#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:54:58 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180809 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/40/2014054.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014054_Fobs loop_ _publ_author_name 'Faulmann, Christophe' 'Pullen, Anthony E.' _publ_section_title ; A substituted EDOT precursor: diethyl 3,4-dihydroxythiophene-2,5-dicarboxylate ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o338 _journal_page_last o340 _journal_volume 60 _journal_year 2004 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 99.059 _cell_angle_gamma 90.000 _cell_length_a 8.7337 _cell_length_b 19.8208 _cell_length_c 13.6271 _exptl_crystal_F_000 1088.00 _reflns_d_resolution_high 0.8103 _cod_data_source_file sk1705IIsup2.hkl _cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' Block in P 21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 230.38 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 259.58 234.76 58.05 o 2 0 0 3281.29 3080.43 75.73 o 3 0 0 259.86 242.19 41.02 o 4 0 0 250.21 312.41 93.86 o 5 0 0 4750.81 4492.43 208.04 o 6 0 0 108.92 100.38 28.50 o 7 0 0 4053.62 4190.35 64.79 o 8 0 0 1260.37 1214.67 44.28 o 9 0 0 352.61 347.51 45.31 o 10 0 0 140.89 115.64 40.59 o 1 1 0 5884.97 5247.11 144.60 o 2 1 0 5490.70 5305.86 86.90 o 3 1 0 601.55 611.36 38.33 o 4 1 0 277.35 269.41 29.04 o 5 1 0 63.12 77.61 28.10 o 6 1 0 143.76 168.58 26.01 o 7 1 0 3.59 25.49 28.88 o 8 1 0 32.68 39.63 25.30 o 9 1 0 3.54 16.09 26.68 o 10 1 0 10.62 11.87 34.84 o 1 2 0 1602.02 1603.21 42.11 o 2 2 0 135.97 129.54 30.76 o 3 2 0 905.94 867.09 37.72 o 4 2 0 290.22 334.73 60.89 o 5 2 0 0.88 3.48 27.55 o 6 2 0 21.96 22.04 21.75 o 7 2 0 1783.34 1902.36 33.46 o 8 2 0 1211.43 1203.17 32.14 o 9 2 0 655.02 672.06 31.46 o 10 2 0 65.43 48.78 35.64 o 1 3 0 2879.48 2719.88 39.01 o 2 3 0 527.68 616.20 60.82 o 3 3 0 972.71 898.38 36.29 o 4 3 0 159.14 108.49 30.43 o 5 3 0 426.29 421.76 29.46 o 6 3 0 0.08 18.73 25.70 o 7 3 0 336.66 366.26 28.62 o 8 3 0 17.95 15.15 26.66 o 9 3 0 0.38 -14.24 28.55 o 10 3 0 324.72 346.32 33.75 o 0 4 0 10082.20 9236.13 96.91 o 1 4 0 5774.19 5641.43 48.81 o 2 4 0 7044.05 6784.02 67.89 o 3 4 0 405.56 405.95 31.00 o 4 4 0 228.35 235.47 27.89 o 5 4 0 1751.47 1732.18 35.04 o 6 4 0 227.93 230.69 27.80 o 7 4 0 1713.24 1752.58 39.42 o 8 4 0 27.45 29.40 26.05 o 9 4 0 165.60 153.10 26.80 o 10 4 0 240.05 201.40 41.73 o 1 5 0 849.29 809.54 