 55.15 2.05 o 0 9 2 9.32 8.91 0.62 o 1 9 2 14.51 13.12 0.50 o 2 9 2 7.48 6.28 0.62 o 3 9 2 145.55 153.06 6.87 o 4 9 2 35.24 41.40 2.96 o 5 9 2 12.81 15.49 0.90 o 6 9 2 5.78 8.78 0.93 o 7 9 2 41.11 42.30 1.94 o 0 10 2 6.18 6.34 0.67 o 1 10 2 150.11 146.75 4.15 o 2 10 2 17.83 16.18 0.83 o 3 10 2 47.35 45.20 2.92 o 4 10 2 42.34 45.28 1.76 o 5 10 2 18.72 18.06 1.04 o 6 10 2 6.48 9.13 0.95 o 7 10 2 0.34 2.11 0.88 o 0 11 2 197.45 200.13 7.61 o 1 11 2 55.13 67.99 3.25 o 2 11 2 114.35 130.93 5.90 o 3 11 2 9.94 10.40 0.80 o 4 11 2 14.12 12.87 0.91 o 5 11 2 20.39 18.12 1.09 o 6 11 2 14.56 20.30 1.20 o 0 12 2 2.61 1.49 0.64 o 1 12 2 18.08 19.19 0.76 o 2 12 2 40.04 42.33 1.60 o 3 12 2 44.54 49.33 1.84 o 4 12 2 22.14 23.74 1.15 o 5 12 2 1.09 1.09 0.79 o 6 12 2 0.14 -0.37 0.83 o 0 13 2 38.45 38.18 2.08 o 1 13 2 3.22 3.21 0.87 o 2 13 2 70.65 69.41 3.12 o 3 13 2 6.97 4.61 0.80 o 4 13 2 8.81 9.34 0.96 o 5 13 2 4.37 5.05 0.93 o 0 14 2 15.27 12.82 1.06 o 1 14 2 6.29 5.67 0.62 o 2 14 2 38.13 38.60 1.83 o 3 14 2 4.22 3.65 0.96 o 4 14 2 0.02 0.14 0.82 o 0 15 2 5.56 7.02 0.98 o 1 15 2 6.32 3.78 0.68 o 2 15 2 26.35 25.30 1.44 o 3 15 2 0.54 1.78 0.83 o 0 16 2 13.01 14.00 1.22 o 1 16 2 27.87 25.94 1.03 o 2 16 2 0.13 1.73 0.82 o 1 0 3 1883.24 1896.00 70.29 o 2 0 3 97.67 78.01 3.09 o 3 0 3 2391.37 2351.21 30.10 o 4 0 3 300.77 275.05 12.93 o 5 0 3 32.45 31.85 1.23 o 6 0 3 94.09 95.33 3.99 o 7 0 3 123.85 135.06 5.56 o 8 0 3 1.53 0.08 0.77 o 9 0 3 0.20 -0.54 0.91 o 0 1 3 1683.55 1624.13 14.96 o 1 1 3 1636.28 1624.10 24.18 o 2 1 3 165.17 177.28 10.38 o 3 1 3 1046.69 1086.04 14.85 o 4 1 3 76.95 79.49 2.45 o 5 1 3 205.91 219.16 5.31 o 6 1 3 151.48 138.72 4.05 o 7 1 3 97.01 88.28 2.39 o 8 1 3 15.08 14.05 0.82 o 9 1 3 6.99 5.72 1.55 o 0 2 3 21.17 22.72 1.03 o 1 2 3 480.06 469.61 13.68 o 2 2 3 409.18 390.48 11.12 o 3 2 3 756.28 852.92 19.55 o 4 2 3 124.10 149.07 5.27 o 5 2 3 10.09 10.72 0.64 o 6 2 3 21.24 20.62 0.93 o 7 2 3 144.56 142.59 6.07 o 8 2 3 4.92 2.39 0.83 o 9 2 3 3.20 1.84 1.03 o 0 3 3 207.55 187.37 7.05 o 1 3 3 1811.54 1839.58 42.77 o 2 3 3 610.15 611.38 14.55 