#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2014178.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014178_Fobs loop_ _publ_author_name 'Kurf\"urst, Pavel' 'Marek, Jarom\'ir' 'Van\R)-4-(4-Fluorophenyl)-1-[2-hydroxy-2-(3-methyl-1-benzofuran-2-yl)ethyl]piperazinium chloride propan-1-ol solvate ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o494 _journal_page_last o495 _journal_volume 60 _journal_year 2004 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.167 _cell_angle_gamma 90.000 _cell_length_a 10.6052 _cell_length_b 8.3553 _cell_length_c 13.0588 _exptl_crystal_F_000 480.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file gg1217Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' JV_03_05 in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 105.39 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 8 -6 0 0.19 0.71 1.57 o 9 -6 0 158.57 159.27 5.26 o 2 -5 0 652.69 655.17 4.05 o 3 -5 0 732.69 722.70 5.04 o 4 -5 0 269.05 262.47 4.08 o 6 -5 0 155.58 155.18 4.48 o 8 -5 0 118.67 118.33 4.65 o 9 -5 0 128.84 132.87 5.16 o 10 -5 0 53.37 53.78 4.64 o 2 -4 0 67.43 60.46 1.95 o 3 -4 0 158.97 139.43 3.01 o 4 -4 0 281.43 238.43 3.86 o 5 -4 0 158.62 145.33 2.70 o 6 -4 0 95.70 84.94 2.87 o 7 -4 0 21.65 25.43 2.91 o 8 -4 0 185.15 179.49 4.87 o 9 -4 0 238.30 228.70 5.67 o 10 -4 0 63.30 62.81 4.92 o 11 -4 0 51.27 46.57 4.33 o 1 -3 0 1160.49 1121.00 3.64 o 2 -3 0 191.63 202.74 2.68 o 3 -3 0 1447.95 1415.63 5.83 o 4 -3 0 167.76 141.41 3.40 o 5 -3 0 96.64 95.01 2.33 o 6 -3 0 618.65 607.29 19.23 o 7 -3 0 323.75 324.27 6.42 o 8 -3 0 13.34 10.57 2.24 o 9 -3 0 68.57 66.75 3.01 o 10 -3 0 30.72 31.04 2.70 o 11 -3 0 41.90 38.31 3.01 o 2 -2 0 1139.65 1099.11 4.17 o 3 -2 0 93.34 97.10 2.53 o 4 -2 0 2247.24 2249.59 8.12 o 5 -2 0 429.93 438.65 15.92 o 6 -2 0 297.57 294.71 5.29 o 7 -2 0 302.67 314.64 5.76 o 8 -2 0 543.01 542.84 7.73 o 9 -2 0 27.25 29.14 3.97 o 10 -2 0 221.54 226.90 4.12 o 11 -2 0 78.10 68.40 2.55 o 12 -2 0 22.53 20.87 2.66 o 2 -1 0 136.60 120.52 1.65 o 3 -1 0 328.57 322.42 8.83 o 4 -1 0 446.68 449.62 16.89 o 5 -1 0 104.40 119.54 6.35 o 6 -1 0 609.86 611.70 12.43 o 7 -1 0 163.14 156.28 3.24 o 8 -1 0 16.22 13.47 2.52 o 9 -1 0 217.59 217.55 5.02 o 10 -1 0 151.82 142.19 4.04 o 11 -1 0 58.61 55.20 2.60 o 12 -1 0 13.48 13.22 2.30 o 3 0 0 4549.36 4437.30 142.51 o 4 0 0 6869.09 6996.99 158.75 o 5 0 0 2367.64 2485.14 70.34 o 6 0 0 860.26 811.11 7.72 o 7 0 0 