#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/42/2014208.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014208_Fobs loop_ _publ_author_name 'Sonar, Vijayakumar N.' 'Parkin, Sean' 'Crooks, Peter A.' _publ_section_title ; 1-(2,5-Dichlorophenyl)-3-methyl-5-phenyl-1H-pyrazole ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o547 _journal_page_last o549 _journal_volume 60 _journal_year 2004 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.780 _cell_angle_gamma 90.000 _cell_length_a 17.3805 _cell_length_b 14.8094 _cell_length_c 11.0596 _exptl_crystal_F_000 1248.00 _reflns_d_resolution_high .7702 _[local]_cod_data_source_file na1669Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' k03295 - P21/c (from P21/a)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 313.51 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1254.20 1209.29 19.39 o 3 0 0 4871.89 4648.53 77.56 o 4 0 0 17937.29 17890.76 257.37 o 5 0 0 60227.39 58694.54 1077.08 o 6 0 0 66262.39 66727.66 1248.07 o 7 0 0 4073.47 4013.92 61.70 o 8 0 0 60.13 59.94 5.29 o 9 0 0 1656.43 2028.99 35.26 o 10 0 0 304.25 338.46 12.34 o 11 0 0 2.57 -1.76 5.29 o 12 0 0 246.50 183.33 12.34 o 13 0 0 625.38 542.95 21.15 o 14 0 0 2084.36 2037.81 54.65 o 15 0 0 193.67 183.33 15.87 o 16 0 0 1219.00 1265.70 68.75 o 17 0 0 122.73 100.48 31.73 o 18 0 0 95.58 89.90 40.54 o 19 0 0 272.82 243.27 47.60 o 20 0 0 2.35 -15.87 35.26 o 21 0 0 88.09 125.16 42.31 o 22 0 0 290.88 259.13 66.99 o 1 1 0 1982.02 1916.10 19.83 o 2 1 0 503.07 474.52 12.34 o 3 1 0 3.03 3.53 1.25 o 4 1 0 1541.51 1455.34 16.79 o 5 1 0 302.21 248.67 5.29 o 6 1 0 398.41 366.06 6.77 o 7 1 0 5647.95 5774.56 64.11 o 8 1 0 414.15 467.47 12.34 o 9 1 0 88.64 93.73 5.29 o 10 1 0 303.78 232.69 6.77 o 11 1 0 192.26 155.13 6.77 o 12 1 0 495.49 501.56 12.46 o 13 1 0 232.27 249.57 15.87 o 14 1 0 155.64 153.00 14.10 o 15 1 0 1.38 -2.64 6.23 o 16 1 0 224.27 207.88 24.84 o 17 1 0 598.92 597.41 34.26 o 18 1 0 248.84 241.16 33.01 o 19 1 0 56.42 41.94 26.26 o 20 1 0 71.31 101.33 31.09 o 21 1 0 74.65 76.22 32.61 o 22 1 0 165.61 111.94 37.39 o 0 2 0 19285.00 18663.65 304.07 o 1 2 0 2088.20 1959.36 21.19 o 2 2 0 936.51 863.59 9.74 o 3 2 0 20246.64 19652.68 206.73 o 4 2 0 11381.67 11195.05 115.11 o 5 2 0 2374.63 2319.46 27.34 o 6 2 0 2956.13 2857.70 31.62 o 7 2 0 1424.31 1459.63 18.70 o 8 2 0 1983.14 2296.47 27.34 o 9 2 0 37.86 14.63 5.29 o 10 2 0 979.73 1018.94 19.39 o 11 2 0 4285.40 4325.64 64.72 o 12 2 0 190.70 201.10 9.29 o 13 2 0 434.67 402.39 11.79 o 14 2 0 583.92 608.54 16.75 o 15 2 0 37.66 13.70 7.47 o 16 2 0 162.25 125.66 14.67 