29.83 o 2 5 0 4057.97 3909.42 50.22 o 3 5 0 2588.85 2425.93 36.73 o 4 5 0 2361.60 2317.67 36.53 o 5 5 0 162.01 197.64 23.29 o 6 5 0 501.11 533.26 29.15 o 7 5 0 582.26 606.11 29.44 o 8 5 0 13.17 14.56 28.47 o 9 5 0 38.52 44.80 30.21 o 10 5 0 360.67 370.77 36.95 o 0 6 0 335.38 274.26 48.98 o 1 6 0 30.01 28.63 25.29 o 2 6 0 267.55 262.53 25.94 o 3 6 0 6041.30 6089.80 83.13 o 4 6 0 2489.76 2612.50 36.82 o 5 6 0 1409.66 1379.58 26.68 o 6 6 0 33.95 54.22 23.24 o 7 6 0 123.30 121.52 25.68 o 8 6 0 12.72 -2.62 29.91 o 9 6 0 19.92 19.82 29.30 o 10 6 0 489.03 454.51 42.55 o 1 7 0 2351.40 2217.28 32.21 o 2 7 0 1307.99 1327.58 28.72 o 3 7 0 2699.45 2603.99 61.74 o 4 7 0 3479.78 3519.39 43.65 o 5 7 0 422.64 380.57 21.10 o 6 7 0 15.10 60.84 28.20 o 7 7 0 19.46 15.15 21.99 o 8 7 0 513.83 532.40 30.11 o 9 7 0 64.62 55.77 31.75 o 10 7 0 451.83 445.09 43.10 o 0 8 0 1642.89 1515.88 48.60 o 1 8 0 0.66 259.17 148.21 o 2 8 0 93.62 39.70 17.85 o 3 8 0 6171.50 6367.09 70.21 o 4 8 0 2686.66 2836.50 40.98 o 5 8 0 1665.46 1602.76 28.05 o 6 8 0 76.95 76.21 21.60 o 7 8 0 89.87 78.39 21.50 o 8 8 0 430.87 412.81 29.91 o 9 8 0 23.67 41.41 29.73 o 10 8 0 69.72 75.79 54.60 o 1 9 0 589.31 554.75 27.78 o 2 9 0 12091.63 12626.81 221.87 o 3 9 0 35.21 27.85 23.57 o 4 9 0 359.95 379.75 21.65 o 5 9 0 553.11 535.57 26.28 o 6 9 0 5.79 -3.74 20.12 o 7 9 0 629.41 669.01 26.66 o 8 9 0 225.71 235.84 30.05 o 9 9 0 453.42 444.65 34.58 o 0 10 0 1731.84 1728.61 56.25 o 1 10 0 422.64 411.01 20.37 o 2 10 0 2196.59 2197.82 33.89 o 3 10 0 2493.92 2468.59 29.01 o 4 10 0 814.27 788.62 24.47 o 5 10 0 37.67 37.10 21.48 o 6 10 0 62.44 44.49 19.99 o 7 10 0 4.97 20.67 28.57 o 8 10 0 144.08 131.83 28.63 o 9 10 0 430.94 430.02 35.65 o 1 11 0 196.89 186.88 17.69 o 2 11 0 1108.34 1091.80 33.97 o 3 11 0 99.98 55.73 22.90 o 4 11 0 487.63 459.53 21.48 o 5 11 0 804.32 826.06 29.14 o 6 11 0 47.25 58.84 21.13 o 7 11 0 173.99 175.04 28.27 o 8 11 0 647.33 607.28 33.21 o 9 11 0 411.21 429.72 34.92 o 0 12 0 89.37 75.62 28.55 o 1 12 0 649.94 695.93 19.82 o 2 12 0 576.06 573.43 22.71 o 3 12 0 475.09 483.65 21.57 o 4 12 0 263.86 246.24 26.98 o 5 12 0 1123.24 1115.91 33.00 o 6 12 0 312.08 297.24 21.79 o 7 12 0 24.71 22.50 26.34 o 8 12 0 7.47 21.84 38.61 o 9 12 0 226.74 219.59 41.28 o 1 13 0 173.18 204.06 21.49 o 2 13 0 0.60 14.07 19.44 o 3 13 0 756.34 720.87 24.09 o 4 13 0 334.73 348.77 26.09 o 5 13 0 1938.95 1967.49 45.35 o 6 13 0 507.74 539.16 31.11 o 7 13 0 63.51 