#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/40/2014098.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014098_Fobs loop_ _publ_author_name 'Naumov, Dmitry Yu.' 'Naumova, Marina I.' 'Podberezskaya, Nina V.' 'Kuratieva, Natalia V.' _publ_section_title ; Lithium and beryllium hypophosphites ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first i73 _journal_page_last i75 _journal_volume 60 _journal_year 2004 _space_group_IT_number 92 _symmetry_space_group_name_Hall 'P 4abw 2nw' _symmetry_space_group_name_H-M 'P 41 21 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 5.0117 _cell_length_b 5.0117 _cell_length_c 20.0511 _exptl_crystal_F_000 280.00 _reflns_d_resolution_high 0.7120 _[local]_cod_data_source_file bc1045IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' Be(H2PO2)2 in P4(1)2(1)2, CAD4' _shelx_refln_list_code 4 _shelx_f_calc_maximum 121.41 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' '-y+1/2, x+1/2, z+1/4' 'y+1/2, -x+1/2, z+3/4' '-x+1/2, y+1/2, -z+1/4' 'x+1/2, -y+1/2, -z+3/4' 'y, x, -z' '-y, -x, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 0 6085.28 5844.82 47.34 o 0 2 0 4338.29 4290.26 14.67 o 1 2 0 16.43 16.10 0.86 o 2 2 0 4.34 0.55 1.14 o 1 3 0 621.82 645.49 5.95 o 2 3 0 6.32 7.83 1.20 o 3 3 0 32.49 33.49 3.15 o 0 4 0 1675.77 1664.44 32.85 o 1 4 0 0.49 0.61 0.92 o 2 4 0 246.07 269.41 5.97 o 3 4 0 20.94 18.29 2.04 o 4 4 0 0.80 0.00 2.23 o 1 5 0 31.69 30.19 2.01 o 2 5 0 0.22 -0.23 1.09 o 3 5 0 24.06 21.59 2.46 o 4 5 0 3.21 4.16 1.67 o 0 6 0 46.39 37.55 2.97 o 1 6 0 13.59 14.61 1.79 o 2 6 0 3.62 7.26 1.91 o 3 6 0 13.46 13.46 3.44 o 0 1 1 6.24 6.22 0.31 o 1 1 1 681.62 683.03 8.82 o -1 2 1 359.76 375.52 3.72 o 0 2 1 7.17 6.19 0.57 o 1 2 1 359.89 372.80 6.46 o 2 2 1 1437.37 1376.36 36.88 o -2 3 1 222.15 201.43 5.18 o -1 3 1 718.02 710.37 13.51 o 0 3 1 0.00 -0.13 0.48 o 1 3 1 717.90 758.09 14.29 o 2 3 1 222.22 212.68 3.76 o 3 3 1 595.50 612.57 6.98 o -3 4 1 13.30 14.14 1.87 o -2 4 1 661.21 678.73 9.34 o -1 4 1 72.85 72.08 2.49 o 0 4 1 288.56 279.59 3.98 o 1 4 1 72.73 69.13 2.12 o 2 4 1 662.19 649.66 16.32 o 3 4 1 13.24 14.17 1.50 o 4 4 1 118.78 114.63 