o 17 2 0 28.65 16.92 18.57 o 18 2 0 45.68 44.53 23.29 o 19 2 0 1511.86 1561.33 62.18 o 20 2 0 323.58 257.61 66.99 o 21 2 0 6.95 -13.02 31.27 o 22 2 0 142.01 79.90 55.53 o 1 3 0 5772.92 5547.50 59.30 o 2 3 0 23179.63 22357.55 243.50 o 3 3 0 2696.91 2636.43 28.80 o 4 3 0 12699.74 12518.73 127.94 o 5 3 0 1588.37 1695.43 19.83 o 6 3 0 564.79 485.57 14.10 o 7 3 0 3387.16 3569.32 37.64 o 8 3 0 2694.79 2473.87 29.22 o 9 3 0 2839.77 2844.46 33.86 o 10 3 0 484.23 407.88 9.74 o 11 3 0 668.15 644.97 13.97 o 12 3 0 2884.62 2774.20 46.43 o 13 3 0 292.90 224.40 9.29 o 14 3 0 260.45 253.33 10.54 o 15 3 0 3089.07 3153.67 61.13 o 16 3 0 1763.32 1796.29 41.64 o 17 3 0 758.42 785.52 41.08 o 18 3 0 2415.85 2450.55 76.53 o 19 3 0 1050.58 1016.38 52.97 o 20 3 0 58.98 20.54 28.59 o 21 3 0 628.53 681.37 50.20 o 22 3 0 1695.51 1767.61 102.83 o 0 4 0 26820.57 26167.98 430.16 o 1 4 0 133.87 151.68 3.74 o 2 4 0 1410.16 1429.50 16.52 o 3 4 0 16.46 20.62 2.64 o 4 4 0 30.56 29.97 2.93 o 5 4 0 94.10 96.15 4.99 o 6 4 0 2649.25 2674.10 30.86 o 7 4 0 3471.18 3334.91 37.15 o 8 4 0 5088.17 5060.31 58.44 o 9 4 0 388.07 453.15 9.97 o 10 4 0 563.38 501.35 12.28 o 11 4 0 3.88 .88 4.99 o 12 4 0 25.63 16.79 9.70 o 13 4 0 267.29 223.93 9.97 o 14 4 0 1805.80 1805.61 36.38 o 15 4 0 92.33 100.42 12.44 o 16 4 0 168.71 154.53 23.80 o 17 4 0 304.39 265.67 23.71 o 18 4 0 248.08 198.32 28.59 o 19 4 0 279.25 312.95 44.95 o 20 4 0 1426.72 1567.10 74.51 o 21 4 0 714.32 778.46 74.92 o 22 4 0 35.56 5.20 35.38 o 1 5 0 3611.01 3621.52 42.34 o 2 5 0 771.10 798.49 11.01 o 3 5 0 35362.22 35543.44 368.63 o 4 5 0 336.28 295.72 11.46 o 5 5 0 853.35 705.13 18.51 o 6 5 0 37.65 29.12 4.53 o 7 5 0 599.77 563.32 10.54 o 8 5 0 1905.60 1822.48 25.38 o 9 5 0 392.82 398.95 15.87 o 10 5 0 446.52 445.64 12.34 o 11 5 0 9828.42 10415.39 154.25 o 12 5 0 .22 -2.12 6.17 o 13 5 0 113.39 96.28 8.73 o 14 5 0 165.47 137.08 10.54 o 15 5 0 39.79 46.90 10.86 o 16 5 0 87.75 60.41 16.75 o 17 5 0 2660.80 2871.22 98.72 o 18 5 0 3.01 9.76 23.71 o 19 5 0 168.19 185.29 33.04 o 20 5 0 202.69 233.00 69.63 o 21 5 0 .97 15.59 32.12 o 0 6 0 4105.62 3779.87 65.75 o 1 6 0 .08 -.88 3.74 o 2 6 0 324.21 344.66 8.81 o 3 6 0 737.65 759.49 13.22 o 4 6 0 1263.48 1339.91 43.19 o 5 6 0 1043.00 1224.86 15.87 o 6 6 0 2897.94 2457.25 28.35 o 7 6 0 577.25 680.28 28.20 o 8 6 0 .21 5.29 7.93 o 9 6 0 3.26 11.16 5.51 o 10 6 0 573.83 442.97 19.39 o 11 6 0 145.64 170.45 9.29 o 12 6 0 4339.01 4554.34 69.43 o 13 6 0 61.00 46.94 10.58 o 14 6 0 1277.25 1148.79 30.37 o 15 6 0 22.12 25.17 12.76 o 16 6 0 420.98 454.97 29.09 o 17 6 0 156.57 105.61 22.44 o 18 