91.45 28.81 o 8 13 0 0.40 -0.40 35.44 o 0 14 0 1291.53 1271.74 54.23 o 1 14 0 685.68 694.58 18.72 o 2 14 0 817.29 797.63 25.00 o 3 14 0 825.58 756.91 22.77 o 4 14 0 1282.35 1242.32 31.58 o 5 14 0 0.05 -13.08 26.67 o 6 14 0 2236.52 2291.28 51.02 o 7 14 0 103.19 92.31 27.18 o 8 14 0 1.86 9.57 36.63 o 1 15 0 380.56 365.21 20.76 o 2 15 0 7.27 -5.24 23.08 o 3 15 0 582.90 578.48 24.43 o 4 15 0 137.94 141.72 24.26 o 5 15 0 8.08 32.00 29.05 o 6 15 0 306.61 305.31 30.85 o 7 15 0 133.94 96.33 33.85 o 8 15 0 523.71 529.11 37.79 o 0 16 0 269.71 273.63 30.18 o 1 16 0 398.13 457.94 20.40 o 2 16 0 2529.05 2427.23 41.28 o 3 16 0 646.16 670.40 22.29 o 4 16 0 1.18 4.22 23.93 o 5 16 0 35.87 53.78 23.35 o 6 16 0 39.57 45.74 23.67 o 7 16 0 14.08 -0.23 28.33 o 1 17 0 9519.35 9397.00 104.64 o 2 17 0 60.33 48.67 21.30 o 3 17 0 1.60 1.41 18.36 o 4 17 0 9.06 -2.99 24.89 o 5 17 0 24.63 55.53 22.95 o 6 17 0 385.97 340.02 28.50 o 7 17 0 21.83 37.10 26.61 o 0 18 0 537.62 607.08 40.50 o 1 18 0 121.21 99.25 24.36 o 2 18 0 273.32 274.73 21.77 o 3 18 0 140.50 159.44 22.10 o 4 18 0 211.07 188.99 24.93 o 5 18 0 177.65 175.00 25.32 o 6 18 0 30.46 46.04 27.90 o 7 18 0 850.22 830.57 32.24 o 1 19 0 456.64 461.35 25.12 o 2 19 0 846.18 880.40 26.48 o 3 19 0 180.31 156.71 22.51 o 4 19 0 596.65 587.58 24.69 o 5 19 0 176.83 168.55 29.08 o 6 19 0 1005.51 942.13 27.95 o 0 20 0 821.41 853.03 33.44 o 1 20 0 36.48 23.53 22.85 o 2 20 0 1.67 24.32 25.66 o 3 20 0 356.84 347.95 27.47 o 4 20 0 172.84 146.88 27.45 o 5 20 0 1.32 -11.16 26.36 o 6 20 0 0.02 94.13 36.30 o 1 21 0 124.28 171.60 24.33 o 2 21 0 60.50 80.76 22.58 o 3 21 0 57.36 49.05 27.97 o 4 21 0 15.86 32.20 29.77 o 5 21 0 11.63 4.04 27.53 o 0 22 0 765.71 753.69 53.38 o 1 22 0 205.74 202.57 25.52 o 2 22 0 476.36 481.37 25.88 o 3 22 0 0.77 -11.80 25.90 o 4 22 0 263.97 238.43 33.11 o 1 23 0 310.46 318.50 23.14 o 2 23 0 247.73 233.10 26.00 o 3 23 0 107.54 92.28 30.58 o 0 24 0 47.06 19.02 35.40 o 1 24 0 3.54 -12.06 26.98 o -10 1 1 156.78 148.84 37.66 o -9 1 1 216.62 243.39 32.41 o -8 1 1 1680.99 1699.77 34.66 o -7 1 1 274.53 284.18 28.07 o -6 1 1 26.74 29.30 21.44 o -5 1 1 1313.03 1254.45 35.92 o -4 1 1 2244.04 1950.07 42.99 o -3 1 1 764.59 768.39 44.01 o -2 1 1 9053.74 8091.67 172.39 o -1 1 1 5406.61 5162.61 274.55 o 1 1 1 1429.86 1362.79 39.66 o 2 1 1 103.48 82.08 27.06 o 3 1 1 477.16 472.89 29.36 o 4 1 1 534.29 651.48 34.20 o 5 1 1 70.59 82.81 24.16 o 6 1 1 2199.27 2206.96 53.79 o 7 