3.76 o -4 5 1 5.26 4.41 3.19 o -3 5 1 135.44 137.94 5.39 o -2 5 1 17.19 15.73 2.10 o -1 5 1 136.95 136.96 3.86 o 0 5 1 29.50 22.00 3.74 o 1 5 1 136.99 118.93 15.73 o 2 5 1 17.20 15.62 1.70 o 3 5 1 135.45 113.30 18.98 o 4 5 1 5.25 7.00 1.53 o -3 6 1 17.08 19.03 3.74 o -2 6 1 70.27 51.05 23.49 o -1 6 1 15.76 16.02 1.87 o 0 6 1 2.56 1.05 1.14 o 1 6 1 15.82 16.52 1.66 o 2 6 1 70.22 78.43 3.50 o 3 6 1 17.13 20.21 2.69 o 0 7 1 5.51 3.43 3.86 o 0 1 2 1959.75 2104.76 63.20 o 1 1 2 8.09 6.84 0.55 o -1 2 2 172.54 209.51 4.91 o 0 2 2 434.71 513.75 8.53 o 1 2 2 172.69 216.50 2.88 o 2 2 2 103.49 89.22 5.97 o -2 3 2 85.32 76.61 4.14 o -1 3 2 252.23 265.26 6.64 o 0 3 2 26.70 31.51 1.71 o 1 3 2 252.23 246.22 6.85 o 2 3 2 85.39 84.57 6.43 o 3 3 2 20.42 17.91 1.84 o -3 4 2 102.48 95.32 5.54 o -2 4 2 272.45 264.12 8.30 o -1 4 2 708.54 771.07 13.29 o 0 4 2 583.23 594.65 8.08 o 1 4 2 708.23 700.91 11.70 o 2 4 2 272.60 266.78 9.23 o 3 4 2 102.33 95.55 3.92 o 4 4 2 4.88 5.78 1.61 o -4 5 2 2.16 3.30 2.25 o -3 5 2 24.29 24.05 3.56 o -2 5 2 65.93 58.29 4.69 o -1 5 2 227.91 230.08 8.80 o 0 5 2 156.62 173.05 15.45 o 1 5 2 227.98 248.67 5.10 o 2 5 2 65.95 53.60 3.30 o 3 5 2 24.27 24.70 2.54 o 4 5 2 2.19 3.13 1.65 o -2 6 2 73.49 68.95 5.97 o -1 6 2 108.81 105.77 7.03 o 0 6 2 141.72 160.92 5.71 o 1 6 2 108.81 109.45 4.04 o 2 6 2 73.35 70.33 4.04 o 3 6 2 39.67 43.27 3.55 o 0 7 2 26.73 33.22 4.72 o 0 1 3 390.97 423.07 8.60 o 1 1 3 133.95 166.76 3.51 o -1 2 3 1298.83 1165.26 11.70 o 0 2 3 579.29 607.13 14.28 o 1 2 3 1300.41 1250.69 22.90 o 2 2 3 731.41 754.99 15.70 o -2 3 3 816.53 856.71 12.96 o -1 3 3 129.65 137.41 4.87 o 0 3 3 12.10 14.02 1.31 o 1 3 3 129.53 135.00 2.85 o 2 3 3 816.22 836.03 34.28 o 3 3 3 149.50 154.74 7.35 o -3 4 3 161.49 177.09 7.36 o -2 4 3 68.18 62.52 4.50 o -1 4 3 289.88 280.46 8.34 o 0 4 3 61.12 56.32 3.96 o 1 4 3 289.84 306.47 4.98 o 2 4 3 68.42 65.42 3.18 o 3 4 3 161.19 168.99 5.32 o 4 4 3 18.04 24.59 2.48 o -4 5 3 42.73 43.89 4.93 o -3 5 3 45.53 51.54 4.81 o -2 5 3 190.99 197.16 8.28 o -1 5 3 11.65 10.50 2.54 o 0 5 3 33.39 36.50 3.37 o 1 5 3 11.68 10.51 1.46 o 2 5 3 190.80 190.25 5.80 o 3 5 3 45.58 51.84 