6 0 1713.27 1825.91 108.41 o 19 6 0 298.01 264.20 37.15 o 20 6 0 10.86 7.99 27.86 o 21 6 0 39.76 31.27 37.27 o 1 7 0 3746.31 3632.16 45.74 o 2 7 0 16295.30 17665.24 211.54 o 3 7 0 12648.36 13664.52 232.69 o 4 7 0 1171.24 1197.00 16.79 o 5 7 0 2302.17 2271.36 31.73 o 6 7 0 9.99 -3.53 4.99 o 7 7 0 164.51 165.99 8.03 o 8 7 0 2941.84 2903.53 40.63 o 9 7 0 272.27 297.55 13.04 o 10 7 0 308.20 317.54 27.32 o 11 7 0 112.73 87.14 10.54 o 12 7 0 258.52 255.13 12.69 o 13 7 0 94.65 66.99 13.04 o 14 7 0 102.42 100.82 15.60 o 15 7 0 145.13 139.82 16.78 o 16 7 0 660.21 634.76 48.48 o 17 7 0 66.78 40.19 18.20 o 18 7 0 21.66 .41 28.33 o 19 7 0 171.20 99.92 29.27 o 20 7 0 168.15 169.03 31.09 o 21 7 0 124.83 72.33 44.95 o 0 8 0 741.57 892.47 23.29 o 1 8 0 1162.07 942.05 17.79 o 2 8 0 415.39 381.83 11.01 o 3 8 0 492.56 466.82 18.51 o 4 8 0 628.20 668.63 18.57 o 5 8 0 1406.75 1335.00 31.73 o 6 8 0 12.01 1.96 5.51 o 7 8 0 4532.74 4463.01 61.62 o 8 8 0 2458.23 2473.17 39.81 o 9 8 0 2056.05 2045.00 36.00 o 10 8 0 703.74 685.82 21.08 o 11 8 0 2907.40 2903.27 54.44 o 12 8 0 24.38 24.40 13.32 o 13 8 0 2971.79 3027.12 73.61 o 14 8 0 545.64 542.94 38.78 o 15 8 0 1136.90 1199.47 66.99 o 16 8 0 57.76 72.49 24.45 o 17 8 0 1.52 27.72 25.36 o 18 8 0 559.30 535.59 45.38 o 19 8 0 659.44 681.27 49.98 o 20 8 0 6.57 24.48 42.31 o 1 9 0 2779.47 2833.31 52.00 o 2 9 0 1040.55 1160.56 24.45 o 3 9 0 6993.60 7087.72 117.23 o 4 9 0 137.26 129.47 10.54 o 5 9 0 4718.78 4977.14 80.87 o 6 9 0 1182.27 1311.47 26.67 o 7 9 0 319.69 318.54 16.75 o 8 9 0 1.41 -9.74 9.74 o 9 9 0 2509.03 2465.89 52.00 o 10 9 0 1722.24 1717.01 38.80 o 11 9 0 767.92 842.65 28.69 o 12 9 0 585.51 598.32 30.07 o 13 9 0 518.58 507.12 24.45 o 14 9 0 251.18 269.63 33.49 o 15 9 0 52.71 84.34 21.15 o 16 9 0 7.23 15.87 22.07 o 17 9 0 31.07 -6.05 57.29 o 18 9 0 250.53 189.91 42.40 o 19 9 0 145.95 154.50 48.84 o 0 10 0 5320.90 5365.25 129.10 o 1 10 0 2530.48 2599.37 78.45 o 2 10 0 1804.56 1922.26 36.79 o 3 10 0 561.94 639.61 19.48 o 4 10 0 927.74 946.19 52.00 o 5 10 0 5018.85 5134.74 91.24 o 6 10 0 40.91 41.98 22.92 o 7 10 0 .13 -9.95 10.11 o 8 10 0 352.76 356.78 16.52 o 9 10 0 149.22 198.57 15.64 o 10 10 0 662.19 689.37 25.08 o 11 10 0 12.32 27.64 13.04 o 12 10 0 69.46 93.98 15.87 o 13 10 0 27.09 30.41 16.28 o 14 10 0 1044.10 1090.70 87.26 o 15 10 0 1192.68 1288.75 47.69 o 16 10 0 234.62 189.87 28.80 o 17 10 0 617.87 582.67 63.46 o 18 10 0 12.95 8.18 50.24 o 19 10 0 239.38 167.01 39.81 o 1 11 0 2797.61 2779.57 98.72 o 2 11 0 36.47 36.20 9.29 o 3 11 0 41.17 59.20 11.01 o 4 11 0 155.21 144.89 14.96 o 5 11 0 3441.96 