1 1 239.80 244.10 22.62 o 8 1 1 74.28 74.73 26.94 o 9 1 1 4.65 19.77 29.91 o 10 1 1 563.77 570.32 38.43 o -10 2 1 80.26 107.16 37.16 o -9 2 1 21.31 23.43 26.71 o -8 2 1 308.83 326.82 28.26 o -7 2 1 327.42 327.36 29.59 o -6 2 1 1135.32 1117.36 31.86 o -5 2 1 226.73 248.09 26.79 o -4 2 1 3657.75 3403.30 49.90 o -3 2 1 155.09 166.29 33.41 o -2 2 1 4213.70 3982.86 198.29 o -1 2 1 12829.07 13057.12 573.09 o 0 2 1 5191.90 5014.94 74.36 o 1 2 1 2612.70 2620.90 45.38 o 2 2 1 1254.86 1377.23 69.27 o 3 2 1 3178.89 3443.74 48.12 o 4 2 1 1377.98 1437.66 30.47 o 5 2 1 896.48 962.82 26.31 o 6 2 1 2777.85 2858.05 37.38 o 7 2 1 114.26 110.56 25.13 o 8 2 1 212.45 198.07 28.65 o 9 2 1 29.41 40.02 27.77 o 10 2 1 89.26 63.28 36.69 o -10 3 1 87.33 71.74 39.35 o -9 3 1 122.84 127.36 29.24 o -8 3 1 1650.69 1675.26 35.89 o -7 3 1 461.07 470.97 29.01 o -6 3 1 279.42 281.81 26.69 o -5 3 1 3350.91 3390.94 71.58 o -4 3 1 6887.36 6574.30 144.63 o -3 3 1 2706.04 2632.77 81.67 o -2 3 1 11751.31 11141.49 330.09 o -1 3 1 2664.78 2540.94 68.64 o 0 3 1 2476.72 2416.08 34.73 o 1 3 1 315.19 315.59 29.72 o 2 3 1 2236.45 2330.50 45.02 o 3 3 1 3461.04 3518.17 46.43 o 4 3 1 4098.72 4045.90 60.52 o 5 3 1 720.05 716.08 28.07 o 6 3 1 2481.84 2459.17 35.53 o 7 3 1 2095.00 2159.78 54.81 o 8 3 1 7.48 9.57 25.61 o 9 3 1 170.64 180.14 32.71 o 10 3 1 371.82 318.06 34.84 o -10 4 1 54.18 54.48 33.32 o -9 4 1 43.20 32.74 28.43 o -8 4 1 594.93 625.97 33.54 o -7 4 1 164.38 160.55 28.14 o -6 4 1 152.58 166.59 23.48 o -5 4 1 2616.29 2709.94 42.96 o -4 4 1 373.84 357.47 27.90 o -3 4 1 974.95 928.28 35.04 o -2 4 1 0.01 2.35 33.87 o -1 4 1 280.08 281.33 29.11 o 0 4 1 1356.93 1266.58 27.30 o 1 4 1 1635.28 1638.64 54.26 o 2 4 1 386.24 436.09 38.64 o 3 4 1 230.28 223.98 23.03 o 4 4 1 5.97 6.05 23.33 o 5 4 1 796.62 841.17 30.60 o 6 4 1 0.05 21.15 27.83 o 7 4 1 311.03 298.53 25.68 o 8 4 1 14.46 19.78 28.84 o 9 4 1 142.18 154.10 28.64 o 10 4 1 265.08 238.70 34.52 o -10 5 1 3.34 24.63 43.06 o -9 5 1 192.26 187.56 34.36 o -8 5 1 650.81 644.43 30.12 o -7 5 1 41.65 57.92 20.59 o -6 5 1 436.42 455.85 28.56 o -5 5 1 184.97 189.06 22.80 o -4 5 1 242.59 252.04 30.72 o -3 5 1 1167.84 1117.36 32.45 o -2 5 1 3586.35 3583.57 128.89 o -1 5 1 12818.75 12983.18 138.70 o 0 5 1 7.32 2227.03 918.53 o 1 5 1 26.73 42.26 25.83 o 2 5 1 32.13 59.13 26.74 o 3 5 1 3506.05 3507.68 41.08 o 4 5 1 1248.46 1183.59 31.00 o 5 5 1 2187.57 2196.57 33.45 o 6 5 1 98.88 79.56 30.25 o 7 5 