3.48 o 4 5 3 42.79 44.21 4.06 o -2 6 3 43.51 39.94 5.09 o -1 6 3 41.46 40.50 4.66 o 0 6 3 29.00 33.30 2.92 o 1 6 3 41.49 44.94 2.73 o 2 6 3 43.38 31.76 16.31 o 3 6 3 51.40 56.00 3.95 o 0 0 4 683.00 754.80 5.88 o 0 1 4 14741.13 14242.33 478.95 o 1 1 4 557.64 569.23 7.98 o -1 2 4 397.19 342.62 6.48 o 0 2 4 151.09 179.71 3.41 o 1 2 4 397.36 337.26 3.74 o 2 2 4 376.44 366.27 5.37 o -2 3 4 146.01 144.40 5.59 o -1 3 4 332.59 360.47 8.05 o 0 3 4 1955.68 2129.75 120.39 o 1 3 4 332.54 333.66 6.99 o 2 3 4 146.18 149.56 3.96 o 3 3 4 125.16 110.64 3.82 o -3 4 4 20.28 19.05 3.05 o -2 4 4 23.19 24.28 2.79 o -1 4 4 499.82 495.68 11.03 o 0 4 4 15.32 13.68 1.65 o 1 4 4 499.96 468.92 10.82 o 2 4 4 23.27 22.22 3.11 o 3 4 4 20.28 20.82 2.09 o 4 4 4 9.81 9.23 1.71 o -4 5 4 41.22 44.54 5.14 o -3 5 4 3.22 2.53 2.21 o -2 5 4 1.19 3.53 2.28 o -1 5 4 9.86 10.07 2.27 o 0 5 4 91.06 80.52 3.72 o 1 5 4 9.86 11.09 1.42 o 2 5 4 1.20 1.19 1.65 o 3 5 4 3.24 1.95 1.66 o 4 5 4 41.25 46.60 3.52 o -2 6 4 12.83 13.72 3.20 o -1 6 4 6.05 5.74 2.54 o 0 6 4 0.04 0.86 1.22 o 1 6 4 6.05 7.33 1.51 o 2 6 4 12.79 14.05 2.36 o 3 6 4 8.30 7.40 2.10 o 0 1 5 19.32 21.61 1.04 o 1 1 5 394.49 418.67 9.16 o -1 2 5 437.52 428.27 7.49 o 0 2 5 50.97 47.15 3.60 o 1 2 5 436.81 422.04 4.28 o 2 2 5 217.85 202.46 4.07 o -2 3 5 857.61 876.95 13.43 o -1 3 5 27.94 26.11 2.53 o 0 3 5 298.70 330.17 8.49 o 1 3 5 27.93 26.05 1.75 o 2 3 5 858.41 850.00 16.53 o 3 3 5 45.30 46.44 2.53 o -3 4 5 302.50 286.73 9.56 o -2 4 5 1.94 2.28 1.73 o -1 4 5 584.79 567.62 11.87 o 0 4 5 216.91 205.13 4.95 o 1 4 5 585.26 564.31 6.82 o 2 4 5 1.92 2.55 1.24 o 3 4 5 302.79 302.95 9.76 o 4 4 5 9.16 8.42 1.77 o -4 5 5 75.07 64.75 6.08 o -3 5 5 5.97 5.55 2.54 o -2 5 5 183.80 188.20 8.36 o -1 5 5 33.37 33.54 3.60 o 0 5 5 33.90 33.63 2.53 o 1 5 5 33.33 31.66 2.07 o 2 5 5 183.93 194.76 5.93 o 3 5 5 5.97 7.31 1.75 o 4 5 5 74.99 76.90 4.34 o -2 6 5 4.15 4.79 2.30 o -1 6 5 30.20 34.09 4.07 o 0 6 5 5.02 -0.34 4.21 o 1 6 5 30.07 32.78 2.44 o 2 6 5 4.18 4.86 1.73 o 3 6 5 66.56 73.78 4.41 o 0 1 6 27.68 29.15 1.00 o 1 1 6 8.32 7.59 0.68 o -1 2 6 22.15 23.24 2.02 o 0 2 6 1311.94 1528.10 27.95 o 1 2 6 