3453.01 62.67 o 6 11 0 43.59 27.52 13.22 o 7 11 0 381.66 380.23 17.60 o 8 11 0 386.67 350.33 29.09 o 9 11 0 1961.07 1961.24 45.32 o 10 11 0 15.35 .44 14.34 o 11 11 0 289.78 285.97 20.53 o 12 11 0 320.61 272.50 21.15 o 13 11 0 405.39 393.14 38.78 o 14 11 0 181.72 199.61 40.54 o 15 11 0 167.74 185.98 37.02 o 16 11 0 200.64 230.74 29.61 o 17 11 0 236.96 311.78 36.00 o 18 11 0 178.19 198.96 38.40 o 0 12 0 1511.33 1530.94 66.99 o 1 12 0 208.09 250.56 17.45 o 2 12 0 245.42 210.73 27.32 o 3 12 0 .07 10.89 10.54 o 4 12 0 51.20 55.71 13.71 o 5 12 0 3540.13 3613.41 72.41 o 6 12 0 1.56 4.09 13.04 o 7 12 0 25.15 25.12 14.34 o 8 12 0 131.31 142.13 29.97 o 9 12 0 2009.68 2297.21 58.34 o 10 12 0 2593.09 2694.10 91.67 o 11 12 0 193.05 209.50 30.85 o 12 12 0 125.58 151.60 20.22 o 13 12 0 300.02 330.88 24.45 o 14 12 0 511.36 485.73 35.89 o 15 12 0 58.74 60.44 25.38 o 16 12 0 755.50 784.30 58.17 o 17 12 0 51.94 14.31 31.27 o 1 13 0 857.56 833.38 29.11 o 2 13 0 3216.77 3085.83 66.03 o 3 13 0 620.24 642.65 48.48 o 4 13 0 1028.76 1029.11 79.33 o 5 13 0 13.73 -7.05 13.71 o 6 13 0 318.99 265.09 36.14 o 7 13 0 861.79 845.72 29.22 o 8 13 0 446.75 444.21 52.00 o 9 13 0 395.57 367.85 24.70 o 10 13 0 144.84 173.57 24.26 o 11 13 0 978.59 980.57 41.91 o 12 13 0 582.35 534.49 77.56 o 13 13 0 660.71 640.63 35.51 o 14 13 0 36.53 58.94 39.66 o 15 13 0 148.64 193.89 31.77 o 16 13 0 1.07 -22.57 31.33 o 0 14 0 264.96 226.59 23.68 o 1 14 0 33.80 17.63 11.73 o 2 14 0 39.70 37.44 15.54 o 3 14 0 2.53 -13.15 17.63 o 4 14 0 39.20 31.87 18.51 o 5 14 0 4.75 -3.53 14.96 o 6 14 0 404.26 381.41 37.90 o 7 14 0 146.11 153.21 19.48 o 8 14 0 232.88 188.89 19.83 o 9 14 0 1598.47 1791.75 59.75 o 10 14 0 636.32 653.18 35.75 o 11 14 0 490.71 404.40 29.96 o 12 14 0 1.94 -1.18 35.26 o 13 14 0 8.07 22.92 26.19 o 14 14 0 100.19 115.88 33.56 o 15 14 0 64.95 79.33 44.07 o 1 15 0 119.13 91.55 19.39 o 2 15 0 84.16 84.43 16.79 o 3 15 0 1605.08 1616.53 52.05 o 4 15 0 557.20 542.83 68.75 o 5 15 0 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146.31 o 3 18 0 113.06 95.19 38.78 o 4 18 0 235.36 218.59 44.07 o 5 18 0 168.46 109.29 35.26 o 6 18 0 133.53 75.80 31.73 o 7 18 0 281.71 206.25 42.31 o 1 19 0 9.65 -37.02 66.99 o 2 19 0 45.19 116.35 45.83 o 3 19 0 36.60 86.38 52.88 o -22 1 1 96.62 84.61 44.07 o -21 1 1 543.55 594.84 44.82 o -20 1 1 183.67 172.02 69.63 o -19 1 1 565.31 610.93 39.81 o -18 1 1 3674.31 3660.44 140.14 o -17 1 1 61.45 81.71 22.44 o -16 1 1 333.93 355.48 25.82 o -15 1 1 12.21 -5.29 7.88 o -14 1 1 302.46 284.81 11.46 o -13 1 1 6267.18 6310.80 163.94 o -12 1 1 6349.45 6470.27 95.59 