#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:54:58 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180809 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/40/2014087.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014087_Fobs loop_ _publ_author_name 'Peng, Yang' 'Li, Yi-Zhi' 'Bao, Song-Song' 'Zheng, Li-Min' _publ_section_title ; Bis[tris(ethylenediamine)cobalt(III)] dichlorobis[\m-(1-hydroxyethylidene)diphosphonato(4--)]diruthenium(II,III)(Ru{--Ru}) chloride trihydrate ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m302 _journal_page_last m304 _journal_volume 60 _journal_year 2004 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 90.788 _cell_angle_beta 91.362 _cell_angle_gamma 96.273 _cell_length_a 10.5166 _cell_length_b 15.2973 _cell_length_c 15.4972 _exptl_crystal_F_000 1262.00 _reflns_d_resolution_high 0.8410 _cod_data_source_file av1174Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title AV1174 _shelx_refln_list_code 4 _shelx_f_calc_maximum 366.03 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 13098.43 13501.69 58.76 o 3 0 0 3235.28 3266.68 54.97 o 4 0 0 425.74 376.10 21.84 o 5 0 0 146.06 143.29 29.28 o 6 0 0 2223.55 2095.28 117.51 o 7 0 0 2.95 7.58 33.01 o 8 0 0 60.28 67.01 23.20 o 9 0 0 1072.36 1036.89 69.65 o 10 0 0 3.16 1.61 28.75 o 11 0 0 1.22 0.95 51.18 o 12 0 0 472.24 507.01 71.08 o -12 1 0 193.21 171.53 59.70 o -11 1 0 764.99 929.68 53.07 o -10 1 0 1500.56 1638.39 137.89 o -9 1 0 151.05 143.56 26.46 o -8 1 0 1.42 12.18 32.43 o -7 1 0 2455.12 2139.47 67.76 o -6 1 0 430.57 453.47 38.24 o -5 1 0 20775.57 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