22.01 22.67 1.16 o 2 2 6 21.06 25.56 1.68 o -2 3 6 314.32 312.92 8.34 o -1 3 6 45.40 45.92 3.06 o 0 3 6 859.42 848.85 12.14 o 1 3 6 45.35 48.73 1.82 o 2 3 6 314.27 317.36 14.57 o 3 3 6 63.27 58.50 2.99 o -3 4 6 1.89 2.34 2.06 o -2 4 6 188.80 170.59 7.08 o -1 4 6 300.29 303.86 9.01 o 0 4 6 304.43 298.04 6.08 o 1 4 6 300.54 278.92 5.75 o 2 4 6 188.67 158.25 4.84 o 3 4 6 1.93 1.59 1.53 o 4 4 6 11.95 10.98 1.94 o -4 5 6 6.10 5.83 2.75 o -3 5 6 19.53 17.17 3.37 o -2 5 6 124.50 123.21 7.18 o -1 5 6 89.97 90.29 5.68 o 0 5 6 312.34 293.61 6.98 o 1 5 6 89.88 84.62 3.17 o 2 5 6 124.47 123.53 4.94 o 3 5 6 19.54 19.26 2.27 o 4 5 6 6.13 1.81 4.01 o -2 6 6 16.71 18.08 3.46 o -1 6 6 98.75 101.54 6.92 o 0 6 6 28.91 35.86 3.06 o 1 6 6 98.67 87.26 16.34 o 2 6 6 16.74 15.80 2.42 o 3 6 6 20.34 19.97 2.78 o 0 1 7 4.29 3.67 0.53 o 1 1 7 1607.55 1633.07 15.56 o -1 2 7 385.64 353.95 7.31 o 0 2 7 110.07 102.62 2.75 o 1 2 7 384.99 376.68 7.47 o 2 2 7 1291.64 1247.91 28.40 o -2 3 7 274.43 270.42 7.90 o -1 3 7 315.49 305.51 7.75 o 0 3 7 358.96 367.71 5.86 o 1 3 7 316.19 287.67 4.66 o 2 3 7 274.34 289.67 5.67 o 3 3 7 151.76 141.32 4.48 o -3 4 7 126.12 122.28 6.60 o -2 4 7 211.36 215.90 7.98 o -1 4 7 14.52 18.01 2.58 o 0 4 7 13.15 5.04 4.17 o 1 4 7 14.60 16.65 1.49 o 2 4 7 211.07 209.89 8.40 o 3 4 7 126.36 130.47 4.85 o 4 4 7 20.34 19.07 2.34 o -4 5 7 45.34 47.50 5.40 o -3 5 7 53.79 52.58 4.97 o -2 5 7 65.97 69.53 5.33 o -1 5 7 102.39 99.36 6.16 o 0 5 7 5.52 8.85 1.75 o 1 5 7 102.40 99.76 3.51 o 2 5 7 66.06 73.18 5.62 o 3 5 7 53.77 53.11 4.74 o 4 5 7 45.36 52.98 3.86 o -1 6 7 27.92 29.54 4.33 o 0 6 7 18.45 20.51 2.58 o 1 6 7 27.85 30.03 2.44 o 2 6 7 61.21 57.67 3.93 o 3 6 7 33.75 37.79 3.42 o 0 0 8 9275.74 9582.43 31.39 o 0 1 8 48.74 31.41 1.17 o 1 1 8 2127.95 2113.56 42.21 o -1 2 8 865.47 911.90 11.84 o 0 2 8 868.18 874.26 18.41 o 1 2 8 865.11 881.81 12.18 o 2 2 8 17.77 13.89 1.49 o -2 3 8 232.54 216.66 7.16 o -1 3 8 832.55 821.60 12.97 o 0 3 8 201.77 219.85 4.66 o 1 3 8 832.78 847.03 7.63 o 2 3 8 232.56 219.78 5.04 o 3 3 8 207.02 184.90 5.18 o -3 4 8 10.51 9.27 2.60 o -2 4 8 34.60 30.48 3.72 o -1 4 8 13.99 17.63 2.58 o 0 4 8 