5.91 6.38 1.71 o 8 0 0 7.76 5.01 1.44 o 9 0 0 143.01 168.09 3.08 o 10 0 0 119.68 121.50 2.84 o 11 0 0 94.18 97.86 3.45 o 12 0 0 43.59 48.52 2.30 o 2 1 0 138.06 104.93 16.63 o 3 1 0 348.30 367.90 2.03 o 4 1 0 443.82 475.44 6.70 o 5 1 0 113.53 139.97 1.22 o 6 1 0 617.72 663.22 14.26 o 7 1 0 161.11 164.06 2.93 o 8 1 0 15.90 15.54 1.79 o 9 1 0 207.56 199.85 5.18 o 10 1 0 147.01 141.23 4.59 o 11 1 0 62.01 59.04 2.61 o 12 1 0 13.34 14.90 1.85 o 0 2 0 1483.73 1363.25 142.11 o 1 2 0 5034.40 4776.05 143.57 o 2 2 0 1135.54 1140.60 5.42 o 3 2 0 93.21 106.28 1.48 o 4 2 0 2231.59 2287.37 5.29 o 5 2 0 433.50 489.32 2.64 o 6 2 0 297.17 300.89 3.96 o 7 2 0 299.62 319.26 3.26 o 8 2 0 543.89 550.97 7.06 o 9 2 0 29.61 29.50 1.99 o 10 2 0 220.47 235.74 6.62 o 11 2 0 80.27 72.52 2.85 o 12 2 0 21.57 21.85 2.11 o 1 3 0 1171.44 1215.46 9.36 o 2 3 0 190.41 207.45 1.94 o 3 3 0 1427.19 1461.10 13.67 o 4 3 0 165.77 143.65 1.49 o 5 3 0 105.51 105.87 1.59 o 6 3 0 615.16 632.79 10.26 o 7 3 0 332.33 332.44 3.34 o 8 3 0 12.34 12.04 1.46 o 9 3 0 73.91 74.63 2.46 o 10 3 0 31.40 29.28 2.16 o 11 3 0 40.83 37.73 2.31 o 0 4 0 1629.16 1561.56 24.16 o 1 4 0 422.51 460.60 2.01 o 2 4 0 67.31 61.29 1.08 o 3 4 0 158.36 143.51 1.44 o 4 4 0 288.14 252.12 3.84 o 5 4 0 161.30 155.23 1.79 o 6 4 0 88.25 82.22 1.95 o 7 4 0 22.27 24.01 1.56 o 8 4 0 178.38 177.19 4.70 o 9 4 0 240.26 239.07 3.46 o 10 4 0 67.42 68.63 2.54 o 11 4 0 50.76 51.12 2.53 o 1 5 0 251.14 245.54 2.52 o 2 5 0 651.16 701.91 3.06 o 3 5 0 735.62 769.27 11.82 o 4 5 0 270.55 283.83 5.67 o 5 5 0 57.62 63.86 1.83 o 6 5 0 155.77 165.22 3.05 o 7 5 0 528.35 540.65 4.44 o 8 5 0 114.78 120.81 3.02 o 9 5 0 122.65 134.29 4.40 o 10 5 0 51.59 52.70 3.09 o 0 6 0 9.40 13.78 2.10 o 1 6 0 172.03 175.71 2.51 o 2 6 0 198.12 191.13 2.21 o 3 6 0 61.24 62.77 1.69 o 4 6 0 179.48 188.52 2.57 o 5 6 0 34.57 34.91 2.15 o 6 6 0 374.33 396.02 4.12 o 7 6 0 170.55 177.10 3.24 o 8 6 0 0.06 0.37 1.00 o 9 6 0 161.93 170.78 3.42 o 10 6 0 110.54 118.27 4.27 o 1 7 0 234.65 233.44 2.88 o 2 7 0 164.99 156.47 3.04 o 3 7 0 132.15 134.58 2.72 o 4 7 0 140.22 139.75 3.80 o 5 7 0 263.46 271.37 4.34 o 6 7 0 196.44 194.02 4.03 o 7 7 0 81.56 82.79 2.69 o 8 7 0 17.80 12.59 1.88 o 0 8 0 469.23 459.08 16.46 o 1 8 0 13.84 11.14 1.27 o 2 8 0 59.87 55.07 2.25 o 3 8 0 149.16 147.68 3.87 o 4 8 0 106.67 115.06 3.98 o 5 8 0 23.37 21.80 2.72 o 6 8 0 21.29 20.38 2.95 o 7 8 0 22.69 22.71 2.73 o 1 9 0 94.00 92.50 