o -11 1 1 169.45 172.83 6.31 o -10 1 1 1801.14 1862.85 27.39 o -9 1 1 844.43 755.52 14.10 o -8 1 1 3490.56 3795.24 56.41 o -7 1 1 11825.41 11375.77 122.79 o -6 1 1 7336.70 7591.15 82.82 o -5 1 1 6069.79 6254.73 69.43 o -4 1 1 3294.33 3239.98 39.25 o -3 1 1 4335.70 4325.10 47.88 o -2 1 1 756.75 726.29 8.73 o -1 1 1 7945.88 7491.86 96.31 o 0 1 1 86.34 86.74 1.58 o 1 1 1 2529.33 2485.12 26.78 o 2 1 1 2.10 5.54 1.76 o 3 1 1 9212.65 8906.35 89.12 o 4 1 1 2845.59 2834.30 31.33 o 5 1 1 7926.80 7802.66 96.95 o 6 1 1 132.23 174.23 10.58 o 7 1 1 1585.04 1510.31 19.29 o 8 1 1 1182.14 1221.63 16.20 o 9 1 1 228.46 197.98 8.81 o 10 1 1 2463.78 2295.52 30.37 o 11 1 1 213.58 243.29 14.10 o 12 1 1 326.67 269.21 9.29 o 13 1 1 356.49 318.31 9.97 o 14 1 1 587.06 572.69 16.06 o 15 1 1 1075.35 1086.13 30.07 o 16 1 1 2866.76 2992.66 66.26 o 17 1 1 14.28 22.79 29.09 o 18 1 1 2349.58 2361.10 76.05 o 19 1 1 61.84 124.64 31.62 o 20 1 1 257.54 250.75 36.79 o 21 1 1 886.77 972.52 59.20 o 22 1 1 692.05 710.96 58.55 o -22 2 1 148.53 148.38 35.57 o -21 2 1 48.38 47.93 29.27 o -20 2 1 539.72 451.64 42.34 o -19 2 1 8.52 -26.27 41.43 o -18 2 1 286.50 318.06 31.77 o -17 2 1 635.08 597.00 36.15 o -16 2 1 331.73 285.48 24.93 o -15 2 1 722.34 722.32 36.14 o -14 2 1 980.85 968.11 22.15 o -13 2 1 115.86 103.10 9.29 o -12 2 1 2397.08 2472.59 41.08 o -11 2 1 66.84 47.69 12.34 o -10 2 1 6848.72 7489.06 94.18 o -9 2 1 .90 .25 4.23 o -8 2 1 1461.04 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548.47 26.44 o -10 4 2 1234.44 1206.71 21.15 o -9 4 2 5403.65 5418.78 69.38 o -8 4 2 2452.31 2534.62 53.77 o -7 4 2 2181.66 2370.35 58.17 o -6 4 2 1881.02 2096.68 28.30 o -5 4 2 1225.93 1106.38 15.54 o -4 4 2 748.58 732.99 10.54 o -3 4 2 17347.05 17391.52 210.46 o -2 4 2 7774.90 7523.25 133.97 o -1 4 2 1247.74 1306.64 17.79 o 0 4 2 9676.97 9820.69 111.17 o 1 4 2 8694.57 8398.25 90.76 o 2 4 2 11002.21 11091.48 127.80 o 3 4 2 601.00 588.12 9.29 o 4 4 2 7478.46 7405.91 75.55 o 5 4 2 847.89 772.69 10.54 o 6 4 2 1299.52 1317.27 16.79 o 7 4 2 70.65 60.59 4.41 o 8 4 2 2.13 1.41 2.93 o 9 4 2 1897.35 1952.79 28.80 o 10 4 2 336.32 348.61 9.74 o 11 4 2 212.10 197.93 7.47 o 12 4 2 138.94 110.45 4.86 o 13 4 2 845.05 836.61 21.79 o 14 4 2 282.49 262.45 14.96 o 15 4 2 192.31 194.49 13.71 o 16 4 2 792.64 725.52 28.03 o 17 4 2 521.05 444.26 27.39 o 18 4 2 685.21 644.20 43.61 o 19 4 2 128.01 69.48 31.63 o 20 4 2 159.58 131.75 68.75 o 21 4 2 31.18 2.62 37.69 o -21 5 2 61.76 84.89 43.92 o -20 5 2 9.68 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94.91 19.83 o 12 13 2 260.27 228.84 41.43 o 13 13 