o 3 3 3 989.87 1088.51 22.72 o 4 3 3 568.08 595.83 19.55 o 5 3 3 7.22 9.16 0.62 o 6 3 3 318.45 313.23 11.42 o 7 3 3 0.63 -0.16 0.67 o 8 3 3 20.48 18.97 1.14 o 9 3 3 9.21 6.92 1.17 o 0 4 3 273.96 302.75 9.65 o 1 4 3 483.67 523.24 9.19 o 2 4 3 381.79 384.89 13.39 o 3 4 3 199.02 210.86 7.47 o 4 4 3 81.89 85.04 3.44 o 5 4 3 1.08 2.58 0.51 o 6 4 3 3.87 2.29 0.61 o 7 4 3 27.05 25.65 1.14 o 8 4 3 9.96 10.72 1.09 o 9 4 3 15.86 14.26 1.51 o 0 5 3 772.39 753.68 16.66 o 1 5 3 1816.90 1906.66 50.21 o 2 5 3 1484.80 1502.32 26.79 o 3 5 3 89.14 103.79 4.34 o 4 5 3 114.77 121.27 4.95 o 5 5 3 3.55 4.73 0.58 o 6 5 3 80.57 75.56 4.12 o 7 5 3 19.64 13.76 0.96 o 8 5 3 17.01 17.80 1.17 o 0 6 3 97.99 101.32 3.94 o 1 6 3 564.65 554.72 11.58 o 2 6 3 1080.95 1053.10 23.73 o 3 6 3 544.57 549.40 18.94 o 4 6 3 5.18 6.36 0.58 o 5 6 3 19.63 20.96 0.85 o 6 6 3 57.24 59.15 3.00 o 7 6 3 96.89 98.09 3.69 o 8 6 3 22.93 26.44 1.33 o 0 7 3 11.25 12.74 0.58 o 1 7 3 144.98 161.41 4.94 o 2 7 3 951.32 981.75 25.41 o 3 7 3 266.65 263.06 9.53 o 4 7 3 19.75 16.77 0.77 o 5 7 3 48.80 52.57 1.55 o 6 7 3 57.90 65.55 2.08 o 7 7 3 0.82 0.80 0.72 o 8 7 3 19.05 18.71 1.28 o 0 8 3 0.24 0.30 0.43 o 1 8 3 1.69 4.07 0.37 o 2 8 3 0.29 0.40 0.48 o 3 8 3 38.31 45.95 1.67 o 4 8 3 142.60 137.61 5.67 o 5 8 3 7.51 6.81 0.74 o 6 8 3 53.83 47.50 2.84 o 7 8 3 4.05 2.98 0.90 o 8 8 3 6.70 7.43 1.11 o 0 9 3 114.68 111.03 4.23 o 1 9 3 29.89 28.03 0.91 o 2 9 3 112.95 106.45 4.31 o 3 9 3 428.85 405.59 19.53 o 4 9 3 51.95 58.56 3.14 o 5 9 3 25.98 25.04 1.04 o 7 9 3 24.05 28.98 1.35 o 0 10 3 65.97 82.53 3.64 o 1 10 3 99.41 97.42 3.43 o 2 10 3 14.47 13.57 1.47 o 3 10 3 43.37 43.58 1.68 o 4 10 3 2.43 2.95 0.67 o 5 10 3 53.11 49.33 2.39 o 6 10 3 5.68 7.43 0.95 o 7 10 3 3.52 3.14 0.98 o 0 11 3 5.06 6.47 0.72 o 1 11 3 34.72 33.53 2.05 o 2 11 3 22.40 26.10 1.03 o 3 11 3 124.37 128.32 5.29 o 4 11 3 15.56 16.57 0.99 o 5 11 3 31.00 34.25 1.35 o 6 11 3 0.38 0.43 0.79 o 0 12 3 16.07 15.35 0.90 o 1 12 3 14.25 11.04 0.62 o 2 12 3 23.44 27.17 1.07 o 3 12 3 23.60 23.62 1.09 o 4 12 3 0.52 0.42 0.70 o 5 12 3 2.44 1.09 0.80 o 