2.76 o 2 9 0 43.46 43.30 3.04 o 3 9 0 207.39 206.29 6.83 o 4 9 0 15.44 12.44 2.22 o 5 9 0 51.42 53.75 3.53 o -10 -6 1 112.85 113.09 4.92 o -9 -6 1 1.38 1.66 1.84 o -8 -6 1 62.15 57.62 3.82 o -7 -6 1 270.43 269.84 5.16 o -6 -6 1 140.77 140.52 4.19 o -10 -5 1 28.76 29.29 3.87 o -9 -5 1 75.01 70.93 4.10 o -8 -5 1 107.40 108.00 4.12 o -7 -5 1 87.52 83.19 4.16 o -5 -5 1 474.41 432.25 5.40 o -4 -5 1 97.35 89.16 3.03 o -3 -5 1 361.46 357.37 4.25 o 3 -5 1 305.86 286.86 3.55 o 4 -5 1 42.27 41.08 2.66 o 5 -5 1 51.19 47.12 2.83 o 6 -5 1 203.17 192.64 4.66 o 7 -5 1 580.09 577.27 7.09 o 8 -5 1 97.78 94.39 4.12 o 9 -5 1 36.42 29.29 3.31 o -11 -4 1 14.30 14.15 3.05 o -10 -4 1 149.19 151.48 5.78 o -9 -4 1 259.01 263.77 5.82 o -8 -4 1 308.41 308.23 6.29 o -7 -4 1 101.20 109.22 4.46 o -6 -4 1 44.32 39.76 2.83 o -5 -4 1 572.63 537.22 5.35 o -4 -4 1 556.09 520.99 18.66 o -3 -4 1 737.54 729.56 5.20 o -2 -4 1 48.91 55.51 2.06 o 1 -4 1 1137.99 1207.37 3.64 o 2 -4 1 2.15 6.80 1.10 o 3 -4 1 208.18 208.39 3.17 o 4 -4 1 625.14 606.71 4.93 o 5 -4 1 243.25 260.00 4.53 o 6 -4 1 467.25 468.06 11.65 o 7 -4 1 19.19 19.23 2.24 o 8 -4 1 189.45 179.72 6.15 o 9 -4 1 0.75 2.13 2.16 o 10 -4 1 160.11 159.51 5.71 o 11 -4 1 21.10 20.96 3.69 o -12 -3 1 45.35 46.33 5.00 o -10 -3 1 35.52 37.29 3.98 o -9 -3 1 12.58 13.15 2.06 o -8 -3 1 14.50 16.13 2.37 o -7 -3 1 751.11 740.74 5.07 o -6 -3 1 407.67 399.11 5.59 o -5 -3 1 107.49 104.06 10.31 o -4 -3 1 171.46 166.05 12.48 o -3 -3 1 888.23 836.39 31.99 o -2 -3 1 305.05 283.91 3.15 o 2 -3 1 162.49 147.34 2.02 o 3 -3 1 130.23 111.33 2.34 o 4 -3 1 67.69 68.81 2.73 o 5 -3 1 1612.62 1574.26 7.67 o 6 -3 1 673.15 651.57 4.89 o 7 -3 1 89.38 73.42 3.12 o 8 -3 1 18.40 15.83 2.23 o 9 -3 1 27.72 25.01 3.32 o 10 -3 1 178.01 173.97 7.13 o 11 -3 1 185.49 177.75 4.06 o -12 -2 1 177.54 191.29 4.38 o -11 -2 1 103.62 97.62 7.67 o -10 -2 1 133.75 126.97 3.57 o -9 -2 1 23.32 21.36 2.32 o -8 -2 1 216.49 211.02 5.21 o -7 -2 1 10.70 10.19 2.50 o -6 -2 1 341.15 330.68 3.65 o -5 -2 1 231.28 232.22 6.43 o -4 -2 1 1466.96 1474.54 7.08 o -3 -2 1 49.45 40.70 2.19 o -2 -2 1 1171.49 1137.35 4.74 o -1 -2 1 1982.16 1935.17 5.01 o 2 -2 1 602.21 578.66 3.26 o 3 -2 1 966.19 914.77 4.66 o 4 -2 1 869.11 872.06 5.82 o 5 -2 1 814.09 844.99 5.83 o 6 -2 1 597.69 599.13 20.84 o 7 -2 1 65.58 57.62 2.80 o 8 -2 1 0.58 0.71 0.87 o 9 -2 1 100.82 81.85 5.33 o 10 -2 1 466.68 510.44 5.62 o 11 -2 1 80.57 78.01 2.93 o 12 -2 