271.85 281.39 6.10 o 1 4 8 13.93 15.58 1.44 o 2 4 8 34.71 34.08 2.56 o 3 4 8 10.55 10.57 1.77 o 4 4 8 29.28 32.30 2.95 o -4 5 8 2.09 1.87 2.35 o -3 5 8 4.91 3.41 2.47 o -2 5 8 0.24 2.08 1.82 o -1 5 8 15.73 19.52 3.11 o 0 5 8 2.92 5.51 1.57 o 1 5 8 15.75 18.45 1.79 o 2 5 8 0.24 0.80 1.46 o 3 5 8 4.91 3.51 2.59 o 4 5 8 2.08 0.28 1.98 o -1 6 8 17.80 18.08 3.55 o 0 6 8 0.35 0.45 1.74 o 1 6 8 17.78 19.04 2.06 o 2 6 8 4.73 0.80 1.77 o 3 6 8 4.05 4.02 2.05 o 0 1 9 807.06 883.88 18.17 o 1 1 9 339.84 329.57 8.57 o -1 2 9 106.98 115.67 4.57 o 0 2 9 66.40 69.29 2.43 o 1 2 9 106.87 107.20 5.00 o 2 2 9 437.60 445.18 8.81 o -2 3 9 60.15 50.40 3.89 o -1 3 9 350.71 352.94 8.81 o 0 3 9 25.85 32.47 2.07 o 1 3 9 350.67 353.38 5.12 o 2 3 9 60.07 50.65 2.64 o 3 3 9 238.89 237.69 6.38 o -3 4 9 9.67 12.13 2.73 o -2 4 9 323.94 318.67 9.93 o -1 4 9 74.59 82.20 4.92 o 0 4 9 246.61 237.71 5.74 o 1 4 9 74.44 81.80 3.51 o 2 4 9 324.31 328.83 12.43 o 3 4 9 9.66 11.71 1.85 o 4 4 9 102.47 97.07 4.64 o -4 5 9 9.65 8.88 3.03 o -3 5 9 100.24 96.59 7.13 o -2 5 9 12.19 14.36 2.96 o -1 5 9 76.00 88.29 6.01 o 0 5 9 106.41 116.39 4.62 o 1 5 9 75.99 87.66 3.63 o 2 5 9 12.17 6.62 7.60 o 3 5 9 100.16 100.59 4.86 o 4 5 9 9.65 10.43 2.29 o -1 6 9 10.52 11.66 3.06 o 0 6 9 10.17 10.33 2.13 o 1 6 9 10.52 12.29 1.89 o 2 6 9 51.56 57.48 3.98 o 0 1 10 78.63 91.13 2.53 o 1 1 10 1.18 0.04 0.58 o -1 2 10 147.17 155.21 5.28 o 0 2 10 226.78 235.52 4.73 o 1 2 10 147.23 149.92 4.50 o 2 2 10 20.48 19.02 1.68 o -2 3 10 129.52 128.22 5.70 o -1 3 10 422.22 379.82 9.44 o 0 3 10 68.11 69.57 2.93 o 1 3 10 422.30 395.78 5.44 o 2 3 10 129.39 136.65 8.37 o 3 3 10 4.36 3.05 1.42 o -3 4 10 39.47 36.71 4.15 o -2 4 10 112.61 127.33 6.65 o -1 4 10 51.03 47.42 3.98 o 0 4 10 355.84 334.46 18.39 o 1 4 10 50.96 46.62 2.31 o 2 4 10 112.67 112.43 4.46 o 3 4 10 39.54 41.03 2.97 o 4 4 10 10.33 12.21 2.24 o -4 5 10 7.22 7.68 2.91 o -3 5 10 7.36 8.29 3.13 o -2 5 10 11.42 12.01 2.72 o -1 5 10 131.12 128.87 7.27 o 0 5 10 32.54 35.24 2.85 o 1 5 10 131.26 127.53 4.23 o 2 5 10 11.40 10.85 2.02 o 3 5 10 7.36 8.17 2.14 o 4 5 10 7.20 5.89 2.11 o 0 6 10 149.77 161.95 6.22 o 1 6 10 0.47 1.22 