6 12 3 4.50 4.55 1.03 o 0 13 3 0.23 0.99 0.66 o 1 13 3 2.92 2.58 1.75 o 2 13 3 12.88 9.65 0.90 o 3 13 3 7.27 9.04 0.88 o 4 13 3 0.83 2.24 0.82 o 5 13 3 1.02 1.73 0.80 o 0 14 3 6.32 3.70 0.83 o 1 14 3 28.04 27.24 1.54 o 2 14 3 28.90 28.63 1.30 o 3 14 3 0.48 1.43 0.75 o 4 14 3 1.44 1.92 0.88 o 0 15 3 0.59 0.42 0.80 o 1 15 3 21.02 20.36 1.50 o 2 15 3 3.56 1.39 0.87 o 3 15 3 0.32 -0.43 0.85 o 0 16 3 5.20 3.52 0.99 o 1 16 3 2.77 2.51 0.68 o 0 0 4 9599.06 9280.55 41.64 o 1 0 4 840.02 847.25 10.55 o 2 0 4 72.73 61.64 2.61 o 3 0 4 141.51 155.41 5.64 o 4 0 4 255.13 234.82 8.56 o 5 0 4 542.21 470.37 19.27 o 6 0 4 442.93 415.85 13.12 o 7 0 4 5.10 2.63 0.75 o 8 0 4 59.09 58.45 2.31 o 9 0 4 12.88 13.04 1.36 o 0 1 4 1991.79 2151.62 14.51 o 1 1 4 1044.14 1134.79 15.03 o 2 1 4 1484.41 1556.29 15.70 o 3 1 4 1273.27 1353.64 22.45 o 4 1 4 112.73 120.22 6.14 o 5 1 4 30.43 35.97 1.77 o 6 1 4 223.41 195.11 5.33 o 7 1 4 18.75 15.81 0.69 o 8 1 4 32.41 33.19 1.47 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7.94 0.77 o 2 12 8 22.84 23.78 1.15 o 3 12 8 7.00 5.27 0.88 o 4 12 8 32.78 36.42 1.60 o 5 12 8 2.44 4.04 0.87 o 0 13 8 42.36 46.01 1.47 o 1 13 8 2.51 2.32 0.90 o 2 13 8 16.78 19.45 1.14 o 3 13 8 25.74 25.81 1.27 o 4 13 8 3.73 5.26 0.98 o 0 14 8 16.27 17.70 1.19 o 1 14 8 6.71 6.54 0.69 o 2 14 8 2.20 3.28 0.87 o 3 14 8 16.18 15.27 1.22 o 0 15 8 2.51 0.80 0.87 o 1 15 8 3.31 1.45 0.62 o 1 0 9 499.07 509.55 27.71 o 2 0 9 70.88 72.75 3.04 o 3 0 9 10.31 10.43 0.56 o 4 0 9 143.11 133.96 5.56 o 5 0 9 99.46 97.99 4.33 o 6 0 9 0.05 1.25 0.66 o 7 0 9 10.78 9.77 0.90 o 8 0 9 3.94 5.05 0.98 o 0 1 9 37.55 47.90 1.20 o 1 1 9 201.58 220.56 4.00 o 2 1 9 619.15 647.77 23.22 o 3 1 9 172.54 178.72 4.92 o 4 1 9 66.15 60.18 1.95 o 5 1 9 609.56 566.80 34.58 o 6 1 9 121.34 123.89 5.07 o 7 1 9 16.15 17.62 0.84 o 8 1 9 4.69 3.17 0.70 o 0 2 9 2.70 2.24 0.35 o 1 2 9 804.12 845.60 16.34 o 2 2 9 336.82 328.00 14.66 o 3 2 9 148.19 150.17 6.39 o 4 2 9 458.76 462.24 19.88 o 5 2 9 152.17 145.56 5.45 o 6 2 9 167.16 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13 10 15.19 18.46 