1 5.27 3.71 1.34 o -12 -1 1 49.71 50.32 3.14 o -11 -1 1 48.23 46.22 3.21 o -10 -1 1 260.90 239.61 4.42 o -9 -1 1 85.45 83.93 2.52 o -8 -1 1 116.90 111.73 3.37 o -7 -1 1 121.79 118.80 2.98 o -6 -1 1 855.75 873.83 4.56 o -5 -1 1 415.93 443.76 3.29 o -4 -1 1 642.85 658.05 3.38 o -3 -1 1 3616.02 3531.10 34.38 o -2 -1 1 6692.47 6403.49 20.67 o 2 -1 1 21.42 23.57 2.00 o 3 -1 1 3668.82 3646.27 8.11 o 4 -1 1 598.19 633.96 12.96 o 5 -1 1 425.89 448.67 14.79 o 6 -1 1 127.31 128.52 3.89 o 7 -1 1 538.09 527.71 6.08 o 8 -1 1 56.09 53.48 4.10 o 9 -1 1 256.03 248.67 4.25 o 10 -1 1 85.92 81.42 2.55 o 11 -1 1 21.16 19.46 2.06 o 12 -1 1 46.12 46.58 2.61 o -12 0 1 137.39 135.82 4.20 o -11 0 1 5.25 1.44 1.58 o -10 0 1 43.27 61.67 2.41 o -9 0 1 3.47 2.49 1.21 o -8 0 1 302.87 302.94 3.77 o -7 0 1 127.38 154.65 3.28 o -6 0 1 2522.77 2711.46 28.88 o -5 0 1 687.46 775.40 10.55 o -4 0 1 115.00 109.43 1.70 o -3 0 1 86.50 83.25 1.92 o -2 0 1 1589.66 1056.72 494.86 o 2 0 1 118.79 119.64 17.62 o 3 0 1 0.91 4.05 3.20 o 4 0 1 1199.98 1154.41 32.26 o 5 0 1 78.83 74.36 2.77 o 6 0 1 475.92 474.41 14.46 o 7 0 1 1.28 0.39 0.57 o 8 0 1 49.69 49.72 2.96 o 9 0 1 84.89 104.90 2.81 o 10 0 1 59.52 59.02 2.54 o 11 0 1 84.89 82.64 2.75 o 12 0 1 22.73 23.56 3.22 o -12 1 1 52.28 53.94 4.75 o -11 1 1 48.85 44.99 2.32 o -10 1 1 258.09 242.65 5.03 o -9 1 1 86.38 86.22 2.38 o -8 1 1 119.99 116.31 2.61 o -7 1 1 112.22 109.34 2.92 o -6 1 1 865.02 906.11 6.60 o -5 1 1 437.41 497.09 7.53 o -4 1 1 634.81 682.45 7.39 o -3 1 1 3657.89 3730.01 42.99 o -2 1 1 6701.98 4546.79 1029.14 o 2 1 1 21.81 23.52 2.43 o 3 1 1 3706.64 3779.75 37.28 o 4 1 1 602.09 667.30 10.16 o 5 1 1 405.06 443.49 12.33 o 6 1 1 129.69 131.36 2.23 o 7 1 1 537.10 551.72 5.02 o 8 1 1 55.80 58.23 2.26 o 9 1 1 262.29 251.50 3.54 o 10 1 1 88.01 84.37 2.73 o 11 1 1 19.50 15.66 2.01 o 12 1 1 46.76 49.82 2.71 o -12 2 1 178.32 196.66 4.64 o -11 2 1 102.02 96.98 2.73 o -10 2 1 132.44 125.56 2.72 o -9 2 1 23.02 21.40 1.75 o -8 2 1 220.95 217.66 5.79 o -7 2 1 9.52 10.68 1.36 o -6 2 1 330.60 317.93 9.00 o -5 2 1 227.85 237.44 3.31 o -4 2 1 1464.68 1494.02 7.93 o -3 2 1 48.71 47.31 1.15 o -2 2 1 1152.78 1173.47 9.60 o -1 2 1 1979.43 2006.58 9.95 o 0 2 1 7687.59 7345.15 127.18 o 1 2 1 3670.95 3475.53 56.64 o 2 2 1 595.63 596.62 6.97 o 3 2 1 967.91 964.70 7.90 o 4 2 1 842.63 852.23 3.31 o 5 2 1 807.35 858.35 9.92 o 6 2 1 598.87 632.39 7.74 o 7 2 1 63.26 62.63 2.18 o 8 2 1 0.11 