1.54 o 2 6 10 69.92 75.15 4.62 o 0 1 11 203.53 217.55 3.34 o 1 1 11 20.61 19.38 1.19 o -1 2 11 452.72 441.88 9.16 o 0 2 11 408.79 372.08 5.83 o 1 2 11 453.12 427.32 13.57 o 2 2 11 200.61 206.59 6.48 o -2 3 11 174.09 170.95 6.74 o -1 3 11 397.39 377.50 9.59 o 0 3 11 8.09 9.12 1.53 o 1 3 11 396.77 384.98 10.69 o 2 3 11 174.00 175.20 5.00 o 3 3 11 306.20 306.41 6.91 o -3 4 11 18.14 18.19 3.13 o -2 4 11 126.57 142.95 6.99 o -1 4 11 58.71 53.08 4.26 o 0 4 11 87.24 84.45 3.71 o 1 4 11 58.75 50.79 2.40 o 2 4 11 126.75 122.70 4.70 o 3 4 11 18.10 17.56 2.20 o 4 4 11 104.21 103.66 4.94 o -4 5 11 12.61 9.34 3.30 o -3 5 11 81.66 91.86 6.70 o -2 5 11 62.30 51.21 5.35 o -1 5 11 21.42 20.52 3.51 o 0 5 11 22.03 19.16 2.30 o 1 5 11 21.44 24.47 2.12 o 2 5 11 62.24 61.39 3.71 o 3 5 11 81.78 77.16 4.59 o 4 5 11 12.62 10.64 2.32 o 0 6 11 14.97 12.42 3.69 o 1 6 11 26.49 23.04 2.79 o 2 6 11 25.95 28.47 3.15 o 0 0 12 307.40 271.35 6.45 o 0 1 12 1437.30 1541.46 26.89 o 1 1 12 489.94 443.80 9.68 o -1 2 12 271.09 297.48 7.87 o 0 2 12 918.45 900.35 19.54 o 1 2 12 271.07 287.80 7.99 o 2 2 12 730.46 672.25 9.29 o -2 3 12 132.80 125.24 6.03 o -1 3 12 161.67 163.05 6.77 o 0 3 12 570.15 585.65 9.69 o 1 3 12 161.30 156.75 4.35 o 2 3 12 132.87 120.17 10.24 o 3 3 12 8.12 8.82 1.74 o -3 4 12 5.02 3.10 2.35 o -2 4 12 35.81 36.34 3.91 o -1 4 12 68.75 69.29 5.12 o 0 4 12 86.30 100.59 4.06 o 1 4 12 68.80 71.36 2.87 o 2 4 12 35.83 35.42 2.83 o 3 4 12 5.00 4.19 1.64 o 4 4 12 2.39 5.27 1.88 o -3 5 12 4.42 3.98 2.49 o -2 5 12 13.71 13.03 3.13 o -1 5 12 9.45 10.33 2.73 o 0 5 12 0.01 0.34 1.22 o 1 5 12 9.40 6.53 2.62 o 2 5 12 13.72 13.22 2.23 o 3 5 12 4.42 2.22 1.91 o 0 6 12 41.36 45.81 5.05 o 1 6 12 0.66 -0.40 1.67 o 2 6 12 8.53 2.54 3.30 o 0 1 13 224.27 219.29 7.37 o 1 1 13 412.66 426.69 12.88 o -1 2 13 282.00 278.59 7.83 o 0 2 13 133.43 137.47 3.89 o 1 2 13 281.70 272.79 5.06 o 2 2 13 0.40 0.78 1.32 o -2 3 13 139.50 137.46 6.79 o -1 3 13 49.55 44.12 3.91 o 0 3 13 78.38 74.52 3.38 o 1 3 13 49.33 48.12 2.27 o 2 3 13 139.49 136.06 4.60 o 3 3 13 3.86 5.19 1.56 o -3 4 13 72.54 71.43 5.92 o -2 4 13 23.13 24.40 3.34 o -1 4 13 145.30 158.18 7.12 o 0 