1 1.37 -2.92 23.57 o 8 5 1 100.60 80.73 28.68 o 9 5 1 12.77 5.01 33.24 o 10 5 1 407.75 396.56 39.99 o -10 6 1 231.85 205.03 47.47 o -9 6 1 129.36 104.13 32.21 o -8 6 1 171.80 194.01 32.36 o -7 6 1 10.17 11.51 22.10 o -6 6 1 27.05 2.14 26.51 o -5 6 1 257.05 278.92 26.13 o -4 6 1 2043.36 1817.39 64.88 o -3 6 1 939.64 975.69 28.64 o -2 6 1 138.58 94.55 27.04 o -1 6 1 3752.71 3668.93 38.24 o 0 6 1 329.10 221.52 25.74 o 1 6 1 5.93 2.14 23.94 o 2 6 1 1283.12 1177.15 29.54 o 3 6 1 2456.78 2162.06 45.77 o 4 6 1 0.10 25.35 21.48 o 5 6 1 82.92 92.23 22.59 o 6 6 1 679.67 812.27 67.16 o 7 6 1 23.29 3.41 24.59 o 8 6 1 14.81 31.73 28.14 o 9 6 1 78.05 100.16 36.65 o 10 6 1 57.49 39.67 33.88 o -10 7 1 101.46 78.82 61.83 o -9 7 1 539.53 542.43 56.69 o -8 7 1 392.33 392.58 31.56 o -7 7 1 773.13 796.07 28.43 o -6 7 1 564.76 586.98 26.88 o -5 7 1 152.76 123.19 23.21 o -4 7 1 15.45 7.44 22.60 o -3 7 1 3637.57 3556.49 43.42 o -2 7 1 32.12 29.95 25.21 o -1 7 1 4861.92 4729.12 101.67 o 0 7 1 93.71 140.05 27.09 o 1 7 1 61.20 58.95 20.89 o 2 7 1 117.20 272.93 96.57 o 3 7 1 3746.40 3773.84 50.12 o 4 7 1 0.56 -0.52 24.98 o 5 7 1 61.05 81.21 23.41 o 6 7 1 125.56 119.74 22.82 o 7 7 1 0.59 -3.98 22.89 o 8 7 1 3.89 2.25 24.07 o 9 7 1 447.76 470.69 33.97 o 10 7 1 111.89 121.31 43.83 o -10 8 1 2.20 38.17 47.26 o -9 8 1 18.80 -17.01 36.77 o -8 8 1 492.56 530.52 33.25 o -7 8 1 42.22 26.98 22.41 o -6 8 1 1417.32 1389.87 36.99 o -5 8 1 37.03 49.98 20.55 o -4 8 1 2.53 4.02 18.63 o -3 8 1 1114.84 1024.91 26.99 o -2 8 1 76.68 89.67 20.46 o -1 8 1 382.82 459.15 32.98 o 0 8 1 1026.28 929.10 36.88 o 1 8 1 3182.53 3303.17 74.14 o 2 8 1 137.12 111.58 22.03 o 3 8 1 564.40 587.98 26.07 o 4 8 1 783.97 803.35 30.39 o 5 8 1 109.21 94.08 20.87 o 6 8 1 35.47 39.91 24.04 o 7 8 1 41.57 46.34 20.18 o 8 8 1 1078.92 1078.22 32.49 o 9 8 1 91.65 77.06 29.19 o -9 9 1 10.50 40.37 43.79 o -8 9 1 21.44 20.01 29.83 o -7 9 1 456.77 449.53 29.18 o -6 9 1 128.93 130.69 23.89 o -5 9 1 16.42 14.12 25.98 o -4 9 1 2.04 25.27 28.43 o -3 9 1 1105.93 1101.44 26.95 o -2 9 1 2.51 1.34 19.28 o -1 9 1 733.58 749.11 36.00 o 0 9 1 1955.00 2073.39 34.95 o 1 9 1 495.10 491.35 19.40 o 2 9 1 131.28 160.25 22.09 o 3 9 1 559.61 492.52 21.97 o 4 9 1 6.35 14.49 17.43 o 5 9 1 295.71 304.14 22.56 o 6 9 1 21.06 4.42 22.72 o 7 9 1 3.70 2.76 22.74 o 8 9 1 224.27 210.18 26.65 o 9 9 1 294.24 321.09 29.75 o -9 10 1 256.61 233.02 39.42 o -8 10 1 147.22 137.03 29.39 o -7 10 1 1146.31 