1.01 0.93 o 9 2 1 102.19 96.75 2.76 o 10 2 1 464.62 515.52 14.79 o 11 2 1 77.33 72.50 2.83 o 12 2 1 5.96 3.58 1.42 o -12 3 1 44.06 47.52 3.32 o -11 3 1 13.12 12.57 1.88 o -10 3 1 35.85 38.44 2.19 o -9 3 1 10.65 11.24 1.67 o -8 3 1 13.49 13.17 1.51 o -7 3 1 758.99 760.43 5.31 o -6 3 1 405.60 415.59 3.64 o -5 3 1 97.88 102.07 1.76 o -4 3 1 175.16 174.69 2.29 o -3 3 1 894.73 926.05 10.51 o -2 3 1 308.04 302.30 3.36 o -1 3 1 889.53 892.03 4.72 o 0 3 1 1.41 2.08 0.58 o 1 3 1 2382.19 2468.94 6.68 o 2 3 1 162.72 157.14 1.47 o 3 3 1 120.55 104.26 1.33 o 4 3 1 66.02 69.71 1.24 o 5 3 1 1634.10 1678.37 13.14 o 6 3 1 678.38 683.39 8.08 o 7 3 1 95.54 83.41 1.98 o 8 3 1 17.02 18.32 1.68 o 9 3 1 24.83 27.71 1.97 o 10 3 1 179.38 184.55 3.48 o 11 3 1 188.10 186.48 3.54 o -11 4 1 13.42 12.49 1.90 o -10 4 1 151.53 156.12 4.10 o -9 4 1 262.08 274.56 4.05 o -8 4 1 304.86 314.56 4.42 o -7 4 1 104.42 113.13 2.46 o -6 4 1 42.75 39.38 1.27 o -5 4 1 565.88 550.15 5.13 o -4 4 1 566.28 587.53 5.25 o -3 4 1 742.87 756.48 8.76 o -2 4 1 46.05 50.90 0.91 o -1 4 1 236.27 245.21 2.82 o 0 4 1 1588.40 1586.38 8.54 o 1 4 1 1138.97 1308.94 11.83 o 2 4 1 3.80 6.70 0.69 o 3 4 1 206.71 209.47 2.88 o 4 4 1 624.45 632.07 7.44 o 5 4 1 245.35 258.57 4.29 o 6 4 1 450.08 460.83 6.45 o 7 4 1 20.47 16.94 1.45 o 8 4 1 188.70 183.76 4.16 o 9 4 1 0.58 1.68 1.12 o 10 4 1 156.64 156.84 3.60 o 11 4 1 19.52 19.78 2.27 o -10 5 1 29.75 35.12 2.78 o -9 5 1 78.10 80.70 3.21 o -8 5 1 103.89 104.98 3.25 o -7 5 1 85.68 86.79 2.79 o -6 5 1 357.70 352.01 2.95 o -5 5 1 480.72 466.50 6.70 o -4 5 1 97.07 94.38 1.91 o -3 5 1 355.32 365.51 2.60 o -2 5 1 47.32 55.75 1.37 o -1 5 1 205.86 219.44 1.94 o 0 5 1 301.57 339.37 4.01 o 1 5 1 1059.73 1113.45 9.92 o 2 5 1 125.36 125.04 1.51 o 3 5 1 316.35 312.83 3.12 o 4 5 1 41.82 43.07 1.32 o 5 5 1 53.22 51.77 1.67 o 6 5 1 201.69 194.99 4.13 o 7 5 1 588.01 589.88 9.60 o 8 5 1 95.12 100.26 2.30 o 9 5 1 38.77 33.80 2.41 o 10 5 1 153.48 167.25 4.19 o -10 6 1 114.92 117.32 3.94 o -9 6 1 1.07 2.13 1.72 o -8 6 1 57.16 54.65 2.27 o -7 6 1 265.12 278.70 3.80 o -6 6 1 142.77 149.41 3.03 o -5 6 1 382.51 369.86 3.40 o -4 6 1 287.59 291.22 3.81 o -3 6 1 247.77 247.14 4.01 o -2 6 1 136.28 133.86 1.86 o -1 6 1 44.97 49.79 1.53 o 0 6 1 1170.41 1219.50 10.59 o 1 6 1 197.09 195.11 2.74 o 2 6 1 67.02 55.53 2.09 o 3 6 1 843.05 885.72 16.98 o 4 6 1 648.59 658.76 9.58 o 5 6 1 231.42 225.22 3.15 o 6 6 1 7.89 6.92 1.30 