2 242.86 193.32 37.02 o 14 13 2 469.99 474.48 46.31 o 15 13 2 40.45 79.80 40.54 o 16 13 2 62.94 -5.64 45.83 o -15 14 2 21.82 72.46 51.12 o -14 14 2 19.12 -5.54 37.02 o -13 14 2 148.66 189.38 29.79 o -12 14 2 88.27 57.54 27.66 o -11 14 2 214.13 192.76 28.04 o -10 14 2 31.51 46.90 34.37 o -9 14 2 170.69 153.06 24.70 o -8 14 2 207.56 167.08 35.26 o -7 14 2 499.95 524.86 31.02 o -6 14 2 146.92 169.33 24.02 o -5 14 2 135.33 172.89 27.39 o -4 14 2 219.10 215.77 20.54 o -3 14 2 334.82 351.07 23.59 o -2 14 2 397.60 395.72 23.29 o -1 14 2 383.99 346.20 22.02 o 0 14 2 54.69 40.97 15.54 o 1 14 2 5.44 18.27 12.24 o 2 14 2 419.31 406.35 40.54 o 3 14 2 501.90 487.57 21.85 o 4 14 2 113.75 99.99 19.39 o 5 14 2 81.37 75.46 17.32 o 6 14 2 41.07 44.73 14.80 o 7 14 2 80.81 94.40 18.91 o 8 14 2 4.58 11.97 17.96 o 9 14 2 26.83 1.51 22.91 o 10 14 2 111.33 81.21 24.70 o 11 14 2 346.05 262.66 31.73 o 12 14 2 289.09 314.50 64.34 o 13 14 2 10.71 28.71 44.95 o 14 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113.17 28.94 o -6 16 2 75.51 51.12 24.49 o -5 16 2 25.87 18.60 25.65 o -4 16 2 354.29 352.71 30.95 o -3 16 2 139.11 122.80 33.49 o -2 16 2 .53 46.19 32.27 o -1 16 2 28.46 42.07 40.54 o 0 16 2 122.94 131.21 28.20 o 1 16 2 1129.63 1122.20 52.15 o 2 16 2 13.83 33.27 22.67 o 3 16 2 1.45 -4.94 23.47 o 4 16 2 .30 25.18 38.78 o 5 16 2 .76 21.12 23.80 o 6 16 2 121.66 78.41 28.02 o 7 16 2 677.09 641.32 44.07 o 8 16 2 132.38 64.64 26.80 o 9 16 2 66.57 49.99 28.68 o 10 16 2 1.86 -28.36 78.45 o 11 16 2 1109.29 1112.33 88.14 o 12 16 2 .05 -29.97 42.31 o -10 17 2 79.09 77.56 38.78 o -9 17 2 89.31 83.44 31.53 o -8 17 2 156.22 125.21 28.94 o -7 17 2 168.35 152.74 34.23 o -6 17 2 21.30 2.20 29.22 o -5 17 2 62.20 -11.65 50.24 o -4 17 2 190.75 239.21 65.22 o -3 17 2 2.77 -12.17 33.01 o -2 17 2 .08 36.85 36.14 o -1 17 2 78.81 76.07 55.53 o 0 17 2 9.76 18.62 31.73 o 1 17 2 21.96 53.86 32.61 o 2 17 2 20.42 46.89 25.62 o 3 17 2 3.24 -21.85 30.95 o 4 17 2 466.81 416.23 40.57 o 5 17 2 .01 -9.27 23.80 o 6 17 2 203.50 219.87 33.11 o 7 17 2 45.28 18.33 27.36 o 8 17 2 1.49 -1.04 29.44 o 9 17 2 908.43 835.04 108.41 o 10 17 2 7.09 -2.94 36.14 o -7 18 2 76.14 59.94 45.83 o -6 18 2 50.33 94.26 61.70 o -5 18 2 422.09 522.21 54.17 o -4 18 2 234.80 309.35 49.10 o -3 18 2 80.17 128.09 40.57 o -2 18 2 455.43 425.45 43.07 o -1 18 2 63.14 57.28 35.38 o 0 18 2 295.87 290.75 34.99 o 1 18 2 691.37 689.84 49.46 o 2 18 2 58.47 19.80 59.94 o 3 18 2 36.79 59.63 32.64 o 4 18 2 42.95 14.54 33.26 o 5 18 2 368.25 391.88 103.12 o 6 18 2 199.96 165.87 31.97 o 7 18 2 683.65 610.68 64.34 o -1 19 2 .77 