1173.67 36.17 o -6 10 1 4264.91 4292.70 82.76 o -5 10 1 20.47 41.76 29.40 o -4 10 1 51.06 67.82 22.35 o -3 10 1 340.03 308.57 22.56 o -2 10 1 3.54 1.93 19.87 o -1 10 1 2777.00 2951.83 28.63 o 0 10 1 242.57 259.48 25.44 o 1 10 1 29947.79 31428.38 469.67 o 2 10 1 1452.91 1461.27 28.00 o 3 10 1 1757.19 1831.57 39.72 o 4 10 1 15.20 4.38 20.94 o 5 10 1 513.88 561.17 28.53 o 6 10 1 1.18 1.55 20.76 o 7 10 1 11.16 -3.48 27.92 o 8 10 1 1887.98 1949.69 34.70 o 9 10 1 433.15 432.75 33.64 o -9 11 1 35.95 36.77 31.16 o -8 11 1 200.47 203.73 31.86 o -7 11 1 8.79 -0.71 27.37 o -6 11 1 795.46 740.77 30.21 o -5 11 1 45.61 59.37 33.96 o -4 11 1 296.11 325.04 23.27 o -3 11 1 357.68 360.55 21.15 o -2 11 1 202.50 210.66 21.42 o -1 11 1 15.01 35.95 17.56 o 0 11 1 5220.99 5381.87 79.59 o 1 11 1 296.08 317.37 23.69 o 2 11 1 3840.66 3850.73 77.13 o 3 11 1 7.29 1.15 19.09 o 4 11 1 6.72 -14.81 21.68 o 5 11 1 49.37 57.13 22.60 o 6 11 1 346.94 377.92 22.63 o 7 11 1 196.56 236.00 26.68 o 8 11 1 23.20 37.39 27.63 o 9 11 1 1.88 -5.96 30.12 o -9 12 1 1.14 -5.27 40.84 o -8 12 1 242.39 239.71 38.83 o -7 12 1 1965.40 1977.92 49.58 o -6 12 1 2522.81 2536.90 64.35 o -5 12 1 23.75 28.02 25.68 o -4 12 1 412.27 372.91 22.04 o -3 12 1 1385.43 1329.12 23.20 o -2 12 1 214.17 207.37 22.37 o -1 12 1 2129.31 2033.06 50.87 o 0 12 1 286.89 235.20 16.87 o 1 12 1 1827.41 1648.77 24.16 o 2 12 1 94.54 63.51 17.41 o 3 12 1 925.78 888.24 24.48 o 4 12 1 90.46 117.69 23.35 o 5 12 1 554.22 544.61 25.68 o 6 12 1 10.70 13.22 24.70 o 7 12 1 71.10 69.26 24.50 o 8 12 1 405.92 423.27 29.81 o 9 12 1 804.10 793.58 38.61 o -8 13 1 518.56 551.14 37.97 o -7 13 1 3.39 -3.10 23.44 o -6 13 1 1611.52 1597.06 45.20 o -5 13 1 931.32 941.05 24.54 o -4 13 1 95.52 93.39 21.44 o -3 13 1 39.83 51.75 18.98 o -2 13 1 15.80 27.70 15.51 o -1 13 1 5.80 3.61 17.81 o 0 13 1 2723.99 2728.14 27.25 o 1 13 1 9.84 51.51 17.36 o 2 13 1 1340.64 1226.35 34.74 o 3 13 1 9.10 -8.46 31.35 o 4 13 1 61.55 68.91 20.92 o 5 13 1 124.15 121.34 23.92 o 6 13 1 110.21 87.56 27.52 o 7 13 1 355.81 377.03 25.83 o 8 13 1 1170.08 1148.87 35.71 o -8 14 1 208.01 155.80 29.82 o -7 14 1 0.28 1.85 24.03 o -6 14 1 69.67 52.44 26.39 o -5 14 1 125.35 153.67 20.13 o -4 14 1 2307.92 2208.97 56.78 o -3 14 1 1955.25 1969.81 30.67 o -2 14 1 2.50 0.30 21.27 o -1 14 1 21.87 34.74 19.51 o 0 14 1 0.56 -1.11 18.07 o 1 14 1 1411.55 1242.18 36.07 o 2 14 1 0.54 9.36 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