4 13 83.28 91.92 3.92 o 1 4 13 145.31 137.96 4.68 o 2 4 13 23.05 26.54 2.48 o 3 4 13 72.54 71.28 3.98 o 4 4 13 33.40 39.51 3.27 o -3 5 13 19.48 22.48 3.89 o -2 5 13 79.50 84.91 6.39 o -1 5 13 49.09 54.88 5.05 o 0 5 13 14.11 11.19 2.01 o 1 5 13 49.07 54.90 2.91 o 2 5 13 79.51 57.76 28.62 o 3 5 13 19.51 19.97 2.75 o 0 6 13 18.44 20.23 4.01 o 1 6 13 14.98 15.30 2.74 o 0 1 14 2.67 2.49 0.85 o 1 1 14 6.84 7.32 1.13 o -1 2 14 124.74 129.52 5.70 o 0 2 14 43.97 40.94 2.41 o 1 2 14 124.78 122.22 3.22 o 2 2 14 0.07 0.40 1.19 o -2 3 14 26.95 28.69 3.53 o -1 3 14 32.29 36.69 3.48 o 0 3 14 149.43 140.59 7.20 o 1 3 14 32.25 33.51 1.99 o 2 3 14 26.89 28.04 2.41 o 3 3 14 34.05 39.34 2.76 o -3 4 14 23.93 29.42 4.12 o -2 4 14 12.08 12.46 2.89 o -1 4 14 238.38 250.17 9.47 o 0 4 14 22.39 21.48 2.28 o 1 4 14 238.57 237.13 9.43 o 2 4 14 12.06 13.00 2.02 o 3 4 14 23.92 27.55 2.85 o 4 4 14 14.00 12.04 2.42 o -3 5 14 14.69 18.34 3.79 o -2 5 14 32.57 34.96 4.57 o -1 5 14 4.17 6.26 2.58 o 0 5 14 67.78 61.27 3.78 o 1 5 14 4.19 4.50 1.62 o 2 5 14 32.60 34.36 3.22 o 3 5 14 14.73 17.08 2.57 o 0 6 14 0.85 -2.15 2.61 o 1 6 14 111.14 57.76 4.21 o 0 1 15 0.64 -0.98 0.98 o 1 1 15 73.23 72.04 3.94 o -1 2 15 160.13 174.01 6.79 o 0 2 15 19.73 23.94 2.12 o 1 2 15 159.63 156.11 3.73 o 2 2 15 86.85 91.82 3.70 o -2 3 15 224.72 210.74 8.33 o -1 3 15 35.24 35.08 3.62 o 0 3 15 406.18 391.11 7.52 o 1 3 15 35.24 38.03 2.80 o 2 3 15 224.61 209.04 10.60 o 3 3 15 5.75 7.59 1.69 o -3 4 15 135.32 127.57 7.60 o -2 4 15 22.58 25.71 3.55 o -1 4 15 72.57 74.55 5.56 o 0 4 15 7.24 6.42 1.63 o 1 4 15 72.50 77.16 3.54 o 2 4 15 22.53 22.98 2.42 o 3 4 15 135.44 127.60 5.36 o 4 4 15 2.14 1.13 1.90 o -3 5 15 7.87 8.29 3.01 o -2 5 15 41.88 41.26 4.95 o -1 5 15 14.16 13.13 3.31 o 0 5 15 12.09 12.18 2.21 o 1 5 15 14.17 7.96 4.49 o 2 5 15 41.98 47.18 3.63 o 3 5 15 7.89 8.20 2.18 o 0 0 16 937.74 950.48 14.47 o 0 1 16 665.36 700.80 7.30 o 1 1 16 91.05 115.00 3.11 o -1 2 16 516.17 485.56 11.62 o 0 2 16 261.55 283.34 6.71 o 1 2 16 515.91 476.56 6.53 o 2 2 16 44.84 44.40 2.69 o -2 3 16 70.00 66.07 5.11 o -1 3 16 43.01 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