1.20 o 0 14 10 2.29 1.17 0.82 o 1 14 10 3.27 3.71 0.65 o 2 14 10 8.53 9.20 1.07 o 1 0 11 47.16 53.04 1.49 o 2 0 11 123.71 121.33 4.82 o 3 0 11 118.35 116.35 5.05 o 4 0 11 3.20 6.28 0.62 o 5 0 11 93.39 93.98 3.89 o 6 0 11 16.50 16.58 0.96 o 7 0 11 1.29 1.33 0.82 o 8 0 11 18.79 18.71 1.27 o 0 1 11 313.20 327.22 10.29 o 1 1 11 7.90 8.17 0.27 o 2 1 11 8.27 10.21 0.56 o 3 1 11 132.21 128.70 3.62 o 4 1 11 157.40 137.51 4.04 o 5 1 11 42.50 39.00 1.06 o 6 1 11 1.94 2.37 1.65 o 7 1 11 30.12 32.68 1.10 o 8 1 11 1.53 0.92 0.67 o 0 2 11 4.84 5.43 0.50 o 1 2 11 120.65 111.84 3.80 o 2 2 11 108.23 99.83 3.69 o 3 2 11 7.90 9.77 0.61 o 4 2 11 3.72 4.68 0.59 o 5 2 11 67.62 61.84 2.74 o 6 2 11 43.46 47.14 1.87 o 7 2 11 15.49 18.10 1.12 o 8 2 11 2.91 3.11 1.01 o 0 3 11 6.87 7.45 0.53 o 1 3 11 626.31 618.12 15.00 o 2 3 11 22.65 19.98 0.98 o 3 3 11 81.27 77.71 3.24 o 4 3 11 66.39 64.12 2.63 o 5 3 11 28.24 29.67 1.09 o 6 3 11 12.25 8.57 0.82 o 7 3 11 2.56 1.38 0.85 o 8 3 11 7.22 7.77 1.14 o 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4.88 4.85 0.98 o 0 9 11 14.74 19.75 0.91 o 1 9 11 70.74 71.59 1.86 o 2 9 11 36.36 39.62 1.35 o 3 9 11 18.13 18.71 0.96 o 4 9 11 33.29 35.74 1.27 o 5 9 11 14.89 15.96 1.01 o 6 9 11 21.72 27.85 1.36 o 0 10 11 67.35 61.36 3.16 o 1 10 11 2.01 3.03 0.69 o 2 10 11 64.98 66.65 2.52 o 3 10 11 1.31 2.98 0.67 o 4 10 11 17.33 20.14 1.14 o 5 10 11 5.17 4.60 0.93 o 0 11 11 0.58 0.59 0.72 o 1 11 11 7.02 6.00 0.57 o 2 11 11 9.72 10.32 1.01 o 3 11 11 0.47 0.46 0.72 o 4 11 11 15.55 21.44 1.59 o 5 11 11 3.65 4.12 0.90 o 0 12 11 1.40 1.44 0.79 o 1 12 11 9.25 6.76 0.64 o 2 12 11 1.56 0.48 0.79 o 3 12 11 8.32 8.72 0.98 o 4 12 11 5.47 5.37 1.01 o 0 13 11 3.70 2.42 0.83 o 1 13 11 8.60 8.50 1.03 o 2 13 11 28.20 28.87 1.41 o 3 13 11 18.98 17.72 1.22 o 0 14 11 2.67 1.57 0.85 o 1 14 11 0.49 0.57 0.59 o 0 0 12 615.62 554.59 19.92 o 1 0 12 119.39 109.88 2.81 o 2 0 12 86.10 83.83 3.97 o 3 0 12 13.18 13.06 0.67 o 4 0 12 11.49 8.32 0.67 o 5 0 12 5.29 4.79 0.77 o 6 0 12 16.50 16.73 0.98 o 7 0 12 27.00 32.46 1.63 o 0 1 12 230.21 222.51 5.56 o 1 1 12 