o 7 6 1 126.91 127.96 3.03 o 8 6 1 196.76 213.62 3.53 o 9 6 1 98.54 101.13 2.98 o -8 7 1 60.18 58.82 2.66 o -7 7 1 363.52 399.17 7.92 o -6 7 1 88.33 82.58 3.77 o -5 7 1 27.47 27.35 2.03 o -4 7 1 172.83 160.05 3.02 o -3 7 1 92.41 92.89 2.55 o -2 7 1 138.10 149.16 2.95 o -1 7 1 140.97 134.45 2.52 o 0 7 1 234.35 234.62 2.85 o 1 7 1 66.96 63.92 2.15 o 2 7 1 63.30 53.37 2.28 o 3 7 1 332.85 341.30 10.91 o 4 7 1 159.17 158.18 4.25 o 5 7 1 30.81 29.73 2.49 o 6 7 1 46.06 40.34 2.83 o 7 7 1 234.29 245.63 3.76 o 8 7 1 15.24 12.01 2.00 o -7 8 1 13.36 14.34 2.80 o -6 8 1 117.55 113.71 4.16 o -5 8 1 2.51 1.88 1.43 o -4 8 1 170.96 175.37 4.36 o -3 8 1 12.44 15.92 1.84 o -2 8 1 193.08 190.02 3.30 o -1 8 1 4.87 4.15 1.20 o 0 8 1 129.40 131.99 2.65 o 1 8 1 72.72 73.34 2.53 o 2 8 1 146.98 145.92 8.27 o 3 8 1 32.28 32.61 2.90 o 4 8 1 434.94 459.44 5.85 o 5 8 1 82.19 86.79 3.71 o 6 8 1 51.70 58.85 3.62 o 7 8 1 422.78 450.59 6.01 o -5 9 1 45.38 43.33 3.13 o -4 9 1 17.21 17.54 2.56 o -3 9 1 70.06 70.11 3.55 o -2 9 1 8.70 3.25 1.57 o -1 9 1 130.39 131.24 2.70 o 0 9 1 76.09 69.70 2.26 o 1 9 1 147.28 156.00 5.87 o 2 9 1 0.12 1.22 1.18 o 3 9 1 142.69 144.90 4.15 o 4 9 1 11.62 10.51 2.28 o 5 9 1 94.61 95.06 3.94 o -10 -6 2 20.51 18.55 3.25 o -9 -6 2 24.77 21.75 2.91 o -8 -6 2 238.36 233.45 5.50 o -6 -6 2 32.69 32.21 2.86 o -5 -6 2 38.50 40.57 2.86 o -4 -6 2 438.82 419.06 5.72 o -10 -5 2 17.69 15.71 3.21 o -9 -5 2 167.41 150.34 5.54 o -8 -5 2 56.24 58.74 4.57 o -6 -5 2 35.34 31.52 3.37 o -5 -5 2 180.56 170.97 4.28 o -4 -5 2 270.43 267.47 4.49 o -3 -5 2 59.62 55.36 2.61 o 5 -5 2 176.31 180.10 4.13 o 6 -5 2 642.14 606.04 6.04 o 7 -5 2 112.00 105.28 3.79 o 8 -5 2 98.48 94.77 4.38 o 9 -5 2 237.61 233.77 5.35 o 10 -5 2 39.93 43.67 3.96 o -11 -4 2 121.61 119.35 5.78 o -10 -4 2 155.13 157.50 5.31 o -9 -4 2 115.38 112.86 5.34 o -8 -4 2 198.18 191.37 5.35 o -7 -4 2 43.46 43.84 3.87 o -6 -4 2 399.42 391.64 5.57 o -5 -4 2 0.65 1.21 1.79 o -4 -4 2 534.36 517.56 5.65 o -3 -4 2 700.40 732.12 5.61 o -2 -4 2 1270.55 1292.31 6.16 o 2 -4 2 71.32 58.19 1.62 o 3 -4 2 271.58 278.45 3.30 o 4 -4 2 334.77 315.18 4.20 o 5 -4 2 277.23 275.48 4.55 o 6 -4 2 557.94 568.15 6.63 o 7 -4 2 16.16 13.43 2.79 o 8 -4 2 669.98 634.32 21.03 o 9 -4 2 148.84 138.62 3.53 o 10 -4 2 42.73 46.76 4.29 o 11 -4 2 24.88 24.26 3.59 o -12 -3 2 32.28 40.10 4.78 o -11 -3 2 98.90 99.79 5.45 o -10 -3 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