86.38 52.88 o 0 19 2 41.00 -12.34 63.46 o 1 19 2 59.77 65.08 34.17 o -22 1 3 728.15 708.11 59.94 o -21 1 3 9.15 -8.23 33.04 o -20 1 3 63.34 40.83 27.34 o -19 1 3 17.72 23.12 23.80 o -18 1 3 59.20 15.34 30.85 o -17 1 3 124.65 71.46 24.09 o -16 1 3 524.42 504.19 28.67 o -15 1 3 10728.90 11346.25 239.95 o -14 1 3 523.56 447.62 44.95 o -13 1 3 52.04 63.65 19.39 o -12 1 3 5985.63 6185.14 102.19 o -11 1 3 51.90 39.44 7.93 o -10 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34.84 o -3 4 3 468.30 503.60 10.54 o -2 4 3 2154.98 2230.35 31.62 o -1 4 3 1205.11 1184.64 27.32 o 0 4 3 4213.91 4399.98 46.15 o 1 4 3 2506.81 2368.76 31.77 o 2 4 3 3642.63 3780.31 46.14 o 3 4 3 638.47 631.64 12.34 o 4 4 3 14402.25 14794.33 224.76 o 5 4 3 1033.26 1100.15 15.54 o 6 4 3 830.00 894.09 17.63 o 7 4 3 5123.56 5454.97 56.71 o 8 4 3 990.52 924.61 14.96 o 9 4 3 75.63 72.07 5.51 o 10 4 3 3246.23 3259.97 50.20 o 11 4 3 937.61 825.92 19.94 o 12 4 3 198.37 179.82 11.01 o 13 4 3 2278.96 2403.57 49.22 o 14 4 3 723.38 696.30 21.52 o 15 4 3 69.82 74.61 16.75 o 16 4 3 334.54 384.02 22.83 o 17 4 3 40.25 32.56 18.91 o 18 4 3 33.68 12.43 22.83 o 19 4 3 813.67 886.37 47.69 o 20 4 3 166.62 230.65 63.46 o 21 4 3 277.45 280.60 55.53 o -21 5 3 15.44 72.63 38.14 o -20 5 3 23.87 22.67 31.77 o -19 5 3 196.18 238.23 28.80 o -18 5 3 18.18 29.97 21.19 o -17 5 3 139.87 126.33 27.32 o -16 5 3 2.67 40.78 18.57 o -15 5 3 74.38 41.40 22.04 o -14 5 3 988.65 978.78 34.13 o -13 5 3 1128.30 1110.47 44.07 o 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505.44 60.82 o 15 11 4 194.19 158.92 31.77 o 16 11 4 129.70 187.81 60.82 o 17 11 4 428.93 433.33 60.57 o -16 12 4 404.06 376.06 95.19 o -15 12 4 9.79 17.11 47.60 o -14 12 4 132.26 146.06 27.36 o -13 12 4 6.16 .53 37.02 o -12 12 4 17.54 19.39 47.60 o -11 12 4 24.57 22.88 29.97 o -10 12 4 3.70 15.12 18.45 o -9 12 4 6.90 6.52 24.68 o -8 12 4 1400.22 1425.82 124.28 o -7 12 4 569.27 587.51 59.94 o -6 12 4 32.32 23.53 21.03 o -5 12 4 1417.26 1465.19 47.39 o -4 12 4 51.08 59.11 19.39 o -3 12 4 375.67 344.50 35.26 o -2 12 4 10049.69 10437.18 285.57 o -1 12 4 22.40 18.47 14.98 o 0 12 4 1306.29 1293.45 36.84 o 1 12 4 757.26 687.47 58.17 o 2 12 4 390.94 402.22 19.21 o 3 12 4 89.90 115.32 12.24 o 4 12 4 3737.50 3909.45 103.12 o 5 12 4 506.93 423.63 24.45 o 6 12 4 689.00 691.92 28.33 o 7 12 4 87.45 54.85 16.20 o 8 12 4 434.12 415.24 46.71 o 9 12 4 3.90 12.34 14.96 o 10 12 4 173.66 136.64 18.57 o 11 12 4 378.83 399.31 27.86 o 12 12 4 69.93 98.21 23.71 o 13 12 4 2.58 1.68 24.45 o 14 12 4 1258.57 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