50.04 48.10 0.96 o 2 1 12 1303.63 1254.85 31.89 o 3 1 12 1.14 1.00 0.35 o 4 1 12 19.28 17.71 1.11 o 5 1 12 1.32 1.48 0.41 o 6 1 12 19.10 17.86 0.75 o 7 1 12 37.89 42.17 2.32 o 0 2 12 868.65 879.15 24.18 o 1 2 12 191.60 196.40 5.40 o 2 2 12 11.72 8.25 0.62 o 3 2 12 131.72 110.68 4.95 o 4 2 12 31.33 24.22 1.04 o 5 2 12 0.03 -0.14 0.56 o 6 2 12 6.68 9.31 0.88 o 7 2 12 34.47 37.99 1.43 o 0 3 12 0.37 1.59 0.48 o 1 3 12 161.87 157.05 4.50 o 2 3 12 461.92 425.49 18.83 o 3 3 12 228.81 207.47 8.38 o 4 3 12 101.83 92.13 3.44 o 5 3 12 14.14 15.65 0.87 o 6 3 12 0.24 0.10 0.59 o 7 3 12 30.40 30.02 1.35 o 0 4 12 273.13 269.29 9.92 o 1 4 12 258.40 275.96 18.82 o 2 4 12 105.05 106.18 4.87 o 3 4 12 384.13 355.01 13.17 o 4 4 12 4.34 2.87 0.59 o 5 4 12 10.71 9.81 0.77 o 6 4 12 29.06 28.44 1.36 o 7 4 12 37.50 39.57 1.49 o 0 5 12 274.36 253.85 9.20 o 1 5 12 115.34 104.89 3.04 o 2 5 12 34.48 32.11 0.99 o 3 5 12 200.35 178.63 7.29 o 4 5 12 19.20 21.08 1.04 o 5 5 12 5.22 3.24 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15 5.70 5.19 0.46 o 4 1 15 41.78 47.46 1.93 o 5 1 15 0.73 1.64 0.68 o 6 1 15 12.08 14.35 0.76 o 0 2 15 16.15 14.20 0.80 o 1 2 15 426.41 396.62 10.82 o 2 2 15 15.30 15.73 0.82 o 3 2 15 64.97 60.85 3.51 o 4 2 15 19.48 21.92 1.03 o 5 2 15 25.67 27.08 1.15 o 6 2 15 7.58 9.95 0.96 o 0 3 15 179.66 185.55 7.27 o 1 3 15 130.71 125.87 6.47 o 2 3 15 102.59 98.31 4.82 o 3 3 15 34.35 30.94 1.09 o 4 3 15 15.56 13.22 0.90 o 5 3 15 32.32 34.17 1.60 o 6 3 15 15.22 15.48 1.11 o 0 4 15 280.47 265.13 10.29 o 1 4 15 10.20 9.58 0.62 o 2 4 15 69.76 64.47 2.53 o 3 4 15 1.33 3.46 0.62 o 4 4 15 47.03 50.20 2.10 o 5 4 15 45.44 47.99 2.24 o 6 4 15 0.97 1.55 0.80 o 0 5 15 35.76 35.54 1.49 o 1 5 15 18.92 20.05 0.70 o 2 5 15 48.36 44.08 1.36 o 3 5 15 18.98 18.99 1.36 o 4 5 15 29.10 31.95 1.22 o 5 5 15 21.86 23.23 1.17 o 6 5 15 8.19 8.86 1.01 o 0 6 15 38.28 44.00 2.47 o 1 6 15 0.81 0.54 0.40 o 2 6 15 8.52 9.93 0.82 o 3 6 15 8.76 10.09 0.80 o 4 6 15 18.06 20.83 1.11 o 5 6 15 5.66 8.27 0.95 o 6 6 15 20.87 21.73 1.25 o 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